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Journal articles on the topic 'Differential Scanning Calorimetry DSC'

Author: Grafiati

Published: 4 June 2021

Last updated: 25 July 2025

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1

Dranca, Ion, and Tudor Lupascu. "Implications of Global and Local Mobility in Amorphous Excipients as Determined by DSC and TM DSC." Chemistry Journal of Moldova 4, no. 2 (2009): 105–15. http://dx.doi.org/10.19261/cjm.2009.04(2).02.

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The paper explores the use of differential scanning calorimetry (DSC) and temperature modulated differential scanning calorimetry (TM DSC) to study α- and β- processes in amorphous sucrose and trehalose. The real part of the complex heat capacity is evaluated at the frequencies, f, from 5 to 20mHz. β-relaxations were studied by annealing glassy samples at different temperatures and subsequently heating at different rates in a differential scanning calorimeter.

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2

Chagovetz, Alexis A., Colette Quinn, Neil Damarse, Lee D. Hansen, Alexander M. Chagovetz, and Randy L. Jensen. "Differential Scanning Calorimetry of Gliomas." Neurosurgery 73, no. 2 (2013): 289–95. http://dx.doi.org/10.1227/01.neu.0000430296.23799.cd.

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Abstract BACKGROUND: Thermal stability signatures of complex molecular interactions in biological fluids can be measured using differential scanning calorimetry (DSC). Evaluating the thermal stability of plasma proteomes offers a method of producing a disease-specific “signature” (thermogram) in neoplastic and autoimmune diseases. OBJECTIVE: The authors describe the use of DSC with human brain tumor tissue to create unique thermograms for correlation with histological tumor classification. METHODS: Primary brain tumors were classified according to the World Health Organization classification.

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3

Yang, Lu, and Shun Hong Lin. "City Sludge’s Differential Scanning Calorimetry Analysis." Advanced Materials Research 989-994 (July 2014): 2791–95. http://dx.doi.org/10.4028/www.scientific.net/amr.989-994.2791.

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The differential scanning calorimetry is a thermal analysis. Under program controlled temperature, measure and input to the relationship between the the sample and the reference’s power difference and temperature. The curve which the differential scanning calorimetry recorded called DSC curve. DSC curve in the sample’s rate of endothermic or exothermic as ordinate and in temperature or time as abscissa, which can determine a variety of thermodynamic and dynamics parameters, such as specific heat capacity, the reaction heat, thermal changes, phase diagram, reaction rate, rate of crystallization

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Saranov, Igor' Aleksandrovich, Oleg Borisovich Rudakov, Konstantin Konstantinovich Polyansky, Natal'ya Leonidovna Kleymenova, and Aleksey Valer'yevich Vetrov. "DIFFERENTIAL SCANNING CALORIMETRY OF LIQUID VEGETABLE." chemistry of plant raw material, no. 4 (December 21, 2020): 157–64. http://dx.doi.org/10.14258/jcprm.2020047603.

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The thermophysical properties of vegetable oils were studied by differential scanning calorimetry method was used to study the fatty acid composition of vegetable oils liquid at room temperature, such as amaranth (Amaránthus), corn (Zea mays), flax (Línum usitatíssimum), sunflower (Helianthus), rape (Brusss napor), milk thistle (Sílybum mariánum), saffron milk cap (Camelina sativa) and pumpkin (Cucurbita pepo). The temperatures of the endothermic peak maxima and their area on the DSC thermograms of these oils were established as characteristic thermal effects. The interconnection between therm

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5

Liu, Peng, Cai Qin Gu, Qing Zhu Zeng, and Hao Huai Liu. "The Extrapolation Method for Hyper Differential Scanning Calorimetry." Advanced Materials Research 554-556 (July 2012): 1994–98. http://dx.doi.org/10.4028/www.scientific.net/amr.554-556.1994.

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In order to eliminate the temperature lag effect and obtain the accurate temperature results from hyper differential scanning calorimetry (Hyper-DSC) operated at high heating rate, an adjustable method, namely “Extrapolation Method”, had been introduced by us in former papers. And in this paper, we wanted to support the accuracy of this method by other instruments. Specifically, the extrapolated glass transition temperatures (Tg, 61.5 °C) of PLA film, which was obtained by Hyper-DSC, was close to the value detected directly by normal DSC (62.0 °C). And the extrapolated Tg of waxy starch film (

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6

Schick, C. "Differential scanning calorimetry (DSC) of semicrystalline polymers." Analytical and Bioanalytical Chemistry 395, no. 6 (2009): 1589–611. http://dx.doi.org/10.1007/s00216-009-3169-y.

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7

Leyva-Porras, César, Pedro Cruz-Alcantar, Vicente Espinosa-Solís, et al. "Application of Differential Scanning Calorimetry (DSC) and Modulated Differential Scanning Calorimetry (MDSC) in Food and Drug Industries." Polymers 12, no. 1 (2019): 5. http://dx.doi.org/10.3390/polym12010005.

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Phase transition issues in the field of foods and drugs have significantly influenced these industries and consequently attracted the attention of scientists and engineers. The study of thermodynamic parameters such as the glass transition temperature (Tg), melting temperature (Tm), crystallization temperature (Tc), enthalpy (H), and heat capacity (Cp) may provide important information that can be used in the development of new products and improvement of those already in the market. The techniques most commonly employed for characterizing phase transitions are thermogravimetric analysis (TGA)

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8

Fellah, Lahcene, and Zakaria Boumerzoug. "DSC Study of Recrystallization in Wiredrawn Industrial Copper." Advanced Materials Research 997 (August 2014): 646–50. http://dx.doi.org/10.4028/www.scientific.net/amr.997.646.

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The goal of this work is to investigate the recrystallization reaction in cold wiredrawn industrial copper. We have used a differential scanning calorimetry and X-ray Diffraction techniques. The stored and apparent activation energies have been determined by differential scanning calorimetry under isochronal conditions. The differential scanning calorimetry results have been analyzed using models developed by Kissinger, Ozawa, Boswell, and Starink. In addition, the transformed fraction, as a function of temperature, and some kinetic parameters have been determined. We have found that cold wire

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9

Stępień, Piotr, Zbigniew Rusin, and Karol Skowera. "Cement Mortar Porosity by Modified Analysis of Differential Scanning Calorimetry Records." Materials 13, no. 5 (2020): 1080. http://dx.doi.org/10.3390/ma13051080.

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A modified method of interpreting a heat flux differential scanning calorimetry records in pore structure determination is presented. The method consists of determining the true phase transition energy distribution due to the melting of water during a differential scanning calorimetry (DSC) heating run. A set of original apparatus functions was developed to approximate the recorded calorimetric signals to the actual processes of the water phase transition at a given temperature. The validity of the proposed calorimetric curves-based algorithm was demonstrated through tests on a cement mortar s

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10

Gao, Jiawu, Lin Li, Yanping Deng, Zongming Gao, Changhua Xu, and Mingxi Zhang. "Study of gelation using differential scanning calorimetry (DSC)." Journal of thermal analysis 49, no. 1 (1997): 303–10. http://dx.doi.org/10.1007/bf01987451.

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11

Saranov, I. A., O. B. Rudakov, and K. K. Polansky. "Differential scanning calorimetry of cocoa butter and chocolate glaze." Proceedings of the Voronezh State University of Engineering Technologies 82, no. 2 (2020): 154–60. http://dx.doi.org/10.20914/2310-1202-2020-2-154-160.

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Nowadays there is a wide market for cocoa butter equivalents, substitutes and improvers for the confectionery and dairy industries. An urgent task is the development of operational instrumental methods for cocoa butter and its substitutes quality control. Thermophysical parameters are among the most important characteristics of the fat phase for the food technology. Differential scanning calorimetry (DSC) is becoming one of the most promising methods for analytical control of fat and oil products. Thermophysical data (temperatures of the maximums of endothermic peaks and their areas) for cocoa

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12

Nedelcu, Dumitru, Nicoleta Monica Lohan, Constantin Carausu, and Octavian Pruteanu. "Some Considerations Concerning the Differential Scanning Calorimetry of Ultra Tough Plastic Materials." Applied Mechanics and Materials 659 (October 2014): 107–11. http://dx.doi.org/10.4028/www.scientific.net/amm.659.107.

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The Differential Scanning Calorimetry (DSC) it’s an important analysis in research since the 20thcentury, being used is various fields such as: physics, chemistry, science and materials technology. Its applicability has also extended to other fields, such as nanothermodynamics and bio-thermodynamics. Calorimetry measures the amount of heat absorbed/dissipated by a test sample as compared to a reference value, when the test sample is subjected to a heating and/or cooling cycle. The calorimetric effect may be revealed by the temperature-and/or time-dependent heat flow variation, and its evaluati

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13

Osten, Julia, Benjamin Milkereit, Michael Reich, et al. "Development of Precipitation Hardening Parameters for High Strength Alloy AA 7068." Materials 13, no. 4 (2020): 918. http://dx.doi.org/10.3390/ma13040918.

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The mechanical properties after age hardening heat treatment and the kinetics of related phase transformations of high strength AlZnMgCu alloy AA 7068 were investigated. The experimental work includes differential scanning calorimetry (DSC), differential fast scanning calorimetry (DFSC), sophisticated differential dilatometry (DIL), scanning electron microscopy (SEM), as well as hardness and tensile tests. For the kinetic analysis of quench induced precipitation by dilatometry new metrological methods and evaluation procedures were established. Using DSC, dissolution behaviour during heating t

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14

Yatagai, Mamiko, Motoko Komaki, and Toshimasa Hashimoto. "Applying Differential Scanning Calorimetry to Detergency Studies of Oily Soil." Textile Research Journal 62, no. 2 (1992): 101–4. http://dx.doi.org/10.1177/004051759206200207.

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Differential scanning calorimetry (DSC) has been applied to studies of oily soil removal from fibrous materials. Fabric and filter paper were soiled with various oily substances present in sebum. After washing, the fibrous samples were subjected to DSC measurements. The residual oily soils on the samples were analyzed by the melting peak areas of the DSC heating curves, a method that is widely applicable to various oily substances with different melting points and polymorphic forms. Various woven or nonwoven fibrous samples can be scanned, regardless of sample size in washing experiments.

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15

Lee, Jaesung, and Gönül Kaletunç. "Evaluation of the Heat Inactivation of Escherichia coli and Lactobacillus plantarum by Differential Scanning Calorimetry." Applied and Environmental Microbiology 68, no. 11 (2002): 5379–86. http://dx.doi.org/10.1128/aem.68.11.5379-5386.2002.

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ABSTRACT Differential scanning calorimetry (DSC) is used to evaluate the thermal stability and reversibility after heat treatment of transitions associated with various cellular components of Escherichia coli and Lactobacillus plantarum. The reversibility and the change in the thermal stability of individual transitions are evaluated by a second temperature scan after preheating in the DSC to various temperatures between 40 and 130°C. The viability of bacteria after a heat treatment between 55 and 70°C in the DSC is determined by both plate count and calorimetric data. The fractional viability

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16

Fatahi, Hazhir, Jérôme Claverie, and Sébastien Poncet. "Thermal Characterization of Phase Change Materials by Differential Scanning Calorimetry: A Review." Applied Sciences 12, no. 23 (2022): 12019. http://dx.doi.org/10.3390/app122312019.

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The use of phase change materials (PCMs) in thermal energy storage (TES) applications as a system that can fill the gap between the energy supply and demand has sharply increased over recent years. Due to the dependence of the storage capacity in a TES on the transition (mostly solid/liquid) of PCMs, knowing the thermal properties of PCMs is of high importance. Calorimetric methods have an inevitable role in PCMs’ characterization methods. The most important properties of PCMs that lead us to integrate them in a specific application can be determined by the calorimetric method. These propertie

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17

เติมเกาะ, กรองทิพย์, กิตติยา ปลื้มใจ, วรพงษ์ เจนธนกิจ та กรองกาญจน์ ศิรินุกุลวัฒนา. "อิทธิพลของสารเจือทังสเตนที่มีผลต่อสมบัติทางโครงสร้างและเทอร์โมโครมิกของวาเนเดียมไดออกไซด์ที่สังเคราะห์ด้วยวิธีไฮโดรเทอร์มอล". วารสารวิทยาศาสตร์ประยุกต์ กรมวิทยาศาสตร์บริการ 8, № 8 (2022): 106–14. http://dx.doi.org/10.60136/bas.v8.2019.270.

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งานวิจัยนี้มีวัตถุประสงค์เพื่อศึกษาอิทธิพลของการเจือโดยโมลทังสเตน (W) ที่มีผลต่อสมบัติทางความร้อนและรูปร่างโครงสร้างของวาเนเดียมไดออกไซด์ (VO2) โดยใช้สารตั้งต้นวาเนเดียมเพนทอกไซด์ (V2O5) และกรดออกซาลิก (H2C2O4) เป็นตัวรีดิวซ์ด้วยอัตราส่วนโมเลกุล 1:3 เตรียมจากกระบวนการไฮโดรเทอร์มอลที่อุณหภูมิ 260 °C และเจือทังสเตนปริมาณที่แตกต่างกันเพื่อลดอุณหภูมิทรานซิชัน หลังจากนั้นนำไปเผาที่อุณหภูมิสูง สาร VO2 และสารที่เจือทังสเตนที่สังเคราะห์ได้ถูกนำมาวิเคราะห์ด้วยเทคนิค differential scanning calorimetry (DSC), X-ray diffraction (XRD), and scanning electron microscope (SEM) ผลจากเทคนิค DSC แสดงให้เห็นว่าการ

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18

Burmester, A. "Investigation of Paint Media by Differential Scanning Calorimetry (DSC)." Studies in Conservation 37, no. 2 (1992): 73. http://dx.doi.org/10.2307/1506399.

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19

Yatagai, Mamiko, Motoko Komaki, Toshinari Nakajima, and Toshimasa Hashimoto. "Analysis of detergency process by differential scanning calorimetry (DSC)." Sen'i Gakkaishi 45, no. 3 (1989): 102–6. http://dx.doi.org/10.2115/fiber.45.102.

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20

Burmester, A. "Investigation of paint media by differential scanning calorimetry (dsc)." Studies in Conservation 37, no. 2 (1992): 73–81. http://dx.doi.org/10.1179/sic.1992.37.2.73.

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21

Harvey, Jean-Philippe, Nooshin Saadatkhah, Guillaume Dumont-Vandewinkel, Sarah L. G. Ackermann, and Gregory S. Patience. "Experimental methods in chemical engineering: Differential scanning calorimetry-DSC." Canadian Journal of Chemical Engineering 96, no. 12 (2018): 2518–25. http://dx.doi.org/10.1002/cjce.23346.

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22

Shamilova, Maltam, and Sevinj Hajiyeva. "Analysis of DSC (differential scanning calorimetry) thermograms of milk fat." Technology audit and production reserves 5, no. 3(61) (2021): 36–39. http://dx.doi.org/10.15587/2706-5448.2021.242804.

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The object of current research is the oxidation and melting properties of milk fat samples in different heating rates. One of the most problematic issues is the evaluation dependence of temperature and oxidation time regarding to heat flow, and the estimation of attitude of enthalpy values to heating rates. In order to gain a comprehensive assessment of oxidation and melting properties of milk fat samples on differential scanning calorimeter in various heating rates, it is necessary to conduct experimental studies. The analysis was performed using the dynamic option of the differential scannin

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23

Chen, Yong Kang, Ming Hua Chen, Tao Zhang, and Xiao Le Wu. "The Application of Differential Scanning Calorimetry to Thermal Analysis for Energetic Materials." Applied Mechanics and Materials 423-426 (September 2013): 588–92. http://dx.doi.org/10.4028/www.scientific.net/amm.423-426.588.

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Differential Scanning Calorimetry (DSC) is a common and useful method for thermal analysis. This paper briefly introduces the thermal decomposition characteristic determination of the main components of propellant by DSC assay and the applications of DSC in thermal stability and compatibility evaluation research of energetic materials.

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Caren, V. Ouverney*1 Jo Dweck2 &. Margarida L. Castelló3. "HOW TO OBTAIN RELIABLE LOWER HEATING VALUES FROM DTA AND DSC ANALYSIS DATA." GLOBAL JOURNAL OF ADVANCED ENGINEERING TECHNOLOGIES AND SCIENCES 7, no. 8 (2020): 1–10. https://doi.org/10.5281/zenodo.3986553.

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The standard method widely used to determinate correctly higher heating values (HHV) is bomb calorimetry. However, a bomb calorimeter is not always available for the analysis, doing the heating value determination a little more limited. On the other hand, some thermal analysis techniques can be part of the solution for this problem as it is possible to estimate heating values from their analysis data. The most used and reliable techniques for this purpose are Differential Scanning Calorimetry (DSC) and Differential Thermal Analysis (DTA), but the heating values obtained from their data cannot

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25

Harju, Mauno E. E. "Solid-State Transition Mechanisms of Ammonium Nitrate Phases IV, III, and II Investigated by Simultaneous Raman Spectrometry and Differential Scanning Calorimetry." Applied Spectroscopy 47, no. 11 (1993): 1926–30. http://dx.doi.org/10.1366/0003702934066127.

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The solid-state transition mechanisms of ammonium nitrate IV, III, and II were studied by measuring samples simultaneously by Raman spectrometry and differential scanning calorimetry (DSC). The Raman instruments were a Fourier transform Raman spectrophotometer and triple monochromator Raman spectrophotometer with charge-coupled-device (CCD) detector. The spectral data of the transitions were collected simultaneously with the calorimetric data in the temperature-scanning mode of the calorimeter and then isothermally between transitions. The phase transition from phase IV to phase III occurred t

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26

Maltam, Shamilova, and Hajiyeva Sevinj. "Analysis of DSC (differential scanning calorimetry) thermograms of milk fat." Technology Audit and Production Reserves 5, no. 3(61) (2021): 36–39. https://doi.org/10.15587/2706-5448.2021.242804.

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<em>The object of current research is </em><em>the oxidation and melting properties of milk fat samples in different heating rates</em><em>. One of the most problematic issues is the evaluation dependence of temperature and oxidation time regarding to heat flow, and the estimation of attitude of enthalpy values to heating rates. In order to gain a comprehensive assessment of </em><em>oxidation and melting properties of milk fat samples on </em><em>differential scanning calorimeter in various heating rates, it is necessary to conduct experimental studies.</em> <em>The analysis wa

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27

Romanowska, Jolanta. "Calorimetric study on Bi-Cu-Sn alloys." High Temperature Materials and Processes 38, no. 2019 (2019): 541–46. http://dx.doi.org/10.1515/htmp-2019-0052.

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AbstractThe paper presents results of calorimetric investigation of the Bi-Cu-Sn system by means of differential scanning calorimetry (DSC) at the temperature interval 25-1250∘C, Values of liquidus, solidus and invariant reactions temperatures, as well as melting enthalpies of the selected alloys were determined. Microstructure investigation of the alloys were performed by the use of a scanning electron microscope (SEM) equipped with an energy-dispersive spectrometer (EDS).

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Zhang, Ru Guo, Hong Zhang, Zheng Zhang, Hua Zheng, Ying Feng, and Wen Wen Zhang. "Characterization of Five Natural Resins and Waxes by Differential Scanning Calorimetry (DSC)." Advanced Materials Research 418-420 (December 2011): 643–50. http://dx.doi.org/10.4028/www.scientific.net/amr.418-420.643.

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Thermal properties of 5 natural resin and wax samples (shellac, rosin, shellac wax, beeswax, Chinese insect wax) were examined by differential scanning calorimetry (DSC). The DSC melting and crystallization curves of the samples were presented in this paper. Three DSC parameters, To, Tf and ΔT (difference between To and Tf), were selected from each curve. Evaluation results of the parameters showed that they were statistically significant with individual excellent reproducibility. Information was provided by evaluation of changes among thermal absorption or release peaks of the curves in diffe

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Gao, Nong. "Applications of Differential Scanning Calorimetry on Materials Subjected by Severe Plastic Deformation." Materials Science Forum 584-586 (June 2008): 255–60. http://dx.doi.org/10.4028/www.scientific.net/msf.584-586.255.

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Differential Scanning Calorimetry (DSC) is a thermal analysis technique that measures the energy absorbed or released by a sample as a function of temperature or time. DSC has wide application for analysis of solid state reactions and solid-liquid reactions in many different materials. In recent years, DSC has been applied to analyze materials and alloys processed through Severe Plastic Deformation (SPD). The basic principle of SPD processing is that a very high strain is introduced into materials which achieve significant grain refinement and improve properties of materials. This review paper

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Nassu, Renata Tieko, and Lireny Aparecida Guaraldo Gonçalves. "Determination of melting point of vegetable oils and fats by differential scanning calorimetry (DSC) technique." Grasas y Aceites 50, no. 1 (1999): 16–21. http://dx.doi.org/10.3989/gya.1999.v50.i1.630.

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Mezbahul-Islam, Mohammad, Elhachmi Essadiqi, and Mamoun Medraj. "A Differential Scanning Calorimetric Study of the Mg-Cu-Y System." Materials Science Forum 706-709 (January 2012): 1215–20. http://dx.doi.org/10.4028/www.scientific.net/msf.706-709.1215.

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The Mg-Cu-Y system has been experimentally investigated using differential scanning calorimetry (DSC). Vertical sections and phase assemblage diagrams are calculated using thermodynamic modeling. Solidification behavior of the key alloys was discussed in light of the thermodynamic calculation. Melting temperatures of two of the ternary compounds; Mg18CuY and Mg4CuY, are predicted using the modified thermodynamic database of this system. Key words: Mg alloys, Bulk metallic glass, Differential scanning calorimetry, Thermodynamic modeling.

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Lv, Jia Yu, Shuiai Wei, Wang Hua Chen, Gu Feng Chen, Li Ping Chen, and Ying Tao Tian. "Thermal Kinetic Analysis of Tert-butyl Peroxybenzoate under Dynamic and Adiabatic Conditions." Advanced Materials Research 550-553 (July 2012): 2782–85. http://dx.doi.org/10.4028/www.scientific.net/amr.550-553.2782.

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This study demonstrates the thermal actions of tert-butyl peroxybenzoate (TBPB) which is widely used in the plastic and rubber industries. The thermodynamic and kinetic analysis were performed on the basis of dynamic and adiabatic calorimetric applications which had been accepted as good assistants for investigating materials’ thermal decomposition. In essence, TBPB is reactive and exothermically unstable. Differential scanning calorimetry (DSC) and accelerating rate calorimeter (ARC) were employed to supply basic data and safety index. Experiments were taken under different scanning rates as

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Zhao, Zi Nian, and Xiao Li Lei. "Research in Non-Isothermal Crystallization Kinetics of LDPE Composite Films." Advanced Materials Research 848 (November 2013): 46–49. http://dx.doi.org/10.4028/www.scientific.net/amr.848.46.

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By means of melt blending process in a co-rotating twin screw extruder and blow molding , the low density polyethylene (LDPE)/thermoplastic elastomer(TPE) mixed membranes and LDPE/inorganic particles composite membrane were prepared. by differential scanning calorimetry(DSC) to study the non-isothermal crystallization kinetics of the LDPE composite system by differential scanning calorimetry (DSC).Use modified Jeziorny method to process the data ,the results shows that ZMS, SiO2, EVA and EMAA all play a role of heterogeneous nucleation and the crystallization rate of LDPE has been increased,es

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Drogoń, Agata, Marcin Skotnicki, Agnieszka Skotnicka, and Marek Pyda. "Physical Ageing of Amorphous Indapamide Characterised by Differential Scanning Calorimetry." Pharmaceutics 12, no. 9 (2020): 800. http://dx.doi.org/10.3390/pharmaceutics12090800.

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The objective of this study was to characterise amorphous indapamide (IND) subjected to the physical ageing process by differential scanning calorimetry (DSC). The amorphous indapamide was annealed at different temperatures below the glass transition, i.e., 35, 40, 45, 65, 75 and 85 °C for different lengths of time, from 30 min up to a maximum of 32 h. DSC was used to characterise both the crystalline and the freshly prepared glass and to monitor the extent of relaxation at temperatures below the glass transition (Tg). No ageing occurred at 35, 40 and 45 °C at the measured lengths of times. Mo

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Bibi, S., D. H. Bremner, M. Macdougall-Heasman, et al. "A preliminary investigation to group disparate batches of licit and illicit diazepam tablets using differential scanning calorimetry." Analytical Methods 7, no. 20 (2015): 8597–604. http://dx.doi.org/10.1039/c5ay01711d.

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36

Johnson, Nathan Brenner, Bhuvsmita Bhargava, Alex Martin Bates, et al. "Identifying Variability across Institutions in Differential Scanning Calorimetry for Materials Level Battery Safety." ECS Meeting Abstracts MA2024-02, no. 1 (2024): 66. https://doi.org/10.1149/ma2024-02166mtgabs.

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With the growing concern over Li-ion battery safety, particularly with cells that utilize lithium metal anodes, differential scanning calorimetry (DSC) has emerged as a promising technique for the safety analysis of prospective chemistries on a materials scale. DSC is generally used for single materials, single cell layers, and combinations of layers to assess the thermal stability of battery materials as well as the interactions between materials. Despite the common use of DSC in the literature, there is no standardization for sample preparation or reporting requirements to ensure cross-insti

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Sopko, Martin, František Kováč, Ivan Petryshynets, Mária Molnárová, and Petra Gavendová. "Differential Scanning Calorimetry and Metallographic Analysis of Fe-Si Electrical Steel." Materials Science Forum 782 (April 2014): 129–32. http://dx.doi.org/10.4028/www.scientific.net/msf.782.129.

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The microstructure development in cold rolled electrical steel under dynamic heat treatments was subjected to investigation. Significantly distinguish types of microstructures were obtained in the investigated steels confirming the different character of grain boundary motion. Application of annealing temperature within two phase region (austenite+ferrite) leads to abnormal grain growth in silicon steels. Moreover, in the optimum temperature range, there was a particular temperature leading to the most optimal microstructure and texture[1]. The effect of Si content on the phase transition temp

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Kuril, Akhilesh Kumar. "Differential Scanning Calorimetry: A Powerful and Versatile Tool for Analyzing Proteins and Peptides." Journal of Pharmaceutical Research International 36, no. 7 (2024): 179–87. http://dx.doi.org/10.9734/jpri/2024/v36i77549.

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Differential Scanning Calorimetry (DSC) is an efficient and versatile analytical technique widely used to study the thermal properties and stability of proteins. This review article provides a comprehensive overview of the principles and applications of DSC in protein research. DSC measures the heat flow associated with temperature-induced conformational changes in proteins, allowing for the direct determination of key thermodynamic parameters such as melting temperature (Tm), enthalpy change (ΔH), and heat capacity change (ΔCp). These parameters provide valuable insights into protein and pept

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Masberg, S., C. Ernst, G. M. Schneider, A. Würflinger, and R. Dąbrowski. "Differential Scanning Calorimetry (DSC) under High Pressure on 10-TPEB." Zeitschrift für Naturforschung A 54, no. 5 (1999): 287–90. http://dx.doi.org/10.1515/zna-1999-0503.

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Abstract The phase behaviour of a new liquid crystal, belonging to the series l-[4-n-alkyl-biphenyl]-2-[4-isothio-cyanato-phenyl]ethane (nTPEB), n = 10, has been investigated with differential scanning calorimetry at ambient and high pressure. The phase behaviour depends on the thermal treatment. Phase transition temperatures have been determined as a function of pressure up to 300 MPa. No pressure-induced or pressure-limited phases are observed in this pressure range. Enthalpy-and volume-changes accompanying the phase transitions have been calculated using the Clausius-Clapeyron equation.

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Rahman, M. Shafiur. "State Diagram of Date Flesh Using Differential Scanning Calorimetry (DSC)." International Journal of Food Properties 7, no. 3 (2004): 407–28. http://dx.doi.org/10.1081/jfp-200032930.

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Battezzati, L., F. Demichelis, C. F. Pirri, and E. Tresso. "Differential scanning calorimetry (DSC) studies of hydrogenated amorphous semiconductor alloys." Physica B: Condensed Matter 176, no. 1-2 (1992): 73–77. http://dx.doi.org/10.1016/0921-4526(92)90599-n.

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Schuch, A., K. Köhler, and H. P. Schuchmann. "Differential scanning calorimetry (DSC) in multiple W/O/W emulsions." Journal of Thermal Analysis and Calorimetry 111, no. 3 (2012): 1881–90. http://dx.doi.org/10.1007/s10973-012-2751-2.

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Bĕhálek, Luboš. "Differential Scanning Calorimetry as a Tool for Quality Testing of Plastics." Key Engineering Materials 669 (October 2015): 485–93. http://dx.doi.org/10.4028/www.scientific.net/kem.669.485.

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Differential scanning calorimetry (DSC) is the most frequently used method from thermal analysis to characterize plastics and which can be applied not only in the R&D but also in the industrial praxis as input and output control. This paper deals with the most important DSC application which arises from results of applied and contractual research at Technical university of Liberec. In the paper are introduced examples of its utilization for plastics identification and characterization, for analysis influence of plastics processing process parameters on their quality, to describe crystalliz

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Almoselhy, Rania I. M. "Applications of Differential Scanning Calorimetry (DSC) in Oils and Fats Research. A Review." American Research Journal of Agriculture 6, no. 1 (2020): 1–9. http://dx.doi.org/10.21694/2378-9018.20002.

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This review is designed to be a comprehensive review in a new way to help you to understand the principle and theory of Thermal Analysis with special emphasis on Differential Scanning Calorimetry (DSC) as a new fast-growing and important technique used for authentication, characterization and detecting adulterations of oils and fats. DSC is a powerful instrument that measures the energy absorbed or released as a function of time or a controlled temperature profile. The sensor of the DSC is the heat flux plate which is designed to give superior performance and rugged reliability. The heat flux

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MENG, F., S. SCHRICKER, W. BRANTLEY, et al. "Differential scanning calorimetry (DSC) and temperature-modulated DSC study of three mouthguard materials☆." Dental Materials 23, no. 12 (2007): 1492–99. http://dx.doi.org/10.1016/j.dental.2007.01.006.

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Fröck, Hannes, Michael Reich, Benjamin Milkereit, and Olaf Kessler. "Scanning Rate Extension of Conventional DSCs through Indirect Measurements." Materials 12, no. 7 (2019): 1085. http://dx.doi.org/10.3390/ma12071085.

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In this work, a method is presented which allows the determination of calorimetric information, and thus, information about the precipitation and dissolution behavior of aluminum alloys during heating rates that could not be previously measured. Differential scanning calorimetry (DSC) is an established method for in-situ recording of dissolution and precipitation reactions in various aluminum alloys. Diverse types of DSC devices are suitable for different ranges of scanning rates. A combination of the various available commercial devices enables heating and cooling rates from 10−4 to 5 Ks−1 to

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Delsante, Simona, Gabriella Borzone, Rada Novakovic, et al. "Synthesis and thermodynamics of Ag–Cu nanoparticles." Physical Chemistry Chemical Physics 17, no. 42 (2015): 28387–93. http://dx.doi.org/10.1039/c5cp02058a.

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Lu, Li, Liao Xia, Hao Zengheng, Sheng Xingyue, Zhang Yi, and Liu Pan. "Investigation on cure kinetics of epoxy resin containing carbon nanotubes modified with hyper-branched polyester." RSC Advances 8, no. 52 (2018): 29830–39. http://dx.doi.org/10.1039/c8ra04525a.

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GHEORGHE, Daniela, Ana NEACSU, Ancuta Mihaela SOFRONIA, and Stefan PERISANU. "Thermodynamic properties of some monoterpenes with pharmacological applications." Revue Roumaine de Chimie 67, no. 10-12 (2023): 549–58. http://dx.doi.org/10.33224/rrch.2022.67.10-12.04.

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"Solid-state thymol, liquid carvacrol and eugenol were characterized by using combustion calorimetry and thermal analysis-simultaneous thermogravimetry (TG) coupled with differential scanning calorimetry (DSC) techniques. The enthalpies of formation were calculated using the measured heat of combustion for the studied compounds. Our values were compared with the literature and calculated data. Information about the stability of the samples was reported. From DSC measurements, the temperatures of melting-decomposition and their corresponding enthalpies were calculated. "

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Nayan, Niraj, S. V. S. Narayana Murty, S. C. Sharma, K. Sreekumar, and Parameshwar Prasad Sinha. "Optimization of Homogenization Parameters of Al-Cu-Li Alloy Cast Ingots Using Calorimetry and Metallographic Techniques." Materials Science Forum 710 (January 2012): 557–62. http://dx.doi.org/10.4028/www.scientific.net/msf.710.557.

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In the present study, thermal treatments for homogenizing cast structures of Al-Cu-Li alloy AA2195 for improved workability are developed chiefly by empirical methods and detailed Differential Scanning Calorimetry (DSC) and microstructural characterization. DSC has been carried out on as-cast samples to establish the homogenization temperatures and avoid incipient melting. Homogenization time has been calculated empirically and microstructural characterization and DSC has been carriedout to after each cycle to validate the empirically established homogenization cycle. Homogenization cycle (435

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