Relevant bibliographies by topics / Dielektrická spektroskopie

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Academic literature on the topic 'Dielektrická spektroskopie'

Author: Grafiati
Published: 4 June 2021
Last updated: 3 February 2022

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Journal articles on the topic "Dielektrická spektroskopie"

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Kurniawan, Widodo Budi. "PENGUKURAN NILAI DIELEKTRIK MATERIAL CALCIUM COPPER TITANAT ( CaCu3Ti4O12) MENGGUNAKAN SPEKTROSKOPI IMPEDANSI TERKOMPUTERISASI." Jurnal Sains Dasar 6, no. 1 (May 22, 2017): 26. http://dx.doi.org/10.21831/jsd.v6i1.13565.

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Telah dilakukan pengukuran tetapan dielektrik kompleks dan besarnya impedansi kapasitor pada material keramik Calcium Copper Titanate dengan struktur material CaCu3Ti4O12 (CCTO) dengan kemurnian 99 % menggunakan metode spektroskopi impedansi terkomputerisasi dalam rentang frekuensi 5 kHz – 120 kHz. Tetapan dielektrik maksimum terukur pada sampel yang disintering dengan suhu 7000C yaitu 745 pada frekuensi 5 kHz dan besarnya impedansi kapasitor maksimum terjadi pada sampel CCTO non sintering yaitu 150434 Ω. Hasil penelitian menunjukkan adanya pengaruh frekuensi terhadap tetapan dielektrik kompleks dan impedansi kapasitor dari material yang diteliti. Kata kunci : spektroskopi impedansi, CaCu3Ti4O12, tetapan dielektrik kompleks dan impedansi kapasitor. MEASUREMENT OF THE DIELECTRIC CONSTANT CALCIUM COPPER TITANATE (CaCu3Ti4O12) MATERIALS USING COMPUTERIZED IMPEDANCE SPECTROSCOPY ABSTRACT The measurement of the complex dielectric constant and the magnitude of the capacitor impedances of the ceramic materials Calcium Copper Titanate CaCu3Ti4O12 (CCTO) with purity of 99% has been done by using the method of computerized impedance spectroscopy in the frequency range 5 kHz - 120 kHz. The highest dielectric constant of the material was found to be 745 at 5 kHz in the sample sintered 7000C and the highest impedance of capacitor occured in CCTO sample non sintered that is 150434Ω. The results showed that complex dielectric constant and impedance of the capacitor of the material under study was frequency dependent. Keywords : impedance spectroscopy, CaCu3Ti4O12,complex dielectric constant and impedance of capacitor
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CAN, Nursel, and Ahmet ALTINDAL. "FTALOSIYANIN İNCE FILMDE EMPEDANS SPEKTROSKOPI VE DIELEKTRIK DURULMA." Uludağ University Journal of The Faculty of Engineering 22, no. 3 (December 28, 2017): 145–52. http://dx.doi.org/10.17482/uumfd.372447.

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Mustawarman, Heriansyah, and Edi Suharyadi. "Kajian Sifat Dielektrik pada Lempeng Nanopartikel Magnetit (Fe3O4) yang dienkapsulasi dengan Polyvinyl Alcohol (PVA) (Halaman 34 s.d. 37)." Jurnal Fisika Indonesia 19, no. 55 (May 25, 2015). http://dx.doi.org/10.22146/jfi.24370.

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Telah dilakukan sintesis nanopartikel Fe3O4 yang kemudian dienkapsulasi dengan Polyvinyl alcohol (PVA) dengan perbandingan 1:0, 1:3, 1:4, 1:5 dan 1:6 menggunakan metode kopresipitasi. Pengukuran dilakukan menggunakan sistem spektroskopi impedansi terkomputerisasi pada wilayah frekuensi 10 kHz hingga 120 kHz untuk mengetahui sifat dielektrik dari nanopartikel. Hasil pengukuran sifat dielektrik menunjukkan nilai permitivitas dielektrik pada seluruh sampel mengalami penurunan dengan bertambahnya frekuensi. Penambahan PVA mempengaruhi sifat dielektrik dari nanopartikel Fe3O4. Nilai permitivitas dielektrik riil seluruh sampel secara berturut-turut pada frekuensi 10 kHz yaitu 522, 212, 36, 234 dan 692. Nilai permitivitas dielektrik yang paling baik adalah nanopartikel Fe3O4+PVA (1:6 ) sehingga dapat digunakan untuk aplikasi biosensor Surface Plasmon Resonance(SPR) sebagai bahan aktif untuk meningkatkan sensitifitas sensor dan mengikat biomolekuler.
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CANIMKURBEY, Betül. "Dielektrik Spektroskopi ile Üleksitin Elektriksel Özellikleri." Erzincan Üniversitesi Fen Bilimleri Enstitüsü Dergisi, March 20, 2020. http://dx.doi.org/10.18185/erzifbed.673647.

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Yeoh, Cheow Keat, Srimala Sreekantan, Sabar Derita Hutagalung, and Zainal Arifin Ahmad. "Dielectric Behaviour Of BaTiO3 Prepared By Sol–Gel Technique When Exposed To Different Oxygen Concentrations." Jurnal Teknologi, January 20, 2012. http://dx.doi.org/10.11113/jt.v45.316.

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Sifat dielektrik serbuk BaTiO3 yang disediakan melalui kaedah akues pada suhu rendah telah dikaji menggunakan kaedah spektroskopi impedans apabila didedahkan terhadap tahap oksigen yang berbeza. Untuk mengatasi masalah kebolehlarutan Ba dan Ti yang berbeza, nisbah sebatian Ba yang ditambah lebih tinggi daripada nisbah stoikiometri (tambahan 10%) dan nilai pH larutan yang tinggi (pH~13) diperlukan. Ujian XRD dan TGDTA menunjukkan BaTiO3 yang hampir tulen dapat disintesis melalui kaedah ini. Suhu pengkalsinan yang lebih tinggi menghasilkan darjah penghabluran bahan yang lebih tinggi. Kajian dielektrik menunjukkan bahan yang dihasilkan mengandungi lebih daripada satu elemen keelektrikan antaranya teras berkerintangan rendah, sempadan butiran berkapasitan tinggi dan suatu elemen pukal feroelektrik. Setelah didedahkan terhadap tahap oksigen yang lebih tinggi, nilai kerintangan sampel bertambah, yang mungkin disebabkan stoikiometri oksigen pada sampel yang diuji. Peningkatan dalam nilai kapasitan daripada sempadan butiran adalah lebih ketara jika dibandingkan dengan peningkatan unsur feroelektrik pukal. Kata kunci: Kaedah sol-gel, sintesis kimia, sifat dielektrik, BaTiO3 The dielectric properties of BaTiO3 powders prepared by a low temperature aqueous route when exposed to different oxygen concentrations have been studied by means of impedance spectroscopy. Due to the differences of solubility of Ba and Ti in aqueous solutions, deviations from stoichiometric ratios (a 10% excess) and higher solution pH (pH~13) were necessary. XRD traces and TG-DTA curves show the formation of nearly phase-pure BaTiO3 with higher calcinations temperatures promoting greater crystallinities. Dielectric measurements using impedance spectroscopy show the samples to consist of more than one electrical element including a low resistivity core, a high capacitance grain boundary and a ferroelectric bulk component. Exposing the samples to different oxygen concentrations caused a slight increase in resistivities with increasing oxygen concentration, which was attributed to the oxygen stoichiometry. A greater increase in the capacitance of the grain boundary component was also observed compared to the ferroelectric bulk. Key words: Sol-gel processes, chemical processes, dielectric properties, BaTiO3
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Dewi, Rahmi, Krisman Krisman, Tiara Pertiwi, and Tengku Luqman. "Pembuatan dan Karakterisasi Kapasitor Barium Strontium Titanat (Bst) Ba0,75 Sr0,25 TiO3." Talenta Conference Series: Science and Technology (ST) 2, no. 2 (June 30, 2019). http://dx.doi.org/10.32734/st.v2i2.490.

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Lapisan tipis Barium Strontium Titanate (BST) telah ditelaah dengan komposisi Ba0.75 Sr0.25 TiO3 menggunakan metode sol-gel yang digabungkan pada suhu 600 dan 650oC. Lapisan tipis BST dikarakterisasi menggunakan Field Emission Scanning Electron Microscopy (FESEM) dan spektroskopi impedansi. Hasil dari karakterisasi FESEM untuk sampel pada suhu 600 dan 650oC ialah 55.83 nm dan 84.88 nm dari segi ketebalan secara berurutan. Hasil dari karakterisasi spektroskopi impedansi berdasarkan nilai frekuensi menunjukkan nilai impedansi yang nyata dan imajiner. Nilai kapasitsa pada frekuensi 20 Hz dari lapisan tipis BST pada suhu 600 dan 650oC ialah 69.36 dan 138.70 F. Konstanta dielektrik dari lapisan tipis BST pada suhu 600 dan 650oC ialah 22.17 dan 131.56 secara berurutan. The thin film of Barium Strontium Titanate (BST) has been studied with composition of Ba0.75 Sr0.25 TiO3 by using sol-gel method that annealed in temperature of 600oC and 650oC. The thin film of BST is characterized by using Field Emission Scanning Electron Microscopy (FESEM) and an impedance spectroscopy. The results of FESEM characterization for samples in temperature of 600 dan 650oC are 55.83 nm and 84.88 nm in thickness respectively. The result of impedance spectroscopy characterization given frequency values obtained by the impedance value of real and imaginary.The capacitance value at a frequency of 20 Hz from a thin film of BST in temperature of 600 dan 650oC are 69.36 F and 138.7oF. The dielectric constant of the thin film of BST in temperature of 600 dan 650oC are 22.17 and 131.56 respectively.
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MAMUK, Atilla Eren, and Nejmettin AVCİ. "4-butoxybenzylidene-4’-butylaniline (BBBA) Sıvı Kristalinin Geniş Sıcaklık Aralığında İncelenmesi: Optik, Dielektrik, Kalorimetrik ve Kızılötesi Spektroskopik Analiz." Bitlis Eren Üniversitesi Fen Bilimleri Dergisi, May 5, 2021. http://dx.doi.org/10.17798/bitlisfen.847874.

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Dissertations / Theses on the topic "Dielektrická spektroskopie"

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Stráník, Rostislav. "Dielektrická relaxační spektroskopie glycerolu." Doctoral thesis, Vysoké učení technické v Brně. Fakulta elektrotechniky a komunikačních technologií, 2008. http://www.nusl.cz/ntk/nusl-233415.

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This doctoral thesis deals with the analysis of dielectric spectra of glycerol with dielectric relaxation spectroscopy (DRS). Dielectric spectra of glycerol have been measured in the frequency range 20 Hz to 10 MHz and in the temperature range 10 K to 300 K. The observed dielectric spectra featured a typical relaxation maximum, which could be in the first approximation described by the Arrhenius equation. The activation energy of the relaxation process observed was 90 MJ/kmol. The relaxation strength as well as the shape of the relaxation peak remained in the temperature interval 180 K - 230 K (visibility of peak) almost the same, thus indicating that no change of the relaxation mechanism comes about. Much attention was in the thesis paid to the analysis of the excess component of the relaxation alfa process, in the literature commonly denoted as "excess wing". The thesis puts forward a procedure for the quantification of the magnitude of the excess wing. The excess wing magnitude thus determined turns out to increase monotonously with increasing temperature. The excess wing is here interpreted as a manifestation of a weakly-pronounced beta relaxation.
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Holcman, Vladimír. "Dielektrická relaxační spektroskopie kompozitních soustav." Doctoral thesis, Vysoké učení technické v Brně. Fakulta elektrotechniky a komunikačních technologií, 2008. http://www.nusl.cz/ntk/nusl-233414.

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The subject of this doctoral thesis is the study of dielectric properties of a binary composite made up of a polymer matrix and metallic filler. Properties of such composites have been extensively examined in the past and they turned out to depend on temperature, frequency and in particular on filler concentration. The objective of this work was first to experimentally establish and second to describe quantitatively the effect of the size of metallic particles on the properties of the composite concerned, yet at the same filler concentration. This study was carried out on the model system ethylene-vinylacetate copolymer – nickel. The acquisition of experimental results required extensive measurements in a wide frequency and temperature interval, as well as a manufacture and preparation of a large set of samples with different concentrations and Ni filler sizes. Measurements were in part carried out at the Centre for Electronic Correlations and Magnetism, Institute of Experimental Physics V of the University of Augsburg (Germany) and, after the installation of a new cryogenic system, at the Department of Physics at FEEC, BUT Brno. Measurements were performed on a number of meters (Alpha-Analyzer of Novocontrol, HP4284A and HP4285A of Hewlett Packard and E4991A of Agilent) in the frequency range 1 Hz – 1 MHz and in the temperature interval 10 K – 300 K. The nickel concentration in systems studied varied from 0 % to 75 % and nickel particles were of a spherical shape with diameters between 35 and 115 m. The measurement results have shown that in the above frequency and temperature window just a single relaxation and a single conductivity mechanism occur. It was also proved that the frequency dependence of complex permittivity is for different Ni particle sizes at the same concentration different. These results have been quantified and a simple mathematical formula based on the Lichtenecker mixture rule has been proposed for their description. The physical origin of the effect of particle size at the same total nickel concentration is sought in different surface areas of internal interfaces between nickel and polymer in the composite
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Palai-Dany, Tomáš. "Dielektrická spektroskopie karboxymetylcelulózy v časové oblasti." Doctoral thesis, Vysoké učení technické v Brně. Fakulta elektrotechniky a komunikačních technologií, 2009. http://www.nusl.cz/ntk/nusl-233477.

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The dissertation deals with the time-domain dielectric relaxation spectroscopy of carboxymethylcellulose. The main attention was paid to the experimental part of research, mainly to the design and subsequent development of an experimental setup for the measurement of discharge currents and for their processing and analysis. The subject of the measurement is carboxymethylcellulose (CMC), which is a simple polysaccharide used in wide range of applications, among else also in biomedical engineering. The study of CMC properties has required the development of a new experimental set-up of original design, which includes the equilibration (short-circuiting) of a sample before the measurement, charging and discharging at defined time intervals, switching between these two modes, recording of measurement, adjustments and processing of measured signals up to Fourier transformation into the frequency domain and, finally, calculation of complex permittivity of the sample. The frequency dependence of complex permittivity or its imaginary part, obtained by Fourier transformation of discharge current in time domain, is then referred to as the dielectric spectrum. In view of the fact that current measurements were done at very low levels of measured signal (below 10-12 A) the whole measurement was no easy matter. The framework of the work also necessitated studies and subsequent resolution of problems associated with shielding, grounding, presence of noise and sensitivity to various ambient influences. The research work focused on a reliable and trustworthy measurement of very low discharge currents and, subsequently, mathematical processing of noise present in them, i.e., operations with the original, experimentally established signal in time domain, leading in principle to a digital filtration of measured dielectric data. A further pursued objective is the explanation of dielectric parameters of tested carboxymethylcellulose sample in the widest possible frequency spectrum. The integral part of the research was the selection and application of the method for the transformation of the adjusted signal to the frequency domain. The experimental works, including data processing, were carried out in the Department of Physics, Brno FEEC BUT. Measurements were done with Keithley 617 Electrometer, HP4284A Frequency Analyzer and Janis CCS-400-204 cryogenic system. The results were completed with results obtained at the V Department of Experimental Physics, Centre for Electronic Correlations and Magnetism, University of Augsburg, Germany.
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Kučera, Miroslav. "Analýza vícefaktorového namáhání na dielektrická spektra materiálů." Master's thesis, Vysoké učení technické v Brně. Fakulta elektrotechniky a komunikačních technologií, 2011. http://www.nusl.cz/ntk/nusl-219190.

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Diploma thesis treat of effect of thermal, electrical and combined (thermal electrical) stress on electrical characteristics of insulation material ISONOM NMN which is used as a slot insulation in electric motors. To monitor the stress is used the method of dielectric relaxation spectroscopy. Under examinations are the resultant dielectric spectra which constitute the frequency dependencies of components of complex permitivity. Compared are the effects of particular stresses on dielectric spectra of surveyed insulative material.
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Abuetwirat, Inas Faisel. "Dielektrické vlastnosti tenkých vrstev oxidů niobu a tantalu." Doctoral thesis, Vysoké učení technické v Brně. Fakulta elektrotechniky a komunikačních technologií, 2014. http://www.nusl.cz/ntk/nusl-233619.

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Dielektrická relaxační spektroskopie je jednou z užitečných metod pro studium molekulární dynamiky materiálů. Díky nedávnému pokroku v přístrojové a měřicí technice je dnes možné získat dielektrické spektrum v širokém frekvenčním intervalu a pro velice rozdílné materiály. Cílem mé práce bylo studium dielektrických relaxačních spekter a vodivosti oxidů titanu, niobu, tantalu, lanthanu a hafnia pro katody pracující na principu studené emise. Cílem výzkumu bylo analyzovat frekvenční a teplotní chování těchto oxidů, včetně jejich vodivosti, v širokém frekvenčním a teplotním rozsahu, a pokusit se stanovit původ relaxačního mechanismu. Vzhledem k tomu, že původně zadaný rozsah oxidů byl dosti široký, soustředila se pozornost pouze na oxidy tantalu a niobu, rovněž s ohledem na jejich aplikace v elektrolytických kondenzátorech. Elektrické, tepelné a mechanické (při zpracování) vlastnosti oxidů tantalu a niobu jsou dnes již dobře prozkoumány. K dispozici je však jen málo poznatků o jejich dielektrických relaxačních mechanismech. Výsledky získané pro Ta2O5 ukazují existence relaxačního maxima, nacházejícího se v experimentálně dostupném teplotním a frekvenčním intervalu 187 K – 385 K a 1 Hz – 10 MHz. Frekvence ztrátového maxima se řídí Arrheniovým zákonem s aktivační energií 0.048 eV. Ve vodivostních spektrech vykazují tenké vrstvy Ta2O5 na nízkých frekvencích ustálenou hodnotu a při vysokých frekvencích monotónní nárůst, který závisí na teplotě. Pozorovanou vodivost lze popsat mocninnou funkcí s exponentem nepatrně větším než jedna (tzv. superlineární závislost). Výsledky získané pro Nb2O5 v podobné teplotní a frekvenční oblasti, 218 K – 373 K, 1 Hz – 1 MHz rovněž ukazují jedno relaxační maximum. Frekvence ztrátového maxima se opět řídí Arrheniovým zákonem s poněkud vyšší aktivační energií 0.055 eV. Niobové kondenzátory vykazují vodivostní mechanismus shodný s kondenzátory tantalovými.
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Ježík, Jan. "Studium dielektrické relaxace v základních materiálech DPS a v izolacích kabelů." Master's thesis, Vysoké učení technické v Brně. Fakulta elektrotechniky a komunikačních technologií, 2011. http://www.nusl.cz/ntk/nusl-219358.

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This study investigates relaxation polarization in some dielectric components of tester UNISPOT S40 developed by company UNITES Systems a.s. Relaxation polarization in the PCB substrates and in tester’s cable insulation causes undesirable deceleration of some test steps. Relaxation polarization in selected PCB substrates and various cables are examined by method of dielectric relaxation spectroscopy in the frequency domain and by measurement of polarization or depolarization current.
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Paščinský, Jiří. "Vliv parametrů vytvrzování na vlastnosti elektroizolačních laků." Master's thesis, Vysoké učení technické v Brně. Fakulta elektrotechniky a komunikačních technologií, 2011. http://www.nusl.cz/ntk/nusl-219047.

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The bachelor thesis submitted deals with properties of electro-insulating lacquer hardenable by ultraviolent radiation and temperature. Within the theoretical part a summary of electro-insulating lacquers used in electrotechnics has been elaborated. Chemical changes that take place in this material group have been described during hardening process. A method of dielectric relaxation spectroscopy specifically focused on mathematic and physical description of polarisation and conductive mechanisms taking place in the structure of the given material has been closely studied. In the experimental part a workplace for hardening and long-term exposition of lacquered samples during simultaneous effect of various climatic elements has been designed and built. The selected electric and mechanical properties have been monitored on three sets of experimental samples prepared by means of different methodical procedures. The results gained have been mathematically evaluated and physically interpreted in term of methodical procedure of hardening and different temperature of measurement.
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Mydlář, Marek. "Analýza složené soustavy s různým podílem plniva." Master's thesis, Vysoké učení technické v Brně. Fakulta elektrotechniky a komunikačních technologií, 2009. http://www.nusl.cz/ntk/nusl-217945.

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This master’s thesis applies dielectric relaxation spectroscopy to analyse impact of climatic changes on dielectric properties of composite material samples (TSA 220S varnish combined with 60.030 mica). Experiments aim to analyse effect of mica composite mass ratio (0, 4, 8 and 16 % of mica), relative humidity (0, 33, 55, 65, 75 and 95 %) and temperature (23, 30, 40 and 50 C) on complex permitivity as a function of frequency.
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Brož, Přemysl. "Analýza složené soustavy s různým podílem plniva." Master's thesis, Vysoké učení technické v Brně. Fakulta elektrotechniky a komunikačních technologií, 2008. http://www.nusl.cz/ntk/nusl-217181.

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Kamenická, Zuzana. "Nejistoty měření v diagnostice izolačních materiálů." Master's thesis, Vysoké učení technické v Brně. Fakulta elektrotechniky a komunikačních technologií, 2009. http://www.nusl.cz/ntk/nusl-217948.

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This work deals with measurement capacity and dissipation factor of capacitor with real dielectric in frequency range 20 Hz to 30 MHz. Liquid and solid dielectrics are measured by LCR instruments and by test fixtures, both from company Agilent. Relative permittivity and loss number are calculated for different instruments settings. The general aim is to specify the influence of parameters as frequency, voltage, integration time and thickness of material on the uncertainties of primary and secondary quantities for measurement.
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