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Journal articles on the topic 'Crystal structure of tin(II)'

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Published: 4 June 2021

Last updated: 10 February 2022

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1

Khanderi, Jayaprakash, Bambar Davaasuren, Buthainah Ameen Alshankiti, and Alexander Rothenberger. "Tin(ii) ketoacidoximates: synthesis, X-ray structures and processing to tin(ii) oxide." Dalton Transactions 44, no. 46 (2015): 19820–28. http://dx.doi.org/10.1039/c5dt03103f.

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The synthesis and crystal structure of novel tin(ii) ketoacidoximates and their utility in forming SnO particles and thin films with a high level of oxidation control under ambient conditions are described.

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2

Hennings, Erik, Horst Schmidt, Martin Köhler, and Wolfgang Voigt. "Crystal structure of tin(II) perchlorate trihydrate." Acta Crystallographica Section E Structure Reports Online 70, no. 12 (2014): 474–76. http://dx.doi.org/10.1107/s1600536814024283.

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The title compound, [Sn(H2O)3](ClO4)2, was synthesized by the redox reaction of copper(II) perchlorate hexahydrate and metallic tin in perchloric acid. Both the trigonal–pyramidal [Sn(H2O)3]2+cations and tetrahedral perchlorate anions lie on crystallographic threefold axes. In the crystal, the cations are linked to the anions by O—H...O hydrogen bonds, generating (001) sheets.

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3

Batchelor, R. J., T. Birchall, and J. P. Johnson. "The crystal structure of Sn6O2(CF3CO2)8•CF3CO2H." Canadian Journal of Chemistry 65, no. 9 (1987): 2187–93. http://dx.doi.org/10.1139/v87-366.

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The X-ray crystal structure of Sn6O2(CF3CO2)8•CF3CO2H has been determined: R1 = 0.0519. The crystals were orthorhombic, space group Pna21, a = 18.327(4) Å, b = 12.209(3) Å, c = 19.218(3) Å, fw = 1762.29, and Z = 4. The structure consists of two sets of three tin(II) atoms, each set linked by a μ3-oxo bridge. The tin atoms are further linked by trifluoroacetate groups to form an extended structure in which the tin atoms can be described as having either SnX4E or SnX5E coordination.

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4

Archer, Steven J., Klaus R. Koch, and Luigi R. Nassimbeni. "Pentacoordinated tin(II); crystal structure of dichloro-[2,2??6?,2?-terpyridyl]-tin(II)." Journal of Crystallographic and Spectroscopic Research 16, no. 4 (1986): 449–58. http://dx.doi.org/10.1007/bf01161033.

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5

Chang, J. H., and J. Köhler. "Crystal structure of tin(II)dioxodecafluorostannate(IV), Sn4O2F10." Zeitschrift für Kristallographie - New Crystal Structures 214, no. 2 (1999): 147–48. http://dx.doi.org/10.1515/ncrs-1999-0204.

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6

Stafeeva, Varvara S., Alexander S. Mitiaev, Artem M. Abakumov, Alexander A. Tsirlin, Artem M. Makarevich, and Evgeny V. Antipov. "Crystal structure and chemical bonding in tin(II) acetate." Polyhedron 26, no. 18 (2007): 5365–69. http://dx.doi.org/10.1016/j.poly.2007.08.010.

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7

Hennings, Erik, Horst Schmidt, Martin Koehler, and Wolfgang Voigt. "ChemInform Abstract: Crystal Structure of Tin(II) Perchlorate Trihydrate." ChemInform 46, no. 18 (2015): no. http://dx.doi.org/10.1002/chin.201518003.

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8

Reuter, H. "Crystal structure of tin(II) acetate acetylacetonate, Sn(C5H7O2)(C2H3O2)." Zeitschrift für Kristallographie - New Crystal Structures 219, no. 1-4 (2004): 119–20. http://dx.doi.org/10.1524/ncrs.2004.219.14.119.

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9

Reuter, H. "Crystal structure of tin(II) acetate acetylacetonate, Sn(C5H7O2)(C2H3O2)." Zeitschrift für Kristallographie - New Crystal Structures 219, no. 2 (2004): 109–10. http://dx.doi.org/10.1524/ncrs.2004.219.2.109.

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10

Abrahams, Isaac, Stephen J. Clark, John D. Donaldson, Zahida I. Khan, and Jeffrey T. Southern. "Hydrolysis of tin(II) fluoride and crystal structure of Sn4OF6." Journal of the Chemical Society, Dalton Transactions, no. 17 (1994): 2581. http://dx.doi.org/10.1039/dt9940002581.

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11

Abrahams, I., and D. Z. Demetriou. "Inert Pair Effects in Tin and Lead Dihalides: Crystal Structure of Tin(II) Bromide." Journal of Solid State Chemistry 149, no. 1 (2000): 28–32. http://dx.doi.org/10.1006/jssc.1999.8489.

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12

Denes, Georges, M. Cecilia Madamba, Hocine Merazig, and Abdualhafed Muntasar. "When crystallography can use help from tin-119 Mössbauer spectroscopy." Acta Crystallographica Section A Foundations and Advances 70, a1 (2014): C1691. http://dx.doi.org/10.1107/s2053273314083089.

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Crystallography, the most powerful method for obtaining structural data, can benefit from help from other techniques. In this work, 119Sn Mössbauer spectroscopy was used to assist crystallography, for finding the tin(II) positions in the unit-cell and determine a tin(II) coordination in agreement with both the diffraction data and the tin electronic structure. Even high quality single crystal data do not guarantee that the right solution will be obtained. A first attempt at the structure of α–SnF2 yielded the tin positions with very reasonable R and Rw residuals, 0.23-0.25. However, the fluori

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13

ABRAHAMS, I., S. J. CLARK, J. D. DONALDSON, Z. I. KHAN, and J. T. SOUTHERN. "ChemInform Abstract: Hydrolysis of Tin(II) Fluoride and Crystal Structure of Sn4OF6." ChemInform 25, no. 51 (2010): no. http://dx.doi.org/10.1002/chin.199451020.

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14

Dolabdjian, Konstantin, Arno L. Görne, Richard Dronskowski, Markus Ströbele, and Hans-Jürgen Meyer. "Tin(ii) oxide carbodiimide and its relationship to SnO." Dalton Transactions 47, no. 38 (2018): 13378–83. http://dx.doi.org/10.1039/c8dt02747a.

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Sn<sub>2</sub>O(CN<sub>2</sub>) was obtained from a solid-state metathesis. Its crystal structure incorporates a Sn<sup>2+</sup> ion with a 5s<sup>2</sup> lone pair and was analyzed in relation to that of SnO by electronicstructure calculations and a COHP bonding analysis.

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15

Secara, Alina M., Justin F. Binder, Ala’aeddeen Swidan, and Charles L. B. Macdonald. "Synthesis and structural characterization of new polyether complexes of germanium(II) and tin(II)." Canadian Journal of Chemistry 96, no. 6 (2018): 570–77. http://dx.doi.org/10.1139/cjc-2017-0763.

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A series of germanium(II) and tin(II) bromide polyether complexes have been synthesized. Specifically, [GeBr([15]crown-5)][GeBr3], [GeBr([18]crown-6)][GeBr3], [GeBr(triglyme)][GeBr3], [GeBr(tetraglyme)][GeBr3], [SnBr([18]crown-6)][SnBr3], [Sn([15]crown-5)2][SnBr3]2, [SnBr(triglyme)][SnBr3], and [SnBr(tetraglyme)][SnBr3] have been fully characterized including by single crystal X-ray diffraction. The synthesis of [GeBr(dibenzo[24]crown-8)][GeBr3] and [GeCl(dibenzo[24]crown-8)][GeCl3] are also reported, along with the crystal structure of the latter’s water adduct, which features a water molecul

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16

Barbe, J. M., C. Ratti, P. Richard, C. Lecomte, R. Gerardin, and R. Guilard. "Tin(II) porphyrins: synthesis and spectroscopic properties of a series of divalent tin porphyrins. X-ray crystal structure of (2,3,7,8,12,13,17,18-octaethylprophinato)tin(II)." Inorganic Chemistry 29, no. 20 (1990): 4126–30. http://dx.doi.org/10.1021/ic00345a043.

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17

Husein, Saddam, Endang Tri Wahyuni, and Mudasir Mudasir. "Synthesis of Tin(II) Oxide (SnO) Nanoparticle by Hydrothermal Method." JKPK (Jurnal Kimia dan Pendidikan Kimia) 4, no. 3 (2019): 145. http://dx.doi.org/10.20961/jkpk.v4i3.29898.

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<p>This study aims to prepare nanomaterial tin(II) oxide (SnO) by using a simple hydrothermal method at low temperatures. The precursors used were tin(II) chloride dihydrate and sodium hydroxide pellets. Solid tin(II) chloride dihydrate and natrium hydroxide pellets are firstly dissolved in ethanol solvents separately and stirred for 3 h for each solution at a constant temperature 26<sup>o</sup>C. Characterization in this study were carried out by using X-ray diffraction (XRD) and Scanning Electron Microscopy-Energy Dispersive X-ray Spectroscopy (SEM-EDX). The results of the

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18

Klepp, K. O., and F. Fabian. "K2Sn4Se8 -ein gemischtvalentes Selenostannat / K2Sn4Se8 -A Mixed-Valent Selenostannate." Zeitschrift für Naturforschung B 47, no. 3 (1992): 406–10. http://dx.doi.org/10.1515/znb-1992-0318.

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AbstractTransparent, ruby red crystals of the new compound K2Sn4Se8 were obtained from K2Se, Sn and Se by high temperature synthesis. K2Sn4Se8 is monoclinic, space-group Cm with a = 6.436(3) Å, b = 18.934(9) Å, c = 7.417(5) Å, β = 96.26(2)°; Z = 2. The crystal structure was refined to a conventional R of 0.022 (Rw = 0.018).In K2Sn4Se8 the tin atoms have two distinct oxidation states +2 and +4. Sn(IV) is tetrahedrally coordinated by Se, Sn(II) has a pseudo-trigonal bipyramidal coordination MA4E which reveals a pronounced stereo-activity of the lone pair of electrons.In the crystal structure the

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19

Asamiya, Yuki, Takahiro Yamada, and Hisanori Yamane. "Synthesis and Characterization of NaCd0.92Sn1.08, Na(Cd0.28Sn0.72)2 and Na2CdSn5 with Three-Dimensional Cd-Sn Frameworks." Inorganics 9, no. 3 (2021): 19. http://dx.doi.org/10.3390/inorganics9030019.

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The crystal structures of three new ternary compounds, NaCd0.92Sn1.08 (I), Na(Cd0.28Sn0.72)2 (II), and Na2CdSn5 (III) synthesized in a sodium-cadmium-tin system were determined by single-crystal X-ray analysis to be the following: (I) LiGeZn-type structure (hexagonal, a = 4.9326(1) Å, c = 10.8508(3) Å, space group P-6m2); (II) CaIn2-type structure (hexagonal, a = 4.8458(2) Å, c = 7.7569(3) Å, P63/mmc); and (III) isotype with tI-Na2ZnSn5 (tetragonal, a = 6.4248(1) Å, c = 22.7993(5) Å, I-42d). Each compound has a three-dimensional framework structure mainly composed of four-fold coordinated Cd a

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20

Shpanchenko, Roman V., Alexander S. Mitiaev, Victoria V. Chernaya, Evgeny V. Antipov, Hiroya Sakurai, and Eiji Takayama-Muromachi. "The first tin(II) vanadium(III) phosphate SnVPO5: Crystal structure and magnetic properties." Journal of Solid State Chemistry 178, no. 10 (2005): 3014–19. http://dx.doi.org/10.1016/j.jssc.2005.07.014.

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21

Leung, Wing-Por, Wai-Him Kwok, Feng Xue, and Thomas C. W. Mak. "Synthesis and Crystal Structure of an Unprecedented Tin(II)−Tin(II) Donor−Acceptor Complex, RN2Sn→SnCl2[RN= CH(SiMe3)C9H6N-8]." Journal of the American Chemical Society 119, no. 5 (1997): 1145–46. http://dx.doi.org/10.1021/ja962687m.

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22

Atwood, David A., Jolin A. Jegier, Kyli J. Martin, and Drew Rutherford. "Tetradentate −N2O2 ligand complexes of Tin(II). X-ray crystal structure of [N,N′-(1,2-ethylene) bis (salicylaldamine)]tin(II), (SaleanH2Sn)." Journal of Organometallic Chemistry 503, no. 1 (1995): C4—C7. http://dx.doi.org/10.1016/0022-328x(95)05666-d.

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23

Brylak, Markus, and Wolfgang Jeitschko. "U3TiSb5, U3VSb5, U3CrSb5, and U3MnSb5 with "Anti"-Hf5Sn3Cu Type Structure." Zeitschrift für Naturforschung B 49, no. 6 (1994): 747–52. http://dx.doi.org/10.1515/znb-1994-0605.

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The title compounds have been prepared from the elemental components by arc-melting and subsequent annealing. Single crystals of U3TiSb5 and U3MnSb5 were obtained from a tin flux and their structures were determined from single-crystal X-ray data: P63/mcm, Z = 2; a = 913.9(2), c = 611.2(1) pm, R = 0.011 (233 structure factors, 14 variables) for U3TiSb5 and a = 916.8(2), c = 613.2(1) pm, R = 0.015 (427 structure factors, 14 variables) for U3MnSb5. The lattice constants of the isotypic compounds are: a = 908.2(2), c = 608.3(2) pm for U3VSb5 and a = 911.0(1), c = 611.5(1) pm for U3CrSb5. The stru

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24

Adams, David C., Thomas Birchall, Romolo Faggiani, Ronald J. Gillespie, and John E. Vekris. "The 119Sn Mössbauer and solid-state NMR and the crystal and molecular structure of tin(II) bisfluorosulfate, Sn(OSO2F)2." Canadian Journal of Chemistry 69, no. 12 (1991): 2122–26. http://dx.doi.org/10.1139/v91-306.

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The reaction of tin(II) fluoride with fluorosulfuric acid has been shown to produce tin(II) bisfluorosulfate. Crystals of Sn(OSO2F)2 are monoclinic, space group P21/c with a = 5.195(1), b = 9.709(1), c = 13.861(1) Å, β = 110.12(1)°, Z = 4, R = 0.029, and Rw = 0.030 for 1461 unique reflections. The structure consists of a three-dimensional framework of fluorosulfate groups linked by O—Sn—O bridges with the two crystallographically independent fluorosulfates acting as tridentate bridging ligands between tin atoms. There are four short bonds (Sn—O = 2.338(3), 2.350(3), 2.398(4), and 2.427(3) Å) a

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25

Reger, Daniel L., Steven J. Knox, and Lukasz Lebioda. "Polyphosphinoylmethanide complexes of tin(II). Crystal and molecular structure of {[(C6H5)2PO]3C}2Sn." Inorganica Chimica Acta 178, no. 1 (1990): 89–92. http://dx.doi.org/10.1016/s0020-1693(00)88139-6.

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26

Olbert, Dirk, Alexander Kalisch, Helmar Görls, Irina Malkin Ondik, Markus Reiher, and Matthias Westerhausen. "Syntheses, Crystal Structure and Reactivity of Tin(II) Bis[N-(diphenylphosphanyl)(2-pyridylmethyl)amide]." Zeitschrift für anorganische und allgemeine Chemie 635, no. 3 (2009): 462–70. http://dx.doi.org/10.1002/zaac.200801328.

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27

Zubkov, V. G., A. P. Tyutyunnik, I. F. Berger, et al. "ChemInform Abstract: Anhydrous Tin and Lead Hexacyanoferrates(II). Part 1. Synthesis and Crystal Structure." ChemInform 32, no. 31 (2010): no. http://dx.doi.org/10.1002/chin.200131006.

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28

Haezam, Farah Natasha, Normah Awang, Nurul Farahana Kamaludin, Mukesh M. Jotani та Edward R. T. Tiekink. "(N,N-Diallyldithiocarbamato-κ2 S,S′)triphenyltin(IV) and bis(N,N-diallyldithiocarbamato-κ2 S,S′)diphenyltin(IV): crystal structure, Hirshfeld surface analysis and computational study". Acta Crystallographica Section E Crystallographic Communications 76, № 2 (2020): 167–76. http://dx.doi.org/10.1107/s2056989020000122.

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The crystal and molecular structures of the title organotin dithiocarbamate compounds, [Sn(C6H5)3(C7H10NS2)] (I) and [Sn(C6H5)2(C7H10NS2)2] (II), present very distinct tin atom coordination geometries. In (I), the dithiocarbamate ligand is asymmetrically coordinating with the resulting C3S2 donor set defining a coordination geometry intermediate between square-pyramidal and trigonal–bipyramidal. In (II), two independent molecules comprise the asymmetric unit, which differ in the conformations of the allyl substituents and in the relative orientations of the tin-bound phenyl rings. The dithioca

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29

Chappell, SD, LM Engelhardt, CL Raston та AH White. "Structural Characterization of Di-μ-hydroxo-bis[trichloro(tetrahydrofuran)tin(II)] Bis(tetrahydrofuran)". Australian Journal of Chemistry 41, № 7 (1988): 1123. http://dx.doi.org/10.1071/ch9881123.

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The title compound [( thf )Cl3Sn(OH)2SnCl3( thf )].2thf ( thf = tetrahydrofuran ) has been characterized by single-crystal X-ray structure determination, allowing comparison of its geometry with the recently recorded [( thf )BrCl2Sn(OH)2Cl2Br( thf )].2thf,1 with which it is isomorphous.

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30

Lieberman, Craig M., Alexander S. Filatov, Volodimir D. Vreshch та Evgeny V. Dikarev. "Bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)tetrakis(μ4-1,1,1,5,5,5-hexafluoropentane-2,2,4,4-tetraolato)copper(II)octatin(II): a prospective precursor for Cu-doped SnO2films". Acta Crystallographica Section C Crystal Structure Communications 69, № 12 (2013): 1427–30. http://dx.doi.org/10.1107/s0108270113025717.

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The crystal structure of a tin-rich heterometallic supramolecular product, [CuSn8(C5HF6O2)2(C5H2F6O4)4] or [Sn4(hfpt)2–Cu(hfac)2–Sn4(hfpt)2], (I), is reported (hfpt is the tetraanion of 1,1,1,5,5,5-hexafluoropentane-2,2,4,4-tetraol and hfac is the anion of 1,1,1,5,5,5-hexafluoropentane-2,4-dione). Reaction between tin(II) tetraolate, [Sn4(hfpt)2], and copper(II) β-diketonate, [Cu(hfac)2], was utilized for the preparation of (I). The asymmetric unit consists of the whole [Sn4(hfpt)2] unit and half of a [Cu(hfac)2] unit, with the Cu atom lying on an inversion center. Intermolecular Cu...O intera

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31

Geller, Jordan M., Ian S. Butler, Denis FR Gilson, Frederick G. Morin, Ivor Wharf, and F. Bélanger-Gariépy. "X-ray diffraction and solid-state 119Sn CP-MAS NMR studies of some triaryltin(IV) chlorides." Canadian Journal of Chemistry 81, no. 11 (2003): 1187–95. http://dx.doi.org/10.1139/v03-115.

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The solid-state 119Sn cross-polarization (CP) magic angle spinning (MAS) NMR spectra of a series of triaryltin chlorides of the form Ar3SnCl have been acquired. The indirect spin-spin coupling constants (J(119Sn-35Cl)), quadrupolar-dipolar shifts (d(119Sn-35Cl)), and the 119Sn chemical shift tensors were extracted. For the spectrum of triphenyltin chloride (I) the validity of the first-order perturbation approximation was tested by comparing results of both the perturbation and cubic-equation approaches and a variable-temperature NMR study undertaken to investigate the influence of the previou

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32

Harmgarth, Nicole, Phil Liebing, Philipp Hillebrand, Sabine Busse, and Frank T. Edelmann. "Synthesis and crystal structures of two new tin bis(carboranylamidinate) complexes." Acta Crystallographica Section E Crystallographic Communications 73, no. 10 (2017): 1443–48. http://dx.doi.org/10.1107/s2056989017012671.

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Reaction of 2 equiv. of the lithium carboranylamidinate Li[o-(C2H10B10)C(NCy)(NHCy)] with SnCl2in THF afforded the stannylene compound bis(N,N′-dicyclohexylamidinatocarboranate)tin(II), SnII[o-(C2H10B10)C(NCy)(NHCy)]2(1). A similar reaction of SnCl4with 2 equiv. of Li[o-(C2H10B10)C(NiPr)(NHiPr)] unexpectedly afforded the known solvated pentachloridostannate(IV) salt [Li(THF)4][SnCl5(THF)] as the main reaction product. Small amounts of the new chlorido-tin(IV) bis(carboranylamidinate) bis(N,N′-diisopropylamidinatocarboranate)chloridotin(IV), SnIVCl[o-(C2H10B10)C(NiPr)(NHiPr)][o-(C2H10B10)C(NiPr

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33

Yu, Dehui, Hongbo Tong, and Meisu Zhou. "Syntheses, crystal structures and catalytic property of two bulky tin(II) complexes." Polyhedron 191 (November 2020): 114817. http://dx.doi.org/10.1016/j.poly.2020.114817.

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34

Henkel, Felix, and Hans Reuter. "Two coordination compounds of SnCl2 with 4-methylpyridine N-oxide." Acta Crystallographica Section E Crystallographic Communications 77, no. 2 (2021): 91–95. http://dx.doi.org/10.1107/s2056989021000025.

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In the solid-state structures of catena-poly[[dichloridotin(II)]-μ2-(4-methylpyridine N-oxide)-κ2 O:O], [SnCl2(C6H7NO)] n , 1, and dichloridobis(4-methylpyridine N-oxide-κO)tin(II), [SnCl2(C6H7NO)2], 2, the bivalent tin atoms reveal a seesaw coordination with both chlorine atoms in equatorial and the Lewis base molecules in axial positions. While the Sn—Cl distances are almost identical, the Sn—O distances vary significantly as a result of the different bonding modes (μ2 for 1, μ1 for 2) of the 4-methylpyridin-N-oxide molecules, giving rise to a one-dimensional coordination polymer for the 1:1

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35

Henkel, Felix, and Hans Reuter. "Two coordination compounds of SnCl2 with 4-methylpyridine N-oxide." Acta Crystallographica Section E Crystallographic Communications 77, no. 2 (2021): 91–95. http://dx.doi.org/10.1107/s2056989021000025.

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In the solid-state structures of catena-poly[[dichloridotin(II)]-μ2-(4-methylpyridine N-oxide)-κ2 O:O], [SnCl2(C6H7NO)] n , 1, and dichloridobis(4-methylpyridine N-oxide-κO)tin(II), [SnCl2(C6H7NO)2], 2, the bivalent tin atoms reveal a seesaw coordination with both chlorine atoms in equatorial and the Lewis base molecules in axial positions. While the Sn—Cl distances are almost identical, the Sn—O distances vary significantly as a result of the different bonding modes (μ2 for 1, μ1 for 2) of the 4-methylpyridin-N-oxide molecules, giving rise to a one-dimensional coordination polymer for the 1:1

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36

Ibarra-Rodríguez, Marisol, H. V. Rasika Dias, Víctor M. Jiménez-Pérez, Blanca M. Muñoz-Flores, Angelina Flores-Parra, and Sonia Sánchez. "Dinuclear Tin(II) Complex of a Bulky cis-Oxamide: Synthesis, Characterization, Crystal Structure, and DFT Studies." Zeitschrift für anorganische und allgemeine Chemie 638, no. 10 (2012): 1486–90. http://dx.doi.org/10.1002/zaac.201200212.

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37

Zhou, Wei, Jing Zhang, Zhen-Gang Sun, et al. "Synthesis, crystal structures, and luminescent properties of tin(II) and lead(II) carboxyphosphonates with 3D framework structures." Inorganic Chemistry Communications 47 (September 2014): 37–41. http://dx.doi.org/10.1016/j.inoche.2014.07.010.

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38

Lafuente, Barbara, Hexiong Yang, and Robert T. Downs. "Crystal structure of tetrawickmanite, Mn2+Sn4+(OH)6." Acta Crystallographica Section E Crystallographic Communications 71, no. 2 (2015): 234–37. http://dx.doi.org/10.1107/s2056989015001632.

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The crystal structure of tetrawickmanite, ideally Mn2+Sn4+(OH)6[manganese(II) tin(IV) hexahydroxide], has been determined based on single-crystal X-ray diffraction data collected from a natural sample from Långban, Sweden. Tetrawickmanite belongs to the octahedral-framework group of hydroxide-perovskite minerals, described by the general formulaBB'(OH)6with a perovskite derivative structure. The structure differs from that of anABO3perovskite in that theAsite is empty while each O atom is bonded to an H atom. The perovskiteB-type cations split into orderedBandB′ sites, which are occupied by Mn

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39

Donaldson, John D., Susan M. Grimes, Simon R. Johnston, and Isaac Abrahams. "Characterisation of the tin(II) hydroxide cation [Sn3(OH)4]2+, and the crystal structure of tritin(II) tetrahydroxide dinitrate." Journal of the Chemical Society, Dalton Transactions, no. 13 (1995): 2273. http://dx.doi.org/10.1039/dt9950002273.

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40

Wiederkehr, Jessica, Christoph Wölper та Stephan Schulz. "Synthesis, solid-state structures and reduction reactions of heteroleptic Ge(II) and Sn(II) β-ketoiminate complexes". Zeitschrift für Naturforschung B 72, № 11 (2017): 813–20. http://dx.doi.org/10.1515/znb-2017-0098.

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AbstractA series of new heteroleptic divalent germaniun and tin complexes of the general type L1,4GeN(SiMe3)2 (1, 2) and L1−4SnN(SiMe3)2 (3–6) were synthesized by reaction of β-ketimines L1−4H with Ge[N(SiMe3)2]2 and Sn[N(SiMe3)2]2, respectively. The reaction of 3 with the strong Mg(I) reductant L5Mg yielded the heteroleptic complex L1MgL57 after ligand transfer from tin to magnesium, whereas analogous reactions of L4GeN(SiMe3)22 and L4SnN(SiMe3)26 with L5Mg occurred with formation of insoluble precipitates, transfer of the amido substituent from the group 14 metal to magnesium and subsequent

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41

Birchall, Thomas, Romolo Faggiani, Colin J. L. Lock, and Veeragathy Manivannan. "Preparation and partial oxidation of tin(II) trifluoroacetate: spectroscopic properties and X-ray crystal structure of di-µ3-oxo-octakis-µ-trifluoroacetato-tetratin(II)tin(IV)." J. Chem. Soc., Dalton Trans., no. 7 (1987): 1675–82. http://dx.doi.org/10.1039/dt9870001675.

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Ryan, M. A., Mark W. Peterson, D. L. Williamson, James S. Frey, Gary E. Maciel, and B. A. Parkinson. "Metal site disorder in zinc tin phosphide." Journal of Materials Research 2, no. 4 (1987): 528–37. http://dx.doi.org/10.1557/jmr.1987.0528.

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The optoelectronic properties of the II-IV-V2 semiconductor ZnSnP2 are studied as a function of the cooling rate of the crystal growth melt. The structure of the material, as studied by x-ray diffraction, is seen to change from chalcopyrite to sphalerite as the cooling rate is increased. Photoelectrochemical measurements show that the bandgap of the material decreases from 1.64 eV for the chalcopyrite to 1.25 eV as the structure approaches sphalerite. The 119Sn Mössbauer spectroscopy shows both an isomer shift and a broadening of the 119Sn resonance as a result of new tin environments produced

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43

Vandenbergen, AM, JD Cashion, GD Fallon, and BO West. "Crystal Structures, Mössbauer Spectra and Reactivity of Sn,II Salicylideneimines." Australian Journal of Chemistry 43, no. 9 (1990): 1559. http://dx.doi.org/10.1071/ch9901559.

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Single-crystal X-ray diffraction studies have been carried out on the tetradentate SnII complex N,N′-(4,5-dimethyl-1,2-phenylene ) bis ( salicylideneiminato )tin(II) [ Sn ( saldph )] and the tetradentate complex N-(2-oxidophenyl) salicylideneiminatotin (II) [ Sn ( salop )]. Sn ( saldph ) is a monomer and has the SnII ion 1.126(1)Ǻ above the plane of the O2N2 donors while Sn ( salop ) is dimeric with bridging between SnII ions by the oxygens of the oxidophenyl groups. SnII ions are raised above the O3N donor planes by 1.109(7)Ǻ while the molecules are bent along the bridging O-O axis with a dih

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Pettinari, Claudio, Fabio Marchetti, Augusto Cingolani, Clara Marciante, Riccardo Spagna, and Marcello Colapietro. "Synthesis and characterization of some tin(II) and tin(IV) derivatives of 4-acyl-5-pyrazolones. Crystal structure of bis(1-phenyl-3-methyl-4-acetyl-pyrazolon-5-ato)tin(II)." Polyhedron 13, no. 6-7 (1994): 939–50. http://dx.doi.org/10.1016/s0277-5387(00)83014-4.

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Flörke, U., та H. J. Haupt. "Crystal structure of dibromo-bis(tricarbonyl-η-cyclopentadienyl-molybdenum)-tin(II), Br2((CO)3(C5H5)Mo)2Sn". Zeitschrift für Kristallographie 202, № 1-2 (1992): 147–49. http://dx.doi.org/10.1524/zkri.1992.202.1-2.147.

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Donaldson, John D., Susan M. Grimes, Anna Nicolaides, and Peter J. Smith. "Evidence for the predominance of trigonal pyramidal environments in tin(II) chemistry: The crystal structure of potassium (hydrogen(bismaleato))stannate(II)." Polyhedron 4, no. 3 (1985): 391–94. http://dx.doi.org/10.1016/s0277-5387(00)86997-1.

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47

Макрушина, А. Н., В. А. Плотников, Б. Ф. Демьянов та С. В. Макаров. "Субструктура интерметаллического соединения Cu-=SUB=-3-=/SUB=-Sn в тонкопленочном состоянии". Журнал технической физики 89, № 6 (2019): 907. http://dx.doi.org/10.21883/jtf.2019.06.47639.298-18.

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AbstractThe crystalline structure of intermetallic Cu_3Sn synthesized by successively condensing thin layers of copper and tin on a substrate at 150°C has been studied. Cu_3Sn compound exists in a very narrow homogeneity range and has a long-period close-packed ordered D0_19 superstructure. It has been found that the crystal lattice exhibits many slip traces associated with dislocation motion. The dislocation motion is due to the stressed state of the crystal, which can be characterized as uniform extension. Electron micrographs show that slip traces in the Cu_3Sn crystal are parallel to the (

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Veith, M., and R. Rosier. "Alkoxistannate, II [1] Tri(tert-butoxi)alkalistannate(II): Darstellung und Strukturen / Alkoxistannate, II [1] Tri(tert-butoxi)alkalistannates(II): Synthesis and Structures." Zeitschrift für Naturforschung B 41, no. 9 (1986): 1071–80. http://dx.doi.org/10.1515/znb-1986-0903.

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Abstract Tri(tert-butoxi)alkalistannates (M(O'Bu)3Sn, M = Li, Na, K, Rb, Cs) are obtained by reaction of alkali-fert-butanolates with tindi-tert-butoxide. If M equals Li or Na (1, 2) molecular com pounds are formed, which consist of two formula units. 1 crystallizes in a m onoclinic cell (space group P21/c; a = 966.5(3), b = 1819(1), c = 1014(1) pm. β = 107.1(1)°, Z = 4); 2 is triclinic (space group P1̄; a = 1041(1), b = 2046(1), c = 1033(1) pm. a = 92.3(2), β = 118.6(1), y = 108.3(3)° and Z = 4). The molecules 1 and 2 are closely related structurally despite their different space groups. The

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Antao, Sytle M. "The crystal structure of tin sulphate, SnSO4, and comparison with isostructural SrSO4, PbSO4, and BaSO4." Powder Diffraction 27, no. 3 (2012): 179–83. http://dx.doi.org/10.1017/s0885715612000450.

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The crystal structure of tin (II) sulphate, SnSO4, was obtained by Rietveld refinement using synchrotron high-resolution powder X-ray diffraction (HRPXRD) data. The structure was refined in space group Pbnm. The unit-cell parameters for SnSO4 are a = 7.12322(1), b = 8.81041(1), c = 5.32809(1) Å, and V = 334.383(1) Å3. The average 〈Sn–O〉 [12] distance is 2.9391(4) Å. However, the Sn2+cation has a pyramidal [3]-coordination to O atoms and the average 〈Sn–O〉 [3] = 2.271(1) Å. If Sn is considered as [12]-coordinated, SnSO4 has a structure similar to barite, BaSO4, and its structural parameters are

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Zhang, Dao Li, Zhi Bing Deng, Jian Bing Zhang, and Liang Yan Chen. "The Optical and Electrical Properties of Antimony-Doped Tin Oxide Transparent Conducting Thin Films Prepared by Sol-Gel Dip-Coating Technique." Key Engineering Materials 336-338 (April 2007): 754–57. http://dx.doi.org/10.4028/www.scientific.net/kem.336-338.754.

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Antimony-doped tin oxide (ATO) transparent conducting thin films were prepared by sol-gel dip-coating technique in the alcohol solution of metal salts of tin (II) chloride dehydrate and antimony tri-chloride. Usual glass slides (25×76×1mm3) were used as the substrates. As-prepared thin films were dried at temperature of 343K and annealed at temperatures of 673~823K. Their optical properties were analyzed by Hitachi U-3310 spectrophotometer. The good optical transmission of the ATO thin films has been obtained as high as 80%-90% in visible region by the optimization of deposition conditions, bu

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