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Journal articles on the topic 'Diethynylbenzene'

Author: Grafiati

Published: 4 June 2021

Last updated: 4 February 2022

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1

Gao, Man, Chengyuan Shang, Jixian Li, Gang Han, Junkun Tang, Qiaolong Yuan, and Farong Huang. "Synthesis and Characterization of Block Copolymers of Poly(silylene diethynylbenzen) and Poly(silylene dipropargyl aryl ether)." Polymers 13, no. 9 (May 7, 2021): 1511. http://dx.doi.org/10.3390/polym13091511.

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Poly(silylene diethynylbenzene)–b–poly(silylene dipropargyloxy diphenyl propane) copolymer (ABA-A), poly(silylene diethynylbenzene)–b–poly(silylene dipropargyloxy diphenyl ether) copolymer (ABA-O), and a contrast poly(silylene diethynylbenzene) with equivalent polymerization degree were synthesized through Grignard reactions. The structures and properties of the copolymers were investigated via hydrogen nuclear magnetic resonance, Fourier transform infrared spectroscopy, Haake torque rheometer, differential scanning calorimetry, dynamic mechanical analysis, thermogravimetric analysis and mechanical tests. The results show that the block copolymers possess comprehensive properties, especially good processability and good mechanical properties. The processing windows of these copolymers are wider than 58 °C. The flexural strength of the cured ABA-A copolymer reaches as high as 40.2 MPa. The degradation temperatures at 5% weight loss (Td5) of the cured copolymers in nitrogen are all above 560 °C.

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2

Chimenti, F., A. Bolasco, D. Secci, P. Chimenti, and A. Granese. "Synthesis of New Diethynylbenzene Derivatives." Synthetic Communications 34, no. 14 (January 1, 2004): 2549–55. http://dx.doi.org/10.1081/scc-200025604.

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3

Zou, Yan, Hui Min Qi, Mei Ling Xu, Fa Rong Huang, and Lei Du. "Synthesis and Characterization of a Novel Hyperbranched Poly(Diethynylbenzene-Silane)." Advanced Materials Research 560-561 (August 2012): 174–78. http://dx.doi.org/10.4028/www.scientific.net/amr.560-561.174.

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Hyperbranched poly(diethynylbenzene-silane) (hb-PDEBS) was synthesized through polycondensation reaction of diethynylbenzene Grignard reagent (A2) and trichlorosilane (B3), and its structure was characterized by FT-IR, 1H-NMR, GPC and Elemental Analysis. The degree of branching of hb-PDEBS was defined by 29Si-NMR and calculated to be about 0.68. The curing behavior of hb-PDEBS was investigated by DSC. Thermal stability of cured hb-PDEBS was examined by TGA, and its residue at 1000°C under nitrogen was 80.6%. Hb-PDEBS displayed a strong absorption due to π-π* transition and exhibited the most intensity structured emission with a maximum around 500 nm.

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4

Neti, Venkata S. Pavan K., Jun Wang, Shuguang Deng, and Luis Echegoyen. "High and selective CO2 adsorption by a phthalocyanine nanoporous polymer." Journal of Materials Chemistry A 3, no. 19 (2015): 10284–88. http://dx.doi.org/10.1039/c5ta00587f.

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5

Yasin, Akram, Yurong Chen, Yanxia Liu, Letao Zhang, Xingjie Zan, and Yagang Zhang. "Hyperbranched multiple polythioamides made from elemental sulfur for mercury adsorption." Polymer Chemistry 11, no. 4 (2020): 810–19. http://dx.doi.org/10.1039/c9py01544b.

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Different from traditional polyethylenimine (PEI) modified Hg(ii) adsorbent materials, a novel hyperbranched polythioamide adsorbent (SPD) was prepared by using sulfur, PEI and 1,4-diethynylbenzene (DEB) as monomers.

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6

Figueira, João, João Rodrigues, Luca Russo, and Kari Rissanen. "Three 2,5-dialkoxy-1,4-diethynylbenzene derivatives." Acta Crystallographica Section C Crystal Structure Communications 64, no. 2 (January 12, 2008): o33—o36. http://dx.doi.org/10.1107/s0108270107065523.

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7

Ichitani, Motokuni, Koji Yonezawa, Kazuhiro Okada, and Toshiya Sugimoto. "Silyl-Carborane Hybridized Diethynylbenzene–Silylene Polymers." Polymer Journal 31, no. 11_1 (November 1999): 908–12. http://dx.doi.org/10.1295/polymj.31.908.

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8

Arenas, J. F., J. I. Marcos, and F. J. Ramirez. "Normal coordinate analysis of 1,4-diethynylbenzene." Spectrochimica Acta Part A: Molecular Spectroscopy 45, no. 8 (January 1989): 781–88. http://dx.doi.org/10.1016/0584-8539(89)80214-4.

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9

Plenzig, Felicitas, Alexey Lyubimtsev, and Michael Hanack. "Synthesis of Acetylene Bridged Germanium Phthalocyanines." Natural Product Communications 7, no. 3 (March 2012): 1934578X1200700. http://dx.doi.org/10.1177/1934578x1200700319.

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The octaalkyl- or octaalkoxysubstituted phthalocyaninatogermanium dichlorides 10b,d,e and 10a-c were reacted with bisbromomagnesiumacetylene 16 and bisbromomagnesium- p-diethynylbenzene 18, respectively with formation of the corresponding acetylene bridged oligomers 17a-c and 19a-c, respectively.

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10

Misin, Vjacheslav, Nikolay Glagolev, and Michael Misin. "Polymers of Phenyldiacetylenes – Functional Thermostable Additions to Industrial Resins." Chemistry and Chemical Technology 4, no. 2 (June 15, 2010): 131–37. http://dx.doi.org/10.23939/chcht04.02.131.

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High thermal and thermooxidation stability of homo and copolymers of diphenyldiacetylene and p-diethynylbenzene was established. The amount of coke residue, obtained from commercial epoxy-resins, is essentially increased upon their modification with added polymers. Additions of polydiethynylbenzene to commercial olygoetheracrylates improved their thermooxidation stability.

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11

Trofimov, B. A., E. Yu Shmidt, N. V. Zorina, and A. I. Mikhaleva. "Nucleophilic addition of acetophenone to 1,4-diethynylbenzene." Russian Journal of Organic Chemistry 46, no. 9 (September 2010): 1414–15. http://dx.doi.org/10.1134/s1070428010090253.

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12

Volkova, N. N., A. F. Zholudev, M. B. Kislov, E. V. Suslova, and L. S. Yanovskiy. "Microstructure of 1,4-diethynylbenzene frontal polymerization products." IOP Conference Series: Materials Science and Engineering 693 (November 28, 2019): 012027. http://dx.doi.org/10.1088/1757-899x/693/1/012027.

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13

Lempert, D. B., I. N. Zyuzin, A. V. Nabatova, A. I. Kazakov, and L. S. Yanovskii. "Thermochemical and Energy Characteristics of 1,4-Diethynylbenzene." Combustion, Explosion, and Shock Waves 55, no. 6 (November 2019): 644–47. http://dx.doi.org/10.1134/s0010508219060029.

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14

Zhan, Xiaowei, Mujie Yang, Gang Xu, Xuchun Liu, and Peixian Ye. "Poly(p-diethynylbenzene) Derivatives for Nonlinear Optics." Macromolecular Rapid Communications 22, no. 5 (March 1, 2001): 358–62. http://dx.doi.org/10.1002/1521-3927(20010301)22:5<358::aid-marc358>3.0.co;2-x.

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15

Hagihara, Masahiko, Yukio Yamamoto, Shigetoshi Takahashi, and Koichiro Hayashi. "Radiation-induced polymerization of crystalline diethynylbenzene derivatives." International Journal of Radiation Applications and Instrumentation. Part C. Radiation Physics and Chemistry 28, no. 2 (January 1986): 165–67. http://dx.doi.org/10.1016/1359-0197(86)90121-9.

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16

Tobe, Yoshito, Naoto Utsumi, Kazuya Kawabata, and Koichiro Naemura. "Synthesis and self-association properties of diethynylbenzene macrocycles." Tetrahedron Letters 37, no. 52 (December 1996): 9325–28. http://dx.doi.org/10.1016/s0040-4039(97)82954-1.

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17

Sajoto, Tissa, Shree Prakash Tiwari, Huifang Li, Chad Risko, Stephen Barlow, Qing Zhang, Jian-Yang Cho, Jean-Luc Brédas, Bernard Kippelen, and Seth R. Marder. "Synthesis and characterization of naphthalene diimide/diethynylbenzene copolymers." Polymer 53, no. 5 (February 2012): 1072–78. http://dx.doi.org/10.1016/j.polymer.2012.01.016.

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18

Kobayashi, Eiichi, Yukihiro Terada, Toyoshi Ohashi, and Junji Furukawa. "Molecular Interaction between 1,4-Benzenedithiol and 1,4-Diethynylbenzene." Polymer Journal 23, no. 4 (April 1991): 267–75. http://dx.doi.org/10.1295/polymj.23.267.

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19

Bosch, Eric. "Cocrystals of 1,4-diethynylbenzene with 1,3-diacetylbenzene and benzene-1,4-dicarbaldehyde exhibiting strong nonconventional alkyne–carbonyl C—H...O hydrogen bonds between the components." Acta Crystallographica Section C Structural Chemistry 72, no. 10 (September 26, 2016): 748–52. http://dx.doi.org/10.1107/s2053229616014972.

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Weak interactions between organic molecules are important in solid-state structures where the sum of the weaker interactions support the overall three-dimensional crystal structure. Thesp-C—H...N hydrogen-bonding interaction is strong enough to promote the deliberate cocrystallization of a series of diynes with a series of dipyridines. It is also possible that a similar series of cocrystals could be formed between molecules containing a terminal alkyne and molecules which contain carbonyl O atoms as the potential hydrogen-bond acceptor. I now report the crystal structure of two cocrystals that support this hypothesis. The 1:1 cocrystal of 1,4-diethynylbenzene with 1,3-diacetylbenzene, C10H6·C10H10O2, (1), and the 1:1 cocrystal of 1,4-diethynylbenzene with benzene-1,4-dicarbaldehyde, C10H6·C8H6O2, (2), are presented. In both cocrystals, a strong nonconventional ethynyl–carbonylsp-C—H...O hydrogen bond is observed between the components. In cocrystal (1), the C—H...O hydrogen-bond angle is 171.8 (16)° and the H...O and C...O hydrogen-bond distances are 2.200 (19) and 3.139 (2) Å, respectively. In cocrystal (2), the C—H...O hydrogen-bond angle is 172.5 (16)° and the H...O and C...O hydrogen-bond distances are 2.25 (2) and 3.203 (2) Å, respectively.

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20

Trofimov, B. A., E. Yu Shmidt, N. V. Zorina, and A. I. Mikhaleva. "ChemInform Abstract: Nucleophilic Addition of Acetophenone to 1,4-Diethynylbenzene." ChemInform 42, no. 11 (February 17, 2011): no. http://dx.doi.org/10.1002/chin.201111103.

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21

Eichhorn, Johanna, Wolfgang M. Heckl, and Markus Lackinger. "On-surface polymerization of 1,4-diethynylbenzene on Cu(111)." Chemical Communications 49, no. 28 (2013): 2900. http://dx.doi.org/10.1039/c3cc40444g.

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22

Benkhäuser, Christian, and Arne Lützen. "Self-assembly of heteroleptic dinuclear metallosupramolecular kites from multivalent ligands via social self-sorting." Beilstein Journal of Organic Chemistry 11 (May 8, 2015): 693–700. http://dx.doi.org/10.3762/bjoc.11.79.

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A Tröger's base-derived racemic bis(1,10-phenanthroline) ligand (rac)-1 and a bis(2,2'-bipyridine) ligand with a central 1,3-diethynylbenzene unit 2 were synthesized. Each of these ligands acts as a multivalent entity for the binding of two copper(I) ions. Upon coordination to the metal ions these two ligands undergo selective self-assembly into heteroleptic dinuclear metallosupramolecular kites in a high-fidelity social self-sorting manner as evidenced by NMR spectroscopy and mass spectrometry.

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23

Ferdousi Moon, Jannatul, Mohammad Mizanur Rahman Khan, M. Ashraful Alam, and Muhammad Younus. "Simple synthesis of poly (1,4-bis(dodecyloxy)-2,5-diethynylbenzene)/Pd composites with catalytic activity in Sonogashira coupling reaction." International Journal of Chemical Reactor Engineering 19, no. 4 (March 22, 2021): 439–46. http://dx.doi.org/10.1515/ijcre-2020-0220.

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Abstract Palladium on the polymeric materials (Pd@polymer) as a catalyst is now very promising due to its great prospect for catalytic application. Such material in the form of composites is found to be stable and can be applied as catalyst in organic synthesis like Sonogashira coupling reaction. In the present work, Pd containing conjugated poly-ynes composites (Poly (1,4-bis(dodecyloxy)-2,5-diethynylbenzene) (Poly-DEB)/Pd) were synthesized by varying the addition of Pd in the range of equivalent weight of 8:4, 8:2 and 8:1, maintaining the fixed amount of 1,4-bis(dodecyloxy)-2,5-diethynylbenzene (DEB) through chemical oxidative polymerization technique. Both FTIR and UV-visible spectroscopy confirmed the interactions between DEB and Pd in the composites. The DSC data revealed the improved melting temperature as well as the crystallinity of the composites than the DEB. The PL spectra showed its florescence property. The catalytic capability of the Poly-DEB/Pd composites were examined using the Sonogashira coupling reactions, which demonstrated good yields. The suggested synthetic protocol is very facile, reproducible and beneficial for the fabrication of diverse mono and bimetallic composites with conjugated polymers. The present study also demonstrates the new example of Poly-DEB/Pd composites catalyzed Sonogashira coupling reaction. These composites have a possibility to develop as a commercial reagent in various organic synthesis subjects to its application prospects.

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24

Zhan, Xiaowei, Mujie Yang, and Ziqiang Lei. "Transition metal acetylide catalysts for polymerization of p-diethynylbenzene 4." Journal of Molecular Catalysis A: Chemical 184, no. 1-2 (June 2002): 139–45. http://dx.doi.org/10.1016/s1381-1169(02)00006-7.

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25

Tobe, Yoshito, Naoto Utsumi, Kazuya Kawabata, Atsushi Nagano, Kiyomi Adachi, Shunji Araki, Motohiro Sonoda, Keiji Hirose, and Koichiro Naemura. "m-Diethynylbenzene Macrocycles: Syntheses and Self-Association Behavior in Solution." Journal of the American Chemical Society 124, no. 19 (May 2002): 5350–64. http://dx.doi.org/10.1021/ja012458m.

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26

Zhan, Xiaowei, Mujie Yang, Youqing Shen, and Meixiang Wan. "Vibration and photoelectron spectroscopies of iodine-doped poly(p-diethynylbenzene)." European Polymer Journal 38, no. 12 (December 2002): 2349–53. http://dx.doi.org/10.1016/s0014-3057(02)00144-1.

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27

TOBE, Y., N. UTSUMI, K. KAWABATA, and K. NAEMURA. "ChemInform Abstract: Synthesis and Self-Association Properties of Diethynylbenzene Macrocycles." ChemInform 28, no. 16 (August 4, 2010): no. http://dx.doi.org/10.1002/chin.199716122.

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28

Stearns, Jaime A., and Timothy S. Zwier. "Infrared and Ultraviolet Spectroscopy of Jet-Cooledortho-,meta-, andpara-Diethynylbenzene†." Journal of Physical Chemistry A 107, no. 49 (December 2003): 10717–24. http://dx.doi.org/10.1021/jp035168w.

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29

Wang, Fan, Yan Zhou, Farong Huang, and Lei Du. "Synthesis and properties of a novel poly(diethynylbenzene-siloxane) resin." High Performance Polymers 24, no. 4 (May 2, 2012): 247–53. http://dx.doi.org/10.1177/0954008311432359.

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30

ITOH, Takahito, Minoru AZUCHI, and Shouji IWATSUKI. "Polymerization of m-diethynylbenzene and electrical properties of the polymer." NIPPON KAGAKU KAISHI, no. 5 (1985): 949–55. http://dx.doi.org/10.1246/nikkashi.1985.949.

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31

Misin, V. M., N. N. Glagolev, and M. V. Misin. "Modification of commercial oligomers with diphenyldiacetylene and p-diethynylbenzene polymers." Russian Journal of Applied Chemistry 81, no. 11 (November 2008): 2008–13. http://dx.doi.org/10.1134/s107042720811027x.

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32

Tobe, Y., T. Nagai, S. Araki, T. Ichikawa, A. Nomoto, M. Sonoda, and K. Hirose. "Self-Assembly ofm-Diethynylbenzene Macrocycles Containing Exoannular Chiral Side Chains." Advanced Functional Materials 16, no. 12 (August 4, 2006): 1549–54. http://dx.doi.org/10.1002/adfm.200500306.

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33

Zhao, Jianwei, Yanwei Li, Hongmei Liu, Peng Li, and Geping Yin. "A quantum chemistry study of diethynylbenzene macrocycles: Structural and electronic properties." Journal of Molecular Structure: THEOCHEM 861, no. 1-3 (July 2008): 7–13. http://dx.doi.org/10.1016/j.theochem.2008.03.031.

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34

Tanaka, K., K. Sato, D. Shiomi, T. Takui, Y. Nozaki, K. Hirai, and H. Tomioka. "Cw/pulsed ESR study of bis[dianthrylcarbene] coupled by 1,4-diethynylbenzene." Synthetic Metals 121, no. 1-3 (March 2001): 1818–19. http://dx.doi.org/10.1016/s0379-6779(00)01001-8.

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35

Lim, Jong Kuk, Sang-Woo Joo, and Kuan Soo Shin. "Concentration dependent Raman study of 1,4-diethynylbenzene on gold nanoparticle surfaces." Vibrational Spectroscopy 43, no. 2 (March 2007): 330–34. http://dx.doi.org/10.1016/j.vibspec.2006.04.006.

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36

Zhan, Xiaowei, Mujie Yang, and Meixiang Wan. "Electrical properties and spectroscopic studies of HClO4-doped poly(p-diethynylbenzene)." Synthetic Metals 94, no. 3 (May 1998): 249–53. http://dx.doi.org/10.1016/s0379-6779(98)00007-1.

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37

Shi, Chenjun, Kaixia Yang, and Yong Cao. "Synthesis and Optical Properties of Soluble Conjugated Poly(p-Diethynylbenzene)s." Synthetic Metals 154, no. 1-3 (September 2005): 121–24. http://dx.doi.org/10.1016/j.synthmet.2005.07.031.

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38

Lei, Z Q, M J Yang, and X F Lin. "A new simple synthesis of soluble copolymers ofp-diethynylbenzene with phenylacetylene." Polymer International 48, no. 9 (September 1999): 781–86. http://dx.doi.org/10.1002/(sici)1097-0126(199909)48:9<781::aid-pi217>3.0.co;2-v.

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39

Fox, Mark A., Julian D. Farmer, Rachel L. Roberts, Mark G. Humphrey, and Paul J. Low. "Noninnocent Ligand Behavior in Diruthenium Complexes Containing a 1,3-Diethynylbenzene Bridge." Organometallics 28, no. 17 (September 14, 2009): 5266–69. http://dx.doi.org/10.1021/om900200n.

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40

Tomassetti, M., L. Campanella, C. Morgia, and G. Ortaggi. "Thermal analysis and conducting properties of polymers of diethynylbenzene and diethynylpyridine." Thermochimica Acta 141 (March 1989): 27–39. http://dx.doi.org/10.1016/0040-6031(89)87038-8.

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41

Yang, Mujie, Yang Li, Xiaowei Zhan, and Mingfang Ling. "A novel resistive-type humidity sensor based on poly(p-diethynylbenzene)." Journal of Applied Polymer Science 74, no. 8 (November 21, 1999): 2010–15. http://dx.doi.org/10.1002/(sici)1097-4628(19991121)74:8<2010::aid-app16>3.0.co;2-1.

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42

Zhan, Xiaowei, Shengang Xu, Mujie Yang, Youqing Shen, and Meixiang Wan. "Vibration and X-ray photoelectron spectroscopies of FeCl3-doped poly(p-diethynylbenzene)." European Polymer Journal 38, no. 10 (October 2002): 2057–61. http://dx.doi.org/10.1016/s0014-3057(02)00091-5.

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43

Choi, Jung-Hwa, and Dong-Gyu Cho. "Synthesis and anion binding properties of m-diethynylbenzene expanded calix[4]pyrrole." Tetrahedron Letters 54, no. 50 (December 2013): 6928–30. http://dx.doi.org/10.1016/j.tetlet.2013.10.046.

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44

Zhang, Baixue, Quan Zhou, Yongli Wang, Ning Song, and Lizhong Ni. "Synthesis of ordered mesoporous carbon using m-Diethynylbenzene as a new precursor." Materials Letters 189 (February 2017): 317–20. http://dx.doi.org/10.1016/j.matlet.2016.11.008.

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45

Madathil, Pramod Kandoth, Benoît Heinrich, Bertrand Donnio, Fabrice Mathevet, Jean-Louis Fave, Daniel Guillon, Andre-Jean Attias, Changjin Lee, Tae-Dong Kim, and Kwang-Sup Lee. "Diethynylbenzene-Based Liquid Crystalline Semiconductor for Solution-Processable Organic Thin-Film Transistors." Journal of Nanoscience and Nanotechnology 10, no. 10 (October 1, 2010): 6800–6804. http://dx.doi.org/10.1166/jnn.2010.2947.

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46

Miki, Koji, Hiroyuki Kuge, Rui Umeda, Motohiro Sonoda, and Yoshito Tobe. "PtCl2-Catalyzed Cyclization of o-Diethynylbenzene Derivatives Triggered by Intramolecular Nucleophilic Attack." Synthetic Communications 41, no. 7 (March 3, 2011): 1077–87. http://dx.doi.org/10.1080/00397911003797817.

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47

Kobayashi, Eiichi, Toyoshi Ohashi, and Junji Furukawa. "Microstructure of an Addition Polymer Composed of 1,4-Benzenedithiol and 1,4-Diethynylbenzene." Polymer Journal 21, no. 2 (February 1989): 111–17. http://dx.doi.org/10.1295/polymj.21.111.

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48

Li, Yang, Mujie Yang, Mingfang Ling, and Yunhai Zhu. "Surface acoustic wave humidity sensors based on poly(p-diethynylbenzene) and sodium polysulfonesulfonate." Sensors and Actuators B: Chemical 122, no. 2 (March 26, 2007): 560–63. http://dx.doi.org/10.1016/j.snb.2006.06.031.

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49

Zhang, Wei, Masashi Shiotsuki, and Toshio Masuda. "Polymerization of o-diethynylbenzene and its derivatives controlled by transition metal catalyst systems." Polymer 47, no. 9 (April 2006): 2956–61. http://dx.doi.org/10.1016/j.polymer.2006.03.011.

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50

Poad, Berwyck L. J., Nicholas D. Reed, Christopher S. Hansen, Adam J. Trevitt, Stephen J. Blanksby, Emily G. Mackay, Michael S. Sherburn, Bun Chan, and Leo Radom. "Preparation of an ion with the highest calculated proton affinity: ortho-diethynylbenzene dianion." Chemical Science 7, no. 9 (2016): 6245–50. http://dx.doi.org/10.1039/c6sc01726f.

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