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Journal articles on the topic 'Cyanoacetohydrazide'

Author: Grafiati

Published: 4 June 2021

Last updated: 1 February 2022

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1

Jadeja, Juvansinh, Mayank Mamtora, Mitesh B. Gondaliya, Rohit Manawar, and Manish K. Shah. "Synthesis, Spectral Analysis and Evolution of Antimicrobial Activity of Schiff Base of Cyanoacetohydrazide." International Letters of Chemistry, Physics and Astronomy 52 (June 2015): 100–110. http://dx.doi.org/10.18052/www.scipress.com/ilcpa.52.100.

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In search of some antimicrobial agents, synthesis of some Schiff base of cyanoacetohydrazide derivatives has been reported. The structures of all the synthesized compounds were established on the bases of various spectroscopic methods. All Schiff base were screened for antimicrobial activity. cyanoacetohydrazide were found to possess better antimicrobial potential.

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2

Pomes Hernandez, R., A. Gómez González, A. Rosado Pérez, B. M. Nápoles Frías, R. A. Toscano, and J. Quincoces Suárez. "N'-[Bis(methylthio)methylene]cyanoacetohydrazide." Acta Crystallographica Section C Crystal Structure Communications 52, no. 11 (1996): 2941–42. http://dx.doi.org/10.1107/s0108270196007147.

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3

Atta-Allah, Saad R., Wael S. I. Abou-Elmagd, Kamal A. A. Kandeel, Magdy M. Hemdan, David S. A. Haneen, and Ahmed S. A. Youssef. "Synthesis and Antimicrobial Activity Evaluation of Some Novel Hydrazone, Pyrazolone, Chromenone, 2-Pyridone and 2-Pyrone Derivatives." Journal of Chemical Research 41, no. 11 (2017): 617–23. http://dx.doi.org/10.3184/174751917x15065183733150.

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A cyanoacetohydrazide derivative underwent a series of reactions with different nucleophilic reagents, such as hydrazine hydrate, p-chlorobenzaldehyde and salicylaldehyde, to give the condensation products. In addition, an arylidene malononitrile was reacted with different nitrogen nucleophiles, such as hydrazine hydrate, thiocarbohydrazide and cyanoacetohydrazide, to afford the hydrazine, hydrazone and pyridin-2-one derivatives, respectively. Furthermore, a pyridin-2-one derivative was reacted with different carbon electrophiles, such as carbon disulfide, p-chlorobenzaldehyde and acetic anhyd

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4

Elkholy, Said S., Khalid D. Khalil, and Maher Zaki Elsabee. "Grafting of acryloyl cyanoacetohydrazide onto chitosan." Journal of Polymer Research 18, no. 3 (2010): 459–67. http://dx.doi.org/10.1007/s10965-010-9437-x.

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5

Hosseini, Hajar, and Mohammad Bayat. "Synthesis of 5-amino-N′-(9H-fluoren-9-ylidene)-8-nitro-7-aryl-1,2,3,7-tetrahydroimidazo[1,2-a]pyridine-6-carbohydrazide derivatives based on heterocyclic ketene aminals." RSC Advances 8, no. 72 (2018): 41218–25. http://dx.doi.org/10.1039/c8ra09308c.

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A new class of tetrahydroimidazo[1,2-a]pyridine derivatives has been successfully prepared via a five-component domino reaction using cyanoacetohydrazide, 9-fluorenone, aromatic aldehydes, 1,1-bis(methylthio)-2-nitroethene and ethylenediamine in ethanol at reflux.

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6

El-Sharief, Marwa A. M. Sh, Samir Y. Abbas, Medhat A. Zahran, Yehia A. Mohamed, Ahmed Ragab, and Yousry A. Ammar. "New 1,3-diaryl-5-thioxo-imidazolidin-2,4-dione derivatives: synthesis, reactions and evaluation of antibacterial and antifungal activities." Zeitschrift für Naturforschung B 71, no. 8 (2016): 875–81. http://dx.doi.org/10.1515/znb-2016-0054.

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AbstractNew cyanothioformamide derivative 1 was prepared by treatment of 3,5-dichlorophenyl isothiocyanate with potassium cyanide at room temperature. Cycloaddition of cyanothioformamide 1 with phenyl isocyanate as electrophile furnished the corresponding imidazolidine 2. Imine hydrolysis of 2 with ethanolic HCl produced the corresponding 4-thioxo-2,5-imidazolidinedione 3. This compound was used as key synthon for the preparation of a wide variety of new substituted imidazole compounds. Condensation of 3 with different types of hydrazine derivatives furnished new series of hydrazone 4a, b, thi

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7

Martins, Marcos A. P., Dayse N. Moreira, Clarissa P. Frizzo, Kelvis Longhi, Nilo Zanatta та Helio G. Bonacorso. "Reaction of β-alkoxyvinyl halomethyl ketones with cyanoacetohydrazide". Journal of the Brazilian Chemical Society 19, № 7 (2008): 1361–68. http://dx.doi.org/10.1590/s0103-50532008000700019.

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8

Nilov, D. B., and V. G. Granik. "Study of reactions of lactim ethers with cyanoacetohydrazide." Russian Chemical Bulletin 55, no. 9 (2006): 1636–41. http://dx.doi.org/10.1007/s11172-006-0466-x.

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9

Mekheimer, Ramadan A., and Rafat M. Shaker. "Synthesis and Reactivity of 3-Alkylthio-5-cyanomethyl-4-phenyl-1,2,4-triazoles." Journal of Chemical Research 23, no. 2 (1999): 76–77. http://dx.doi.org/10.1177/174751989902300205.

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Phenyl isothiocyanate reacts with 2-cyanoacetohydrazide (1) to yield the corresponding 1-cyanoacetyl-4-phenylthiosemicarbazide (3), via acid hydrolysis of the intermediate 2 whereas cyclization of 3 gave the 1,2,4-triazoles 4, 1,3,4-thiadiazoles 7 and 1,3,4-thiadiazine-5-ones 9; compound 4a was reacted with phenyl isothiocyanate, dicyandiamide, sulfanylacetic acid and benzaldehyde to afford 11, 13, 14 and 15, respectively.

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10

Al-Awadi, Nouria A., and Maher Z. Elsabee. "Pyrolysis of N-acryloyl, N′cyanoacetohydrazide and its polymer." Polymer Degradation and Stability 50, no. 3 (1995): 319–22. http://dx.doi.org/10.1016/0141-3910(95)00140-9.

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11

Salman, Asmaa S. "Utility of Activated Nitriles in the Synthesis of Novel Heterocyclic Compounds with Antitumor Activity." Organic Chemistry International 2013 (October 3, 2013): 1–9. http://dx.doi.org/10.1155/2013/259348.

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Reaction of cyanoacetic acid hydrazide (1) with 4-methoxyacetophenone and 4-chlorobenzaldehyde (2a,b) afforded the corresponding 2-cyanoacetohydrazide derivatives (3a,b) respectively. The latter compounds were utilized as a key intermediate for the synthesis of new heterocyclic compounds. Newly synthesized compounds were characterized by elemental analyses and spectral data. The antitumor evaluation of some newly synthesized compounds was screened in vitro against human breast cancer cell line (MCF-7).

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12

Borstad, Gustav M., Iskander G. Batyrev, and Jennifer A. Ciezak-Jenkins. "Cyanoacetohydrazide under Pressure: Chemical Changes in a Hydrogen-Bonded Material." Journal of Physical Chemistry A 120, no. 17 (2016): 2712–19. http://dx.doi.org/10.1021/acs.jpca.5b11954.

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13

Mokhtar, Samia M., Maher Z. El-Sabee, Said S. Elkholy, and Magdy W. Sabaa. "Radical Polymerization and Copolymerization Behavior of N-Acryloyl N′-Cyanoacetohydrazide." Polymer Journal 29, no. 12 (1997): 964–69. http://dx.doi.org/10.1295/polymj.29.964.

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14

Al-Omar, Mohamed A., Nagy M. Khalifa, Hazem A. Ghabbour, Tze Shyang Chia, and Hoong-Kun Fun. "(E)-2-Cyano-N′-(1,2,3,4-tetrahydronaphthalen-1-ylidene)acetohydrazide." Acta Crystallographica Section E Structure Reports Online 68, no. 6 (2012): o1740. http://dx.doi.org/10.1107/s160053681202106x.

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In the title compound, C13H13N3O, the tetrahydrobenzene ring adopts a half-boat (envelope) conformation. The mean plane of the tetrahydronaphthalene ring system forms a dihedral angle of 9.56 (6)° with the mean plane of the cyanoacetohydrazide group. In the crystal, inversion dimers linked by pairs of N—H...O hydrogen bonds generate R 2 2(8) loops. The dimers are connected by C—H...N hydrogen bonds into a chain propagating along [101]. The crystal packing also features C—H...π interactions.

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15

Zhang, Wei-Ming, Shao-Song Qian, and Zhonglu You. "Synthesis, Characterization and Crystal Structures of Hydrazone Compounds Derived from Cyanoacetohydrazide." Asian Journal of Chemistry 26, no. 22 (2014): 7707–10. http://dx.doi.org/10.14233/ajchem.2014.17637.

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16

Abdelhamid, Abdou O., and Sobhi M. Gomha. "Synthesis of New Pyrazolo[1,5-a]pyrimidine, Triazolo[4,3-a]pyrimidine Derivatives, and Thieno[2,3-b]pyridine Derivatives from Sodium 3-(5-Methyl-1-phenyl-1H-pyrazol-4-yl)-3-oxoprop-1-en-1-olate." Journal of Chemistry 2013 (2013): 1–7. http://dx.doi.org/10.1155/2013/327095.

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Condensation of sodium 3-oxo-3-(1-phenyl-1H-pyrazol-4-yl)prop-1-en-1-olate (2) with several heterocyclic amines, cyanoacetamide, cyanothioacetamide, and 2-cyanoacetohydrazide gives pyrazolo[1,5-a]pyrimidines (5a–d), pyrido[2′,3′:3,4]pyrazolo[1,5-a]pyrimidine (9), benzo[4,5]imidazo[1,2-a]pyrimidine (10), [1,2,4]triazolo[1,5-a]pyrimidine (11), and pyridine derivatives (12–14). Also, thieno[2,3-b]pyridines (15–18) were synthesized via pyridinethione (13) withα-halo ketones andα-halo ester. Structures of the newly synthesized compounds were elucidated by elemental analysis, spectral data, alternat

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17

Fouda, A. S., M. Abdallah, and A. Attia. "INHIBITION OF CARBON STEEL CORROSION BY SOME CYANOACETOHYDRAZIDE DERIVATIVES IN HCl SOLUTION." Chemical Engineering Communications 197, no. 8 (2010): 1091–108. http://dx.doi.org/10.1080/00986440903412944.

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18

Alotaibi, Mohammad Hayal, Hanan A. Mohamed, Bakr F. Abdel-Wahab, Amany S. Hegazy, Benson M. Kariuki, and Gamal A. El-Hiti. "Crystal structure of N′-(1-(benzofuran-2-yl)ethylidene)-2-cyanoacetohydrazide, C13H11N3O2." Zeitschrift für Kristallographie - New Crystal Structures 234, no. 2 (2019): 361–62. http://dx.doi.org/10.1515/ncrs-2018-0420.

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AbstractC13H11N3O2, triclinic, P1̄ (no. 2), a = 7.889(2) Å, b = 9.367(3) Å, c = 9.630(3) Å, α = 64.82(3)°, β = 106.507(4)°, γ = 84.57(2), V = 585.1(3) Å3, Z = 2, Rgt(F) = 0.0550, wRref(F2) = 0.1455, T = 293(2) K.

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19

Mohamed, Nadia A., and Magdy W. Sabaa. "N-acryloyl,N′-cyanoacetohydrazide as a thermal stabilizer for rigid poly(vinyl chloride)." Polymer International 45, no. 2 (1998): 147–56. http://dx.doi.org/10.1002/(sici)1097-0126(199802)45:2<147::aid-pi851>3.0.co;2-#.

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20

HAGGAG, B. M., L. M. CHABAKA, Y. A. ALLAM, and G. A. M. NAWWAR. "ChemInform Abstract: Effect of the N-Protecting Groups on the Chemical Behavior of Cyanoacetohydrazide." ChemInform 28, no. 19 (2010): no. http://dx.doi.org/10.1002/chin.199719080.

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21

Harrison, William T. A., Ola K. Al-Sakka, Daisy H. Fleita, Amina Saleh, and Sara Salem. "Crystal structure of 2-cyano-N′-(cyclohexylidene)acetohydrazide." Acta Crystallographica Section E Structure Reports Online 70, no. 9 (2014): o886. http://dx.doi.org/10.1107/s1600536814009350.

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In the title compound, C9H13N3O, the cyclohexylidene ring adopts a chair conformation and the bond-angle sum at the C atom linked to the N atom is 359.6°. The cyanoacetohydrazide grouping is close to planar (r.m.s. deviation for the non-H atoms = 0.031 Å) and subtends a dihedral angle of 64.08 (4)° with the four C atoms forming the seat of the chair. The C=O and N—H groups are in asynconformation (O—C—N—H = −5°). In the crystal, inversion dimers linked by pairs of N—H...O hydrogen bonds generateR22(8) loops; this dimer linkage is reinforced by a pair of C—H...O interactions, which generateR22(

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22

Shaker, Soheir, and Magda Marzouk. "Utilization of Cyanoacetohydrazide and Oxadiazolyl Acetonitrile in the Synthesis of Some New Cytotoxic Heterocyclic Compounds." Molecules 21, no. 2 (2016): 155. http://dx.doi.org/10.3390/molecules21020155.

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23

Mohamed, Nadia A., and Nahed A. Abd El-Ghany. "Synthesis, Characterization, and Antimicrobial Activity of Carboxymethyl Chitosan-Graft-Poly(N-acryloyl,N′-cyanoacetohydrazide) Copolymers." Journal of Carbohydrate Chemistry 31, no. 3 (2012): 220–40. http://dx.doi.org/10.1080/07328303.2011.650338.

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24

Mohamed, Nadia A., Zeinab R. Farag, and Magdy W. Sabaa. "Thermal degradation behavior of poly(vinyl chloride) in presence of poly(N-acryloyl-N′-cyanoacetohydrazide)." Journal of Applied Polymer Science 109, no. 4 (2008): 2362–68. http://dx.doi.org/10.1002/app.27530.

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25

Mikhael, Michael G. "Synthesis and thermal behaviour of poly(N-acryloyl,N′-cyanoacetohydrazide) and some of its metal complexes." Polymer Degradation and Stability 36, no. 1 (1992): 43–47. http://dx.doi.org/10.1016/0141-3910(92)90046-8.

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26

Kumaran, T. Saravana, A. Prakasam, P. Vennila, S. Parveen Banu, and G. Venkatesh. "New Carbazole-Based Organic Dyes with Various Acceptors for Dye-Sensitized Solar Cells: Synthesis, Characterization, DSSCs Fabrications and DFT Study." Asian Journal of Chemistry 33, no. 7 (2021): 1541–50. http://dx.doi.org/10.14233/ajchem.2021.23197.

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The molecular configuration, synthesis and characterization of (E)-3-(6-bromo-9-phenyl-9H-carbazol- 3-yl)acrylic acid (BPA), (E)-3-(6-bromo-9-phenyl-9H-carbazol-3-yl)-2-cyanoacrylic acid (BPCA) and (E)-N′-((6-bromo-9-phenyl-9H-carbazol-3-yl)methylene)-2-cyanoacetohydrazide (BPCH) configured D-π-A sensitizers and the sensitizers are used in DSSCs. Dye molecules are described by FT-IR, NMR and UV-Vis analysis. The study shows that the non-planar structure of BPA, BPCA and BPCH can effectively slow down the aggregation and conjugation of the dye. Computed vibrational modes are compared with obser

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27

Elsayed, Galal A., Samir A. Omara, and Rabaa M. Kamel. "Utility of N ′-((2-chloroquinolin-3-yl)methylene)-2-cyanoacetohydrazide as a Source of Biologically Active Novel Heterocycles." Journal of Heterocyclic Chemistry 54, no. 6 (2017): 3427–33. http://dx.doi.org/10.1002/jhet.2965.

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28

Tharini, K., and K. Sundaresan. "IN SILICO DOCKING STUDIES OF ANTI-DIABETIC AND BREAST CANCER ACTIVITY BY N'-(1-BENZYLPIPERIDIN-4-YLIDENE)-2-CYANOACETOHYDRAZIDE." International Journal of Advanced Research 5, no. 12 (2017): 601–7. http://dx.doi.org/10.21474/ijar01/5998.

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29

NAWWAR, G. A. M., and Y. A. A. ALLAM. "ChemInform Abstract: Utility of Cyanoacetohydrazide in Heterocyclic Synthesis: Simple Synthesis of Condensed Pyrazoles via Ring Closure of a Single Component." ChemInform 25, no. 11 (2010): no. http://dx.doi.org/10.1002/chin.199411136.

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30

El-Mossalamy, E. H., and Shaeel A. Al-Thabaiti. "Synthesis and thermal studies of poly(N-acryloyl,N?-cyanoacetohydrazide) complexes with Co(II), Fe(III), and UO2(II) ions." Journal of Applied Polymer Science 90, no. 12 (2003): 3354–58. http://dx.doi.org/10.1002/app.13008.

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31

Hekal, Mohamed H., Yasmeen M. Ali, and Fatma S. M. Abu El-Azm. "Utilization of cyanoacetohydrazide and 2-(1,3-dioxoisoindolin-2-yl) acetyl chloride in the synthesis of some novel anti-proliferative heterocyclic compounds." Synthetic Communications 50, no. 18 (2020): 2839–52. http://dx.doi.org/10.1080/00397911.2020.1786125.

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32

El-mahdy, Kamelia, Azza El-Kazak, Mohamed Abdel-Megid, Magdy Seada, and Osama Farouk. "Synthesis, Characterization and Biological Evaluation of some New Thieno[2,3-d]Pyrimidine Derivatives." JOURNAL OF ADVANCES IN CHEMISTRY 5, no. 1 (2009): 581–91. http://dx.doi.org/10.24297/jac.v5i1.937.

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10-Oxo-4,6,7,8,9,10-hexahydroprazolo[1,5-a][1]benzothieno[2,3-d]pyrimidine-3-carbaldehyde (2) was prepared by Vilsmeier-Haack reaction of 3-amino-2-methyl-5,6,7,8-tetrahydro[1]benzothieno[2,3-d]pyrimidin-4(3H)-one (1). Reaction of carbaldehyde derivative 2 with malononitrile afforded arylidene malononitrile 3. Cyclization of the latter compound with thiourea yielded pyrimidinethione 4. Interaction of carbaldehyde derivative 2 in presence of thiourea with keto- compounds such as ethyl acetoacetate, or acetylacetone, or dimedone or ethyl cyanoacetate gave pyrimidine derivatives 5-8. Hydrazinolys

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33

Nanni, R. G., J. R. Ruble, G. A. Jeffrey та R. K. McMullan. "Neutron diffraction analysis at 15 K and ab initio molecular orbital calculations for α-cyanoacetohydrazide: A crystal structure with a high energy conformer". Journal of Molecular Structure 147, № 3-4 (1986): 369–80. http://dx.doi.org/10.1016/0022-2860(86)80391-x.

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34

Wardakhan, Wagnat Wahba, El-Sayed Nahed Nasser Eid, and Rafat Milad Mohareb. "Synthesis and anti-tumor evaluation of novel hydrazide and hydrazide-hydrazone derivatives." Acta Pharmaceutica 63, no. 1 (2013): 45–57. http://dx.doi.org/10.2478/acph-2013-0004.

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The reaction of cyclopentanone with cyanoacetylhydrazine gave 2-cyano-2-cyclopentylideneacetohydrazide (1). Treatment of compound 1 with elemental sulphur in the presence of triethylamine afforded 2-amino-5,6-dihydro- -4H-cyclopenta[b]thiophene-3-carbohydrazide (2), which in-turn formed the corresponding intermediate diazonium salt. The latter was coupled with either ethyl cyanoacetate or ethyl acetoacetate to form 2-cyano-2-(3-(hydrazinecarbonyl)- 5,6-dihydro-4H-cyclopenta[b]thiophen-2-yl)hydrazono) acetate (3) and ethyl 2-(2-(3-(hydrazinecarbonyl)-5,6-dihydro- 4H-cyclopenta[b]thiophen-2-yl)h

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35

Kurdi, Asmaa A., Moataz Morad, Hana M. Abumelha, et al. "Synthesis and characterization for novel VO(II) complexes from cyanoacetohydrazide-based ligands; Hirshfeld crystals, DFT study and biodiesel catalytic synthesis from waste frying oil." Journal of Molecular Structure 1240 (September 2021): 130603. http://dx.doi.org/10.1016/j.molstruc.2021.130603.

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36

L. Soto, José, Nazario Mart地, and Carlos Seoane. "On the Reanction of Cyanoacetohydrazine with a-Substituted Cinnamonitriles." HETEROCYCLES 23, no. 8 (1985): 2013. http://dx.doi.org/10.3987/r-1985-08-2013.

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37

AbouEl-Enein, Saeyda, Fathy A. El-Saied, Sanaa M. Emam, and M. A. Ell-Salamony. "First raw transition metal complexes of salicylidene and 2- hydroxy-1-naphthylidene-N-cyanoacetohydrazone." Spectrochimica Acta Part A: Molecular and Biomolecular Spectroscopy 71, no. 2 (2008): 421–29. http://dx.doi.org/10.1016/j.saa.2007.12.031.

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38

Nilov, D. B., and V. G. Granik. "Study of Reactions of Lactim Ethers with Cyanoacetohydrazide." ChemInform 38, no. 28 (2007). http://dx.doi.org/10.1002/chin.200728039.

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39

MARTIN, N., C. SEOANE та J. L. SOTO. "ChemInform Abstract: On the Reaction of Cyanoacetohydrazide with α-Substituted Cinnamonitriles." Chemischer Informationsdienst 17, № 3 (1986). http://dx.doi.org/10.1002/chin.198603209.

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40

Hamed, Nancy A., Magda I. Marzouk, Mahmoud F. Ismail, and Mohamed H. Hekal. "N'-(1-([1,1'-biphenyl]-4-yl)ethylidene)-2-cyanoacetohydrazide as scaffold for the synthesis of diverse heterocyclic compounds as prospective antitumor and antimicrobial activities." Synthetic Communications, August 27, 2019, 1–13. http://dx.doi.org/10.1080/00397911.2019.1655578.

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41

NANNI, R. G., J. R. RUBLE, G. A. JEFFREY та R. K. MCMULLAN. "ChemInform Abstract: Neutron Diffraction Analysis at 15 K and ab initio Molecular Orbital Calculations for α-Cyanoacetohydrazide: a Crystal Structure with a High Energy Conformer". ChemInform 18, № 8 (1987). http://dx.doi.org/10.1002/chin.198708072.

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42

Hosseini, Hajar, and Mohammad Bayat. "Cyanoacetohydrazides in Synthesis of Heterocyclic Compounds." Topics in Current Chemistry 376, no. 6 (2018). http://dx.doi.org/10.1007/s41061-018-0218-z.

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43

Sharma, Harish Kumar, Pernita Dogra, Akhilesh Kumar Gupta, and Fardad Koohyar. "POTENTIOMETRIC DETERMINATION OF NICKEL (II) ION USING 2-HYDROXY-1-NAPHTHYLIDENE-N-CYANOACETOHYDRAZONE AS ELECTROACTIVE MATERIAL." Química Nova, 2014. http://dx.doi.org/10.5935/0100-4042.20140198.

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