Relevant bibliographies by topics / DSC raman spectroscopy

Contents

  1. Journal articles
  2. Dissertations / Theses
  3. Book chapters
  4. Conference papers

Academic literature on the topic 'DSC raman spectroscopy'

Author: Grafiati
Published: 4 June 2025
Last updated: 1 August 2025

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Journal articles on the topic "DSC raman spectroscopy"

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Atef, Eman, Harsh Chauhan, Dev Prasad, Dunesh Kumari, and Charles Pidgeon. "Quantifying Solid-State Mixtures of Crystalline Indomethacin by Raman Spectroscopy Comparison with Thermal Analysis." ISRN Chromatography 2012 (February 6, 2012): 1–6. http://dx.doi.org/10.5402/2012/892806.

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This paper investigates Raman spectroscopy as a quick and reliable method to quantify the alpha (α) and gamma (γ) polymorphic forms of indomethacin compared to differential scanning calorimetry (DSC). Binary mixtures with different ratios of α and γ indomethacin were prepared and analyzed by Raman and DSC. The Raman method was found to be more reliable and superior compared to DSC. The partial conversion of the alpha to gamma polymorphic form during the DSC measurement was the major limitation for the use of full DSC as a quantitative method and resulted in difference between the calculated an
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T., B. Sundaresan. "Solid State Mixture Identification of Crystal Indomethacin by Spectroscopy Comparison with Thermal Analysis." International Journal of Trend in Scientific Research and Development 2, no. 6 (2018): 626–30. https://doi.org/10.31142/ijtsrd18583.

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This research investigates Raman spectroscopy as a quick and reliable method to quantify the alpha a and gamma polymorphic forms of indomethacin compared to differential scanning calorimetry DSC . Binary mixtures with different ratios of a and indomethacin were prepared and analyzed by Raman and DSC. The Raman method was found to be more reliable and superior compared to DSC. The partial conversion of the alpha to gamma polymorphic form during the DSC measurement was the major limitation for the use of full DSC as a quantitative method and resulted in difference between the calculated and meas
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Muresan-Pop, Marieta, Irina Kacsó, Xenia Filip, et al. "Spectroscopic and physical–chemical characterization of ambazone–glutamate salt." Spectroscopy 26, no. 2 (2011): 115–28. http://dx.doi.org/10.1155/2011/414103.

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Ambazone monohydrate C8H11N7S · H2O (AMB), a well-known antimicrobial compound, was used together with Glutamic Acid C5H9NO4(Glu) to obtain a new solid form using the solvent-drop grinding procedure. The screening of the new solid form was best achieved by the combined use of X-ray Powder Diffraction (XRPD) and several spectroscopic techniques (Fourier Transformed Infrared Spectroscopy (FTIR), X-ray Photoelectron Spectroscopy (XPS), Raman and13C-NMR spectroscopy) together with Differential Scanning Calorimetry (DSC), Differential thermal analysis and thermogravimetry (DTA–TGA). The combination
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Harju, Mauno E. E. "Solid-State Transition Mechanisms of Ammonium Nitrate Phases IV, III, and II Investigated by Simultaneous Raman Spectrometry and Differential Scanning Calorimetry." Applied Spectroscopy 47, no. 11 (1993): 1926–30. http://dx.doi.org/10.1366/0003702934066127.

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The solid-state transition mechanisms of ammonium nitrate IV, III, and II were studied by measuring samples simultaneously by Raman spectrometry and differential scanning calorimetry (DSC). The Raman instruments were a Fourier transform Raman spectrophotometer and triple monochromator Raman spectrophotometer with charge-coupled-device (CCD) detector. The spectral data of the transitions were collected simultaneously with the calorimetric data in the temperature-scanning mode of the calorimeter and then isothermally between transitions. The phase transition from phase IV to phase III occurred t
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Gotts, H. "Characterization of Process Induced Contamination and Residues on Semiconductor Components Via FTIR and Raman Microanalysis." Microscopy and Microanalysis 7, S2 (2001): 152–53. http://dx.doi.org/10.1017/s1431927600026830.

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FTIR and Raman microanalysis may be used as a powerful combination to determine the identity, and hence infer the source, of contaminant particles which diminish yields of semiconductor components and devices. The complimentarity of these techniques arises from the underlying spectroscopic selection rules.Vibrational spectroscopic techniques are commonly used to characterize the molecular structure of bulk organic materials. These bulk materials typically represent purified fractions of components which may be further investigated with various classical instrumental techniques such as Differen
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Sagitova, E. A., P. Donfack, K. A. Prokhorov, et al. "Sensitive temperature-dependent phase resolution of polyethylene-clay nanocomposites." Laser Physics 32, no. 8 (2022): 084009. http://dx.doi.org/10.1088/1555-6611/ac7334.

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Abstract With the help of spectroscopic and differential scanning calorimetry (DSC) techniques, we have studied conformational and phase reorganizations as function of temperature in intercalated polymer-clay nanocomposites based on low-, middle-, and high-density polyethylene (PE) matrices. We show that Raman spectroscopy is sensitive to structural changes appearing during heating at much lower temperatures (about 47 °C) in comparison to DSC measurements. In fact, in the melting region where DSC traces show endotherms, Raman spectra reveal dramatic changes in the phase and conformational comp
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Shiota, K., Y. Izato, and A. Miyake. "Analysis of guanylurea dinitramide pyrolysis using DSC/Raman spectroscopy." Journal of Analytical and Applied Pyrolysis 156 (June 2021): 105113. http://dx.doi.org/10.1016/j.jaap.2021.105113.

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Adichtchev, Sergey V., Konstantin A. Okotrub, Alexey M. Pugachev, Irina V. Zaytseva, and Nikolay V. Surovtsev. "Raman Spectroscopic Study of Phase Coexistence in Binary Phospholipid Bilayers." Applied Spectroscopy 75, no. 1 (2020): 87–93. http://dx.doi.org/10.1177/0003702820945764.

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Binary phospholipid bilayers composed of 1,2-dioleoyl-sn-glycero-3-phosphocholine and 1,2-palmitoyl-sn-glycero-3-phosphocholine (DPPC) were studied by Raman spectroscopy and differential scanning calorimetry (DSC). We examined features in Raman scattering spectra that are sensitive to the lipid phase and, therefore, could indicate the phase coexistence. It was found that the low-frequency half-width of half-maximum (LHWHM) of the 2850 cm−1 Raman line, corresponding to the symmetric CH2 stretching vibrations, unequivocally reveals the coexisting phospholipids in ordered and disordered conformat
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Thakur, Priya, Vimal Sharma, and Nagesh Thakur. "Exothermic behaviour of aluminium and graphene as a fuel in Fe2O3 based nanothermite." Zeitschrift für Naturforschung A 76, no. 8 (2021): 703–10. http://dx.doi.org/10.1515/zna-2021-0051.

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Abstract The main frontier of this research is to study the influence of multi-layer graphene (MLG) and aluminium as a fuel in Al/Fe2O3 and MLG/Fe2O3 nanothermites, fabricated by physical mixing and ultrasonication techniques. To study the structural and energy release properties, prepared samples were characterized by XRD, FESEM, EDS, FTIR, Raman spectroscopy and DSC. The X-ray diffraction (XRD) technique showed that all the phases remain intact during the synthesis. Field emission electron microscopy (FESEM) micrographs displayed the surface morphology of the samples, and besides this, energ
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Larosa, Claudio, Niranjan Patra, Marco Salerno, Lara Mikac, Remo Merijs Meri, and Mile Ivanda. "Preparation and characterization of polycarbonate/multiwalled carbon nanotube nanocomposites." Beilstein Journal of Nanotechnology 8 (September 27, 2017): 2026–31. http://dx.doi.org/10.3762/bjnano.8.203.

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A polymer nanocomposite was produced by ultrasonic-assisted dispersion of multiwalled carbon nanotubes (MWCNTs) in a polycarbonate matrix using p-xylene and dichloromethane as the solvents. The filler loading was varied from 1 to 3 wt % in order to examine the effect of MWCNTs on the structure and properties of the composites. The nanocomposites were characterized by DSC, DTA, TGA, UV–vis, FTIR and Raman spectroscopy to evaluate the changes induced by the filler in the polymer matrix. UV–vis, FTIR and Raman spectroscopy measurements confirmed the presence of the dispersed phase in the composit
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Dissertations / Theses on the topic "DSC raman spectroscopy"

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Sprunt, John. "Structural polymorph characterisation using fibre-optic linked FT-Raman-DSC." Thesis, University of East Anglia, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.267561.

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A low-cost fibre-optic probe was constructed, and used to provide an optical link between an FT-Raman spectrometer and a Differential Scanning Calorimeter (DSC). The resulting Simultaneous Raman-DSC (SRD) method combines the vibrational structural information of FT-Raman spectroscopy with the thermal data of DSC, which is particularly useful for characterisation of samples exhibiting temperature- and thermal conditioning-dependent polymorphic (i. e. structural) changes. The samples chosen for method development and structural study were ammonium nitrate (NH4NO3), the triglyceride sn-1,3-distea
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Ali, H. R. H. "Vibrational spectroscopic techniques (Raman, FT-IR and FT-NIR spectroscopy) as a means for the solid-state structural analysis of pharmaceuticals." Thesis, University of Bradford, 2009. http://hdl.handle.net/10454/3343.

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The aim of this work was to assess the suitability of vibrational spectroscopic techniques (Raman, FT-IR and FT-NIR spectroscopy) as a means for the solid-state structural analysis of pharmaceuticals. Budesonide, fluticasone propionate, salbutamol hemisulfate, terbutaline hemisulfate, ipratropium bromide, polymorphic forms of salmeterol xinafoate and two polymorphic forms of sulfathiazole were selected since they are used in the management of certain respiratory disorders and from different chemical and pharmacological entities along with some pharmaceutical excipients. Conventional visual exa
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Ogier, Stéphane. "Étude et optimisation de procédés d’encapsulation de cellules photovoltaïques." Thesis, Université de Lorraine, 2017. http://www.theses.fr/2017LORR0396/document.

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Les cellules photovoltaïques (PV) des modules ou panneaux solaires, sont protégées des agressions extérieures par des résines polymères encapsulantes qui, pour la plupart, sont des matériaux élastomériques réticulés. L’optimisation et le contrôle de l’étape d’encapsulation peut permettre un gain de productivité et augmenter la durée de vie des modules, ce qui réduit les coûts de l’électricité générée. Deux voies ont ainsi été explorées dans ce travail : 1) La première concerne l’étude de l’état de réticulation de l’encapsulant majoritairement utilisé actuellement, un copolymère d’éthylène et d
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Bouita, Mouad. "Étude des propriétés et des lois de comportement mécaniques à différentes échelles de polyesters par WAXS et spectroscopie Raman in situ." Electronic Thesis or Diss., Université de Lorraine, 2024. http://www.theses.fr/2024LORR0010.

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L'un des objectifs principaux de la thèse a été d'établir des corrélations étroites entre le comportement mécanique réel des échantillons à l'échelle macroscopique locale et les champs de contrainte et de déformation développés à l'échelle de la microstructure dans le poly(téréphtalate d'éthylène) (PET) et du poly(2,5-furandicarboxylate d'éthylène) (PEF). Grâce à l'ensemble des données WAXS et Raman obtenues de manière in situ à un essai de traction uniaxiale, les micromécanismes de déformation ont été identifiés et mesurés en temps réel avec la déformation et la contrainte locales et la contr
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Agrebi, Fatma. "Étude des propriétés diélectriques, thermiques et vibrationnelles de matériaux nano-composites à base du caoutchouc naturel renforcés par des nano-renforts cellulosiques." Electronic Thesis or Diss., Amiens, 2018. http://www.theses.fr/2018AMIE0001.

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Le caoutchouc naturel (CN) isolé de l'hévéa brésiliens et renforcé par différents pourcentages de nano-renforts de cellulose a été caractérisé en utilisant les techniques suivantes: la Calorimétrique Différentielle à Balayage, la Spectroscopie Diélectrique et enfin la Spectroscopie vibrationnelle (Infrarouge et Raman). L'objectif était la compréhension de l'impact des nano-renforts cellulosiques à différentes formes et fractions massiques sur les propriétés diélectriques, thermiques et vibrationnelles des matériaux de l’étude. L'ensemble des résultats obtenus nous a permis d’élucider la qualit
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Elbagerma, Mohamed A. "Analytical method development for structural studies of pharmaceutical and related materials in solution and solid state : an investigation of the solid forms and mechanisms of formation of cocrystal systems using vibrational spectroscopic and X-ray diffraction techniques." Thesis, University of Bradford, 2010. http://hdl.handle.net/10454/4467.

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Analysis of the molecular speciation of organic compounds in solution is essential for the understanding of ionic complexation. The Raman spectroscopic technique was chosen for this purpose because it allows the identification of compounds in different states and it can give information about the molecular geometry from the analysis of the vibrational spectra. In this research the ionisation steps of relevant pharmaceutical material have been studied by means of potentiometry coupled with Raman spectroscopy; the protonation and deprotonation behaviour of the molecules were studied in different
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Gulbiten, Ozgur. "An Investigation of Dynamic Processes in Selenium Based Chalcogenide Glasses." Diss., The University of Arizona, 2014. http://hdl.handle.net/10150/317040.

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Owing to their excellent infrared transmittance and good rheological properties, selenium based chalcogenide glasses have been materials of choice for a number of technological applications. However, chalcogenide glasses can undergo substantial structural relaxation even at room temperature due to their low glass transition temperatures. The origins of these dynamic processes and their correlation to the glass structure is therefore of fundamental and practical interest. In particular, a deep understanding of the dynamic response near the glass transition region could help elucidate the mechan
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Chbeir, Ralph. "Correlating Melt Dynamics with Topological Phases of Homogeneous Chalcogenide- and Modified Oxide- Glasses Using Raman Scattering, Infra-Red Spectroscopy, Modulated-Differential Scanning Calorimetry and Volumetric Experiments." University of Cincinnati / OhioLINK, 2019. http://rave.ohiolink.edu/etdc/view?acc_num=ucin1573224465185235.

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Wang, Wenhu. "Effect of Fullerene Nano-spheres on Evaporation Kinetics of Fluids." Wright State University / OhioLINK, 2011. http://rave.ohiolink.edu/etdc/view?acc_num=wright1323918423.

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Junior, Virgilio Tattini. "Etapas críticas na liofilização do pericárdio bovino." Universidade de São Paulo, 2008. http://www.teses.usp.br/teses/disponiveis/9/9134/tde-06032009-184216/.

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Em um sistema biológico, a água é responsável por inúmeras reações metabólicas, assim como pela estabilidade estrutural dos constituintes celulares do material. A liofilização é um processo de secagem comumente utilizado para a conservação de materiais biológicos. Entretanto, devido a complexidade do processo e às mudanças térmicas aplicadas ao material, se as etapas da liofilização não forem bem conduzidas, poderão ocorrer danos estruturais irreversíveis. Este projeto tem como objetivo determinar as etapas críticas na liofilização do pericárdio bovino. Através das técnicas de caracterização t
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Book chapters on the topic "DSC raman spectroscopy"

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Wartewig, S., K. Hesse, R. Neubert, and W. Rettig. "Thermotropic Behaviour of Ceramides/Oleic Acid Mixtures Studied by FT-Raman Spectroscopy and DSC." In Spectroscopy of Biological Molecules: Modern Trends. Springer Netherlands, 1997. http://dx.doi.org/10.1007/978-94-011-5622-6_145.

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Gardikis, Konstantinos, Sophia Hatziantoniou, Kyriakos Viras, Matthias Wagner, and Costas Demetzos. "Interaction of Dendrimers with Model Lipid Membranes Assessed by DSC and Raman Spectroscopy." In Nanocarrier Technologies. Springer Netherlands, 2006. http://dx.doi.org/10.1007/978-1-4020-5041-1_12.

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Priyadarshi, Gautam, Sagar Prajapati, and Mrugesh Trivedi. "Tools and Techniques to Analyse Microplastic Pollution in Aquatic and Terrestrial Ecosystems." In Microplastic Pollution: Causes, Effects and Control. BENTHAM SCIENCE PUBLISHERS, 2023. http://dx.doi.org/10.2174/9789815165104123010004.

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The estimation of microplastic pollution in the terrestrial and aquatic ecosystem is carried out by quantification and identification of the contaminated environment. Microplastic estimation consists of various steps such as sampling, visualization and quantification. Generally, the planktonic net, bongo net, manta net, and neuston net have been used for water sampling. While, grab samplers, tweezers, tablespoons, trowels, shovels, spatulas, or hand picking methods have been used for soil and sediment sampling. The biological sample from the study sites comprises the direct collection of the w
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Balanagu, Haranatha Babu, Tatavarti SVS Gopala Krishna, Ramesh Cheruvu, and Buchi N. Nalluri. "Development and Validation of HPLC Method for Quantification of Parecoxib in Parecoxib Injection." In Current Trends in Drug Discovery, Development and Delivery (CTD4-2022). Royal Society of Chemistry, 2023. http://dx.doi.org/10.1039/9781837671090-00199.

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The purpose of the present study was to evaluate and optimize lyophilization cycle time for the manufacturing of Parecoxib Injection than reported longer lyophilization cycle times. Optimization of lyophilization cycle time reduces the manufacturing costs since lyophilization process involves longer times which incurs cost to the finished product. Optimization of lyophilization cycle was done by using inputs from the results of Differential Scanning Calorimetry (DSC), Differential Thermal Analysis (DTA) and Impedance analysis. HPLC method was developed for quantification of Parecoxib Active Ph
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Eremets, M. I. "Raman Scattering." In High Pressure Experimental Methods. Oxford University PressOxford, 1996. http://dx.doi.org/10.1093/oso/9780198562696.003.0013.

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Abstract It is difficult to provide an overview from the physical standpoint of the enormous number of Raman scattering studies performed under pressure. On the other hand, the experimental aspect seems too simple: only a slight modification of the optical scheme is needed to replace a sample by a high-pressure cell, especially by a small DAC. From this point of view Raman spectroscopy is one of the easiest high-pressure methods. However, there are many specific problems with weak scatterers and with studies in the megabar region.
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Conference papers on the topic "DSC raman spectroscopy"

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Diz, E. Lozano, K. Menard, D. Norman, et al. "Applications of Hyphenated DSC-Raman Spectroscopy to Polymers." In XXII INTERNATIONAL CONFERENCE ON RAMAN SPECTROSCOPY. AIP, 2010. http://dx.doi.org/10.1063/1.3482826.

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Menard, K., E. Lozano Diz, D. Norman, et al. "Investigating Crystallization of Pharmaceutical Materials With Simultaneous DSC and Raman Spectroscopy." In XXII INTERNATIONAL CONFERENCE ON RAMAN SPECTROSCOPY. AIP, 2010. http://dx.doi.org/10.1063/1.3482779.

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Chakraborty, Ishita, Indira Govindaraju, Guan-Yu Zhuo, et al. "Illucidating the structural components of starch granules using advanced analytical techniques." In Frontiers in Optics. Optica Publishing Group, 2022. http://dx.doi.org/10.1364/fio.2022.jtu5a.55.

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Thermal and chemical characterization are performed in different rice varities originated in Northeast India to illucidate their composition and physicochemical characteristics using Raman spectroscopy, non linear optical microscopy, and differential scanning calorimetry (DSC).
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Jumeau, Richard, Patrice Bourson, Michel Ferriol, François Lahure, Franck Ducos, and Jéro^me Ligneron. "Comparative Study Of Various Grades Of Polyethylene By Differential Scanning Calorimetry (DSC) Correlated With Raman Spectroscopy." In THE 14TH INTERNATIONAL ESAFORM CONFERENCE ON MATERIAL FORMING: ESAFORM 2011. AIP, 2011. http://dx.doi.org/10.1063/1.3589612.

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Fialkova, Svitlana, Jair Flores, Sergey Yarmolenko, Jagannathan Sankar, Geoffrey Ndungu, and Kevin Wilkinson. "Effect of Thermal Treatment on Bioactivity of Experimental Dental Cement." In ASME 2017 International Mechanical Engineering Congress and Exposition. American Society of Mechanical Engineers, 2017. http://dx.doi.org/10.1115/imece2017-70970.

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Objective. The purpose of this study was to characterize and to evaluate the effect of thermal treatment on properties and bioactivity of experimental dental cement. Methods. Specimens of the dental cement (pellets 13 mm in diameter × 3 mm thick) were prepared by cold pressing of micronized powder of set Alborg White Portland cement. The thermo-gravimetric analysis and differential scanning calorimetry (TGA/DSC) were used to analyze the phase composition and determine the transition temperatures for sintering process. The effect of heat rate and dwell time on density, crystal morphologies, cry
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Fialkova, Svitlana, Sergey Yarmolenko, Jagannathan Sankar, Geoffrey Ndungu, and Kevin Wilkinson. "Bioactive Coating From White Portland Cement Deposited by Pulsed Laser Deposition." In ASME 2017 International Mechanical Engineering Congress and Exposition. American Society of Mechanical Engineers, 2017. http://dx.doi.org/10.1115/imece2017-70986.

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Objective. We report the study of feasibility to produce the thing bioactive coating from experimental dental cement using pulsed laser deposition (PLD) technique. Methods. The targets for PLD system (disks 30 mm in diameter × 5 mm thick) were sintered from micronized powder of set Alborg White Portland cement (WPC). The parameters for sintering process were chosen based thermo-gravimetric analysis and differential scanning calorimetry (TGA/DSC). The coatings were deposited by PLD on silicon substrates. The effect of laser power on coating crystallinity and morphology was evaluated by scanning
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Sepaniak, Michael, Sabrina Wells, Deepak Bhandari, Nickolay Lavrik, P. M. Champion, and L. D. Ziegler. "Nanofabrication of Disc on Pillar Substrates for Surface Enhanced Raman Spectroscopy." In XXII INTERNATIONAL CONFERENCE ON RAMAN SPECTROSCOPY. AIP, 2010. http://dx.doi.org/10.1063/1.3482508.

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KOWALCZYK, J. "Characterization and Properties of Diamond-Like Carbon Coatings." In Terotechnology XII. Materials Research Forum LLC, 2022. http://dx.doi.org/10.21741/9781644902059-7.

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Abstract. The paper presents the results of the research on the tribological properties of the DLC coating. The coating was applied using plasma-assisted chemical vapour deposition (PACVD). The obtained coating was determined to be a DLC coating using a Raman spectroscope. Friction tests were performed using a tribometer working in a ball-disc friction configuration at various loads applied. For the tests, a disc with a DLC coating was used as a sample, and a ball made of 100Cr6 steel was used as a counter-sample. The friction tests were carried out in the conditions of technically dry frictio
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Yanagisawa, M., M. Kunimoto, and T. Homma. "Life Estimation of Carbon Overcoat on Magnetic Media for Heat-Assisted Magnetic Recording Using Novel Raman Spectroscopy." In ASME 2016 Conference on Information Storage and Processing Systems. American Society of Mechanical Engineers, 2016. http://dx.doi.org/10.1115/isps2016-9513.

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A heat-assisted magnetic recording (HAMR) is expected for a future high density recording of a hard disk drive. However, a carbon overcoat (COC) composed of diamond-like carbon (DLC) or a lubricant film is possibly damaged when a magnetic medium, i.e. CoPt alloy, is heated at around Curie temperature (Tc) of 600K by a near-field HAMR head. We carried out HAMR simulation experiments by using newly developed Raman spectroscopic systems, composed of plasmonic sensors for surface-enhanced Raman scattering (SERS), a pulsed laser heating, and an in-situ temperature measurement with an intensity rati
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Zhang, Ruijun, and Hongtao Ma. "Nano-Mechanical Property and Nano-Tribological Behaviors of Nitrogen-Doped Diamond-Like (DLC) Coatings." In World Tribology Congress III. ASMEDC, 2005. http://dx.doi.org/10.1115/wtc2005-63323.

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Diamond-like carbon (DLC) films doped with different nitrogen contents were prepared by an ECWR-CVD deposition technique, and their composition, structure, nano-mechanical property and nano-tribological behaviors were characterized using PHI680 type Auger Electron Spectrometer (AES), Renishaw Raman system 1000 type Laser Raman Spectroscopic technique and Hysitron Nano-indentor, respectively. It has been found that, with the increasing of nitrogen content in the films, the resultant N-doped DLC films show a monotonous drop in the sp3 ratio and a significant increase in the sp2 ratio, and, accor
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