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Journal articles on the topic 'Cinnamoyl chloride'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

D'Souza, Malcolm J., Anthony M. Darrington, and Dennis N. Kevill. "On the Importance of the Aromatic Ring Parameter in Studies of the Solvolyses of Cinnamyl and Cinnamoyl Halides." Organic Chemistry International 2010 (June 29, 2010): 1–9. http://dx.doi.org/10.1155/2010/130506.

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In solvolysis studies using Grunwald-Winstein plots, dispersions were observed for substrates with aromatic rings at the α-carbon. Several examples for the unimolecular solvolysis of monoaryl benzylic derivatives and related diaryl- or naphthyl-substituted derivatives have now been reported, where the application of the aromatic ring parameter (I) removes this dispersion. A recent claim suggesting the presence of an appreciable nucleophilic component to the I scale has now been shown, in a review of the solvolysis of highly-hindered alkyl halides, to be unlikely to be correct. Attention is now

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2

Bejblová-Voláková, M., J. Vlk, and D. Procházková. "Acylation of Ferrocene with Adamantoyl Chloride and Cinnamoyl Chloride." Topics in Catalysis 53, no. 19-20 (2010): 1411–18. http://dx.doi.org/10.1007/s11244-010-9601-x.

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3

Schildknecht, Hermann, Horst Sauer та Peter Kunzelmann. "Pflanzenabwehrstoffe XXXIV [1]. Synthese der 2-(E)-O-(4-Hydroxy-cinnamoyI)-ᴅ,ʟ-galactarsäure, eines vermeintlich photosensitiven Faktors aus Glycine max / Synthesis of 2-(E)-O-(4-Hydroxy-cinnamoyl)-ᴅ,ʟ-galactaric Acid, a Presumptive Photosensitive Factor from Glycine max". Zeitschrift für Naturforschung C 43, № 7-8 (1988): 519–28. http://dx.doi.org/10.1515/znc-1988-7-808.

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The synthesis of 2-(E)-O-(4-hydroxy-cinnamoyl)-ᴅ,ʟ-galactaric acid (1a) is described. Starting with free galactaric acid (2) and 4-acetoxy-cinnamoyl-chloride (3), these compounds were esterified under regioselective conditions to racemic 2-(E)-O-(4-acetoxy-cinnamoyl)-galactaric acid (4). After deprotection of the p-coumaroyl moiety 1a was obtained as a photo-unstable product. Optical resolution of racemate l a on bovine serum albumin covalently bound to silica resulted in the isolation of the pure optical isomers. The (+)-dextrorotatory synthetic enantiomer l a proved to be identical with the

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4

Toma, Štefan, та Marta Sališová. "Acylation of ω-phenylalkanoylferrocenes by cinnamoyl and phenylpropiolyl chlorides". Collection of Czechoslovak Chemical Communications 52, № 6 (1987): 1520–26. http://dx.doi.org/10.1135/cccc19871520.

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In Friedel-Crafts acylation of ω-phenylalkanoylferrocenes, the site of electrophilic attack depends on the reagent used. The acylation with cinnamoyl chloride yields preferentially the products of substitution of the unsubstituted cyclopentadienyl ring of ferrocene. The acylation with phenylpropionyl chloride affords the products of acylation of the benzene ring of the starting compound. The different behaviour of both acylating agents is discussed.

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5

Kawamura, Aki, Haijing Liu, Chika Takai, Takashi Takei, Hadi K. Razavi, and Masayoshi Fuji. "Surface modification of fumed silica by photo-dimerization reaction of cinnamyl alcohol and cinnamoyl chloride." Advanced Powder Technology 27, no. 2 (2016): 765–72. http://dx.doi.org/10.1016/j.apt.2016.03.003.

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6

Lowe, Henry IC, Ngeh J. Toyang, Charah T. Watson, and Joseph Bryant. "Synthesis of Substituted 1,3-Diesters of Glycerol Using Wittig Chemistry." Natural Product Communications 9, no. 5 (2014): 1934578X1400900. http://dx.doi.org/10.1177/1934578x1400900526.

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1,3-di-O-Cinnamoyl-glycerol is a natural compound isolated from a Jamaican medicinal plant commonly referred to as Ball moss (Tillandsia recurvata). The synthesis of this compound was achieved via a Wittig chemistry process. The synthetic approach started with acylation of a di-protected glycerol with cinnamoyl chloride, deprotection of the glycerol moiety, reaction of the primary alcohol with bromo acetylbromide followed by treatment with triphenyl phosphine to give the corresponding phosphonium bromide. The phosphonium bromide was then converted in situ to the Wittig reagent which is the bas

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7

Teponno, Rémy B., Sara R. Noumeur, and Marc Stadler. "Semisynthetic derivatives of massarilactone D with cytotoxic and nematicidal activities." Beilstein Journal of Organic Chemistry 21 (March 17, 2025): 607–15. https://doi.org/10.3762/bjoc.21.48.

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Massarilactones constitute a rare class of polyketides produced mainly by endophytic fungi. Given that semisynthetic derivatives often exhibit biological activities greater than those of the substrates, seven previously unreported derivatives of massarilactone D, compounds 2–8, were synthetized by acylation with methacryloyl chloride, cinnamoyl chloride, 4-bromobenzoyl chloride, trans-2-methyl-2-butenoyl chloride, and crotonyl chloride. These compounds were evaluated for their cytotoxic activity against the murine fibroblasts L929, human cervix carcinoma KB-3-1, human lung carcinoma A549, huma

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8

Nechifor, Marioara. "Aromatic polyesters with photosensitive side chains: Synthesis, characterization and properties." Journal of the Serbian Chemical Society 81, no. 6 (2016): 673–85. http://dx.doi.org/10.2298/jsc160111026n.

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New aromatic polyesters with photosensitive groups in their pendant chains were prepared from a diphenol carrying as substituent a cinnamoyl group extended with a flexible oxyethyleneoxy spacer and different aromatic dicarboxylic acids via direct polyesterification reaction in the presence of tosyl chloride/pyridine/dimethylformamide system as condensing agent. The resulting polyesters were characterized using Fourier-transform IR, proton and carbon nuclear magnetic resonance and ultraviolet spectroscopy, differential scanning calorimetry, thermogravimetric analysis, wide-angle X-ray diffracto

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9

Ma, Yuan, Zhen Zhang, and Yufen Zhao. "Microwave-Assisted One-Pot Synthesis of Dihydrocoumarins from Phenols and Cinnamoyl Chloride." Synlett 2008, no. 07 (2008): 1091–95. http://dx.doi.org/10.1055/s-2008-1042921.

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10

NEELAKUMARI, S., and G. RAVEENDRAN. "A Mechanistic Approach on the Solvolysis of Cinnamoyl Chloride in the Presence and Absence of Mercuric Chloride Catalyst." Oriental Journal Of Chemistry 29, no. 1 (2013): 341–46. http://dx.doi.org/10.13005/ojc/290155.

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11

Gan, LH. "Hydrolysis of Cinnamoyl Fluoride Catalyzed by Micelles of a Copper(II) Complex." Australian Journal of Chemistry 41, no. 5 (1988): 677. http://dx.doi.org/10.1071/ch9880677.

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Cinnamoyl fluoride was catalytically hydrolysed in the micelles formed by the copper(II) complex of N,N,N°- trimethyl -N°- tetradecylethylenediamine . A 25-times rate enhancement relative to the reaction in the micelles of hexadecyltrimethylammonium chloride was observed, but it was not as good a simulant as p- nitrophenyl diphenyl phosphate for nerve agents of the soman type. It was also found that aggregation of the copper(II) complex was essential in promoting the reactivity as the monomeric copper(II) complex of N, N, N′, N′- tetramethylethylenediamine had very little effect on the hydroly

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12

S., K. Sahu, K. Mishra S., P. Mahapatra S., Bhatta D., and S. Panda C. "Synthesis and hypoglycemic activities of 3-(phthalimidomethyl)-4-substituted-cinnamoyl salicylanilides." Journal of Indian Chemical Society Vol. 81, Mar 2004 (2004): 258–60. https://doi.org/10.5281/zenodo.5830629.

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University Department of Pharmaceutical Sciences, Utkal University, Vani Vihar, Bhubaneswar-751 004, India <em>E-mail</em> : headchemuu09@sify.com         <em> Fax</em>: 91-0674-2581850 Department of Chemistry, Berhampur University, Berhampur-760 007, India <em>Manuscript received 9 December 2002, revised 4 July 2003, accepted 22 August 2003</em> 3-Phthalimidomethylsalicylic acid (2) was prepared by refluxing <em>N</em>-hydroxymethyl phthalimide (1) with salicylic acid. The corresponding acid chloride (3) was condensed with 4-aminoacetophenone in anhydrous potassium ca

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13

Mahmoud, Mahmoud R., Eman A. A. El-Bordany, Naglaa F. Hassan, and Fatma S. M. Abu El-Azm. "New 2,3-Disubstituted Quinazolin-4(3H)-Ones from 2-Undecyl-3,1-Benzoxazin-4-One." Journal of Chemical Research 2007, no. 9 (2007): 541–44. http://dx.doi.org/10.3184/030823407x248315.

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2-undecyl-4H-3,1-benzoxazin-4-one (2) was prepared and reacted with primary and secondary amines affording compounds 3–7, while with hydrazine hydrate it gave the quinazolinone derivative 8. The reaction of 8 with 3,4,5-trimethoxybenzaldehyde followed by thioglycollic acid yielded 9 and 10, respectively. Acylation of 8 using cinnamoyl chloride gave 11. Furthermore, treatment of 2 with hydrazine derivatives provided 12 and 13. Fusion of 2 with ammonium acetate gave the quinazolinone derivative 14 which upon treatment with ethyl chloroacetate yielded the ester 15. The hydrazide 17 was obtained f

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14

Gangwar, Devendra Kumar, та A. K. Agarwal. "Synthesis of α-Diazoketones by The Action of Diazo-N-Octane on 3-Methoxy Cinnamoyl Chloride". Oriental Journal of Chemistry 32, № 3 (2016): 1675–78. http://dx.doi.org/10.13005/ojc/320345.

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15

Nakayama, Yuushou, Naoki Matsubara, Zhennguo Cai, Takeshi Shiono, Kei Inumaru, and Hiroyuki Shirahama. "Effect of end-group modification of poly(lactide)s by cinnamoyl chloride on their thermal stability." Polymer Degradation and Stability 141 (July 2017): 97–103. http://dx.doi.org/10.1016/j.polymdegradstab.2017.05.015.

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16

RAVEENDRAN, G., and S. NEELAKUMARI. "Effect of added Dimethyl sulphoxide on the Solvolysis of Cinnamoyl Chloride in Aqueous Acetone and Acetonitrile." Oriental Journal Of Chemistry 28, no. 3 (2012): 1371–78. http://dx.doi.org/10.13005/ojc/280337.

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17

De, Asit, Shubhajit Ghosh, and Javed Iqbal. "A remarkable stereocontrol during cobalt(II) chloride catalysed opening of cinnamoyl epoxides with N-substituted anilines." Tetrahedron Letters 38, no. 48 (1997): 8379–82. http://dx.doi.org/10.1016/s0040-4039(97)10171-x.

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18

Majewski, Marek, Marc DeCaire, Pawel Nowak, and Fan Wang. "Studies on enolate chemistry of 8-thiabicyclo[3.2.1]- octan-3-one: enantioselective deprotonation and synthesis of sulfur analogs of tropane alkaloids." Canadian Journal of Chemistry 79, no. 11 (2001): 1792–98. http://dx.doi.org/10.1139/v01-157.

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Enantioselective deprotonation of 8-thiabicyclo[3.2.1]octan-3-one (1) with chiral lithium amides, followed by reactions with electrophiles affords sulfur analogs of tropane alkaloids of pyranotropane family. Thus, deprotonation of 1 with (S)-N-(diphenyl)methyl-1-phenylethylamine (11d), followed by the reaction of the resulting nonracemic enolate with benzaldehyde gives the corresponding aldol product as one diastereoisomer (exo, threo) and in high enanatiomeric purity (95% ee). Trimethylsilyl chloride, acetic anhydride, and acyl cyanides react readily with the lithium enolate to give the corre

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19

Ngurah, Budiana I. Gusti M., Jumina Jumina, Chairil Anwar, Sunardi Sunardi, and Mustofa Mustofa. "Synthesis and In Vitro Evaluation of C-methylcalix[4]resorcinaryl octacinnamate and C-methylcalix[4]resorcinaryl octabenzoate as the Sunscreen." Indonesian Journal of Chemistry 17, no. 1 (2017): 63. http://dx.doi.org/10.22146/ijc.23575.

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The present study was aimed to synthesize and evaluate sunscreen activity of C-methylcalix[4]resorcinaryl octacinnamate and C-methylcalix[4]resorcinaryl octabenzoate. The target compounds were synthesized in 2 steps. They were a synthesis of C-methylcalix[4]-resorcinarene via acid catalyzed the condensation of resorcinol and acetaldehyde by using HCl catalyst, followed by esterification using cinnamoyl chloride and benzoyl chloride. The characterization of the target compounds was performed by IR, 1H-NMR, 13C-NMR, and LC-MS spectrometers. The sunscreen activity test was conducted by spectrosco

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20

Itnawita, Itnawita, Zamri Adel, Ganis Fia Kartika, et al. "Use of the compound (2-(4-chlorophenyl)-3-hydroxy-4H-chromene-4-one) as a ligand complex formation by copper (II)." Current Chemistry Letters 11, no. 4 (2022): 353–58. http://dx.doi.org/10.5267/j.ccl.2022.6.002.

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Flavanol compounds are chalcone derivatives, generally found in hydroxy substituted forms that can act as ligands. Hydroxy-substituted flavonols are found in many plants but in very small amounts. In order to enrich and expand the use of this compound as a ligand, the synthetic methods were carried out through structural variations, one of which was by substitution using chloride and then the compound (2-(4-chlorophenyl)-3-hydroxy-4H-chromene-4-one) was obtained. In this research, the study was conducted using the compound (2-(4-chlorophenyl)-3-hydroxy-4H-chromene-4-one) as a ligand for comple

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21

DE, A., S. GHOSH, and J. IQBAL. "ChemInform Abstract: A Remarkable Stereocontrol During Cobalt(II) Chloride Catalyzed Opening of Cinnamoyl Epoxides with N-Substituted Anilines." ChemInform 29, no. 8 (2010): no. http://dx.doi.org/10.1002/chin.199808073.

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22

Nurmaganbetov, Zh S., O. A. Nurkenov, S. D. Fazylov, et al. "Synthesis and Spatial Structure of 3-Phenylacrylic Acid Octahydroquinolizin-1-Ylmethyl Ester and 2-(Octahydroquinolizin-1-Ylmethyl)Isoindole-1,3-Dione." Eurasian Chemico-Technological Journal 26, no. 3 (2024): 175–83. http://dx.doi.org/10.18321/ectj1641.

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The reactions of lupinine alkaloid and its chlorine derivative with cinnamoyl chloride and 2-K-isoindole-1,3-dione were investigated to obtain 3-phenylacrylic acid octahydroquinolizin-1-ylmethyl ester and 2-(octahydroquinolizin-1-ylmethyl)isoindole-1,3-dione, respectively. The optimal conditions for carrying out the aforementioned reactions were determined, taking into account the nature of the solvent and medium. It was established that acylation of the molecule in a benzene medium, in the presence of trimethylamine, resulted in the formation of 3-phenylacrylic acid octahydroquinolizin-1-ylme

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23

Pangaribowo, Dian Agung, Fathunnisa Fathunnisa, Ari Satia Nugraha, Ayik Rosita Puspaningtyas, and Indah Purnama Sary. "Structure Modification of Cinnamic Acid to (E)-1-(3,4-dihydroisoquinoline-2(1H)-yl)-3-phenylprop-2-en-1-one and Antioxidant Activity Test by DPPH Method." Borneo Journal of Pharmacy 7, no. 3 (2024): 254–63. http://dx.doi.org/10.33084/bjop.v7i3.6163.

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Antioxidants can protect cells from free radical damage by stabilizing them. One of the compounds that has antioxidant activity is cinnamic acid. Cinnamic acid and its derivatives have several activities: antibacterial, anticancer, and antioxidant. However, the ability of cinnamic acid to capture free radicals is still relatively low. One of the efforts that can be made to increase the antioxidant activity of cinnamic acid is to modify its structure. Structure modification is an effort to improve the pharmacological activity of a compound through chemical synthesis reactions. The cinnamic acid

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24

Jumina, Jumina, Dwi Siswanta, Abdul Karim Zulkarnain, et al. "Development of C-Arylcalix[4]resorcinarenes and C-Arylcalix[4]pyrogallolarenes as Antioxidant and UV-B Protector." Indonesian Journal of Chemistry 19, no. 2 (2019): 273. http://dx.doi.org/10.22146/ijc.26868.

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Indonesia is rich with essential oils such as anise and clove leave oils. In respect to explore the potential utilization of these resources, it has been conducted the transformation of p-hydroxybenzaldehyde and vanillin (4-hydroxy-3-methoxy benzaldehyde) respectively derived from anise oil and clove leaves oil to a series of C-arylcalix[4]resorcinarenes and C-arylcalix[4]pyrogallolarene macrocycles. Treatment of these aldehydes with resorcinol in the presence of HCl in absolute ethanol at reflux for 8 h afforded C-4-hydroxyphenylcalix[4]resorcinarene (3a) and C-4-hydroxy-3-methoxy phenyl-cali

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25

Beheshti, S. Hamidreza, Mehran Javanbakht, Hamid Omidvar, et al. "Effects of Structural Substituents on the Electrochemical Decomposition of Carbonyl Derivatives and Formation of the Solid–Electrolyte Interphase in Lithium-Ion Batteries." Energies 14, no. 21 (2021): 7352. http://dx.doi.org/10.3390/en14217352.

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The solid–electrolyte interphase (SEI), the passivation layer formed on anode particles during the initial cycles, affects the performance of lithium-ion batteries (LIBs) in terms of capacity, power output, and cycle life. SEI features are dependent on the electrolyte content, as this complex layer originates from electrolyte decomposition products. Despite a variety of studies devoted to understanding SEI formation, the complexity of this process has caused uncertainty in its chemistry. In order to clarify the role of the substituted functional groups of the SEI-forming compounds in their eff

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26

Amin, Md Ruhul, Farhana Yasmin, Mohammed Anowar Hosen та ін. "Synthesis, Antimicrobial, Anticancer, PASS, Molecular Docking, Molecular Dynamic Simulations & Pharmacokinetic Predictions of Some Methyl β-D-Galactopyranoside Analogs". Molecules 26, № 22 (2021): 7016. http://dx.doi.org/10.3390/molecules26227016.

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A series of methyl β-D-galactopyranoside (MGP, 1) analogs were selectively acylated with cinnamoyl chloride in anhydrous N,N-dimethylformamide/triethylamine to yield 6-O-substitution products, which was subsequently converted into 2,3,4-tri-O-acyl analogs with different acyl halides. Analysis of the physicochemical, elemental, and spectroscopic data of these analogs revealed their chemical structures. In vitro antimicrobial testing against five bacteria and two fungi and the prediction of activity spectra for substances (PASS) showed promising antifungal functionality comparing to their antiba

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27

De, Ranjit, Kyung Won Jo, and Kyong-Tai Kim. "Influence of Molecular Structures on Fluorescence of Flavonoids and Their Detection in Mammalian Cells." Biomedicines 10, no. 6 (2022): 1265. http://dx.doi.org/10.3390/biomedicines10061265.

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Flavonoids are being increasingly applied for the treatment of various diseases due to their anti-cancer, anti-oxidant, anti-inflammatory, and anti-viral properties. However, it is often challenging to detect their presence in cells and tissues through bioimaging, as most of them are not fluorescent or are too weak to visualize. Here, fluorescence possibilities of nine naturally occurring analogous flavonoids have been investigated through UV/visible spectroscopy, molecular structure examination, fluorescent images in mammalian cells and their statistical analysis employing aluminum chloride a

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28

Martínez-Martínez, Mónica, María Alcaide, Anatoli Tchigvintsev, et al. "Biochemical Diversity of Carboxyl Esterases and Lipases from Lake Arreo (Spain): a Metagenomic Approach." Applied and Environmental Microbiology 79, no. 12 (2013): 3553–62. http://dx.doi.org/10.1128/aem.00240-13.

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ABSTRACTThe esterases and lipases from the α/β hydrolase superfamily exhibit an enormous sequence diversity, fold plasticity, and activities. Here, we present the comprehensive sequence and biochemical analyses of seven distinct esterases and lipases from the metagenome of Lake Arreo, an evaporite karstic lake in Spain (42°46′N, 2°59′W; altitude, 655 m). Together with oligonucleotide usage patterns and BLASTP analysis, our study of esterases/lipases mined from Lake Arreo suggests that its sediment contains moderately halophilic and cold-adapted proteobacteria containing DNA fragments of distan

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29

Soares-Bezerra, Rômulo José, Edson F. da Silva, Aurea Echevarria, et al. "Effect of mesoionic 4-phenyl-5-(cinnamoyl)-1,3,4-thiadiazolium-2-phenylamine chloride derivative salts on the activities of the nitric oxide synthase and arginase of Leishmania amazonensis." Journal of Enzyme Inhibition and Medicinal Chemistry 23, no. 3 (2008): 328–33. http://dx.doi.org/10.1080/14756360701585619.

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30

Zhao, Yu-Long, Li Chen, Shao-Chun Yang, Cui Tian та Qun Liu. "A Synthetic Strategy for Polyfunctionalized Bicyclo[3.3.1]nonanes Based on a Tandem Three-Component [3 + 2] Cycloaddition of α-Cinnamoyl Ketene-S,S-acetals with Oxalyl Chloride". Journal of Organic Chemistry 74, № 15 (2009): 5622–25. http://dx.doi.org/10.1021/jo900764s.

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31

Maraš, Nenad, Franc Perdih, and Marijan Kočevar. "Synthesis of 1-aryl-1-phenylpropenes using an alkylation-rearrangement-methylation-isomerization one-pot reaction sequence." Open Chemistry 9, no. 5 (2011): 904–9. http://dx.doi.org/10.2478/s11532-011-0074-y.

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Abstract(Z/E)-1-(2-Methoxyaryl)-1-phenylpropenes have been prepared in good yields by heating a mixture of a phenolic substrate, cinnamyl chloride, tetramethylammonium chloride and K2CO3 in polyethyleneglycol at 180°C. The one-pot synthesis proceeds through four discrete reaction steps: alkylation of the phenol with cinnamyl chloride, Claisen rearrangement, O-methylation and double-bond migration. The configuration of one crystalline product was determined using a single-crystal X-ray diffraction analysis. The thermodynamic and structural features of the products were evaluated using computati

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32

M., L. Sharma, and Kaur Sukhvir. "Synthesis of quaternary salts of ammonia from cinnamic acids and their plant growth retardant activity." Journal of Indian Chemical Society Vol. 84, Jun 2007 (2007): 612–14. https://doi.org/10.5281/zenodo.5820897.

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Department of Biochemistry and Chemistry, Punjab Agricultural University, Ludhiana-141 004, Punjab, India <em>Manuscript received 21 December 2005, accepted 19 April 2007</em> A series of <em>N</em>,<em>N</em>-dimethyl-<em>N</em>-benzyl ammonium chloride cinnamides (la-e) were prepared from the reaction between cinnamyl chlorides (4a-e) and <em>N</em>,<em>N</em>-dimethylphenylmethanamines (6a-e). These salts were tested for their biological activity on germination, seedling growth and adventitious root formation on hypocotyl cuttings of <em>Vigina radiata</em> (SML- 668) and Were found to be m

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33

Ibrahim, Samer, and Seham Y.Abo-Kora. "Evaluation of the protective effect of Cinnamomum Zeylanicum on cadmium testicular toxicity and Nrf2 gene expression in albino rats." International Journal of Pharmacology and Toxicology 5, no. 1 (2017): 5. http://dx.doi.org/10.14419/ijpt.v5i1.7030.

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Cadmium is an industrial pollutant that may exert specific toxic effect on mammals. The aim of study was to investigate the protective effect of Cinnamon on male reproductive system of albino rat induced by cadmium toxicity. Forty male albino rats were divided into 4 groups. 1st Group administrated saline and kept as control.2nd Group administrated 200mg/kg / day Cinnamon extract. 3rd Group administrated 20mg/kg/day cadmium chloride.4th Group administrated 200mg/kg/day Cinnamon extract and 20mg/kg/day cadmium chloride orally for 8 weeks. . Our results revealed significant decrease in testoster

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34

Wu, La-Xia, Ying-Guo Zhao, Ye-Bin Guan, et al. "Silver encapsulated copper salen complex: efficient catalyst for electrocarboxylation of cinnamyl chloride with CO2." RSC Advances 9, no. 56 (2019): 32628–33. http://dx.doi.org/10.1039/c9ra05253d.

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Chang, Meng-Yang, Min-Chen Tsai, and Chun-Yi Lin. "A novel one-pot synthesis of flavones." RSC Advances 11, no. 19 (2021): 11655–62. http://dx.doi.org/10.1039/d1ra00534k.

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A one-pot facile route for the BiCl<sub>3</sub>/RuCl<sub>3</sub>-mediated synthesis of functionalized flavones is described, including: (i) ortho-acylation of phenols with cinnamoyl chlorides, and (ii) cyclodehydrogenation of the resulting o-hydroxychalcones.

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36

van Haaren, Richard J., Henk Oevering, Paul C. J. Kamer, et al. "The mechanism for palladium catalyzed carbonylation of cinnamyl chloride." Journal of Organometallic Chemistry 689, no. 23 (2004): 3800–3805. http://dx.doi.org/10.1016/j.jorganchem.2004.07.016.

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37

Koo, In Sun, Sun Kyoung An, Kiyull Yang, Ikchoon Lee, and T. William Bentley. "Correlation of the rates of solvolyses of cinnamyl chloride." Journal of Physical Organic Chemistry 15, no. 11 (2002): 758–64. http://dx.doi.org/10.1002/poc.550.

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38

Gilman, Henry, and Stanton A. Harris. "The preparation of cinnamyl chloride and its grignard reagent." Recueil des Travaux Chimiques des Pays-Bas 50, no. 12 (2010): 1052–55. http://dx.doi.org/10.1002/recl.19310501204.

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Muhammad, Aisha, Hafsa Muhammad, Atika Aslam, Zaeem Sohail Jafar, and Talha Laique. "Effect of Cinnamon Bark Oil on Leydig Cell Count and Morphology along with Serum Testosterone Levels in Rats after Cadmium Induced Testicular Toxicity." Pakistan Journal of Medical and Health Sciences 15, no. 9 (2021): 2958–60. http://dx.doi.org/10.53350/pjmhs211592958.

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Cadmium is a toxic heavy metal that causes number of health issues. Purpose: To demonstrate the effect of cinnamon bark oil on Leydig cell count and morphology with measurement of serum testosterone levels. Study Design: Experimental study. Methodology: Healthy male wistar rats (n=30) were taken and divided into 3 groups with n= 10. Group A functioned as control. Cadmium chloride was administered to the rats to induce testicular toxicity in group B. Group C was the treatment group. Animals were euthanized on day 15. Leydig cell count and morphology was done after haematoxylin and eosin stainin

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Xu, Bin, Ludovic Troian-Gautier, Ryan Dykstra, Robert T. Martin, Osvaldo Gutierrez, and Uttam K. Tambar. "Photocatalyzed Diastereoselective Isomerization of Cinnamyl Chlorides to Cyclopropanes." Journal of the American Chemical Society 142, no. 13 (2020): 6206–15. http://dx.doi.org/10.1021/jacs.0c00147.

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Şahin, Neslihan, İsmail Özdemir, and David Sémeril. "Dichloro-Bis(1-cinnamyl-benzimidazole)-Cobalt(II)." Molbank 2024, no. 4 (2024): M1911. http://dx.doi.org/10.3390/m1911.

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Dichloro-bis(1-cinnamyl-benzimidazole)-cobalt(II) was prepared in one step using a cobalt precursor CoCl2 and corresponding substituted benzimidazole. The complex was fully characterized using IR, elemental analysis, and mass- and NMR spectroscopy. In the solid state, the cobalt atom displays a typical tetrahedral geometry and is coordinated to two chlorine atoms and two benzimidazole moieties.

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Ohta, A., G. Bu, T. Matsubayashi, et al. "DIFFERENTIAL RESPONSES OF COPPER(I) AND COPPER(II) ON LIVER COPPER ACCUMULATION IN THE LONG-EVANS CINNAMON (LEC) RATS STUDIED BY PIXE DETERMINATION." International Journal of PIXE 10, no. 03n04 (2000): 155–59. http://dx.doi.org/10.1142/s0129083500000213.

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Effects of supplementation by copper(I) and copper (II) in Long-Evans Cinnamon(LEC) rats and life survival of rats are given. Long-Evans Cinnamon(LEC) strain rats were used at age of 8 weeks. The rats were randomly assigned to either copper(I) chloride or copper (II) chloride group. We have performed x-ray emissivite determination of copper in liver of LEC rats using PIXE and detected increase in copper in liver at early stage which could be supplemented by copper(I) and copper (II). During the supplementation period, clinical deterioration continued accompanied by daily body sway. The rats lo

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Pound, B. G., P. Cox, and K. E. Mortelmans. "The Use of Quaternary Phosphonium Compounds as Antibacterial Corrosion Inhibitors for Low-Alloy Steel." Corrosion 74, no. 6 (2018): 694–704. http://dx.doi.org/10.5006/2692.

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Triphenyl-based quaternary phosphonium compounds were evaluated as corrosion inhibitors with biocidal properties for controlling microbiologically influenced corrosion. Several compounds displayed biocidal activity for acid-producing bacteria or for sulfate-reducing bacteria, but not both. Electrochemical impedance spectroscopy was used to examine the effect of the compounds on the corrosion behavior of a low-alloy steel Fe-Ni-Cr-Mo (HY-80) in deaerated artificial seawater with and without bacteria present. The performance of the compounds as corrosion inhibitors appeared to be governed by ste

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Kumar, Subodh, Vijay Kumar, and Swapandeep Singh Chimni. "Indium-Mediated Barbier allylations of Hydroxyanthraquinones: An Expedient synthesis of Novel 10-Alkenyl-10-Hydroxy-9(10H)-Anthracenones." Journal of Chemical Research 2000, no. 7 (2000): 314–15. http://dx.doi.org/10.3184/030823400103167660.

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Indium-mediated allylations of 1,8-dihydroxy-9,10-anthraquinone with allyl, cinnamyl and crotonyl bromides/ chlorides and 1,4- and 1,5- dihydroxy derivatives with allyl bromide in THF–MeOH–H2O gave the respective 10-alkenyl-10-hydroxy-9(10H)-anthracenones in excellent yields.

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Čišovská, Kristína, and Katarína Hroboňová. "The Application of Ultrasonic Assisted Extraction in Analysis Cinnamon and Food Products." Czech Chemical Society Symposium Series 20, no. 5 (2022): 323–26. http://dx.doi.org/10.54779/ccsss20220323.

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The objective of this study was to select suitable experimental conditions for extraction of coumarin by Ultrasonic Assisted Extraction (UAE). Type of extraction solvent, extraction time and temperature were optimized to increase the extraction yield of coumarin from samples of cinnamon and foods containing cinnamon. Optimal UAE conditions include extraction time of 10 min, temperature of 50 °C and extraction solvent based on choline chloride and ʟ-lactic acid. The extraction yields were comparable to traditional solvents – water and methanol.

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Florio, Saverio, Luigino Troisi, Vito Capriati, and Giovanna Suppa. "Lithiation of Cinnamyl Chloride: Stereoselective Synthesis of Propargylic Oxiranes and Aziridines." European Journal of Organic Chemistry 2000, no. 22 (2000): 3793–97. http://dx.doi.org/10.1002/1099-0690(200011)2000:22<3793::aid-ejoc3793>3.0.co;2-m.

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Augustia, Venitalitya A. S., Yuni Kusumastuti, and Sang Kompiang Wirawan. "Pectin Based Edible Film for Cinnamaldehyde Delivery System: Effect of Calcium Chloride Content on the Physical Characteristics of the Films." Materials Science Forum 998 (June 2020): 266–70. http://dx.doi.org/10.4028/www.scientific.net/msf.998.266.

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The cinnamon essential oil has antibacterial characteristic and sensitive to light and oxygen [1]. Due to its benefits from cinnamaldehyde, this compound has already used for antibacterial agent injected in polymer film [2]. Films are usually made from natural polymers as their main materials such as pectin. This research observed the influence of calcium chloride addition (0; 0.01; 0.02; and 0.03 g/mL solution) in the physical characteristics of pectin based edible films using the immersion method. The results indicated that calcium chloride content did not effect significantly. On the other

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Abdeen, Ahmed, Ahmed Ghonim, Ragab El-Shawarby, et al. "Protective effect of cinnamon against cadmium-induced hepatorenal oxidative damage in rats." International Journal of Pharmacology and Toxicology 5, no. 1 (2017): 17. http://dx.doi.org/10.14419/ijpt.v5i1.7119.

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Background: Cadmium (Cd) is a well-known hazardous environmental contaminant. It exerts its toxicity through induction of lipid peroxidation and reduction of cellular antioxidant. Therefore, in this study, we investigated whether cinnamon could protect against Cd toxicity in liver and kidney.Materials and methods: Forty male Wister rats (130-135 gm) were divided randomly into 4 groups/ 10 rats each. Control, cinnamon, cadmium, and Cinn+Cd groups received distilled water, cinnamon extract (200 mg/kg b.wt. orally), cadmium chloride (5 mg/kg b.wt. orally), and Cd plus cinnamon, respectively. Bloo

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Journal, Baghdad Science. "Curing of Maleimidyl Phenol-Formaldehyde Resins Via Esterification and Free Radical Polymerization." Baghdad Science Journal 4, no. 1 (2007): 110–18. http://dx.doi.org/10.21123/bsj.4.1.110-118.

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Three phenol-formaldehyde resins having pendant maleimides were prepared by poly condensation of N-(hydroxyphenyl) maleimides with formaldehyde under conditions similar to those in Novolac preparation. The prepared resins were modified by two methods, the first one includes esterification of phenolic hydroxyl groups in the prepared resins via their treatment with benzoyl, acryloyl, methacryloyl and cinnamoyl chlorides respectively in the presence of triethylamine, while the second modification includes free radical polymerization of vinylic bonds in the prepared resins to produce cross-linked

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Ahluwalia, Vinod K., Madhu Chopra, and Ramesh Chandra. "A convenient synthesis of novel pyrimidine analogues of o-hydroxy chalcones and pyrano [2,3-d]pyrimidines and their biological activities." Journal of Chemical Research 2000, no. 4 (2000): 162–63. http://dx.doi.org/10.3184/030823400103166995.

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A convenient method for the synthesis of new pyrimidine analogues of chalcones by condensation of 5-acetyl-1,3-diaryl-1,2,3,4-tetrahydro-6-hydroxy-4-oxo-2-thioxopyrimidines with aromatic aldehydes in aqueous methanolic potassium hydroxide (method A) and by condensation of 1,3-diaryl-2-thiobarbituric acids with cinnamoyl chlorides in presence of triethylamine (method B) is reported which on subsequent oxidative cyclization afforded 1,3,7-triaryl-1,2,3,4-tetrahydro-4,5-dioxo-2-thioxo-5 H-pyrano[2,3- d]pyrimidines which were evaluated for their antimicrobial activity.

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