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Journal articles on the topic 'Diacetone alcohol'

Author: Grafiati

Published: 4 June 2021

Last updated: 28 July 2025

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1

March, Raymond Evans, and Alexander Baldwin Young. "An investigation of the structures of isomeric ions derived from acetone, diacetone alcohol, and mesityl oxide." Canadian Journal of Chemistry 66, no. 4 (1988): 591–97. http://dx.doi.org/10.1139/v88-102.

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An investigation of the structures of isomeric ions formed in ion/molecule reactions occurring in 2-propanone (acetone), 4-hydroxy-4-mefhyl-2-pentanone (diacetone alcohol), and 4-methyl-3-penten-2-one (mesityl oxide) has been performed using a hybrid mass spectrometer of reversed geometry. Ions of m/z 117, which have been observed as products of ion/molecule reactions in acetone and in diacetone alcohol, may have a single structure if an aldol type condensation reaction occurs under acidic conditions in the gas phase; however, high energy collision induced dissociation (CID) results proved the

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2

Chen, Fang, Ning Li, Shanshan Li, et al. "Synthesis of jet fuel range cycloalkanes with diacetone alcohol from lignocellulose." Green Chemistry 18, no. 21 (2016): 5751–55. http://dx.doi.org/10.1039/c6gc01497f.

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3

Du, Chang Hai, Yan Shen, Lin Ping Sun, and Xiang Chun Meng. "Condensation of Acetone to Diacetone Alcohol over Structured MgO/Al₂O₃-Al Catalyst Packing." Advanced Materials Research 347-353 (October 2011): 3050–53. http://dx.doi.org/10.4028/www.scientific.net/amr.347-353.3050.

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A novel solid base catalyst, structured MgO/Al2O3-Al catalyst packing, was prepared by supporting MgO onto a thin film of alumina that was formed by anodic oxidation of high purity aluminium foils. Some preparation parameters including the molar ratio of Mg(NO3)2•6H2O to CH3(CH2)16COOH, the aging time, the calcination temperature and time were investigated by using the catalyst for the condensation of acetone to diacetone alcohol. Each of those factors had some influence on the catalyst activity and an optimum value was obtained. The conversion of acetone was 20.2%, and the selectivity to diac

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4

Podrebarac, G. G., F. T. T. Ng, and G. L. Rempel. "The production of diacetone alcohol with catalytic distillation." Chemical Engineering Science 53, no. 5 (1998): 1067–75. http://dx.doi.org/10.1016/s0009-2509(97)00427-2.

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5

Podrebarac, G. G., F. T. T. Ng, and G. L. Rempel. "The production of diacetone alcohol with catalytic distillation." Chemical Engineering Science 53, no. 5 (1998): 1077–88. http://dx.doi.org/10.1016/s0009-2509(97)00428-4.

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6

Baeva, L. A., L. F. Biktasheva, and A. A. Fatykhov. "CONDENSATION OF DIACETONE ALCOHOL WITH FORMALDEHYDE AND THIOLS." Vestnik Bashkirskogo universiteta 7, no. 4 (2018): 1018. http://dx.doi.org/10.33184/bulletin-bsu-2018.4.12.

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7

Scheepers, Matthew C., Manuel A. Fernandes, and Andreas Lemmerer. "Chains or rings? Polymorphism of an isoniazid derivative derivatized with diacetone alcohol." RSC Advances 12, no. 19 (2022): 11658–64. http://dx.doi.org/10.1039/d2ra02057b.

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8

Xu, Xuebing, Hong Meng, Yingzhou Lu, and Chunxi Li. "Aldol condensation of refluxing acetone on CaC2 achieves efficient coproduction of diacetone alcohol, mesityl oxide and isophorone." RSC Advances 8, no. 53 (2018): 30610–15. http://dx.doi.org/10.1039/c8ra05965a.

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9

Hu, Yancheng, Lin Yuan, Xiuli Zhang, et al. "Production of 1,2-Cyclohexanedicarboxylates from Diacetone Alcohol and Fumarates." ACS Sustainable Chemistry & Engineering 7, no. 3 (2019): 2980–88. http://dx.doi.org/10.1021/acssuschemeng.8b04310.

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10

Sišul, N., N. Ciković, and J. Jeleňić. "Catalytic preparation of diacetone alcohol in controlled flow conditions." Reaction Kinetics & Catalysis Letters 45, no. 1 (1991): 111–17. http://dx.doi.org/10.1007/bf02078617.

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11

Magneron, I., V. Bossoutrot, A. Mellouki, G. Laverdet, and G. Le Bras. "The OH-Initiated Oxidation of Hexylene Glycol and Diacetone Alcohol." Environmental Science & Technology 37, no. 18 (2003): 4170–81. http://dx.doi.org/10.1021/es0264450.

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12

S., SONDU, SETHURAM B., and NAVANEETH RAO T. "Kinetics and Mechanism of Ruthenium (III)-catalysed Oxidation of Diacetone Alcohol by Cerium(iv) in H2S04 Medium." Journal of Indian Chemical Society Vol. 66, JUNE 1989 (1989): 365–67. https://doi.org/10.5281/zenodo.5958535.

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Department of Chemistry, Osmania University, Hyderabad-500 007 <em>Manuscript received 23 November 1988. accepted 25 AprIl 1989</em> <strong>T</strong>he kinetics of Ru<sup>III</sup>-catalysis in Ce<sup>IV</sup>-diacetone alcohol (DAA) redox system have been studied and the orders found to be unity in [Ce<sup>IV </sup>] and fractional each in [DAA] and [RU<sup>III </sup>]. The rate increased with increase in [H<sup>+</sup>] at constant ionic strength but decreased at varying ionic strength. The increase in [HS\(O^-_4\)] or [S\(O^2_4\)] decreased the rate

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13

Houssaini, Jamal, Mohammed Naciri Bennani, Hamid Ziyat, Said Arhzaf, O. Qabaqous, and Abdellatid Amhoud. "Study of the Catalytic Activity of the Compounds Hydrotalcite Type Treated by Microwave in the Self-Condensation of Acetone." International Journal of Analytical Chemistry 2021 (December 23, 2021): 1–7. http://dx.doi.org/10.1155/2021/1551586.

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The self-condensation reaction of acetone, producing diacetone alcohol (DAA), is of great industrial importance. It was used to study the catalytic activity of Mg-Al catalysts synthesized by the coprecipitation method. For this purpose, we synthesized Mg-Al based hydrotalcite with a molar ratio of 3, obtained either after conventional heating or after microwave irradiation with of 100 W for three minutes. Structural and chemical properties of the obtained catalysts were characterized, using different techniques: X-ray diffraction (XRD), Fourier transform infrared spectra (FTIR), scanning elect

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14

Zheng, Yuxiang, Flora T. T. Ng, and Garry L. Rempel. "Process Analysis for the Production of Diacetone Alcohol via Catalytic Distillation." Industrial & Engineering Chemistry Research 42, no. 17 (2003): 3962–72. http://dx.doi.org/10.1021/ie0207921.

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15

Kulov, N. N., N. P. Slaikovskaya, and V. A. Lotkhov. "Phase equilibrium in acetone-water-mesityl oxide-diacetone alcohol four-component system." Theoretical Foundations of Chemical Engineering 46, no. 2 (2012): 113–19. http://dx.doi.org/10.1134/s0040579512020066.

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16

Kamar, Afaf, Alexander Baldwin Young, and Raymond Evans March. "A comparative ion chemistry study of acetone, diacetone alcohol, and mesityl oxide." Canadian Journal of Chemistry 64, no. 10 (1986): 1979–88. http://dx.doi.org/10.1139/v86-328.

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The evolution of ion species by unimolecular and bimolecular reactions, both concurrent and sequential, has been investigated for each of 2-propanone, d6-2-propanone, 4-hydroxy-4-methyl-2-pentanone, and 4-methyl-3-penten-2-one. Infrared multiphoton dissociation (IRMPD) has been used in order to differentiate between gaseous ionic isomers. It is concluded that the isomeric species, protonated 2-propanone dimer and protonated 4-hydroxy-4-methyl-2-pentanone, both of m/z 117, are of different structures. The ion species C6H11O+ of m/z 99, and its perdeuterated analogue, which is observed in all th

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17

Jańczuk, Bronisław, Wiesław Wójcik, and Anna Zdziennicka. "The surface free energy of low rank coals precovered with diacetone alcohol." Fuel 71, no. 6 (1992): 708–11. http://dx.doi.org/10.1016/0016-2361(92)90177-p.

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18

Chandrasekhar, S., Ch Narsihmulu, N. Ramakrishna Reddy, and S. Shameem Sultana. "l-Proline catalyzed asymmetric transfer aldol reaction between diacetone alcohol and aldehydes." Chemical Communications, no. 21 (2004): 2450. http://dx.doi.org/10.1039/b409053p.

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19

Chae, Sudong, Akhtar Siddiqa, Seungbae Oh, et al. "Isolation of Nb2Se9 Molecular Chain from Bulk One-Dimensional Crystal by Liquid Exfoliation." Nanomaterials 8, no. 10 (2018): 794. http://dx.doi.org/10.3390/nano8100794.

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The optimum solvent for Nb2Se9 dispersion, which is a new type of one dimensional (1D) material, is investigated. Among several solvents (16 solvents in total), strong dispersion was observed in benzyl alcohol, isopropyl alcohol, isobutyl alcohol, and diacetone alcohol, which have medium dielectric constants in the range of 10 to 30 and surface tension in the range of 25 to 35 mJ m−2. 1D Nb2Se9 chains, whose size is less than 10 nm, are well dispersed and it is possible to disperse mono-chains of 1 nm or less in a specific dispersion region. The 1D unit chain with dangling bond free surface an

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20

Baskaran, R., and T. R. Kubendran. "Thermophysical Properties of P-Anisaldehyde and Diacetone Alcohol with Bromobenzene at Different Temperatures." Journal of Thermophysics and Heat Transfer 25, no. 4 (2011): 614–19. http://dx.doi.org/10.2514/1.51425.

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21

Dechaine, Greg P., and Flora T. T. Ng. "A New Coated Catalyst for the Production of Diacetone Alcohol via Catalytic Distillation." Industrial & Engineering Chemistry Research 47, no. 23 (2008): 9304–13. http://dx.doi.org/10.1021/ie800009u.

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22

Larina, L. I., T. N. Komarova, and V. G. Rozinov. "Phosphorus-containing dienes derived from diacetone alcohol: synthesis and study by NMR spectroscopy." Russian Chemical Bulletin 64, no. 11 (2015): 2744–46. http://dx.doi.org/10.1007/s11172-015-1218-6.

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23

Thotla, Suman, Vishal Agarwal, and Sanjay M. Mahajani. "Simultaneous production of diacetone alcohol and mesityl oxide from acetone using reactive distillation." Chemical Engineering Science 62, no. 18-20 (2007): 5567–74. http://dx.doi.org/10.1016/j.ces.2007.01.045.

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24

Nageswar Rao, K., S. Sondu, B. Sethuram, and T. Navaneeth Rao. "Ag(I) - Catalysed Oxidation of Diacetone Alcohol by ce(iv) in H2SO4 Medium." Bulletin des Sociétés Chimiques Belges 93, no. 6 (2010): 431–36. http://dx.doi.org/10.1002/bscb.19840930603.

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25

Rios, Daniel, and John K. Gibson. "Activation of Gas-Phase Uranyl Diacetone Alcohol Coordination Complexes by Spectator Ligand Addition." European Journal of Inorganic Chemistry 2012, no. 7 (2012): 1054–60. http://dx.doi.org/10.1002/ejic.201200024.

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26

Linek, Jan, Ivan Wichterle, and Kenneth N. Marsh. "Vapor−Liquid Equilibria for Water + Diacetone Alcohol, Ethyl Methanoate + Water, and Ethyl Methanoate + Phenol." Journal of Chemical & Engineering Data 41, no. 6 (1996): 1219–22. http://dx.doi.org/10.1021/je960183y.

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27

Rios, Daniel, George Schoendorff, Michael J. Van Stipdonk, et al. "Roles of Acetone and Diacetone Alcohol in Coordination and Dissociation Reactions of Uranyl Complexes." Inorganic Chemistry 51, no. 23 (2012): 12768–75. http://dx.doi.org/10.1021/ic3015964.

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28

Nicol, W. "Comparing Catalytic Distillation to Separate Reaction and Distillation for the Production of Diacetone Alcohol." Chemical Engineering Research and Design 81, no. 8 (2003): 1026–32. http://dx.doi.org/10.1205/026387603322482257.

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29

P., NARASIMHA CHAR, SONDU S., SETHURAM B., and NAVANEETH RAO T. "A Comparative Kinetic Study of lridium(III) Catalysis in H2SO4 and HClO4 Media in the Cerium(IV) Oxidation of Diacetone Alcohol." Journal of Indian Chemical Society Vol. 64, Apr 1987 (1987): 209–12. https://doi.org/10.5281/zenodo.6162135.

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Department of Chemistry, Osmania University, Hyderabad-500 007 <em>Manuscript received 26 February 1985, revised 8 October 1985, accepted 9 March 1987</em> A study of Ir<sup>III</sup> catalysed oxidation of diacetone alcohol (DAA) by Ce<sup>IV</sup> in H2SO<sub>4</sub> and HCIO<sub>4</sub> media was undertaken to understand the mechanism of catalysis. The change in reactive species of Ce<sup>IV</sup> in tnese media produces a marked effect on the relative rates of catalysed and uncatalysed reactions. <em>The </em>catalysis was found to be more pronounced in H<sub>2</sub>SO<sub>4</sub> medium.

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30

J[adot]nczuk, Bronisław, WieBław W[odot]Jcik, and TomaBz Białopiotrowicz. "THE WETTABILITY OF LOW COAL RANKS IN THE PRESENCE OF N-ALKANES AND DIACETONE ALCOHOL." Fuel Science and Technology International 9, no. 1 (1991): 31–57. http://dx.doi.org/10.1080/08843759108942252.

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31

Tadanaga, Kiyoharu, Tsutomu Minami, and Noboru Tohge. "27Al NMR Study of Coordination States of Aluminum-tri-sec-butoxide Dissolved in Diacetone Alcohol." Chemistry Letters 23, no. 8 (1994): 1507–10. http://dx.doi.org/10.1246/cl.1994.1507.

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32

Jouyban, Abolghasem, Elaheh Rahimpour, and William E. Acree Jr. "Further Analysis on Solubility Measurement and Thermodynamic Modeling of Benzoic Acid in Monosolvents and Binary Mixtures." Pharmaceutical Sciences 25, no. 2 (2019): 165–70. http://dx.doi.org/10.15171/ps.2019.24.

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Background: Recently Sandeepa et al. reported the solubility of benzoic acid in six monosolvents (i.e. tributyl phosphate, diacetone alcohol, methyl-n-propyl ketone, methyl acetate, amyl acetate, and isooctane) and ﬁve binary systems (i.e. ethanol + hexane, isopropyl alcohol + hexane and chloroform + hexane, acetone + hexane, and acetone + water) along with some numerical analyses. The reported calculations have been reanalyzed and some recommendations and further computations were proposed. Methods: Further analyses were performed based on combined nearly ideal binary solvent/Redlich-Kister,

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33

Kamar, Afaf, Alexander Baldwin Young, and Raymond Evans March. "Experimentally determined proton affinities of 4-methyl-3-penten-2-one, 2-propyl ethanoate, and 4-hydroxy-4-methyl-2-pentanone in the gas phase." Canadian Journal of Chemistry 64, no. 12 (1986): 2368–70. http://dx.doi.org/10.1139/v86-391.

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Proton affinities have been determined for 4-methyl-3-penten-2-one, 2-propyl ethanoate, and 4-hydroxy-4-methyl-2-pentanone in the gas phase at 333 K. A quadrupole ion store (QUISTOR) was employed to study mass spectrometrically the equilibrium between a species of known proton affinity and one of the above compounds; equilibrium between protonated species was monitored over an ion storage duration of 100 ms. The values of the proton affinities were found to be 870.5 ± 0.8 kJ mol−1 for 4-methyl-3-penten-2-one (mesityl oxide); 842.7 ± 0.6 kJ mol−1 for 2-propyl ethanoate; and 831.6 ± 0.8 kJ mol−1

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34

Eisenacher, M., M. Venschott, D. Dylong, W. F. Hoelderich, J. Schütz, and W. Bonrath. "Upgrading bio-based acetone to diacetone alcohol by aldol reaction using Amberlyst A26-OH as catalyst." Reaction Kinetics, Mechanisms and Catalysis 135, no. 2 (2022): 971–86. http://dx.doi.org/10.1007/s11144-022-02168-z.

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AbstractThe aldol reaction of bio acetone in presence of a strongly basic ion exchange resin was carried out with and without the addition of water in a temperature range between − 30 °C and 45 °C. The conversion, selectivity and service time of the ion exchange resins were investigated in a stirred batch reactor and a continuous fixed bed reactor. For the batch experiments, both conversion and selectivity increased with decreasing temperature. Furthermore, the addition of water to the reaction medium has a positive effect on selectivity and catalyst service time of the resins. For the continu

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35

Boned, C., M. Moha-ouchane, and J. Jose. "Excess Volume of Ternary Water + Diacetone Alcohol + 2-Propanol as a Function of Pressure, Temperature and Composition." Physics and Chemistry of Liquids 38, no. 1 (2000): 113–36. http://dx.doi.org/10.1080/00319100008045302.

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36

Jańczuk, Bronislaw, Wieslaw Wójcik, and Tomasz Bialopiotrowicz. "The influence of diacetone alcohol on adhesion of air bubbles to the surface of low rank coals." Fuel 68, no. 7 (1989): 917–20. http://dx.doi.org/10.1016/0016-2361(89)90130-0.

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37

Pauwels, Danny, Bart Geboes, Jonas Hereijgers, Daniel Choukroun, Karolien De Wael, and Tom Breugelmans. "The application of an electrochemical microflow reactor for the electrosynthetic aldol reaction of acetone to diacetone alcohol." Chemical Engineering Research and Design 128 (December 2017): 205–13. http://dx.doi.org/10.1016/j.cherd.2017.10.014.

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38

Huang, Kai, Lei Xue, Mei-Yu Huang, and Ying-Yan Jiang. "Catalytic behaviors of silica-supported methylcellulose-L-phenyl alanine-platinum complexes in asymmetric hydrogenation of diacetone alcohol." Polymers for Advanced Technologies 13, no. 3-4 (2002): 165–68. http://dx.doi.org/10.1002/pat.168.

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39

Singh, Kamini, and R. A. Singh. "Kinetics and Mechanism of Ru(III) Catalyzed Periodate Oxidation of Methyl Glycol and Diacetone Alcohol in Perchloric Acid." Asian Journal of Chemistry 26, no. 16 (2014): 5125–28. http://dx.doi.org/10.14233/ajchem.2014.16444.

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40

Yin, Mao-Ya, Guo-Li Yuan, Mei-Yu Huang, and Ying-Yan Jiang. "Catalytic behavior of a Wool–Pd complex in asymmetric hydrogenation of diacetone alcohol and 3-methyl-2-butanone." Journal of Molecular Catalysis A: Chemical 147, no. 1-2 (1999): 89–92. http://dx.doi.org/10.1016/s1381-1169(99)00132-6.

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41

Kitulagodage, M., L. B. Astheimer, and W. A. Buttemer. "Diacetone alcohol, a dispersant solvent, contributes to acute toxicity of a fipronil-based insecticide in a passerine bird." Ecotoxicology and Environmental Safety 71, no. 2 (2008): 597–600. http://dx.doi.org/10.1016/j.ecoenv.2007.11.001.

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42

Kim, Yong K., and John D. Hatfield. "Kinetics and equilibrium data of the dehydration-hydration reaction between diacetone alcohol and mesityl oxide in phosphoric acid." Journal of Chemical & Engineering Data 30, no. 2 (1985): 149–53. http://dx.doi.org/10.1021/je00040a005.

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43

Srinivas, P., K. Nageswar Rao, B. Sethuram, and T. Navaneeth Rao. "Termination of CE(IV)-Diacetone Alcohol Redox System Initiated Polymerization of Acrylonitrile by V(V): A Kinetic Study." Bulletin des Sociétés Chimiques Belges 93, no. 1 (2010): 43–46. http://dx.doi.org/10.1002/bscb.19840930106.

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44

Thongnuam, Worawaran, Suwapich Pornsatitworakul, Thana Maihom, et al. "An Experimental and Theoretical Study on the Aldol Condensation on Zirconium-Based Metal-Organic Framework." Key Engineering Materials 757 (October 2017): 98–102. http://dx.doi.org/10.4028/www.scientific.net/kem.757.98.

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The aldol condensation of acetone in zirconium-based metal-organic framework functionalized by a sulfonic acid group (UiO-66-SO3H) has been theoretically investigated using the density functional theory. Acetone adsorbed on the UiO-66-SO3H with the adsorption energy of -17.4 kcal/mol. The catalyzed reaction has been proposed to be a two-step mechanism: the tautomerization of keto form to produce enol form of acetone, and the aldol condensation to produce diacetone alcohol. The activation energies were calculated to be 27.2 and 6.4 kcal/mol, respectively. For the experimental part, UiO-66-SO3H

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45

Hui-Hao, Gong, Wang Shou-Xiang, and Xu Hai-Han. "Study on the Briggs-Rauscher Type Oscillatary System Using Diacetone Alcohol as Organic Compound and Cerium (III) as Catalyst." Acta Physico-Chimica Sinica 7, no. 02 (1991): 184–90. http://dx.doi.org/10.3866/pku.whxb19910211.

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46

Raju, K. V. S. N. "Trace Level Determination of Mesityl Oxide and Diacetone Alcohol in Atazanavir Sulfate Drug Substance by a Gas Chromatography Method." Scientia Pharmaceutica 84, no. 2 (2016): 321–31. http://dx.doi.org/10.3797/scipharm.1507-05.

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47

Moha-Ouchane, M., C. Boned, and P. Xans. "Variations with pressure, temperature and composition of the excess volume VE of the ternary system water+diacetone alcohol+2-propanol." Physica B: Condensed Matter 265, no. 1-4 (1999): 287–90. http://dx.doi.org/10.1016/s0921-4526(98)01409-4.

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48

Wójcik, Wieslaw, Bronislaw Jańczuk, and Tomasz Bialopiotrowicz. "The Relationship between the Floatability of Low-Rank Coal and Its Adhesion to Air Bubbles in Aqueous Diacetone Alcohol Solutions." Separation Science and Technology 25, no. 6 (1990): 689–99. http://dx.doi.org/10.1080/01496399008050359.

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49

Schneider, Christoph, and Markus Hansch. "Zr(OtBu)4-catalysed synthesis of acetone aldol adducts and domino aldol-Tishchenko reactions with diacetone alcohol as enol equivalent." Chemical Communications, no. 13 (2001): 1218–19. http://dx.doi.org/10.1039/b102941j.

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50

Matsuhashi, Hiromi. "Synthesis of a Solid Base Catalyst Formed from Zinc(II) Acetylacetonate and Consisting of MgO Modified with ZnO." Catalysis Research 2, no. 2 (2022): 1. http://dx.doi.org/10.21926/cr.2202015.

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Solid base catalysts consisting of MgO modified with 10 mol% ZnO (ZnO/MgO) were prepared by depositing zinc(II) acetylacetonate (Zn(acac)2) in polar and nonpolar organic solvents on the surface of MgO and Mg(OH)2. The process was followed by thermal decomposition in air at 773 K over a period of 3 h. The activity of MgO modified with Zn(acac)2 for base-catalyzed retroaldol reaction (the decomposition of diacetone alcohol (4-hydroxy-4-methyl-2-pentanone) to acetone) at 299 K was higher than the activity of unmodified MgO prepared by thermal decomposition of Mg(OH)2. The activity of the catalyst

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