Academic literature on the topic 'Dynamic elastic modulus'

The focus of this study is to investigate the effect of carboxylated styrene-butadiene rubber (SBR) latex on the dynamic rheologcial properties of paper coating suspensions modified with nanosized particles. The elastic storage modulus G′ and the viscid loss modulus G′′ are used to evaluate the dynamic rheologcial properties of paper coating suspensions. The effects of different amount carboxylated styrene-butadiene rubber latex on the flow parameters of paper coating suspensions are comparatively presented. It is shown that the dynamic elastic storage modulus G′ and viscid loss modules G′′ of paper coating suspensions increase with the SBR content change from 13% to 18%. The dynamic rheologcial properties are related to the strength of the network structure of paper coating suspensions. It is also found that the elastic storage modulus G′ of paper coating suspensions is larger than viscid loss modulus G′′, which indicates that paper coating suspensions in this investigation all behave like a viscoelastic solid.

The phase transformation characteristics, the dynamic elastic modulus and the static tensile elastic modulus of Ti50Ni47.5Fe2.5 alloy were investigated. It is found that, the two mutations in the dynamic elastic modulus is caused by reverse martensite phase transformation and austenite phase transformation respectively; Static tensile test can not reflect the intrinsic elastic modulus when the test temperature is close to martensite transformation temperature(Ms). The static elastic modulus and the dynamic elastic modulus have the same trend when the test temperature is enough higher than Ms.

Cracks caused by environmental temperature and humidity variation are generally considered one of the most important factors causing durability deterioration of concrete structures. The seasonal or daily variation of ambient temperature and humidity can be considered periodic. The dynamic modulus of elasticity is an important parameter used to evaluate the performance of structural concrete under periodic loads. Hence, in this paper, the dynamic elastic modulus test of concrete under simulating periodic temperature-humidity variation is carried out according to monthly meteorological data of representative areas (Nanjing, China). The dynamic elastic modulus attenuation pattern and a dynamic elastic modulus degradation model of concrete under periodic temperature-humidity are investigated. The test results show that the dynamic elastic modulus of concrete decreases and tends to be stable under the action of periodic temperature-humidity. Comparative analysis shows that the two-parameter dynamic elastic modulus degradation model is more suitable for describing the dynamic elastic modulus attenuation pattern of concrete under periodic temperature-humidity action than the single-parameter one.

The elastic modulus of cement paste is the key parameter for characterizing the mechanical response of concrete. In modern concrete technology, the admixtures are often used to enhance the performance of concrete. This paper introduces a nondestructive testing method to evaluate the dynamic elastic modulus of cement paste. Moreover, the effect of water-cement ratio and conventional admixtures on the dynamic elastic modulus of cement paste is investigated, in which three kinds of admixtures are taken into account including Viscosity Modifying Admixture (VMA), Silica Fume (SF), and Shrinkage-Reducing Admixture (SRA). The results from experimental investigation indicate that the dynamic elastic modulus of cement paste increases with decreasing water-cement ratio. The addition of SF increases the dynamic elastic modulus, however, the overdosage of VMA causes its reduction. SRA reduces the elastic modulus at early age without affecting the elastic modulus at later period.

Water content is one of key effect factors on the dynamic elastic modulus, which is an important damage assessment index of concrete structures induced by freeze-thaw cycles, fire and chemical attacks. Through the ultrasonic and bending vibration test, the regularity of dynamic elastic modulus changed with the water content of concrete specimens was analyzed in this paper. The results show that the ultrasonic velocity has a low sensitivity to water content when it is below 1.5%. The bending vibration method can better reflect the effect of water content change on dynamic elastic modulus. The regression equation of dynamic elastic modulus and water content was set up by introducing the index function. The research results offer technical reference for the predicting of actual concrete dynamic elastic modulus in different humidity environment.

In order to ensure the high-speed railway train running safety and stabilization, the subgrade should keep adequate strength, rigidity and long-term stabilization under the repeated train load. When the subgrade soil is poor, we can treat it with cement. Whether the performance of cement-treated soil can meet the demand of high-speed railway, so the dynamic triaxial test of cement-treated soil is studied in this paper. The dynamic performance of cement-treated soil under repeated train load is analyzed. The variation and influence factors of critical dynamic stress, accumulated plastic strain, elastic strain and resilient module of cement-treated soil are studied.When the dynamical stress more than the critical dynamical stress, the cumulate plastic strain and the elastic strain will rapidly increase with the increase of the loading time of the dynamical stress. The resilience modulus will decrease along with the increase of the dynamical stress. When the dynamical stress less than the he critical dynamical stress, the elastic strain and the resilience modulus remain constant with the increase of the loading time of the dynamical stress. And the elastic strain and the resilience modulus linearly increase with the increase of the dynamical stress.

Sonic log compressional and shear-wave velocities combined with logged bulk density can be used to calculate dynamic elastic moduli in organic shale reservoirs. We use linear multivariate regression to investigate modulus prediction when shear-wave velocities are not available in seven unconventional shale reservoirs. Using only P-wave modulus derived from logged compressional-wave velocity and density as a predictor of dynamic shear modulus in a single bivariate regression equation for all seven shale reservoirs results in prediction standard error of less than 1 GPa. By incorporating compositional variables in addition to P-wave modulus in the regression, the prediction standard error is reduced to less than 0.8 GPa with a single equation for all formations. Relationships between formation bulk and shear moduli are less well defined. Regressing against formation composition only, we find the two most important variables in predicting average formation moduli to be fractional volume of organic matter and volume of clay in that order. While average formation bulk modulus is found to be linearly related to volume fraction of total organic carbon, shear modulus is better predicted using the square of the volume fraction of total organic carbon. Both Young’s modulus and Poisson’s ratio decrease with increasing TOC while increasing clay volume decreases Young’s modulus and increases Poisson’s ratio.

In this paper, the dynamic characteristics for three different kinds of copper tailings are studied through a series of cyclic triaxial tests. It is found that under confining pressure 200 and 300 kPa, elastic modulus raises with the increasement of coarse grain content to a certain degree and then declines, and the maximum elastic modulus corresponds to good gradation. While, as for confining pressure 100 kPa, elastic modulus raises with the increasement of fine grain content. It is also found that elastic modulus raises with the increasement of confning pressure. And, damping ratio raises with the increasement of shear strain and finally to a stable value. Finally, the fitting Gd/Gdmax~ curve for three kinds of tailings shows the reasonableness of test results.

Dynamic atomic force microscopy (AFM) was employed to spatially map the elastic modulus of highly oriented pyrolytic graphite (HOPG), specifically by using force modulation microscopy (FMM) and contact resonance (CR) AFM. In both of these techniques, a variation in the amplitude signal was observed when scanning over an uncovered step edge of HOPG. In comparison, no variation in the amplitude signal was observed when scanning over a covered step on the same surface. These observations qualitatively indicate that there is a variation in the elastic modulus over uncovered steps and no variation over covered ones. The quantitative results of the elastic modulus required the use of FMM, while the CR mode better highlighted areas of reduced elastic modulus (although it was difficult to convert the data into a quantifiable modulus). In the FMM measurements, single atomic steps of graphene with uncovered step edges showed a decrease in the elastic modulus of approximately 0.5%, which is compared with no change in the elastic modulus for covered steps. The analysis of the experimental data taken under varying normal loads and with several different tips showed that the elastic modulus determination was unaffected by these parameters.

The movement and control of the vocal folds within the laryngeal cavity enables three crucial physiological functions: 1) allowing respiration by opening, 2) aiding in airway protection by closing, and 3) regulating sound production during phonation. Although treatment options have improved, many of the estimated 7.5 million individuals in the United States who are annually affected by voice-related disorders still face serious challenges related to dysphonia and dysphagia. The need for improved voice-disorder treatments has motivated the work presented in this dissertation which focuses on modeling and manufacturing the vocal folds and aims to answer three main questions: 1) what are the mechanical properties of the vocal folds and how do they change across the full vocal range? 2) how do those properties influence the dynamic behavior of the tissue? and 3) can we manufacture a synthetic vocal fold model that exhibits a desired and controllable dynamic behavior? First, the elastic properties of sixteen porcine vocal folds were evaluated through uniaxial tensile tests on a custom built experimental setup. Stress-strain data was analyzed using an optimization method to yield continuous model parameters which described the linear and nonlinear elastic regions as well as transition points between those regions. Next, the impact of the vocal fold elastic properties on the frequencies of vibration was evaluated through dynamic tests on excised porcine larynges. Sound data was analyzed via a spectrogram and through the use of fast Fourier transforms to study changes in the frequency of vibration while the vocal folds were stretched. Additionally, a mathematical aeroelastic model of phonation was implemented to further evaluate the changing elastic properties on vocal fold dynamics. Next, eight synthetic vocal fold models were created, each with varying mechanical properties and a geometry based on reported anatomical measurements of porcine vocal folds. The synthetic models were then dynamically tested to further study the impact of changes in mechanical properties on the dynamic behavior of the synthetic vocal folds.
Doctor of Philosophy
The movement and control of the vocal folds within the voice-box enables three crucial physiological functions: 1) allowing respiration by opening, 2) aiding in airway protection and swallowing by closing, and 3) regulating sound production during vocalization. Although treatment options have improved, many of the estimated 7.5 million individuals in the United States who are annually affected by voice-related disorders still face serious challenges related to speech production and swallowing which often results in significant detrimental impacts to quality of life. The need for improved treatments is most easily observed in the evaluation of treatment options following a total laryngectomy, which is a procedure where the entire voice-box is removed often due to cancer. Following a laryngectomy, all three of the vital functions of the vocal folds are immediately impacted as patients adjust to breathing through and protecting a redirected airway and are forced to use alternative methods of speech production which often result in monotone or robotic-sounding speech. The need for improved voice-disorder treatments has motivated the work presented in this dissertation which focuses on modeling and manufacturing the vocal folds and aims to answer three main questions: 1) what are the mechanical properties of the vocal folds? 2) how do those properties influence the dynamic behavior of the tissue during sound production? and 3) can we manufacture synthetic vocal folds that produce a desired and controllable dynamic behavior? Sixteen porcine vocal fold samples were mechanical tested to evaluate the elastic properties of the tissue. Next, porcine voice-box samples were experimentally tested in a way that simulated sound production by subjecting the samples to a heated and humidified air flow, similar to the air flow conditions coming out of the lungs. In this way, the relationship between the tissue properties and the frequencies of sound was investigated. Lastly, the synthetic vocal fold samples were evaluated using a similar experimental protocol to further investigate the impact of changing structural properties on the dynamics of the vocal folds during sound production.

Environment conditions and moisture presence in masonry structures may affect durability or even mechanical properties of architectural heritage. Among all the deterioration causes, the degradation of historic masonry by freeze-thaw cycles and different moisture amount are considered to evaluate their influence on elastic properties. Therefore, two experimental campaigns were carried out in the present study. The first one was performed at the Dept. of Geotechincal Engineering at Tongji University, to assess the influence of freeze-thaw cycles on elastic modulus of historic Chinese brick. The static elastic modulus was evaluated from the compressive strength test on masonry specimens subjected to different numbers of freeze-thaw cycles. Moreover, strength decay of the masonry was investigated, also analysing data obtained during ultrasonic test (UPV, non-destructive test). The aim of this step was to obtain the dynamic elastic modulus. Thanks to interpolation of the obtained data it was possible to improve the knowledge of the Elasticity modulus’ reduction of historic masonry subjected to freeze-thaw cycles. The second experimental campaign was performed at DICAM, University of Bologna, on ancient Chinese and Italian bricks, to assess the sensitivity of dynamic elastic modulus to moisture amount. In particular the influence of water presence in the material pores on the UPV measurements. The close relationship between the ultrasonic pulse velocity and the moisture content was investigated on brick cores in dry, 50% saturated and saturated conditions. Practical value and one of the main contribution of the experiments was the investigation of external factor and intrinsic properties of porous materials which directly influence the ultrasonic pulse velocity test.

Free-layer hard or soft coating material can be used for enhancing the inherent damping capacity (energy dissipation ability) of a structure under cyclic bending deformation. This may help to attenuate the vibration amplitude at the resonance frequency. In this study, dynamic mechanical and damping properties of a carbon based (CNx) coating material have been investigated. For determining the material properties of this coating, two samples (600 μm and 800 μm thick carbon nitride (CNx) film layers) were produced and deposited onto two internal turning tools by using the plasma enhanced chemical vapor deposition (PECVD) process. The deposition process was conducted at the room temperature with the magnetron sputtering of a copper and a subsequent graphite target plate in a highly ionized plasma and reactive environment of Ar, N2 and C2H2 gases. Eigen frequencies and system loss factors of the uncoated and coated tools were extracted, for the first two fundamental bending modes (mode X and mode Y), from the ‘drive point’ measurements of free hanging impact tests at the free-free boundary condition. Modulus of elasticity and loss factor of the coating material has been deduced through the comparison between the eigen frequencies and resonance amplitudes of the identical bending modes extracted from the experimental and analytical frequency response functions. The results obtained from the experimental modal analyses and the iterative finite element analyses show that, compared to the substrate, the flexural stiffness and the damping capacity of the coated tools have increased notably. The resonant frequencies of the coated samples have been shifted to the higher frequency levels, and the frequency response acceleration amplitudes have been attenuated dramatically. Elastic modulus and loss factor range of the coating material have been found to be in the range of 32.5 GPa to 49.1 GPa and 0.004 to 0.0245 respectively. Comparison between the analytical frequency response functions of the CNx coating material and 3M-112 viscoelastic material coated samples (for 800 μm film thickness) has anticipated that the coating material has higher loss modulus (energy dissipation ability) as opposed to the viscoelastic material. Scanning electron microscope images of the cross-section of a coated sample have revealed that the frictional energy losses between the interfaces of the carbon-nitride columnar micro-structures dominate the inherent damping mechanism of the coating material. Voids and porosities, present between the columnar clusters, further increase the energy dissipation ability of the coating material by enhancing the interface slippage mechanism during the cyclic bending deformation.

Moisture-induced damage is one the major causes of deterioration of asphalt pavements and extensive research has been conducted on this topic. Theoretical and experimental results have led the researchers to believe that moisture-induced damages are caused mainly by the generation of pore water pressure in asphalt mixtures when traffic passes over a pavement. The Moisture Induced Sensitivity Tester (MIST) has been recently developed to simulate the phenomenon of repeated pore pressure generation and deterioration in the laboratory. The objective of this study was to evaluate moisture-induced damage in typical Maine Department of Transportation (DOT) asphalt mixes, with the use of MIST, pre and post testing, and analysis of data. The MIST was used to condition Hot Mix Asphalt (HMA) samples that were compacted from eight typical Maine DOT mixes, with different types of aggregates and asphalt binder. A modified Dynamic modulus test in Indirect Tensile Mode was used for the determination of damage. A layered elastic model, along with a fatigue-cracking criterion, was utilized to assess the total impact on the pavement lives. Monte Carlo analysis was conducted to determine the distribution of number of repetitions to failure of pavements that are subjected to moisture damage. The major conclusions are that most of the mixes are likely to experience a reduction in their life due to the effect of moisture and that the Micro-Deval and the fine aggregate absorption test results can be related to such damage. A composite factor, consisting of both of these test results, is recommended for regular use by the DOT to screen mixes with high moisture damage potential.

Ultrasonic Pulse Velocity (UPV) and Rebound test as non-destructive techniques may effectively contribute to in situ analysis of bricks and masonries elements for the restoration, rehabilitation and strengthening of historic buildings. Fired-clay bricks were commonly used in buildings in ancient China, but there is few knowledge on their behaviour in environmental conditions. Moisture is one of the main factors that cause deterioration in historic building, in particular in areas with natural freeze-thaw cycles. In this work, two laboratory experiments were carried out, at Tongji University, China, and DICAM Department of Bologna University, Italy, respectively. Fired-clay bricks about 200 years old were collected from demolished buildings in Changzhi City in Shanxi Province, belonging to the Yellow River Region, where the climate involves natural freeze-thaw cycles. The aim was to evaluate how the frost damage changes the physical and mechanical properties of Chinese historical bricks and masonries. Several non-destructive methods were used, focusing on the effectiveness of Ultrasonic Pulse Velocity (UPV) for evaluating physical and mechanical properties of Chinese historic grey bricks and masonries. Destructive tests were also used to evaluate compressive strength and static elastic modulus. The samples showed a reduction of their properties due to freeze-thaw cycles. The presence of water affected the values of the analysed parameters, leading to a decrease of UPV. The trend determined by these methods can be used to assess the uniformity of bricks and to detect areas of poor quality or deteriorated masonry structures.

This work solves creation of calibration relations to determine cube compressive strength, dynamic and static elastic modulus of alkali-activated concrete by non-destructive methods. Alkali-activated concrete is spoken of as a new material used in civil engineering. It shows different properties than normal concrete based on Portland cement. That's why the modification of common calibration relation seems necessary. Fresh concrete was made in the concrete plan ŽPSV a.s., Uherský Ostroh in three mixtures and always in the number of 18 cubes and 3 prisms. The samples were tested by impact hammer Schmidt type L, type N, SilverSchmidt PC-N and by ultrasound in 6 time periods of three specimens. After that, the cube compressive strength was determined. Status of static elastic modulus was determined in a time period of 28 days. The results are calibration relations to determine the progress of compressive strength and modulus of elasticity for each method and their combination.

Este trabalho apresenta dois tipos de ensaios não destrutivos para a correlação do módulo dinâmico com a resistência à compressão para elementos de concreto. Os métodos de ensaio são a ultrassonografia e o método de excitação por impulso utilizando o equipamento Sonelastic®. Neste trabalho estão descritos seus funcionamentos, aplicações e limitações. A ultrassonografia, através da propagação de ondas sonoras, fornece, indiretamente, o módulo de elasticidade dinâmico. Com o método de excitação por impulso obtêm-se as frequências naturais e os modos de vibração do elemento estudado, o que permite determinar seu módulo dinâmico. Primeiramente, estes ensaios foram utilizados em corpos-de-prova cilíndricos e lajes alveolares produzidas em laboratório para a obtenção das curvas de correlação e, em seguida, estes mesmos ensaios foram realizados na fábrica de concreto pré-moldado. Para elementos de geometria complexa, como é o caso das lajes alveolares, apresenta-se uma metodologia para a obtenção de uma equação analítica para o cálculo do módulo dinâmico no ensaio de excitação por impulso. Estes métodos tiveram o objetivo final de avaliar a resistência à compressão do concreto na pista de protensão da fábrica, e então determinar o melhor momento para a desforma e corte do cabo de protensão. Com ambos os métodos, obteve-se ótimas correlações do módulo dinâmico com a resistência à compressão dos elementos em laboratório. Na fábrica de concreto pré-moldado não foi possível obter uma curva de correlação representativa de toda a laje na pista de protensão, porém foi possível registrar um bom indicativo de que é possível obter boas correlações para futuras pesquisas no assunto
This work presents two types of non-destructive testing for the correlation of the dynamic elastic modulus with the compressive strength. The test methods are the ultrasonography and the impulse excitation using the Sonelastic® equipment. In this work the equipaments operations, applications and limitations are also described. The ultrasound test indirectly supplies the dynamic elastic modulus through the propagation of sound waves. The natural frequencies and the vibration modes of the studied elements are obtained through impulse excitation method allowing to determine its dynamic modulus. To start, these tests were used in cylindrical specimens and hollow core slabs produced in the laboratory to obtain the correlation curves, and then these same methods were performed in the pre-cast concrete plant. As for complex geometric elements, as in the case of hollow core slabs, a methodology is applied in order to obtain an analytic equation to calculate the dynamic modulus in the impulse excitation test. These methods had the final goal the evaluation of the strength of prestressed concrete lying on track of the plant, so as to determine the best moment to demold and cut the prestressed cable. Excellent correlations of the dynamic modulus with compressive strength of the elements made in laboratory were obtained using both methods. It was not possible to obtain in the precast concrete plant a representative correlation curve of the whole slab on the track, nevertheless, it was possible to record a good indication that it is possible to obtain good correlations for future research.

Předložená magisterská práce se zabývá možným použitím vitrifikovaného lignitového lóžového popele jako náhrada slinku v kompozitních cementech. Byly zkoumány vlivy přidaného vitrifikovaného lóžového popele, jeho jemnosti, alkalických roztoků a jejich koncentrací. Byly připraveny kompozitní cementy v souladu s normou DIN EN 197 – 1. V těchto cementech bylo nahrazeno 30 % slinku vitrifikovaným lóžovým popelem. Konkrétně byly připraveny kompozitní cementy s vitrifikovaným lóžovým popelem o jemnosti 5549 cm2/g a 8397 cm2/g. Dále byly přidány alkalické roztoky hydroxidů a síranů vždy o dvou různých koncentracích, za účelem stimulace pucolánové a/nebo geopolymerní reakce. Mechanické vlastnosti připravených vzorků byly charakterizovány mechanickým testováním na prizmách s rozměry 40×40×160 mm, jak je specifikováno v normě DIN EN 196 – 1. Byla provedena nedestruktivní měření dynamického elastického modulu a destruktivní testovaní na pevnosti v tlaku a v ohybu. Distribuce velikosti částic a chemická analýza vstupních materiálů byla vykonána pomocí laserové granulometrie a rentgenové fluorescence. U zatvrdlých kompozitů bylo dále zkoumáno po 2 a 28 dnech hydratace fázové složení s využitím metody rentgenové difrakce a mikrostruktura s využitím skenovací elektronové mikroskopie. Výsledky ukázaly, že mechanické vlastnosti jsou nezávislé na množství přidaných alkálií stejně jako na jemnosti přidaného vitrifikovaného lóžového popele. Nicméně, znatelně nižší mechanické pevnosti byly pozorovány pro vzorky, které byly aktivovány hydroxidy, pravděpodobně kvůli brzké tvorbě silikátového hydrogelu. Vzorky aktivované sírany nedosáhly pevností jako referenční malta.

Collagen type I is an extracellular matrix (ECM) protein that affords tensile strength and biological scaffolding to numerous vertebrate and invertebrate tissues. This strength has been attributed to the triple-helical structure of the collagen type I molecules, their organization into fibrils, and the presence of inter-molecular, covalent, enzymatic crosslinks. There are several different types of these crosslinks; their composition is tissue-specific and dependent upon factors such as age and health. Furthermore, these enzymatic crosslinks tend to form specifically at amino/N- and carboxy/C-terminal crosslinking sites. The mechanical behavior of collagen type I has been investigated, via experiment and theory, at the level of the molecule, microfibril, fibril, and fiber. However, the influence of different enzymatic crosslinks and their location (e.g., N- vs. C-site) on the mechanics of collagen type I has not been investigated in the literature.

We employed molecular dynamics to model the mechanical behavior of uncrosslinked and crosslinked ~23-nm-long molecular segments and ~65-nm-long microfibril units of collagen type I. We then used these molecular simulations to construct a model of a single collagen type I fibril by considering the ~65-nm-long microfibril units arranged in series and then in parallel.

When a uniaxial deformation was applied along the long axis of the molecular models, N-crosslinks aligned rapidly at lower strains followed by C-crosslinks more gradually at higher strains, leading to a two-stage crosslink recruitment. Then when comparing the influence of different enzymatic crosslinks, significant differences were observed for the high-strain elastic moduli of our microfibril unit models, namely and in increasing order, uncrosslinked, immature crosslinked (HLKNL and deH-HLNL), mature HHL-crosslinked, and mature PYD-crosslinked. At the fibril level, our low- and high-strain elastic moduli were in good agreement with some literature data, but in over-estimation of several other literature reports. Future work will seek to address simplifications and limitations in our modeling approach. A model such as this, accounting for different enzymatic crosslink types, may allow for the prediction of the mechanics of collagen fibrils and collagenous tissues, in representation of healthy and diseased states.
Ph. D.

[EN] The test for determining the resonance frequencies has traditionally been used to investigate the mechanical integrity of concrete cores, to assess the conformity of concrete constituents in different accelerated durability tests, and to ascertain constitutive properties such as the elastic modulus and the damping factor. This nondestructive technique has been quite appealed for evaluation of mechanical properties in all kinds of durability tests. The damage evolution is commonly assessed from the reduction of dynamic modulus which is produced as a result of any cracking process. However, the mechanical behavior of concrete is intrinsically nonlinear and hysteretic. As a result of a hysteretic stress-strain behavior, the elastic modulus is a function of the strain. In dynamic tests, the nonlinearity of the material is manifested by a decrease of the resonance frequencies, which is inversely proportional to the excitation amplitude. This phenomenon is commonly referred as fast dynamic effect. Once the dynamic excitation ceases, the material undergoes a relaxation process whereby the elastic modulus is restored to that at rest. This phenomenon is termed as slow dynamics. These phenomena (fast and slow dynamics) find their origin in the internal friction of the material. Therefore, in cement-based materials, the presence of microcracks and interfaces between its constituents plays an important role in the material nonlinearity. In the context of the assessment of concrete durability, the damage evolution is based on the increase of hysteresis, as a result of any cracking process. In this thesis three different nondestructive techniques are investigated, which use impacts for exciting the resonant frequencies. The first technique consists in determining the resonance frequencies over a range of impact forces. The technique is termed Nonlinear Impact Resonant Acoustic Spectroscopy (NIRAS). It consists in ascertaining the downward resonant frequency shift that the material undergoes upon increasing excitation amplitude. The second technique consists in investigating the nonlinear behavior by analyzing the signal corresponding to a single impact. This is, to determine the instantaneous frequency, amplitude and attenuation variations corresponding to a single impact event. This technique is termed as Nonlinear Resonant Acoustic Single Impact Spectroscopy (NSIRAS). Two techniques are proposed to extract the nonlinear behavior by analyzing the instantaneous frequency variations and attenuation over the signal ring down. The first technique consists in discretizing the frequency variation with time through a Short-Time Fourier Transform (STFT) based analysis. The second technique consists of a least-squares fit of the vibration signals to a model that considers the frequency and attenuation variations over time. The third technique used in this thesis can be used for on-site evaluation of structures. The technique is based on the Dynamic Acousto- Elastic Test (DAET). The variations of elastic modulus as derived through NIRAS and NSIRAS techniques provide an average behavior and do not allow derivation of the elastic modulus variations over one vibration cycle. Currently, DAET technique is the only one capable to investigate the entire range of nonlinear phenomena in the material. Moreover, unlike other DAET approaches, this study uses a continuous wave source as probe. The use of a continuous wave allows investigation of the relative variations of the elastic modulus, as produced by an impact. Moreover, the experimental configuration allows one-sided inspection.
[ES] El ensayo de determinación de las frecuencias de resonancia ha sido tradicionalmente empleado para determinar la integridad mecánica de testigos de hormigón, en la evaluación de la conformidad de mezclas de hormigón en diversos ensayos de durabilidad, y en la terminación de propiedades constitutivas como son el módulo elástico y el factor de amortiguamiento. Esta técnica no destructiva ha sido ampliamente apelada para la evaluación de las propiedades mecánicas en todo tipo de ensayos de durabilidad. La evolución del daño es comúnmente evaluada a partir de la reducción del módulo dinámico, producido como resultado de cualquier proceso de fisuración. Sin embargo, el comportamiento mecánico del hormigón es intrínsecamente no lineal y presenta histéresis. Como resultado de un comportamiento tensión-deformación con histéresis, el módulo elástico depende de la deformación. En ensayos dinámicos, la no linealidad del material se manifiesta por una disminución de las frecuencias de resonancia, la cual es inversamente proporcional a la amplitud de excitación. Este fenómeno es normalmente denominado como dinámica rápida. Una vez la excitación cesa, el material experimenta un proceso de relajación por el cual, el módulo elástico es restaurado a aquel en situación de reposo. Este fenómeno es denominado como dinámica lenta. Estos fenómenos ¿dinámicas rápida y lenta¿ encuentran su origen en la fricción interna del material. Por tanto, en materiales basados en cemento, la presencia de microfisuras y las interfaces entre sus constituyentes juegan un rol importante en la no linealidad mecánica del material. En el contexto de evaluación de la durabilidad del hormigón, la evolución del daño está basada en el incremento de histéresis, como resultado de cualquier proceso de fisuración. En esta tesis se investigan tres técnicas diferentes las cuales utilizan el impacto como medio de excitación de las frecuencias de resonancia. La primera técnica consiste en determinar las frecuencias de resonancia a diferentes energías de impacto. La técnica es denominada en inglés: Nonlinear Impact Resonant Acoustic Spectroscopy (NIRAS). Ésta consiste en relacionar el detrimento que el material experimenta en sus frecuencias de resonancia, con el aumento de la amplitud de la excitación. La segunda técnica consiste en investigar el comportamiento no lineal mediante el análisis de la señal correspondiente a un solo impacto. Ésta consiste en determinar las propiedades instantáneas de frecuencia, atenuación y amplitud. Esta técnica se denomina, en inglés, Nonlinear Single Impact Resonant Acoustic Spectroscopy (NSIRAS). Se proponen dos técnicas de extracción del comportamiento no lineal mediante el análisis de las variaciones instantáneas de frecuencia y atenuación. La primera técnica consiste en la discretización de la variación de la frecuencia con el tiempo, mediante un análisis basado en Short-Time Fourier Transform (STFT). La segunda técnica consiste en un ajuste por mínimos cuadrados de las señales de vibración a un modelo que considera las variaciones de frecuencia y atenuación con el tiempo. La tercera técnica empleada en esta tesis puede ser empleada para la evaluación de estructuras in situ. La técnica se trata de un ensayo acusto-elástico en régimen dinámico. En inglés Dynamic Acousto-Elastic Test (DAET). Las variaciones del módulo elástico obtenidas mediante los métodos NIRAS y NSIRAS proporcionan un comportamiento promedio y no permiten derivar las variaciones del módulo elástico en un solo ciclo de vibración. Actualmente, la técnica DAET es la única que permite investigar todo el rango de fenómenos no lineales en el material. Por otra parte, a diferencia de otras técnicas DAET, en este estudio se emplea como contraste una onda continua. El uso de una onda continua permite investigar las variaciones relativas del módulo elástico, para una señal transito
[CAT] L'assaig de determinació de les freqüències de ressonància ha sigut tradicionalment empleat per a determinar la integritat mecànica de testimonis de formigó, en l'avaluació de la conformitat de mescles de formigó en diversos assajos de durabilitat, i en la terminació de propietats constitutives com són el mòdul elàstic i el factor d'amortiment. Esta tècnica no destructiva ha sigut àmpliament apel·lada per a l'avaluació de les propietats mecàniques en tot tipus d'assajos de durabilitat. L'evolució del dany és comunament avaluada a partir de la reducció del mòdul dinàmic, produït com resultat de qualsevol procés de fisuración. No obstant això, el comportament mecànic del formigó és intrínsecament no lineal i presenta histèresi. Com resultat d'un comportament tensió-deformació amb histèresi, el mòdul elàstic depén de la deformació. En assajos dinàmics, la no linealitat del material es manifesta per una disminució de les freqüències de ressonància, la qual és inversament proporcional a l'amplitud d'excitació. Este fenomen és normalment denominat com a dinàmica ràpida. Una vegada l'excitació cessa, el material experimenta un procés de relaxació pel qual, el mòdul elàstic és restaurat a aquell en situació de repòs. Este fenomen és denominat com a dinàmica lenta. Estos fenòmens --dinámicas ràpida i lenta troben el seu origen en la fricció interna del material. Per tant, en materials basats en ciment, la presència de microfissures i les interfícies entre els seus constituents juguen un rol important en la no linealitat mecànica del material. En el context d'avaluació de la durabilitat del formigó, l'evolució del dany està basada en l'increment d'histèresi, com resultat de qualsevol procés de fisuración. En esta tesi s'investiguen tres tècniques diferents les quals utilitzen l'impacte com a mitjà d'excitació de les freqüències de ressonància. La primera tècnica consistix a determinar les freqüències de ressonància a diferents energies d'impacte. La tècnica és denominada en anglés: Nonlinear Impact Resonant Acoustic Spectroscopy (NIRAS). Esta consistix a relacionar el detriment que el material experimenta en les seues freqüències de ressonància, amb l'augment de l'amplitud de l'excitació. La segona tècnica consistix a investigar el comportament no lineal per mitjà de l'anàlisi del senyal corresponent a un sol impacte. Esta consistix a determinar les propietats instantànies de freqüència, atenuació i amplitud. Esta tècnica es denomina, en anglés, Nonlinear Single Impact Resonant Acoustic Spectroscopy (NSIRAS). Es proposen dos tècniques d'extracció del comportament no lineal per mitjà de l'anàlisi de les variacions instantànies de freqüència i atenuació. La primera tècnica consistix en la discretización de la variació de la freqüència amb el temps, per mitjà d'una anàlisi basat en Short-Time Fourier Transform (STFT). La segona tècnica consistix en un ajust per mínims quadrats dels senyals de vibració a un model que considera les variacions de freqüència i atenuació amb el temps. La tercera tècnica empleada en esta tesi pot ser empleada per a l'avaluació d'estructures in situ. La tècnica es tracta d'un assaig acusto-elástico en règim dinàmic. En anglés Dynamic Acousto-Elastic Test (DAET). Les variacions del mòdul elàstic obtingudes per mitjà dels mètodes NIRAS i NSIRAS proporcionen un comportament mitjà i no permeten derivar les variacions del mòdul elàstic en un sol cicle de vibració. Actualment, la tècnica DAET és l'única que permet investigar tot el rang de fenòmens no lineals en el material. D'altra banda, a diferència d'altres tècniques DAET, en este estudi s'empra com contrast una ona contínua. L'ús d'una ona contínua permet investigar les variacions relatives del mòdul elàstic, per a un senyal transitori. A més, permet la inspecció d'elements per mitjà de l'accés per una sola cara.
Eiras Fernández, JN. (2016). Studies on nonlinear mechanical wave behavior to characterize cement based materials and its durability [Tesis doctoral no publicada]. Universitat Politècnica de València. https://doi.org/10.4995/Thesis/10251/71439
TESIS
Premiado

AbstractThe global aerospace industry is driving a demand for flexible manufacturing systems to accommodate multiple programs with variable capacities within a modular, economical production cell [1]. Traditional manufacturing cells often involve bespoke, monolithic hardware limited to single program use. This inherent restraint results in significant incurred costs and program disruption when reacting to design and capacity changes. This paper describes the development of a reconfigurable panel-indexing cell with a dynamic cost architecture as an alternative approach to established, monolithic tooling structures.

Following the rapid formation of the surface of a surfactant so′′lution, the dynamic interfacial tension falls with time as a result of the finite time needed for surfactant adsorption. Surfaces can either be sheared (involving shape change) or dilated (area is changed), and both these processes can give a viscous and/or elastic response. Usually, surfaces of surfactant solutions exhibit a combination of the two and are viscoelastic. If small sinusoidal area changes are imposed on the surface, changes in tension and area are out of phase because surfactant adsorption is relatively slow. The responses to area change are frequency dependent. The complex dilational viscoelastic modulus, ε‎*, has real (elastic) and imaginary (viscous) parts, ε‎′ and ε‎′′, respectively, whose variation with frequency provides insights into relaxation processes occurring at the surface. The way in which dynamic tensions can give insights into the kinetics of surfactant adsorption is explained.

Nowadays many indentation techniques are being commonly employed for determining some mechanical properties (harness, elastic modulus, toughness, etc.) using simple method of measuring the indentation depth. On the basis of measurement of depth of penetration, indentation technique has be classified into major categories i.e. microindentation and nanoindentation. Nanoindentation technique uses indirect method of determining the contact area as the depth of penetration is measured in nanometers, while in conventional indentation the area in contact is measured by elementary measurement of the residual area after the indenter is removed from the specimen. Dynamic hardness is the best result of dynamic indentation which can be expressed as the ratio of energy consumed during a rapid indentation to the volume of indentation. The parameter which are taken into consideration are indentation depth, contact force, contact area, mean contact pressure.

Electronic modules for a guidance system are mounted in a rack with spring clips resisting motion normal to the printed wiring board (PWB) and an aluminum bar with an elastomer pad keeping the module connected to a backplane. The elastomer pad also resists motion normal to the board. The proper boundary conditions for the spring clips, retention bar, and connector are needed in a finite element model in order to evaluate the shock and vibration transmitted to the module’s electrical components. The finite element model of the module was assembled, and an actual module was tested under random vibration and a 1g sine sweep. The printed wiring board elastic modulus was artificially set higher in the FEM than a measured value to account for the stiffening effect of board components which were omitted from the model. By also choosing the proper boundary conditions to represent the spring clips, retention bars, and backplane connection, the finite element model was able to match the first and second mode frequencies from the hardware test results.

This paper develops governing equations for material strain and tension based on a temperature distribution model when the flexible materials (often called webs) are transported on rollers through heat transfer processes within roll-to-roll (R2R) processing machines. Heat transfer processes are employed widely in R2R systems that contain process operations such as printing, coating, lamination, etc., which require heating/cooling of the moving web material. The heat transfer processes introduce the thermal expansion/contraction of the material and changes in the elastic modulus. Thus, the temperature distribution in the moving material affects the strain distribution in the material. Because of change in strain as well as modulus as a function of temperature, tension in the material resulting from elastic strain is also affected by heating/cooling of the web. To obtain the temperature distribution, two basic heat transfer modes are considered: web wrapped on a heat transfer roller and the web span between two consecutive rollers. The governing equations for strain is then obtained using the law of conservation of mass considering the temperature effects. Subsequently, a governing equation for web tension is obtained by assuming the web is elastic with the modulus varying with temperature; an average modulus is considered for defining the constitutive relation between web strain and tension. Since it is difficult to obtain measurement of tension using load cell rollers within heat transfer processes, a tension observer is designed. To evaluate the developed governing equations, numerical simulations for a single tension zone consisting of a heat transfer roller, a web span, and a driven roller are conducted. Results from these numerical model simulations are presented and discussed.

The flow around an elastic body is treated as a fluid-structure interaction (FSI), numerous fluid-structure coupled problems have been performed. Recently, two-way coupled analysis, which considers the fluid-structure interaction, has been performed extensively. In the present paper, we simulate a flow field around an elastic heaving flat plate with a variable surface shape and various Young’s moduli and perform bi-directional coupling analysis using ANSYS 12.1/ANSYS-CFX 12.1. In the case of the results without projection, the vorticity that grows along the plate surface, rolled up from the trailing edge, and developed in the wake are dependent on Strouhal number, independent of the Young’s modulus. However, in the case of the results with the projections, the vortex behaviors are different with the Young’s modulus. At E = 3.53 [MPa], the projections effect on the vortex behavior and the dynamic thrust exhibit approximately the same tendency with or without a projection. On the other hand, at E = 10.0 [MPa], the projection effect has an impact on the vortex behavior and the dynamic thrust. The vorticity and the dynamic thrust of E = 10.0 [MPa] become smaller than that of E = 3.53 [MPa] because of strong effects from the projections of the heaving elastic plate.

Advanced fiber reinforced composite materials offer substantial advantages over metallic materials for the structural applications subjected to fatigue loading. With the increasing use of these composites, it is required to understand their mechanical response to cyclic loading [1–4]. Our major concern in this work is to macroscopically evaluate the damage development in composites during fatigue loading. For this purpose, we examine what effect the fatigue damage may have on the material properties and how they can be related mathematically to each other. In general, as the damage initiates in composite materials and grows during cyclic loading, material properties such as modulus, residual strength and strain would vary and, in many cases, they may be significantly reduced because of the progressive accumulation of cracks. Therefore, the damage can be characterized by the change in material properties, which is expected to be available for non-destructive evaluation of the fatigue damage development in composites. Here, the tensiontension fatigue tests are firstly conducted on the plain woven fabric carbon fiber composites for different loading levels. In the fatigue tests, the dynamic elastic moduli are measured on real-time, which will decrease with an increasing number of cycles due to the degradation of stiffness. Then, the damage fimction presenting the damage development during fatigue loading is determined from the dynamic elastic moduli thus obtained, from which the damage function is formulated in terms of a number of cycles and an applied loading level. Finally, the damage function is shown to be applied for predicting the remaining fifetime of the CFRP composites subjected to two-stress level fatigue loading.

Abstract An analytical solution to the free vibration of a damped three-layer thick sandwiched cylinder of infinite extend is presented. The constrained layer damping is accomplished by sandwiching a linear viscoelastic material between two isotropic elastic cylinders with the same properties. The governing equation is derived based on elasto-dynamic theory utilizing complex elastic moduli. Dimensionless natural frequencies and modal loss-factors are extracted. Special case for a three-layer sandwiched cylinder with similar elastic properties is considered. The computed dimensionless frequencies are compared with previously established results. The comparison indicates the validity of the proposed mathematical procedures. In addition, the effects of various values of material damping for the core layer and ratio of the core shear modulus to the shear modulus of the elastic cylinders on natural frequencies and modal loss-factors are studied. For a given configuration, modal information for the first two modes for n = 0, 1, 2, 3 and 4 are presented for a wide range of core material damping and G2/G1 ratio.

The dynamic response of an adhesively patched repaired composite beam under a harmonic peeling load was obtained theoretically and experimentally. In the theoretical part, dynamic responses of the repaired composite beams were obtained by modeling the parent beam as the Euler-Bernouli beam and the repaired patch as the Euler-Bernouli beam supported on a viscoelastic foundation, which resist both peeling and shear stresses. Both axial and transverse displacements were considered in deriving the coupled equations of motion. The effects of the adhesive loss factor, as well as its elastic modulus on the vibrational behavior of the repaired composite beams were investigated theoretically. In addition, finite element modal analyses were performed to justify the results of the proposed theoretical model. In the experimental part, unidirectional fiberglass reinforced epoxy composite specimens with various repaired patch length, thickness and material properties were manufactured. The patch section was either the fiberglass epoxy or E-glass fiber reinforced composites with various ply sequences. Patches were bonded to the composite beam using an epoxy. The system response was measured by the hammer test technique using a non-contact laser vibrometer. The resonant frequencies and damping ratio of the specimens were evaluated from the dynamic response of the composite beam and the results were compared to that of the theoretical and finite element analyses. The results showed that the dynamic response of the repaired composite depended on the adhesive elastic modulus. For the composite repaired with a high adhesive elastic modulus, the beam may act as a classical Euler-Bernouli composite beam. For the composite patched with a low elastic modulus adhesive, the first resonant frequency of the system may decrease up to 22%. In contrast, the natural frequencies may not significantly change having used adhesive with a high elastic modulus.

This article presents the investigation of the dynamic behavior of the cytoskeleton of live human cells, enabled by a recently-developed control-based approach on scanning probe microscope (SPM). Mechanical behaviors of live cells play an important role in various cell physiological and pathological activities, and have been studied via various techniques and approaches. Studies of evolutions of mechanical properties of live cell, however, are still rather limited and scarce, due to the limitations of current instruments including SPM for single cellular measurements. Particularly, currently nanomechanical measurements using SPM is too slow to excite the mechanical behavior and then measure the corresponding response of life biological species over a large frequency range (broadband). Moreover, large uncertainty is induced in the in-liquid nanomechanical measurement using SPM, as in the indentation quantification, the effects of the acceleration force from the cantilever motion and the hydrodynamic force are not accounted for. The main contribution of this article is the use of a control-based nanomechanical protocol to interrogate the viscoelasticity oscillation of live human prostate cancer cell (PC-3 cells) and its dependence on myosin activities. The experiment results show that as the oscillation of static elastic modulus reported earlier in the literature, the oscillation of dynamic viscoelastic modulus measured is also periodic with a 200-second period. Moreover, as the elastic modulus oscillation, both the amplitude and the period of the viscoelasticity oscillation also strongly depend on the myosin activities, and closely regulated by the calcium density of the cytoskeleton.