Academic literature on the topic 'Dry-column flash chromatography'

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Journal articles on the topic "Dry-column flash chromatography"

1

Shusterman, Alan J., Patrick G. McDougal, and Arthur Glasfeld. "Dry-Column Flash Chromatography." Journal of Chemical Education 74, no. 10 (1997): 1222. http://dx.doi.org/10.1021/ed074p1222.

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Cvetković, Mirjana, Ana Damjanović, Tatjana P. Stanojković, et al. "Integration of dry-column flash chromatography with NMR and FTIR metabolomics to reveal cytotoxic metabolites from Amphoricarpos autariatus." Talanta 206, Jan 1 (2020): 120248. https://doi.org/10.1016/j.talanta.2019.120248.

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Metabolomics generate a profile of small molecules from plant extracts, which could be directly responsible for bioactivity effects. Using dry-column flash chromatography enabled a rapid and inexpensive method for the very efficient separation of plant extract with a high resolution. This separation method coupled to NMR and FTIR-based metabolomics is applied to identify bioactive natural products. OPLS multivariate analysis method, was used for correlation the chemical composition of the plant extracts, Amphoricarpos autariatus, with the results of cytotoxic activity against Human cervical ad
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Cvetković, Mirjana, Ana Damjanović, Tatjana P. Stanojković, et al. "Integration of dry-column flash chromatography with NMR and FTIR metabolomics to reveal cytotoxic metabolites from Amphoricarpos autariatus." Talanta 206 (January 2020): 120248. http://dx.doi.org/10.1016/j.talanta.2019.120248.

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de Avellar, Isa G. J., Taís A. P. G. Cotta, and Amarílis de V. Finageiv Neder. "Using Artificial Soil and Dry-Column Flash Chromatography To Simulate Organic Substance Leaching Process: A Colorful Environmental Chemistry Experiment." Journal of Chemical Education 89, no. 2 (2011): 248–53. http://dx.doi.org/10.1021/ed100728j.

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Santos-Rebelo, Ana, Catarina Garcia, Carla Eleutério, et al. "Development of Parvifloron D-loaded Smart Nanoparticles to Target Pancreatic Cancer." Pharmaceutics 10, no. 4 (2018): 216. http://dx.doi.org/10.3390/pharmaceutics10040216.

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Pancreatic cancer is the eighth leading cause of cancer death worldwide. For this reason, the development of more effective therapies is a major concern for the scientific community. Accordingly, plants belonging to Plectranthus genus and their isolated compounds, such as Parvifloron D, were found to have cytotoxic and antiproliferative activities. However, Parvifloron D is a very low water-soluble compound. Thus, nanotechnology can be a promising delivery system to enhance drug solubility and targeted delivery. The extraction of Parvifloron D from P. ecklonii was optimized through an acetone
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Mekarunothai, Amita, Markus Bacher, Raveevatoo Buathong та ін. "β-sitosterol isolated from the leaves of Trema orientalis (Cannabaceae) promotes viability and proliferation of BF-2 cells". PeerJ 12 (23 січня 2024): e16774. http://dx.doi.org/10.7717/peerj.16774.

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Trema orientalis is a pioneer species in the cannabis family (Cannabaceae) that is widely distributed in Thai community forests and forest edges. The mature leaves are predominantly used as an anti-parasite treatment and feed for local freshwater fish, inspiring investigation of their phytochemical composition and bioactivity. The purpose of this work was to investigate the bioactive compounds in T. orientalis leaf extract and their cytotoxicity in the BF-2 fish cell line (ATCC CCL-91). Flash column chromatography was used to produce 25 mL fractions with a mixture solvent system comprised of h
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Fatharani, Deika Zhillan, Safri Ishmayana, Reginawanti Hindersyah, and Ukun M. S. Soedjanaatmadja. "Isolation and Characterization of Gibberellin (GA-3) from Banana Blossom of Musa balbisiana Colla and Effect of The Isolate Addition on The Growth of Soybean (Glycine max) Plant." Research Journal of Chemistry and Environment 26, no. 11 (2022): 28–37. http://dx.doi.org/10.25303/2611rjce28037.

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There is a type of banana that is unique because the flesh is filled with black seeds locally known as “pisang batu” (Musa balbisiana Colla). The objective of research was directed to determine the content of GA3 in banana blossom of M. balbisiana Colla and its effect on the growth of soybean (Glycine max) plant in vegetative and generative phase. GA3 was prepared by maceration followed by extraction using ethyl acetate and further purified using adsorption column chromatography and preparative TLC. The isolated product was then characterized using FTIR and HPLC. Sprouts of soybeans with unifo
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Shankar Lankalapalli, Ravi, Ambili Sasikumar Athira, Ramkumar Kiruthika, et al. "NMR-based phytochemical profiling of palmyra palm syrup infused with dry ginger, black pepper, and long pepper." Current Nutraceuticals 04 (January 12, 2023). http://dx.doi.org/10.2174/2665978604666230112144757.

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Background: Trikatu, a vital ingredient in many Indian Ayurvedic drugs, is a consortium of three spices, viz. dry ginger, black pepper, and long pepper, known for its peculiar pungency. To convert Trikatu into a widely acceptable palatable form, we blended these three spices in a decoction form and added them to syrup prepared from palmyra palm neera, which resulted in ‘Trikatu Syrup’ (TS). Recently, we reported in vivo immunomodulatory properties of TS [1]. Introduction: The immunomodulatory effects of spices are attributed largely to the presence of certain phytochemicals. The importance of
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sprotocols. "Copolymerization preparation of cationic cyclodextrin chiral stationary phases for drug enantioseparation in chromatography." January 10, 2015. https://doi.org/10.5281/zenodo.13871.

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Authors: Ren-Qi Wang, Teng-Teng Ong, Ke Huang, Weihua Tang & Siu-Choon Ng ### Abstract We described a facile and effective protocol wherein radical copolymerization is employed to covalently bond cationic β-cyclodextrin (β-CD) onto silica particles with extended linkage, resulting in a chiral stationary phase (IMPCSP) that can be used for the enantioseparation of racemic drugs in both high-performance liquid chromatography (HPLC) and supercritical fluid chromatography (SFC). Starting from commercially available chemicals, the IMPCSP is prepared in several steps: (i) reaction of β-CD with 1
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sprotocols. "Synthesis of nNOS-Capon interaction inhibitors: ZLc-002 and its derivatives." December 31, 2014. https://doi.org/10.5281/zenodo.13641.

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Authors: Ting-You Li, Lei Chang, Yu Ma & Dong-Ya Zhu ### Abstract nNOS-Capon interaction is involved in anxiety disorder, disrupting the nNOS-Capon interaction has been demonstrated to show anxiolytic-like effect. In this protocol, N-(2-carbomethoxyacetyl)-D-valine methyl ester, a nNOS-Capon interaction inhibitor, we named it ZLc-002, was prepared by condensation of D-valine methyl ester hydrochloride with methyl malonyl chloride. The synthesis of some analogues of ZLc-002 was also described. ### Introduction Anxiety disorders are highly prevalent psychiatric diseases (1). Selective seroto
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