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Dissertations / Theses on the topic 'Cleavage of Carbon'

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Published: 5 June 2025

Last updated: 1 August 2025

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1

Allpress, Caleb J. "Oxidative Aliphatic Carbon-Carbon Bond Cleavage Reactions." DigitalCommons@USU, 2013. https://digitalcommons.usu.edu/etd/2003.

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The work presented in this dissertation has focused on synthesizing complexes of relevance to dioxygenase enzymes that oxidatively cleave aliphatic carbon-carbon bonds. The goal of this research was to elucidate mechanistic aspects of the activation of aliphatic carbon-carbon bonds towards cleavage by reaction with oxygen, and also investigate the regioselectivity of these reactions. The oxidative cleavage of a variety of enolizable substrates has been explored by utilizing several transition metal complexes supported by an aryl-appended tris(pyridylmethyl)amine ligand. In order to probe the w

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2

Nicholls, Julian Charles. "Carbon-carbon bond cleavage in agostic cobalt complexes." Thesis, University of Salford, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.258557.

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3

Sau, Roca Míriam. "From Click Chemistry to catalytic cleavage of unstrained C-C bonds." Doctoral thesis, Universitat Rovira i Virgili, 2016. http://hdl.handle.net/10803/396080.

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Aquesta tesi doctoral es basa principalment amb la síntesis de molècules petites potencialment útils per investigacions avançades. S'han utilitzat diferents metodologies per obtenir-les: 1) Cicloaddicions intramoleculars entre un alkí i una azida lliures de coure per l'obtenció de derivats de benzodiazepines. Obtenint-se una gran varietat de triazols fusionats a heterocicles de set membres. Posteriorment, s'han dut a terme proves d'activitat biològica. 2) a) Trencament d'enllaços carboni-carboni no activats d'amino alcohols i utilització d'aquest com a nucleòfil juntament amb bromurs d'ari

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4

Dombrowski, James Michael. "Catalytic Cleavage of Carbon-Carbon Sigma Bonds Using Transition Metals." Thesis, Boston College, 2005. http://hdl.handle.net/2345/407.

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Thesis advisor: Lawrence T. Scott<br>The focus of this project was to probe the ability of various transition metal complexes to cleave carbon-carbon bonds in a C30H12 hemifullerene. The hemifullerene was synthesized in our lab from commercial 1-tetralone and bromonaphthalene in six steps. Palladium and nickel complexes were used to open the five membered rings along the periphery of the C30H12 bowl. Diphosphine complexes of nickel were capable of opening either all three five membered rings or one of the periphery five membered rings and the central six membered ring<br>Thesis (BS) — Boston C

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5

King, Janice E. "Carbon-sulfur bond cleavage by environmental bacteria." Thesis, Queen's University Belfast, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.318772.

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6

Gripton, Christopher J. G. "Germyl linker cleavage with carbon-based electrophiles." Thesis, University of Sheffield, 2004. http://etheses.whiterose.ac.uk/15093/.

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This thesis describes the successful identification of a novel cross-coupling protocol for alkylaryldichlorogermanes, as part of an investigation towards the development of organogermanium linkers for solid phase synthesis. The application of Friedel-Crafts acylation towards the ipso degermylation of aromatic molecules with concomitant introduction of acyl functionality is also described. By way of introduction, an in depth review of the literature surrounding Group 14 organometallic cross-couplings is presented, concentrating on the recent developments in the area of organosilicon and organog

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7

Morris, A. D. "A study of carbon carbon bond cleavage in strained hydrocarbon systems." Thesis, Imperial College London, 1988. http://hdl.handle.net/10044/1/47189.

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8

Fernandez, Gimenez Marta. "Iridium-catalysed cleavage and formation of unstrained aliphatic carbon-carbon bonds." Thesis, University of Liverpool, 2018. http://livrepository.liverpool.ac.uk/3018330/.

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9

Johnson, Anne Elizabeth. "L-ribulose-5-phosphate 4-epimerase, epimerisation through carbon-carbon bond cleavage." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1998. http://www.collectionscanada.ca/obj/s4/f2/dsk2/ftp02/NQ27169.pdf.

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10

Saraf, Sushma L. "Oxidative Carbon-Carbon Bond Cleavage Reactions of Metal Flavonolato and Chlorodiketonate Complexes." DigitalCommons@USU, 2016. https://digitalcommons.usu.edu/etd/5161.

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The research presented in this dissertation has focused on studies of metal complexes which undergo oxidative aliphatic carbon-carbon bond cleavage using dioxygen as the oxidant. The goal of this research was to assess the reactivity and elucidate mechanistic details of the carbon-carbon bond cleavage reactions. The first part of this dissertation explores the light-induced dioxygenase reactivity of ruthenium flavonolato compounds. These compounds are of particular interest as they are currently being explored for their anti-cancer activity. The RuII(n6-p-cymene) flavonolato compounds studied

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11

Shigeno, Masanori. "Development of new synthetic reactions via carbon-carbon bond cleavage of cyclobutane derivatives." 京都大学 (Kyoto University), 2009. http://hdl.handle.net/2433/126510.

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Kyoto University (京都大学)<br>0048<br>新制・課程博士<br>博士(工学)<br>甲第14946号<br>工博第3173号<br>新制||工||1476(附属図書館)<br>27384<br>UT51-2009-M860<br>京都大学大学院工学研究科合成・生物化学専攻<br>(主査)教授村上正浩, 教授吉田潤一, 教授杉野目道紀<br>学位規則第4条第1項該当

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12

Maeda, Yasunari. "Studies on vanadium-, palladium-, and copper-catalyzed oxidation and carbon-carbon bond cleavage of organic compounds." 京都大学 (Kyoto University), 2005. http://hdl.handle.net/2433/144888.

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Kyoto University (京都大学)<br>0048<br>新制・課程博士<br>博士(工学)<br>甲第11533号<br>工博第2479号<br>新制||工||1336(附属図書館)<br>23176<br>UT51-2005-D283<br>京都大学大学院工学研究科物質ｴﾈﾙｷﾞｰ化学専攻<br>(主査)教授光藤武明, 教授檜山爲次郎, 教授大江浩一<br>学位規則第4条第1項該当

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13

Okumura, Shintaro. "New Ring-opening Reactions of Four-membered Carbo- and Sila-cyclic Compounds and Synthesis of 2-Alkoxy-1、3-dienes from Propargylic Alcohol Derivatives." Kyoto University, 2018. http://hdl.handle.net/2433/232487.

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14

Fartel, Beata. "Titanocene and zirconocene complexes for the carbon-oxygen bond cleavage of lignin model compounds." Thesis, University of British Columbia, 2014. http://hdl.handle.net/2429/46434.

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The development of well-defined transition metal catalysts for the selective cleavage of carbon-oxygen bonds is a critical challenge for the conversion of lignin to useful chemicals. Oxophilic titanocene complexes are particularly attractive for this application. They have been thoroughly studied in a variety of oxidation states and their reactivity can be dramatically altered by simple modifications of the ancillary ligands. Additionally, titanium is earth-abundant, inexpensive, and relatively non-toxic. Titanocene-mediated carbon-oxygen bond cleavage of the α-aryloxy ketones 2-phenoxy-1-phe

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15

Sawano, Shota. "Transformation of Organic Molecules Based on Ring Opening of Four-Membered Carbon Skeletons." 京都大学 (Kyoto University), 2015. http://hdl.handle.net/2433/200505.

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16

Gray, Steven Daniel. "Activation of nitrogen heterocycles towards the fundamental reactions of hydrodenitrogenation catalysis: Transition metal mediated carbon-nitrogen bond cleavage, hydrogenation, and ring degradation." Diss., The University of Arizona, 1995. http://hdl.handle.net/10150/187054.

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Treatment of the η(N,C)-pyridine complex [η²(N,C)-2,4,6-NC₅ᵗBU₃H₂]TA(DIPP)₂Cl (DIPP = 2,6-diisopropylphenoxide) with LiBEt₃H affords the C-N bond scission product (DIPP)₂Ta(=NCᵗBu=CHCᵗBu=CHCHᵗBu) (4). Reaction of [η²(N,C)-2,4,6-NC₅ᵗBU₃H₂]TA(DIPP)₂Cl with the appropriate alkyl lithium or Grignard reagent provides the alkyl derivatives [η²(N,C)-2,4,6-NC₅ᵗBU₃H₂]TA(DIPP)₂R [R = Me (5); Et (6); ⁿPr (7); ⁿBu (8); Ph (9); CH₂SiMe₃ (10)] in high yield. The molecular structure of the ethyl complex, [η²(N,C)-2,4,6-NC₅ᵗBU₃H₂]TA(DIPP)₂Et (6) has been determined. Upon thermolyzing complexes 5 - 9, a metal-

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17

Perini, Lorenzo. "Electrochemical Approaches for the Synthesis and Characterization of Innovative Electrode Materials." Doctoral thesis, Università degli studi di Padova, 2014. http://hdl.handle.net/11577/3423642.

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The synthesis of nanoscale catalysts is a cornerstone technology to meet the current energy challenges, spanning in a wide range of applications from fuel cell efficiency to pollutant degradation [1]. On this regard, electrocatalysis is a field of particular interest and one of the most promising, owing to the ability of electrochemical methods to study the reaction mechanisms and electron transfer (ET) dynamics at a molecular level, at the electrode surface. With the rapid advances in nanostructure synthesis, new nanoscale catalysts and novel catalytic properties continue to emerge [2]. Often

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18

Yang, Kaiyuan. "Substitution Chemistry of the Cobalt Complexes [Co₂(CO)₆(PhC≡CR) (R=Ph, H) and PhCCo₃(CO)₉] with the Diphosphine Ligands [Bis(diphenylphosphino)maleic Anhydride (BMA) and (Z)-Ph₂PCH=CHPPh₂]. Reversible Chelate-to-Bridge Diphosphine Ligand Exchange, Phosphorus-Carbon Bond Cleavage and Phosphorus-Carbon Bond Formation." Thesis, University of North Texas, 1994. https://digital.library.unt.edu/ark:/67531/metadc279206/.

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The tricobalt cluster PhCCo3(CO)9 (1) reacts with the bidentate phosphine ligand 2,3-bis(diphenylphosphino)maleic anhydride (bma) in the presence of added Me3NO to give the diphosphine-substituted cluster PhCCo3(CO)7(bma) (2). Cluster 2 is unstable in solution, readily losing CO to afford Co3(CO)6[(μ2-η2/η1-C(Ph)C=C(PPh2)C(O)OC(O)](μ2-PPh2) (3) as the sole observed product. VT-31P NMR measurements on cluster 2 indicate that the bma ligand functions as both a chelating and a bridging ligand. At -97 °C, 31P NMR analysis of 2 reveals a Keq of 5.7 in favor of the bridging isomer. The bridged bma c

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19

Patil, Nikhil Dilip. "A STUDY OF LIGNIN DEPOLYMERIZATION BY SELECTIVE CLEAVAGE OF THE Cα-Cβ LINKAGES IN LIGNIN MODEL COMPOUNDS VIA BAEYER-VILLIGER OXIDATION & AN INVESTIGATION OF THE CHANNELING REACTION IN NITROGEN-DOPED MULTIWALLED CARBON NANOTUBES (N-MWCNTS)". UKnowledge, 2014. http://uknowledge.uky.edu/chemistry_etds/43.

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A STUDY OF LIGNIN DEPOLYMERIZATION BY SELECTIVE CLEAVAGE OF THE Cα-Cβ LINKAGES IN LIGNIN MODEL COMPOUNDS VIA BAEYER-VILLIGER OXIDATION Lignin is amorphous aromatic polymer derived from plants and is a potential source of fuels and bulk chemicals. Herein, we present a survey of reagents for selective stepwise oxidation of lignin model compounds. Specifically, we have targeted the oxidative cleavage of Cα-Cβ bonds as a means to depolymerize lignin and obtain useful aromatic compounds. In this work, we prepared several lignin model compounds that possess structures, characteristic reactivity, and

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20

Bach, Delpeuch Antoine. "Etude du mécanisme de la réaction d'oxydation de l'éthanol sur électrocatalyseurs à base de Pt, Rh, SnO2 sur support carboné en milieu acide." Thesis, Grenoble, 2014. http://www.theses.fr/2014GRENI089/document.

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L'étude du mécanisme de la réaction d'oxydation de l'éthanol (EOR) a été réalisée sur des électrocatalyseurs bi- et tri-métalliques à base de Pt, Rh et SnO2 sur support carboné à l'aide de méthodes électrochimiques couplées (DEMS, in situ FTIR). Deux importantes problématiques de l'EOR ont été abordées: la déshydrogénation de la molécule d'éthanol et la cassure de sa liaison C-C.L'investigation de certains paramètres expérimentaux, comme l'épaisseur de la couche d'électrocatalyseur, a permis de démontrer q'une couche active épaisse conduit à une meilleure électrooxydation plus complète de l'ét

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21

McSorley, Fern R. "Enzymatic Cleavage of Carbon-Phosphorus Bonds." Thesis, 2013. http://hdl.handle.net/1974/8280.

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Inorganic phosphate (Pi) plays a critical role in many biological structures and processes. However, Pi typically occurs at low concentrations, particularly in marine environments. In comparison, naturally occurring organophosphonates, which are characterized by a stable carbon-phosphorus (CP) bond, are frequently present at higher concentrations. Accordingly, bacteria have evolved different mechanisms for cleaving the CP bond of organophosphonates to liberate Pi for metabolic use. Two prominent enzyme pathways for catabolic cleavage of a CP bond are examined in this thesis. The first, called

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22

Feng-Hong, Luo, and 羅峰宏. "Carbon-Carbon Bond Formation and Carbon-Carbon Bond Cleavage Catalyzed by Nickel and Palladium Complexes." Thesis, 1995. http://ndltd.ncl.edu.tw/handle/92123678239558196285.

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23

"Investigation of vinyl carbon-bromine bond cleavage by group 9 metalloporphyrin complexes and application of aryl carbon-bromine bond cleavage with rhodium porphyrin complexes." 2015. http://repository.lib.cuhk.edu.hk/en/item/cuhk-1291780.

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Wong, Ka Lai.<br>Thesis M.Phil. Chinese University of Hong Kong 2015.<br>Includes bibliographical references.<br>Abstracts also in Chinese.<br>Title from PDF title page (viewed on 11, November, 2016).

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24

"Reductive cleavage of the carbon-sulfur bond in bridged thiolato complexes." Chinese University of Hong Kong, 1987. http://library.cuhk.edu.hk/record=b5885804.

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25

Cheng, Cheng-Wei. "Synthesis and Reactivity of Osmium and Ruthenium Vinylidene Complexes: Cleavage and Reconstruction of Carbon-Carbon Bond." 2007. http://www.cetd.com.tw/ec/thesisdetail.aspx?etdun=U0001-2407200714232000.

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26

Rahman, Abul Kasem Fazlur. "The cleavage of carbon-carbon bond in [hapto]4-strained diolefin complexes of transition metals by protonation." Phd thesis, 1989. http://hdl.handle.net/1885/138854.

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27

Mahoney, Stuart James. "Innovative Methods for the Catalyzed Construction of Carbon-Carbon and Carbon-Hydrogen Bonds." Thesis, 2012. http://hdl.handle.net/10012/7015.

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The selective transformation of carbon-carbon and carbon-hydrogen bonds represents an attractive approach and rapidly developing frontier in synthesis. Benefits include step and atom economy, as well as the ubiquitous presence in organic molecules. Advances to this exciting realm of synthesis are described in this thesis with an emphasis on the development of catalytic, selective reactions under mild conditions. Additionally some applications of the methodologies are demonstrated. In Chapter 1, the first examples of inter-and intramolecular enantioselective conjugate alkenylations employing o

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28

Chen, Bo-Wei, and 陳柏維. "Preparation of palladium/ stacked graphene platelet nanofiber catalyst in supercritical fluid carbon dioxide for remediation of environmental contaminants—carbon/carbon bond cleavage of biphenyl." Thesis, 2015. http://ndltd.ncl.edu.tw/handle/h59zqh.

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Huang, Yu-Ting, and 黃鈺婷. "Palladium/Graphene Catalyst for Remediation of Environmental Contaminants— Carbon-Oxygen Bond Cleavage of Dioxins." Thesis, 2017. http://ndltd.ncl.edu.tw/handle/jj455k.

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碩士<br>中原大學<br>化學研究所<br>105<br>According to the Stockholm Convention, dioxins is a class of substances which is hard to break down in the natural environment, with high toxicity. It will accumulate in the environment and the body, thus is listed as one of the persistent organic pollutants. Question on how to reduce persistent organic pollutants''s concentration and toxicity, or how to degrade it into small molecules is still a key topic of scientists who have been concerned about environmental issues. In recent years, related research of dioxins, such as ball milling, photodegra

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30

Chang, Chia-Lung, та 張嘉隆. "New Ruthenium-Catalyzed Cleavage of a Carbon -Carbon Triple Bond and Rearrangement of α,β-Epoxy Ketones into 1,2-Diketones". Thesis, 2003. http://ndltd.ncl.edu.tw/handle/69039992051066760056.

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31

"Investigation and application of aryl carbon-halogen bond cleavage with rhodium and iridium porphyrin complexes." 2014. http://library.cuhk.edu.hk/record=b6115998.

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本論文主要研究銥和銠卟啉絡合物與鹵代苯 (ArX, X = Cl, Br, I)的碳-鹵鍵(Ar-X)的斷裂反應及其應用。本論文分為四個部分：（1）銠卟啉絡合物與鹵代苯(ArX, X = Cl, Br, I)之間的碳-鹵鍵(Ar-X)斷裂反應；（2）氟氯化苯的碳-氟鍵(Ar-F)與碳-氯鍵(Ar-Cl)斷裂的競爭反應；（3）氟取代基對金屬（銥和銠）-芳香碳(M-Ar)鍵強弱的影響；以及（4）銥卟啉氟硼荧絡合物的合成。<br>第一部分闡述了銠卟啉絡合物(Rh(ttp)Cl)與鹵代苯(ArX, X = Cl, Br, I) 之間的碳-鹵鍵 (Ar-X) 斷裂反應以及反應機理。在鹼性條件下，無論富電子還是缺電子的鹵代苯都能與Rh(ttp)Cl反應，生成Ar-X鍵斷裂的產物──銠卟啉芳基絡合物(Rh(ttp)Ar) 。機理研究顯示， Rh(ttp)Cl 首先與氫氧根離子反應生成Rh(ttp)OH，進而通過二聚反應生成[Rh(ttp)]₂。[Rh(ttp)]₂在加熱條件下與Rh(ttp)自由基可以互相轉化，產生的Rh(ttp)自由基與鹵代苯進行原位取代反應，生成銠卟啉芳基絡合物(Rh(ttp)Ar)和鹵素自由基。鹵素自由基可以和另一個Rh(ttp)自由基反應生成Rh(ttp)X，在氫氧根離子存在的條件下，Rh(ttp)X將再次轉化為Rh(ttp)OH繼續反應。<br>第二部分描述了氟氯化苯中

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32

張聖岳. "Proton-induced acceleration in the carbon-sulfur bond cleavage reactions unsaturated cyclic sulfones with ultransonically dispersed postassium." Thesis, 1992. http://ndltd.ncl.edu.tw/handle/35200220322823754419.

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33

Wöckel, Simone. "Synthetic Models for Dizinc Metallohydrolases." Doctoral thesis, 2011. http://hdl.handle.net/11858/00-1735-0000-0006-B09B-E.

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34

Abdelgawwad, Haytham Mohamed Gamaleldin Wahba. "Structural and biochemical characterization of the irganomercurial Lyase MerB." Thèse, 2016. http://hdl.handle.net/1866/18547.

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Le mercure est présent dans l'environnement à cause de phénomènes naturels (volcans) ou des activités humaines (combustion de combustibles fossiles). Le mercure existe sous forme de mercure élémentaire (Hg0), ionique (HgII) ou organique tel le méthylmercure (MeHg). Ces diverses formes sont en flux constant les uns avec les autres dans le cycle biogéochimique naturel. De par leur grande hydrophobicité et leur capacité à pénétrer les membranes biologiques, les composés organomercuriels contituent la forme la plus toxique de mercure retrouvée dans l’environnement Des niveaux élevés de MeHg ont d’

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Shiao, Shui-Sheng, and 蕭水生. "Silicon-Controlled Carbon-Carbon Bond Formations and Cleavages Involving Carbonyl Compounds and Silicon Reagents." Thesis, 1996. http://ndltd.ncl.edu.tw/handle/19826282833025353101.

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"Base-promoted aryl carbon-halogen bond cleavages by Iridium (III) porphyrins." Thesis, 2011. http://library.cuhk.edu.hk/record=b6075157.

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Cheung, Chi Wai.<br>"December 2010."<br>Thesis (Ph.D.)--Chinese University of Hong Kong, 2011.<br>Includes bibliographical references.<br>Electronic reproduction. Hong Kong : Chinese University of Hong Kong, [2012] System requirements: Adobe Acrobat Reader. Available via World Wide Web.<br>Abstract also in Chinese.

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Mala, Deep. "Chemistry of Ru(II) Complexes Bearing N-heterocyclic Carbene, Hydride, and Dihydrogen Ligands : Synthesis, Mechanistic Insights, and Applications." Thesis, 2016. http://etd.iisc.ac.in/handle/2005/4162.

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Introduction N-heterocyclic carbenes (NHC) are strong  donors and weak acceptors. Also, NHC forms strong metal-carbon bonds in metal complexes and hence complexes bearing NHC ligands are in general, thermally stable. Chemistry of NHCs and their transition metal complexes has been explored extensively in catalysis. Metal hydride or dihydrogen complexes are reactive intermediates and also employed as catalysts in several catalytic reactions such as hydrogenation, transfer hydrogenation, and hydroformylation. The binding of H2 to a metal center and its cleavage for the oxidative addition to a

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