Academic literature on the topic 'Citrate-gel auto combustion method'

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Journal articles on the topic "Citrate-gel auto combustion method"

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Sun, Jie, Zhen Hua Zhang, and Xiao Hui Cao. "Synthesis and Dielectric Property of Perovskite-Type LaMnO3 Nanoparticle." Solid State Phenomena 121-123 (March 2007): 967–70. http://dx.doi.org/10.4028/www.scientific.net/ssp.121-123.967.

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The perovskite-type nanocrystal LaMnO3 was prepared using sol-gel auto-combustion method with citric acid as the chelating agent. Some analytical methods consisted of FT-IR, XRD, TEM and wave-guide method were used to characterize the gel and the final products. The metal ions coordination compound, obtained from nitrate and citrate, underwent an auto-combustion process and voluminous ashes formed when calcining the complex in the air. From the result of the dielectric properity. It was shown that the dielectric coefficient curves and dielectric loss curve of LaMnO3 nanocrystals were smooth in
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Megha, Unikoth, Karakat Shijina, and George Varghese. "Nanosized LaCo0.6Fe0.4O3 perovskites synthesized by citrate sol gel auto combustion method." Processing and Application of Ceramics 8, no. 2 (2014): 87–92. http://dx.doi.org/10.2298/pac1402087m.

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LaCo0.6Fe0.4O3 (LCFO) nanopowder was synthesized from constituent metal nitrates, citric acid and ethylene glycol by citrate sol gel autocombustion method and calcined at different temperatures. The powders were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM), energy dispersive X-ray analysis (EDAX) and Fourier transform infrared spectra (FTIR), whereas dielectric properties were investigated with LCR-meter. The FTIR spectra, taken for the xerogel and the sample calcined at 1000?C, confirm that the organic groups were removed during calcination and oxide structure
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Devi, Sujatha P., and H. S. Maiti. "A modified citrate gel route for the synthesis of phase pure Bi2Sr2CaCu2O8 superconductor." Journal of Materials Research 9, no. 6 (1994): 1357–62. http://dx.doi.org/10.1557/jmr.1994.1357.

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A simple method for the bulk synthesis of 80 K bismuth-based superconducting phase (2212) is described. It employs a modified citrate gel route giving rise to an auto-ignited combustion process. The precursor ash obtained after combustion is further calcined at 800 °C to produce the desired superconducting powder with excellent homogeneity and fineness, leading to good sinterability and fairly sharp transition temperature. For a particular citrate-nitrate ratio, the nature of combustion of the gels containing two different bases has been compared. The thermal decomposition characteristics of t
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Abdellatif, M. H., and A. A. Azab. "Fractal Growth of Ferrite Nanoparticles Prepared by Citrate-Gel Auto-Combustion Method." Silicon 10, no. 5 (2018): 1991–97. http://dx.doi.org/10.1007/s12633-017-9711-1.

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Barati, M. R., S. A. Seyyed Ebrahimi, and A. Badiei. "Influence of Different Calcination Conditions on the Microstructure and Phase Constitution of Nickel-Zinc Ferrite Nanocrystalline Powders Prepared by a Sol-Gel Auto-Combustion Method." Key Engineering Materials 368-372 (February 2008): 598–600. http://dx.doi.org/10.4028/www.scientific.net/kem.368-372.598.

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In this work, nickel-zinc ferrite nanocrystalline powder has been prepared by a sol-gel autocombustion technique using nitrate-citrate gel obtained from metal nitrates and citric acid solution. Characterization of the nitrate-citrate gel, as-burnt powder and calcined powder at different calcination conditions were investigated by using XRD, FTIR and SEM techniques. The results revealed that the nitrate-citrate gel exhibits a self-propagating behavior after ignition and showed that the different calcination conditions affect the crystallite size of the synthesized powder as well as its phase co
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Bao, Li, Xi Wei Qi, Bo Ni, Min Zhang, and Rui Bin Mei. "BiFeO3 Powders Synthesized by Different Sol-Gel Methods." Key Engineering Materials 697 (July 2016): 84–88. http://dx.doi.org/10.4028/www.scientific.net/kem.697.84.

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The multiferroic BiFeO3 powders with perovskite structure were synthesized by sol-gel auto-combustion and conventional sol-gel methods, respectively. As-prepared powders were characterized by XRD, SEM and VSM techniques to investigate phase structure, microstructure and magnetic properties. The results show that the pure phase BiFeO3 powders are obtained successfully by sol-gel auto-combustion after calcining at 650°C for 2h and leaching by HNO3. Compared with conventional sol-gel method which got pure phase BiFeO3 powders at 800°C for 3h, the sol-gel auto-combustion technique can get more pur
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Raghasudha, M. "Characterization Of Nano-Structured Magnesiumchromium Ferrites Synthesized By Citrate-Gel Auto Combustion Method." Advanced Materials Letters 4, no. 12 (2013): 910–16. http://dx.doi.org/10.5185/amlett.2013.5479.

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Raghasudha, M., D. Ravinder, and P. Veerasomaiah. "Characterization of Chromium Substituted Cobalt Nano Ferrites Synthesized by Citrate-Gel Auto Combustion Method." Advances in Materials Physics and Chemistry 03, no. 02 (2013): 89–96. http://dx.doi.org/10.4236/ampc.2013.32014.

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Boddolla, Sathish, and D. Ravinder. "Eu3+ Doped CoFe2O4 Nanoparticles with XRD and FTIR Analysis." Journal for Research in Applied Sciences and Biotechnology 3, no. 2 (2024): 135–38. http://dx.doi.org/10.55544/jrasb.3.2.23.

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Pure and Eu3+ doped cobalt ferrite nanoparticles with the formula CoEuxFe2-xO4(x = 0.00,0.10) were synthesized by citrate gel auto combustion method. X-ray diffraction analysis validated both the phase formation and purity of the synthesized nanoparticles. The Fourier-transform infrared (FTIR) spectra of the sample were meticulously recorded within the spectral range of 200-1000 cm^-1. This analysis provided insights into the formation of the spinel structure.
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M. Venkata Narayana. "Effect of Sm3+ doped Ni-Cd Nano ferrite synthesis and structural characterization by citrate-gel auto combustion method." International Journal of Science and Research Archive 7, no. 2 (2022): 326–31. http://dx.doi.org/10.30574/ijsra.2022.7.2.0284.

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Ferrite nano particles of basic composition Ni Cd Smx Fe2-xO4(0.0 ≤ x ≤ 0.05, X=0.01) where synthesized by citrate-gel auto combustion method have investigated. X-ray diffraction profile indicates that the samples are in single phase structure for the sample without Sm content. For the samples with Sm ions, some diffraction peaks appeared which belongs to the orthorhombic phase structure further, the XRD have been used calculated the lattice parameter, density and grain size. The particle size of the starting powder composition varied from 30 nm to 45 nm. The values of lattice parameter (a) de
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Dissertations / Theses on the topic "Citrate-gel auto combustion method"

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Horta, André Filipe Castanheira. "Synthesis optimization of Zn-Mn ferrites for magnetic fluid applications." Master's thesis, 2019. http://hdl.handle.net/10773/29834.

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Manganese-Zinc ferrite nanoparticles have been the subject of increasing research due to their desired properties for a wide range of applications. These properties include nanometer particle size control, tunable magnetic properties, high saturation magnetization and low toxicity, providing these ferrites with the necessary requirements for cancer treatment via magnetic hyperthermia. During this research, powders of Mn-Zn ferrite were synthesized and characterized, aiming to optimize their structural and magnetic properties for further application in a ferrofluid. Samples with Mn1-xZn
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Book chapters on the topic "Citrate-gel auto combustion method"

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Hashim, Mohd, Alimuddin, M. Wasi Khan, Shalendra Kumar, Sagar E. Shirsath, and Ravi Kumar. "Structural, Dielectric and Magnetic Properties of Nano-Crystalline Ni-Mg Ferrites Prepared by Citrate-Gel Auto Combustion Method." In Springer Proceedings in Physics. Springer Berlin Heidelberg, 2013. http://dx.doi.org/10.1007/978-3-642-34216-5_22.

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Yadav, Pooja, R. K. Beniwal, Anchal, et al. "Structural and Morphological Characterization of Cr0.2Ni0.8-xCoxFe2O4 Nanocrystalline Samples Synthesized via Sol-Gel Auto-Combustion Method." In Springer Proceedings in Physics. Springer Nature Singapore, 2025. https://doi.org/10.1007/978-981-96-6795-6_30.

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Barati, M. R., S. A. Seyyed Ebrahimi, and A. Badiei. "Influence of Different Calcination Conditions on the Microstructure and Phase Constitution of Nickel-Zinc Ferrite Nanocrystalline Powders Prepared by a Sol-Gel Auto-Combustion Method." In High-Performance Ceramics V. Trans Tech Publications Ltd., 2008. http://dx.doi.org/10.4028/0-87849-473-1.598.

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Sheikh, Hassan, Ebrahim Paimozd, Ali Sharbati, and Sedigheh Sheikh. "Characteristics of Superconducting YBCO Phase Formation through Auto Combustion Citrate-Nitrate Sol-Gel." In Ceramic Transactions Series. John Wiley & Sons, Inc., 2011. http://dx.doi.org/10.1002/9781118144480.ch18.

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Sridhar, Rapolu, D. Ravinder, J. Laxman Naik, K. Vijaya Kumar, N. Maramu, and S. Katlakunta. "Investigation of Structural, Magnetic and Electrical Properties of Chromium Substituted Nickel Ceramic Nanopowders." In Advanced Ceramic Materials. IntechOpen, 2021. http://dx.doi.org/10.5772/intechopen.94941.

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Nano-ceramic of NiCrxFe2-xO4 (0.1 ≤ x ≤ 1.0) ferrites were synthesized by citrate-gel auto combustion method. The structural parameter such as lattice parameter, X-ray density, bulk density and porosity variations with Cr doping were studied. The average crystallite size is in the range 8.5–10.5 nm. The surface morphology and elemental analysis was studied with SEM (EDAX) spectrum and the structural information analyzed with FTIR spectra. Magnetic properties were discussed with Cr3+ion concentration. Electrical parameters like dc resistivity and drift mobility were reported with function of te
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Chandrasekhar, Thalari, Ravi Naik, Sharanappa Chapi, and Dr Madhukumar R. "CONTROLLABLE SYNTHESIS AND CHARACTERIZATION OF CU-COZNFE2O4 NANO FERRITES BY AUTO-COMBUSTION ROUTE." In Futuristic Trends in Physical Sciences Volume 3 Book 1. Iterative International Publishers, Selfypage Developers Pvt Ltd, 2024. http://dx.doi.org/10.58532/v3bkps1ch1.

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The methods employed to prepare nano crystalline mixed ferrite materials during experimentation significantly affect the resulting particle size. The quality of ferrite materials greatly influences the performance of devices. The chemical composition and microstructure of ferrites, which determine their properties, are both determined by the preparation process. TheCoCuZnFe2O4 ferrite nanoferites were prepared by sol-gel method. The prepared samples were calcinated at 750oC shows sharper X-ray diffraction peaks, indicating increased crystallinity of the materials. Average crystallite sizes wer
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Shinde, V. S. "SYNTHESIS AND STRUCTURAL DETERMINATION OF CO SUBSTITUTED M-TYPE CA HEXAFERRITE." In Futuristic Trends in Physical Sciences Volume 3 Book 3. Iterative International Publishers, Selfypage Developers Pvt Ltd, 2024. http://dx.doi.org/10.58532/v3bkps3p2ch5.

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Co-substituted M-type Ca hexaferrite of composition CaCoFe 11 O 19 was synthesized by sol-gel auto-combustion method using metal nitrates as oxidants and citric acid as a reducing agent. The prepared sample was characterized by X-ray diffraction technology. The peaks observed in the XRD pattern confirm the M type of hexaferrite structure. No secondary peaks were observed that confirmed the purity of the sample. The calculated values of lattices parameters ‘a’ and ‘c’ were 5.9500 Å and 22.0779 Å respectively are well within the range of M type of hexaferrite. c/a ratio for the prepared sample i
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Elaya Kumar, Kannan, S. Muthulingam, and A. Manikandan. "Impact of Rare Earth Element Cerium on Structural and Magnetic Characterization of Different Nanoferrites." In Cerium - Chemistry, Technology, Geology, Soil Science and Economics [Working Title]. IntechOpen, 2024. http://dx.doi.org/10.5772/intechopen.1004167.

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Due to its numerous uses in the fields of magnetic recording devices, electronic devices, biosensors, high-frequency transformers, microwave devices, and radar devices, magnetic nanoferrites have drawn increased attention from society. There are several ways to make rare earth ion-doped spinel ferrites, including the sol-gel approach, auto-combustion method, hydrothermal method, co-precipitation method, ball milling method, and green synthesis method. Numerous studies have recently discussed the effect of rare earth ion substitution on spinel ferrite, concluding that it improved the material’s
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Sumalatha, Edapalli, Dachepalli Ravinder, Nyathani Maramu, et al. "Crystal Chemistry, Rietveld Analysis, Structural and Electrical Properties of Cobalt-Erbium Nano-Ferrites." In Ferrite [Working Title]. IntechOpen, 2021. http://dx.doi.org/10.5772/intechopen.98864.

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Synthesis of Cobalt-Erbium nano-ferrites with formulation CoErxFe2-xO4 (x = 0, 0.005, 0.010, 0.015, 0.020, 0.025, and 0.030) using technique of citrate-gel auto-combustion was done. Characterization of prepared powders was done by using XRD, EDAX, FESEM, AFM and FTIR Spectroscopy, DC resistivity properties respectively. XRD Rietveld Analysis, SEM, TEM and EDAX analysis were taken up in studying spectral, structural, magnetic and electrical properties. XRD pattern of CEF nano particles confirm single phase cubic spinal structure. The structural variables given by lattice constant (a), lattice v
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Conference papers on the topic "Citrate-gel auto combustion method"

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Rasmi, T., and K. A. Malini. "Synthesis of thermoelectric bismuth telluride alloys by sol-gel auto-combustion method." In 3RD INTERNATIONAL CONFERENCE ON MATHEMATICAL TECHNIQUES AND APPLICATIONS (e-ICMTA-2022). AIP Publishing, 2023. http://dx.doi.org/10.1063/5.0158459.

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Yuan, Guangbai, Jie Song, Fengwu Du, et al. "Structural and magnetic properties of Ni0.5Zn0.5SmxFe2-xO4 nanoferrite by sol-gel auto-combustion method." In 2016 6th International Conference on Advanced Design and Manufacturing Engineering (ICADME 2016). Atlantis Press, 2016. http://dx.doi.org/10.2991/icadme-16.2016.155.

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John, Subin P., and Jacob Mathew. "Superparamagnetism of Mg0.5Zn0.5Fe2O4 nanoparticles: Dependence of pH in the sol-gel auto-combustion method." In PROCEEDINGS OF THE INTERNATIONAL CONFERENCE ON ADVANCED MATERIALS: ICAM 2019. AIP Publishing, 2019. http://dx.doi.org/10.1063/1.5130276.

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Shukla, Jyoti, Mehjabeen Khan, Supriya Bisen, and Ashutosh Mishra. "Study of FT-IR spectrums of barium zirconate titanate synthesized via sol-gel auto combustion method." In PROF. DINESH VARSHNEY MEMORIAL NATIONAL CONFERENCE ON PHYSICS AND CHEMISTRY OF MATERIALS: NCPCM 2018. Author(s), 2019. http://dx.doi.org/10.1063/1.5098682.

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Wicaksono, Yusuf Aji, Poppy Puspitasari, M. Mirza Abdillah Pratama, Avita Ayu Permanasari, and Sukarni Sukarni. "Synthesis and characterisation of cobalt oxide (Co3O4) using sol-gel auto combustion method with stirring time variations." In PROCEEDINGS OF THE 1ST INTERNATIONAL CONFERENCE ON CIVIL ENGINEERING EDUCATION (ICCEE 2021). AIP Publishing, 2022. http://dx.doi.org/10.1063/5.0093867.

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Shukla, Jyoti, Supriya Bisen, Mehjabeen Khan, and Ashutosh Mishra. "Study of structural and optical properties of barium zirconate titanate prepared through sol – gel auto combustion method." In DAE SOLID STATE PHYSICS SYMPOSIUM 2018. AIP Publishing, 2019. http://dx.doi.org/10.1063/1.5113033.

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Bhandare, S. V., Harish Kumar Choudhary, Aroli Venkateshwara Anupama, et al. "Structure and magnetic properties of Ni substituted Co-Mg nanocrystal line ferrites synthesized by sol-gel auto-combustion method." In PROCEEDINGS OF THE INTERNATIONAL CONFERENCE ON PHYSICS OF MATERIALS AND NANOTECHNOLOGY ICPN 2019. AIP Publishing, 2020. http://dx.doi.org/10.1063/5.0009023.

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R, Anjana, Vishnu Narayanan V, Raguram T, and Rajni K.S. "Influence of Metal Ions (Cu, Ni, Zn) Substituted Cobalt Ferrite Nanoparticles Synthesized by Sol-Gel Auto Combustion Method for Magnetic Application." In The Second National Conference on Emerging Materials for Sustainable Future. Asian Research Association, 2024. http://dx.doi.org/10.54392/ara24117.

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The impact of metal ion substitution on the characteristics of cobalt ferrite nanoparticles is investigated in this work. Sol-gel auto-combustion was used to insert copper (Cu), nickel (Ni), and zinc (Zn) into the spinel lattice. The goal of the study is to comprehend the effects of these substitutions (CuCoFe, NiCoFe, and ZnCoFe) on the magnetic, spectral, and structural properties of the resultant nanoparticles. For every synthetic sample, the successful development of a cubic spinel phase has been confirmed by X-ray diffraction examination. The estimated crystallographic size is roughly 25
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Manteghi, Faranak, Mahnaz Kamel Attar Kar, and Reza Fazaeli. "Synthesis of NiFe2O4 nanoparticles by organic surfactants-assisted sol-gel auto-combustion method, characterization and determination of band gap." In The 19th International Electronic Conference on Synthetic Organic Chemistry. MDPI, 2015. http://dx.doi.org/10.3390/ecsoc-19-a046.

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Barati, M. R., S. A. Seyyed Ebrahimi, A. Badiei, Mohamad Rusop, and Tetsuo Soga. "Influence of the Metal Nitrates to Citric Acid Molar Ratio on the Processing of Nickel Zinc Ferrite Nanocrystalline Powders Synthesized by a Sol-Gel Auto Combustion Method." In NANOSCIENCE AND NANOTECHNOLOGY: International Conference on Nanoscience and Nanotechnology—2008. AIP, 2009. http://dx.doi.org/10.1063/1.3160195.

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