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Dissertations / Theses on the topic 'Copper(I) Phosphine Complexes'

Author: Grafiati

Published: 4 June 2021

Last updated: 6 September 2023

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1

Black, Jane R. "Group 15 and 16 donor ligand complexes of copper and silver." Thesis, University of Southampton, 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.307087.

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2

Coventry, David N. "Tertiary-phosphine gold(I) and copper(I) complexes : precursors for metal deposition." Thesis, University of Edinburgh, 2002. http://hdl.handle.net/1842/12017.

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Tertiary-phosphine stabilised gold and copper complexes have been prepared with the intention to deposit elemental metal from solution. These complexes were intended to be delivered as a component of an ink on to a suitable substrate by an ink-jet printing process. Testing the compatibility of these complexes with ink-jet technology has been undertaken by Avecia and Seiko-Epson (this project's industrial sponsors). Four methyl(tertiary-phosphine)gold(I) complexes with a general molecular formula, [R<sub>3</sub>PAuCH<sub>3</sub>] (R = Ph, Ph-<i>p</i>-F, Ph-<i>p</i>-OMe and Me) were prepared by

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3

Determan, John J. "Photophysics and Photochemistry of Copper(I) Phosphine and Collidine Complexes: An Experimental/Theoretical Investigation." Thesis, University of North Texas, 2011. https://digital.library.unt.edu/ark:/67531/metadc84199/.

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Copper(I) complexes have been studied through both experimental and computational means in the presented work. Overall, the work focuses on photophysical and photochemical properties of copper(I) complexes. Photophysical and photochemical properties are found to be dependent on the geometries of the copper(I) complexes. One of the geometric properties that are important for both photochemical and photophysical properties is coordination number. Coordination numbers have been observed to be dependent on both ligand size and recrystallization conditions. The complexes geometric structure, a

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4

Mohan, Kumar Sreelatha Meera. "Synthèse de complexes cuivreux luminescents." Thesis, Strasbourg, 2012. http://www.theses.fr/2012STRAF068/document.

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La présente thèse décrit la préparation de complexes de Cu(I) stables grâce à l’ingénierie moléculaire de ligands permettant d’éviter la formation de plusieurs espèces en équilibre. Dans le cas de ligands P-N, la stratégie proposée repose sur l’utilisation d’un ligand ayant des substituants permettant de masquer un centre métallique et ainsi d’empêcher les réactions avec des nucléophiles permettant la dissociation du ligand. Dans le cas des dérivés [Cu(NN)(PP)]+, l’approche synthétique développée repose sur l’utilisation de ligands phénanthrolines macrocycliques empêchant la formation des comp

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5

Noack, Cassandra, and n/a. "Studies in Coordination Chemistry." Griffith University. School of Science, 2003. http://www4.gu.edu.au:8080/adt-root/public/adt-QGU20031030.145610.

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The research reported in this thesis was carried out in Brisbane, Australia and Calgary, Canada. The aim of the research conducted in Brisbane was to prepare a series of copper(I) and ruthenium(II) based complexes incorporating a hemilabile phosphine ligand and to determine whether or not these compounds possessed catalytic activity. The history, uses, properties and recent work incorporating hemilabile phosphine ligands is discussed in detail as well as the application of hemilabile ligands to atom transfer radical polymerization (ATRP) and the usefulness of the 'windscreen wiper' action of

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6

Noack, Cassandra. "Studies in Coordination Chemistry." Thesis, Griffith University, 2003. http://hdl.handle.net/10072/366798.

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The research reported in this thesis was carried out in Brisbane, Australia and Calgary, Canada. The aim of the research conducted in Brisbane was to prepare a series of copper(I) and ruthenium(II) based complexes incorporating a hemilabile phosphine ligand and to determine whether or not these compounds possessed catalytic activity. The history, uses, properties and recent work incorporating hemilabile phosphine ligands is discussed in detail as well as the application of hemilabile ligands to atom transfer radical polymerization (ATRP) and the usefulness of the 'windscreen wiper' action of

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7

Umuhire, Mahoro Gilbert. "Development of new cationic copper (l) complexes for white light-emitting electrochemical cells." Thesis, Normandie, 2021. http://www.theses.fr/2021NORMC202.

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De nouveaux complexes de cuivre(I) cationiques de formule générale [Cu(P^P)(N^N)][PF6] où P^P représente un ligand bis-phosphine chélatant, bis-[2- (diphenylphosphino)phenyl]ether (DPEPhos) et N^N, des ligands 2,2-bis-pyridyls ont été développés. Les complexes ont montré des émissions à l’état solide couvrant tout le spectre du visible et la présence de la fluorescence retardée activée thermiquement (TADF) a été démontrée. Ces complexes ont été évaluées dans des cellules électrochimiques luminescentes (LECs) et ont conduit aux LECs émettant dans de différentes couleurs, i.e., bleue, verte, jau

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8

Delavaux, Béatrice. "Complexes heterobimetalliques hydrures (ru-m) (m=rh,ir,cu) a ligands bisdiphenylphosphinomethane : synthese et reactivite." Toulouse 3, 1986. http://www.theses.fr/1986TOU30078.

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Synthese de complexes hydruro a coordinat dppm : ph::(2) pch::(2) pph::(2). L'etude de la reactivite de certains complexes comme rurhh::(2)cl(cod) (dppm)::(2), conduit a la preparation de nouveaux hydrures dont on etudie les structures

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9

Fry, Fiona Helen 1972. "Metal complexes based on macrocyclic ligands and their ability to hydrolyse phosphate esters." Monash University, School of Chemistry, 2002. http://arrow.monash.edu.au/hdl/1959.1/8279.

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10

Endrizzi, Francesco. "Thermodynamic studies on Cu(I) and Ag(I) phosphino complexes with potential anti-tumor activity." Doctoral thesis, Università degli studi di Padova, 2013. http://hdl.handle.net/11577/3423107.

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Some thermodynamic studies on the formation equilibria of new copper(I) and silver(I) complexes with the hydrophilic phosphine PTA (1,3,5-7-triazaphosphaadamantane) are presented. With the aim of finding new metal-based compounds with potential antitumor activity, some new copper(I) and silver(I) complexes of PTA phosphine were recently prepared. These compounds show a good cytotoxicity in-vitro against several human tumor cell lines, and their biological activity was related to the ability of copper to bind biologically important substates, after dissociation of one or more phosphines during

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11

Riegel, Nadège. "Synthèse de complexes de métaux de transition à partir des phosphines borane : application en catalyse homogène supportée sur polypyrrole." Cergy-Pontoise, 1997. http://www.theses.fr/1997CERG0023.

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Ce travail en deux parties avait pour objet l'utilisation des phosphines borane pour préparer des complexes de métaux de transition, en vue de leur application en catalyse homogène supportée ou non. La premiere partie concerne l'utilisation directe des phosphines borane pour préparer des complexes organometalliques. Pour cela deux strategies ont ete developpees, qui consistent soit en un echange de ligand entre une phosphine borane et un complexe organometallique (tungstene-thf), soit en l'utilisation des proprietes reductrices du groupement borane vis a vis de complexes du palladium(ii), du c

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12

Bissessar, Damien. "Synthèse de nouveaux composés phosphorés : vers de nouveaux additifs pour polymères et des complexes cuivreux luminescents innovants." Thesis, Strasbourg, 2018. http://www.theses.fr/2018STRAE029.

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Ce travail de thèse s’est inscrit dans le cadre d’un projet en relation étroite avec une industrie chimique. La problématique initiale concerne le développement de nouvelles molécules antioxydantes permettant de protéger les matériaux plastiques. Dans un premier temps, la stratégie envisagée s’appuie sur la synthèse de phosphines par hydrophosphination, réaction répondant aux principes de la chimie verte. La réaction est hautement régiosélective et la simplicité de la synthèse a permis d’obtenir de nombreuses nouvelles phosphines qui ont alors été testées pour leurs propriétés anti-oxydantes.

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13

Plancq, Sabine. "Heteronuclear carbonyl phosphine complexes." Thesis, Heriot-Watt University, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.335276.

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14

Rampazzi, Vincent. "Chimie de coordination du phosphore aux métaux du groupe 11 : progrès en catalyse de couplage C-N au Cu(I) et nouveaux complexes polyphosphines de l'Au(I)." Thesis, Dijon, 2014. http://www.theses.fr/2014DIJOS025/document.

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De nos jours et depuis quelques années maintenant, le principe de développement durable encourage les chimistes de tous horizons à développer de nouvelles méthodes de synthèse économiques et écologiques, les ressources naturelles de notre planète ne sont pas illimitées. Parmi les ressources les plus exploitées, nous trouvons le pétrole et le gaz. Outre ces derniers et le gaz, les métaux précieux sont également devenus indispensables.Cette thèse se concentre sur la valorisation de complexes de cuivre et d’or, obtenus à partir de ligands phosphorés synthétisés au sein du laboratoire. Dans un pre

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15

Lavender, Mark Harley. "Phosphine stabilised di-iron complexes." Thesis, University College London (University of London), 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.283749.

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16

Wells, F. J. "Tertiary phosphine complexes of vanadium." Thesis, Imperial College London, 1987. http://hdl.handle.net/10044/1/46906.

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17

Cartwright, Jonathan. "Organometallic chemistry of ruthenium phosphine complexes." Thesis, University of Warwick, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.307976.

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18

Norman, Timothy. "Imido and phosphine bridged organometallic complexes." Thesis, University College London (University of London), 1995. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.243522.

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19

Morton, David Alexander Vodden. "Structural studies of metal phosphine complexes." Thesis, University of Bristol, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.303770.

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20

Henderson, Steven G. D. "Spectroscopic studies of platinum halo-phosphine complexes." Thesis, University of Edinburgh, 1986. http://hdl.handle.net/1842/28226.

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21

Douglas, Thomas Mark. "Chemistry of cationic rhodium alkyl phosphine complexes." Thesis, University of Oxford, 2009. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.504386.

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22

Merle, Nicolas. "Transition metal complexes of chelating phosphine boranes." Thesis, University of Bath, 2006. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.426296.

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23

Haddad, Timothy S. "Group 4 diene complexes stabilized by phosphine donors." Thesis, University of British Columbia, 1987. http://hdl.handle.net/2429/26414.

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The synthesis of eight fluxional, diamagnetic group 4 complexes MR'(C₄H₆)[N(SiMe₂CH₂PR₂)₂] (M = Hf, Zr; R' = Ph, CH₂CMe₃; R = Me) and (M = Hf, Zr, R' = Cl; R = Me, CHMe₂ has been achieved. The X-ray crystallographic results of two of these complexes (M = Hf, Zr; R' = Ph; R = Me) indicate that the bonding of the diene unit has a significantly higher degree of ƞ⁴-π character than is present in Cp₂M(diene) (M = Hf, Zr) complexes, and therefore the M(II) resonance structure has more contribution to the overall bonding scheme. Consistent with all the NMR data available is that these complexes main

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24

Herring, A. M. "New transition metal complexes containing functionalised phosphine ligands." Thesis, University of Leeds, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.383967.

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25

Broadwood-Strong, Gillian. "Novel phosphine complexes of platinum and palladium (0)." Thesis, University of Sussex, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.385600.

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26

Doyle, Laurence. "Dinitrogen activation and reduction with iron phosphine complexes." Thesis, Imperial College London, 2015. http://hdl.handle.net/10044/1/51149.

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The conversion of dinitrogen to ammonia is a fundamental process for sustaining life on our planet. Ammonia provides a source of fixed nitrogen for nitrification and assimilation into plants, and is the ultimate source of almost all nitrogenated compounds. Synthetic ammonia is produced on a colossal scale by the Haber Bosch process, with an annual ammonia output exceeding 130 million tonnes. However, the intensive operating conditions of this process require a staggering energy cost; hence, the development of a lower energy solution is recognised as one of the major challenges of modern chemis

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27

Phelps, Jennifer. "Synthesis of homoleptic PT(0) acceptor phosphine complexes." Laramie, Wyo. : University of Wyoming, 2008. http://proquest.umi.com/pqdweb?did=1594481221&sid=1&Fmt=2&clientId=18949&RQT=309&VName=PQD.

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28

Dearling, Jason L. J. "Hypoxia targeting copper complexes." Thesis, University of Kent, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.297352.

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29

Lu, Qin. "Copper complexes of polyazacryptands." Thesis, Open University, 1999. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.298997.

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30

Kirkham, Matthew Samuel. "Activation of carbon-fluorine bonds using ruthenium dihydride complexes." Thesis, University of Bath, 2001. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.340990.

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31

Dallanegra, Romaeo. "Cationic rhodium complexes with chelating phosphine and phosphine alkene ligands. Application in dehydrogenation and dehydrocoupling reactions." Thesis, University of Oxford, 2011. http://ora.ox.ac.uk/objects/uuid:c6841db3-aadf-428f-bd4e-a16e9eaa3511.

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A series of cationic Rh(I) diphosphine and phosphine-alkene complexes have been isolated and fully characterised. The reactivity of these species towards hydrogenation, dehydrogenation and dehydrocoupling reactions has been investigated. The use of potentially hemilabile ligands DPEphos and XANTphos in the intramolecular dehydrogenation chemistry of tricyclopentylphosphine is reported. The comparison in reactivity of these isolated diphosphine phosphine-alkene complexes towards hydrogenation and with acetonitrile is discussed along with their ability to dehydrocouple secondary silane, Ph₂SiH₂,

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32

Carter, Alan. "Tertiary phosphine complexes of zirconium(IV) and hafnium(IV)." Thesis, University of British Columbia, 1985. http://hdl.handle.net/2429/24492.

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The tetra-halides of zirconium and hafnium were reacted with one equivalent of the potentially tridentate hybrid ligand, N(SiMe₂CH₂PR₂)2-, (R = Me, i-Pr, t-Bu) to generate the corresponding mono-ligand complexes MCl₃{N(SiMe₂CH₂PR₂)₂), (M = Zr, Hf). Based on the results obtained from the solution spectroscopic data and the single crystal X-ray diffraction analyses of HfCI₃{N(SiMe₂CH₂PMe₂)₂> and ZrCl₃{N(SiMe₂CH₂P(i-Pr)₂)₂) the stereochemistries of all the MCI ₃{N(SiMe ₂CH₂PR₂) ₂) complexes were found to be meridional in solution, but both facial and meridional geometries were displayed in the so

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33

Haddad, Timothy Samir. "Phosphine complexes of zirconium, hafnium and the lanthanoid metals." Thesis, University of British Columbia, 1990. http://hdl.handle.net/2429/31012.

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The synthesis of a variety of new lanthanoid phosphine complexes has been achieved by complexing either one or two amido-diphosphine ligands to yttrium, lutetium or lanthanum. At room temperature, the seven-coordinate bis(amido- diphosphine) complexes, MCl[N(SiMe₂CH₂PR₂)₂]₂- are fluxional and display NMR spectra indicative of complexes where the phosphorus donors are rapidly exchanging, probably via a dissociation-reassociation pathway. It is possible to generate thermally unstable hydrocarbyl complexes of the type, M(R)[N(SiMe₂CH₂PMe₂)₂]₂, which undergo a clean first order elimination of

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34

Larkin, Scott A. "Synthesis and Supermolecular Chemistry of Biphenylthioatogold(I)Phosphine Complexes." Fogler Library, University of Maine, 2007. http://www.library.umaine.edu/theses/pdf/LarkinSA2007.pdf.

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35

Farrer, M. J. "Synthesis of electrospray-active phosphine ligands and their complexes." Thesis, University of Cambridge, 2007. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.598946.

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This thesis is concerned with the synthesis and characterisation of electrospray-active phosphine ligands and their complexes, focusing on derivatives of proton sponges and bisphosphine monoxides (BPMOs). Phosphines containing Proton Sponge<sup>®</sup> (1,8-<i>bis</i>(dimethylamino)naphthalene, 1a) have been synthesised via sequential bromination, lithiation and phosphination to give [{1,8-<i>bis</i>(dimethylamino)naphthalen-4-yl}diphenylphosphine] (12b), [{1,8-bis(dimethylamino)naphthalen-2-yl}diphenylphosphine] (12a) and [<i>bis</i>{1,8-<i>bis</i>(dimethylamino)naphthalen-2-yl}phenylphosphin

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36

林觀陽 and Guanyang Lin. "The chemistry of organolanthanide complexes containing functionalized phosphine ligands." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 1996. http://hub.hku.hk/bib/B31235050.

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37

Robertson, Graham Stuart. "Studies of transition metal phosphine complexes relevant to catalysis." Thesis, Durham University, 1997. http://etheses.dur.ac.uk/5062/.

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Methoxycarbonyl compounds of the type [Pd(X)(CO(_2)Me)(L(_2))] (1) and [Pd(X)(CO(_2)Me)(L)(_2)] (2) were used as models in the work related to hydroesterification using methyl formate instead of CO and MeOH. The behaviour of the complexes (1) and (2) in solution was examined, as was their behaviour in the presence of alkenes and nucleophiles. Many of these derivatives were too unstable to isolate, forming the corresponding dichloride complexes [Pd(X)(_2)(L(_2))] (3) and [Pd(X)(_2)(L)(_2)] (4). Several crystal structures of such complexes were obtained. The cationic complex [Pd(CO(_2)Me)(MeCN)(

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38

Hawkins, I. M. "New transition metal complexes containing phosphine and sulphur ligands." Thesis, University of East Anglia, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.235225.

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39

Layzell, Timothy. "Rhenium hydride and related complexes containing tertiary phosphine ligands." Thesis, University of Leeds, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.303633.

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40

Markham, D. P. "The chemistry of heterobimetallic complexes containing bridging phosphine ligands." Thesis, University of Leeds, 1986. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.373519.

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41

Forder, Robin James. "Transition metal complexes of phosphine and mixed phosphathia ligands." Thesis, University of Southampton, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.243129.

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42

Kirk, Andrew Stuart. "Reactions of novel self-assembled iron(II) phosphine complexes." Thesis, University of Bath, 2008. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.512270.

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This thesis describes the synthesis and coordination chemistry of self-assembled multidentate iron(II) phosphine complexes. Chapter 1 introduces the background to phosphine ligands, their properties, interactions with transition metals and applications. The chapter then discusses macrocyclic and medium ring P,N-containing ligands, as well as some water soluble phosphines. The chapter also introduces the novel self-assembled macrocyclic phosphine complex [FeL1(H2O)2]SO4 (1) and its tetradentate cyclic phosphine ligand L1. Chapter 2 describes the synthesis of [FeL1(H2O)2]SO4 (1) and its coordina

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43

Hall, David Andrew. "Iron (II) phosphine complexes as models of nitrogenase function." Thesis, University of Sussex, 1994. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.240655.

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44

Dixon, Casey Michelle. "Phosphine-borane-stabilised carbanion complexes of main group elements." Thesis, University of Newcastle upon Tyne, 2016. http://hdl.handle.net/10443/3369.

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An array of phosphorus-stabilised-carbanion complexes of group 1, 2 and 14 elements and their behaviour in the solid state is reviewed, along with a brief overview of the chemistry of phosphine-boranes, stannyl-stannylenes, heteroleptic stannylenes and oxidative addition. The synthesis and characterisation of a range of novel phosphine-borane precursors is described: [Me2P(BH3)CH2SiMe2CH2]2 (1), [Ph2P(BH3)CH2Si(Me2)CH2]2 (2), 1,2- C6H4{CH2PiPr2(BH3)}2 (3), 1,2-C6H4{CH2PPh2(BH3)}2 (4), 1,2-C6H4{CH2PCy2(BH3)}2 (5), C6H5CH2PiPr2(BH3) (6), C6H5CH2PPh2(BH3) (7), C6H5CH2PCy2(BH3) (8), C6H5{CH2SiMe3P

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45

Lin, Guanyang. "The chemistry of organolanthanide complexes containing functionalized phosphine ligands /." Hong Kong : University of Hong Kong, 1996. http://sunzi.lib.hku.hk/hkuto/record.jsp?B19671519.

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46

Yau, Benita Chui Kam. "Organometallic chemistry of phosphine complexes of iron and ruthenium." Thesis, The University of Sydney, 1992. https://hdl.handle.net/2123/26717.

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This thesis describes two projects involving the organometallic chemistry of iron and ruthenium complexes with DMPE ligands [DMPE = 1,2-bis(dimethylphosphino)ethane]. The first study involves an investigation into the kinetics and mechanisms of OH bond activation reactions of [Fe(DMPE)2]. The second project involves an investigation into the synthesis of RuH2(DMPE)2, the formation and properties of trans-[RuH(n2-H2)(DMPE)2]*, and the reactions of RuH2(DMPE)2 with alkyl and aryl thiols. In Part I of this work, the kinetics of the cis/trans isomerization of FeH(C6H5)(DMPE)2 and FeD(C6D5)(DMPE

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47

Hodson, Annabelle G. W. "Phosphine and allyl halocarbonyl complexes of molybdenum and tungsten." Thesis, University of Bath, 1988. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.381895.

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48

Pounds, Thomas John. "Redox group-functionalised diphosphine complexes." Thesis, University of Liverpool, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.367302.

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49

Green, Lisa Marie. "Synthesis, characterization and reactivity of platinum(0)-tetraphosphion complexes and group VIII metal phosphine complexes coordinated to alkoxide and hydroxide ligands /." The Ohio State University, 1987. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487331541709992.

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50

Kramer, Ulrike. "Complexation of divalent copper, zinc and calcium ions by phosphate esters in aqueous solution." Doctoral thesis, University of Cape Town, 1988. http://hdl.handle.net/11427/17083.

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The role of metal ions as catalysts for numerous biochemical reactions has been the subject of many investigations. One of the most important classes of ligands are phosphate esters. In this thesis I describe the investigation of some phosphate ester-metal ion equilibria. Formation constants for the complexation of p-nitrophenyl phosphate, phenyl phosphate, 1-naphthyl phosphate, α-D-glucose-1'-phosphate, glycerol-2-phosphate, methyl phosphate, 8-quinolyl phosphate, 8-quinolyl methyl phosphate, triphosphate and fluorotriphosphate with protons, copper, zinc and calcium ions were determined by po

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