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Journal articles on the topic 'Electrochemistry Experiments'

Author: Grafiati

Published: 4 June 2021

Last updated: 1 February 2022

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1

Ibáñez Cornejo, Jorge G. "Electrochemistry for environmental remediation. Laboratory experiments." Educación Química 17, no. 4e (2018): 274. http://dx.doi.org/10.22201/fq.18708404e.2006.4e.66015.

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<span>Muchos contaminantes pueden convertirse en especies menos peligrosas mediante una transferencia de electrones. Estas transferencias pueden llevarse a cabo en interfases electrificadas (electrodos), ser directas o indirectas, oxidaciones o reducciones, usarse para tratar líquidos, gases, suelos, etc. En este artículo discutimos algunas aplicaciones y experimentos.</span>

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2

Eggen, Per-Odd. "Current Chemistry, Experiments and practice in Electrochemistry Education." Nordic Studies in Science Education 7, no. 1 (2012): 101. http://dx.doi.org/10.5617/nordina.329.

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3

Santos, Diogo M. F., Rui F. M. Lobo, and César A. C. Sequeira. "On the Features of Ultramicroelectrodes." Defect and Diffusion Forum 273-276 (February 2008): 602–7. http://dx.doi.org/10.4028/www.scientific.net/ddf.273-276.602.

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Ultramicroelectrodes offer several unique characteristics which enable new types of electrochemical measurements. These include: 1) small size; 2) minimisation of iR effects; 3) rapid response; and 4) steady-state response at moderate times. These features enable experiments as diverse as in vivo electrochemistry, electrochemistry in pharmacology, nanoelectrochemistry, electrochemistry in solvents such as benzene, microsecond electrochemistry, and flow-rate independent electrochemistry. Thus, it is apparent that the use of ultramicroelectrodes has become a rapidly growing area of interest. In

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4

Kumar, Anup, Prakash Mondal, and Claudio Fontanesi. "Chiral Magneto-Electrochemistry." Magnetochemistry 4, no. 3 (2018): 36. http://dx.doi.org/10.3390/magnetochemistry4030036.

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Magneto-electrochemistry (MEC) is a unique paradigm in science, where electrochemical experiments are carried out as a function of an applied magnetic field, creating a new horizon of potential scientific interest and technological applications. Over time, detailed understanding of this research domain was developed to identify and rationalize the possible effects exerted by a magnetic field on the various microscopic processes occurring in an electrochemical system. Notably, until a few years ago, the role of spin was not taken into account in the field of magneto-electrochemistry. Remarkably

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5

Peroff, A. G., E. Weitz, and R. P. Van Duyne. "Mechanistic studies of pyridinium electrochemistry: alternative chemical pathways in the presence of CO2." Physical Chemistry Chemical Physics 18, no. 3 (2016): 1578–86. http://dx.doi.org/10.1039/c5cp04757a.

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Pyridinium has been described as a catalyst for CO<sub>2</sub> reduction, however with low faradaic efficiency. This article discusses a series of electrochemistry experiments to study other chemical processes occurring during pyridinium electrochemistry which might provide insight into the low faradaic efficiency.

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6

Rieker, A., B. Speiser, K. M. Mangold, and M. Hanack. "Notizen: Potential Error Sources in Combined Electrochemistry/Neutron Detection Experiments." Zeitschrift für Naturforschung B 46, no. 8 (1991): 1125–26. http://dx.doi.org/10.1515/znb-1991-0826.

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Recently, experimental evidence for the occurrence of electrochemically induced (“cold”) nuclear fusion of deuterium nuclei has been proposed by several groups [1-3]. In particular, increased neutron counts and excess heat production of the electrolytic cell have been reported. Although much debated, the results have neither been proven nor refuted unequivocally [4].

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7

Supasorn, Saksri. "Grade 12 students' conceptual understanding and mental models of galvanic cells before and after learning by using small-scale experiments in conjunction with a model kit." Chemistry Education Research and Practice 16, no. 2 (2015): 393–407. http://dx.doi.org/10.1039/c4rp00247d.

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This study aimed to develop the small-scale experiments involving electrochemistry and the galvanic cell model kit featuring the sub-microscopic level. The small-scale experiments in conjunction with the model kit were implemented based on the 5E inquiry learning approach to enhance students' conceptual understanding of electrochemistry. The research tools consisted of (1) four small-scale experiments involving electrochemistry, which were oxidation and reduction reactions, galvanic cells, cathodic protection of iron nails, and connecting batteries in series, and (2) the galvanic cell model ki

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8

Saxena, Sachin, and Soami P. Satsangee. "Offering Remotely Triggered, Real-Time Experiments in Electrochemistry for Distance Learners." Journal of Chemical Education 91, no. 3 (2014): 368–73. http://dx.doi.org/10.1021/ed300349t.

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9

Broch, Laurent, Luc Johann, Nicolas Stein, Alexandre Zimmer, and Raphaël Beck. "Real time in situ ellipsometric and gravimetric monitoring for electrochemistry experiments." Review of Scientific Instruments 78, no. 6 (2007): 064101. http://dx.doi.org/10.1063/1.2743273.

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10

Kwon, Seong Jung, Hongjun Zhou, Fu-Ren F. Fan, Vasily Vorobyev, Bo Zhang, and Allen J. Bard. "Stochastic electrochemistry with electrocatalytic nanoparticles at inert ultramicroelectrodes—theory and experiments." Physical Chemistry Chemical Physics 13, no. 12 (2011): 5394. http://dx.doi.org/10.1039/c0cp02543g.

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11

Widmer, R., and H. Siegenthaler. "Nanostructuring experiments in the system Ag(111)/Pb2+." Electrochemistry Communications 7, no. 4 (2005): 421–26. http://dx.doi.org/10.1016/j.elecom.2005.02.020.

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12

Vesztergom, S., N. Barankai, N. Kovács, et al. "Electrical cross-talk in rotating ring–disk experiments." Electrochemistry Communications 68 (July 2016): 54–58. http://dx.doi.org/10.1016/j.elecom.2016.04.012.

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13

Mani, Ali, and Karen May Wang. "Electroconvection Near Electrochemical Interfaces: Experiments, Modeling, and Computation." Annual Review of Fluid Mechanics 52, no. 1 (2020): 509–29. http://dx.doi.org/10.1146/annurev-fluid-010719-060358.

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Many electrochemical and microfluidic systems involve voltage-driven transport of ions from a fluid electrolyte toward an ion-selective interface. These systems are governed by intimate coupling between fluid flow, mass transport, and electrostatic effects. When counterions are driven toward a selective interface, this coupling is shown to lead to a hydrodynamic instability called electroconvection. This phenomenon is an example of electrochemistry inducing flow, which in turn affects the transport and ohmic resistance of the bulk electrolyte. These effects have implications in a wide range of

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14

Li, Ru Yin, Guo Rong Tan, Wen Juan Chen, and Jian Zhang. "The Electrochemistry Treatment on Fracturing Sewage of Oilfield." Advanced Materials Research 726-731 (August 2013): 1981–84. http://dx.doi.org/10.4028/www.scientific.net/amr.726-731.1981.

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The treatment of fracturing fluid sewage of oilfield must be accomplished in short time and high efficiency, with no secondary pollution. No proven technique of oilfield could be used for reference. In this work, suitable electrodes are selected for the method of electrochemistry oxidation; the data of experiments has confirmed COD of sewage could be easily decreased.

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15

Martinez, J. G., and T. F. Otero. "Structural electrochemistry. Chronopotentiometric responses from rising compacted polypyrrole electrodes: experiments and model." RSC Adv. 4, no. 55 (2014): 29139–45. http://dx.doi.org/10.1039/c4ra04530k.

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16

Eggen, Per-Odd, Lise Kvittingen, Annette Lykknes, and Roland Wittje. "Reconstructing Iconic Experiments in Electrochemistry: Experiences from a History of Science Course." Science & Education 21, no. 2 (2011): 179–89. http://dx.doi.org/10.1007/s11191-010-9316-1.

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17

Oltra, R., B. Vuillemin, F. Thebault, and F. Rechou. "Effect of the surrounding aeration on microcapillary electrochemical cell experiments." Electrochemistry Communications 10, no. 6 (2008): 848–50. http://dx.doi.org/10.1016/j.elecom.2008.03.014.

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18

Crooks, Richard M. "Concluding remarks: single entity electrochemistry one step at a time." Faraday Discussions 193 (2016): 533–47. http://dx.doi.org/10.1039/c6fd00203j.

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This article provides a summary of the Faraday Discussion on single entity electrochemistry held in York, U.K., in early September, 2016. The introduction provides some context for thinking about electrochemical studies of single entities. The next four sections follow the themes of the meeting as they relate to single-entity electrochemistry: (1) nanoparticles, nanotubes, and nanowires; (2) nanopores and nanofluidics; (3) complex surfaces and reactions at the nanoscale; and (4) molecular electroanalysis. Each paper presented at the Discussion is summarized, and some personal thoughts as to th

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19

Vesztergom, S., M. Ujvári, and G. G. Láng. "RRDE experiments with potential scans at the ring and disk electrodes." Electrochemistry Communications 13, no. 4 (2011): 378–81. http://dx.doi.org/10.1016/j.elecom.2011.01.032.

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20

EFTEKHARI, ALI, MAHMOOD KAZEMZAD, and MANSOOR KEYANPOUR-RAD. "A PRACTICAL APPROACH FOR SENSING SURFACE NANOSTRUCTURES IN ELECTROCHEMICAL EXPERIMENTS." Surface Review and Letters 13, no. 05 (2006): 703–10. http://dx.doi.org/10.1142/s0218625x06008694.

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Fractal analysis of electrode surfaces by means of electrochemical techniques is an efficient tool to reveal surface structures via a geometrical model. Since this is based on the concept of "diffusion toward electrode surfaces", detectable scale depends on the diffusion coefficient, and it is in the range of 1–100 μm for conventional electrochemistry. By taking this issue into account, a simple approach is proposed to perform fractal analysis at nanoscale, which is an important requirement in surface studies. Increasing the electrolyte viscosity and decreasing the environment temperature lead

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21

Nouraei, S., and S. Roy. "Design of experiments in electrochemical microfabrication." Electrochimica Acta 54, no. 9 (2009): 2444–49. http://dx.doi.org/10.1016/j.electacta.2008.11.058.

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22

Marken, Frank, and Richard G. Compton. "Electrochemistry in the presence of ultrasound: the need for bipotentiostatic control in sonovoltammetric experiments." Ultrasonics Sonochemistry 3, no. 2 (1996): S131—S134. http://dx.doi.org/10.1016/1350-1477(96)00005-x.

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23

Khene, Samson, Kevin Lobb, and Tebello Nyokong. "Interaction between nickel hydroxy phthalocyanine derivatives with p-chlorophenol: Linking electrochemistry experiments with theory." Electrochimica Acta 56, no. 2 (2010): 706–16. http://dx.doi.org/10.1016/j.electacta.2010.10.007.

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24

Nikolelis, Dimitrios P., Christina G. Siontorou, Vangelis G. Andreou, and Ulrich J. Krull. "Stabilized bilayer lipid membranes for flow-through experiments." Electroanalysis 7, no. 6 (1995): 531–36. http://dx.doi.org/10.1002/elan.1140070605.

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25

Sun, Qi Lei, Ze Rui Liu, Ji Liang Liu, Chong Fang, and Qing Nan Zhang. "Investigation on Electrochemistry Behavior of Fe-Cr-Ni Alloy in Caustic Solution." Advanced Materials Research 941-944 (June 2014): 1402–5. http://dx.doi.org/10.4028/www.scientific.net/amr.941-944.1402.

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Electrochemistry experiments such as polarization curve and alternating-current impedance are adopted to study the electrochemistry behavior of Fe-Cr-Ni alloy (Inconel 690 alloy) in the caustic solution of 50% NaOH +0.3%SiO2+0.3%Na2S2O3. The results show that Inconel 690 alloy appears two anodic passivation areas, the passivation of the alloy elements Cr and Ni mainly contributes to the lower potential passivation area and the higher potential passivation area is mainly attributed to the passivation effect of the alloy elements Fe and Ni, especially the later. When Na2S2O is added into the hig

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26

Knehr, K. W., and E. C. Kumbur. "Open circuit voltage of vanadium redox flow batteries: Discrepancy between models and experiments." Electrochemistry Communications 13, no. 4 (2011): 342–45. http://dx.doi.org/10.1016/j.elecom.2011.01.020.

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27

Hassissene, S., E. Chainet, and B. Nguyen. "Corrosion potential analysis during electrochemical cementation experiments." Electrochimica Acta 39, no. 1 (1994): 151–53. http://dx.doi.org/10.1016/0013-4686(94)85022-4.

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28

Bernhardt, Paul V. "Enzyme Electrochemistry — Biocatalysis on an Electrode." Australian Journal of Chemistry 59, no. 4 (2006): 233. http://dx.doi.org/10.1071/ch05340.

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Oxidoreductase enzymes catalyze single- or multi-electron reduction/oxidation reactions of small molecule inorganic or organic substrates, and they are integral to a wide variety of biological processes including respiration, energy production, biosynthesis, metabolism, and detoxification. All redox enzymes require a natural redox partner such as an electron-transfer protein (e.g. cytochrome, ferredoxin, flavoprotein) or a small molecule cosubstrate (e.g. NAD(P)H, dioxygen) to sustain catalysis, in effect to balance the substrate/product redox half-reaction. In principle, the natural electron-

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29

Zhou, Yiqi, and Dirk Lars Engelberg. "Fast testing of ambient temperature pitting corrosion in type 2205 duplex stainless steel by bipolar electrochemistry experiments." Electrochemistry Communications 117 (August 2020): 106779. http://dx.doi.org/10.1016/j.elecom.2020.106779.

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30

Lussier, Félix, Thibault Brulé, Marie-Josée Bourque, Charles Ducrot, Louis-Éric Trudeau, and Jean-François Masson. "Dynamic SERS nanosensor for neurotransmitter sensing near neurons." Faraday Discussions 205 (2017): 387–407. http://dx.doi.org/10.1039/c7fd00131b.

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Current electrophysiology and electrochemistry techniques have provided unprecedented understanding of neuronal activity. However, these techniques are suited to a small, albeit important, panel of neurotransmitters such as glutamate, GABA and dopamine, and these constitute only a subset of the broader range of neurotransmitters involved in brain chemistry. Surface-enhanced Raman scattering (SERS) provides a unique opportunity to detect a broader range of neurotransmitters in close proximity to neurons. Dynamic SERS (D-SERS) nanosensors based on patch-clamp-like nanopipettes decorated with gol

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31

Cummings, Charles Y., Gary A. Attard, John M. Mitchels, and Frank Marken. "Surface State Trapping and Mobility Revealed by Junction Electrochemistry of Nano-Cr2O3." Australian Journal of Chemistry 65, no. 1 (2012): 65. http://dx.doi.org/10.1071/ch11382.

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Hydrous chromium oxide nanoparticles (~15 nm diameter) are assembled from a colloidal solution onto tin-doped indium oxide (ITO) substrates by layer-by-layer electrostatic deposition with aqueous carboxymethyl-cellulose sodium salt binder. Calcination produces purely inorganic mesoporous films (average thickness increase per layer of 1 nm) of chromia Cr2O3. When immersed in aqueous carbonate buffer at pH 10 and investigated by cyclic voltammetry, a chemically reversible oxidation is observed because of a conductive layer at the chromia surface (formed during initial potential cycling). This is

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32

Strutwolf, JÖRg, and Wolfgang W. Schoeller. "Digital simulation of potential step experiments using the extrapolation method." Electroanalysis 9, no. 18 (1997): 1403–8. http://dx.doi.org/10.1002/elan.1140091806.

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33

Li, Jie Lan, Cheng Hao Liang, and Nai Bao Huang. "The Electrochemistry Behaviour of Carbon Steel in 55% LiBr Solution with A-Mo Inhibitor." Advanced Materials Research 881-883 (January 2014): 1280–87. http://dx.doi.org/10.4028/www.scientific.net/amr.881-883.1280.

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The inhibition effects of A-Mo inhibitor on corrosion of carbon steel in 55% LiBr solution were investigated using cyclic potentiodynamic polarization curves EIS experiments, Mott-Schottky analysis, SEM, EDAX and XRD methods. The results revealed that A-Mo inhibitor was capable of inhibiting the corrosion of carbon steel in 55%LiBr solution, exhibiting high inhibition efficiencies around 99.7%. A-Mo inhibitor promoted the formation of a protective passive film composed of Fe, Mo and O elements. The passive film improved the electrochemistry performance and enhanced corrosion resistance of carb

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34

Habrioux, Aurélien, Seydou Hebié, Teko W. Napporn, Julie Rousseau, Karine Servat, and K. Boniface Kokoh. "One-Step Synthesis of Clean and Size-Controlled Gold Electrocatalysts: Modeling by Taguchi Design of Experiments." Electrocatalysis 2, no. 4 (2011): 279–84. http://dx.doi.org/10.1007/s12678-011-0064-z.

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35

Richtering, Werner, and Karl Doblhofer. "Effect of uncompensated resistance on large-amplitude chronoamperometric experiments." Electrochimica Acta 34, no. 12 (1989): 1685–88. http://dx.doi.org/10.1016/0013-4686(89)85049-2.

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36

Ciani, Ilenia, Salvatore Daniele, Carlo Bragato, and M. Antonietta Baldo. "Stability of mercury-coated platinum microelectrodes upon touching a solid surface in scanning electrochemical microscopy (SECM) experiments." Electrochemistry Communications 5, no. 4 (2003): 354–58. http://dx.doi.org/10.1016/s1388-2481(03)00068-7.

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37

Gebhardt, Olaf. "A phase reference procedure for interpretation of impedance spectroscopy experiments." Electrochimica Acta 38, no. 5 (1993): 633–41. http://dx.doi.org/10.1016/0013-4686(93)80231-n.

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38

Justin, Gusphyl, Abdur Rub Abdur Rahman, and Anthony Guiseppi-Elie. "Bioactive Hydrogel Layers on Microdisk Electrode Arrays: Cyclic Voltammetry Experiments and Simulations." Electroanalysis 21, no. 10 (2009): 1125–34. http://dx.doi.org/10.1002/elan.200804548.

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39

Khramov, A. P., A. A. Chernyshev, A. V. Isakov, and Yu P. Zaykov. "Secondary Reduction of Refractory Metal near the Smooth Cathode during Molten Salt Electrolysis. 2. Calculations for Some Hypothetical Experiments." Russian Journal of Electrochemistry 56, no. 9 (2020): 709–14. http://dx.doi.org/10.1134/s1023193520090062.

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40

Li, Dong, Delin Sun, Siyang Hu, Jing Hu, and Xingzhong Yuan. "Conceptual design and experiments of electrochemistry-flushing technology for the remediation of historically Cr(Ⅵ)-contaminated soil." Chemosphere 144 (February 2016): 1823–30. http://dx.doi.org/10.1016/j.chemosphere.2015.09.077.

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41

Chang, Hasok. "How Historical Experiments Can Improve Scientific Knowledge and Science Education: The Cases of Boiling Water and Electrochemistry." Science & Education 20, no. 3-4 (2010): 317–41. http://dx.doi.org/10.1007/s11191-010-9301-8.

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42

Sagandykova, Gulyaim, Justyna Walczak-Skierska, Fernanda Monedeiro, Paweł Pomastowski, and Bogusław Buszewski. "New Methodology for the Identification of Metabolites of Saccharides and Cyclitols by Off-Line EC-MALDI-TOF-MS." International Journal of Molecular Sciences 21, no. 15 (2020): 5265. http://dx.doi.org/10.3390/ijms21155265.

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A combination of electrochemistry (EC) and matrix-assisted laser desorption/ionization time-of-flight mass spectrometry (off-line EC-MALDI-TOF-MS) was applied for determination of the studied biologically active compounds (D-glucose, D-fructose, D-galactose, D-pinitol, L-chiro-inositol, and myo-inositol) and their possible electrochemical metabolites. In this work, boron-doped diamond electrode (BDD) was used as a working electrode. MALDI-TOF-MS experiments were carried out (both in positive and negative ion modes and using two matrices) to identify the structures of electrochemical products.

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43

Bampos, Georgios, Athanasia Petala, and Zacharias Frontistis. "Recent Trends in Pharmaceuticals Removal from Water Using Electrochemical Oxidation Processes." Environments 8, no. 8 (2021): 85. http://dx.doi.org/10.3390/environments8080085.

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Nowadays, the research on the environmental applications of electrochemistry to remove recalcitrant and priority pollutants and, in particular, drugs from the aqueous phase has increased dramatically. This literature review summarizes the applications of electrochemical oxidation in recent years to decompose pharmaceuticals that are often detected in environmental samples such as carbamazapine, sulfamethoxazole, tetracycline, diclofenac, ibuprofen, ceftazidime, ciprofloxacin, etc. Similar to most physicochemical processes, efficiency depends on many operating parameters, while the combination

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44

Kreysa, G., G. Marx, and W. Plieth. "A critical analysis of electrochemical nuclear fusion experiments." Journal of Electroanalytical Chemistry and Interfacial Electrochemistry 266, no. 2 (1989): 437–50. http://dx.doi.org/10.1016/0022-0728(89)85087-9.

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45

Wu, Wei Ming, Ding Li, and Hai Yan Du. "The Effect of Corrosion Inhibitor in Hydrofluoric Acid Medium." Advanced Materials Research 750-752 (August 2013): 2258–62. http://dx.doi.org/10.4028/www.scientific.net/amr.750-752.2258.

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The experiments were done to find some good corrosion inhibitors for mild steel in 5% HF solution by the method of weight loss and electrochemistry including polarization curves and electrochemical impedance spectroscopy (EIS). Results show that the thiourea, potassium thiocyanate, and hexamethylenetetramine have good inhibition effect for mild steel in 5% HF solution, especially potassium thiocyanate and thiourea. Their corrosion resistance was greatly enhanced in the presence of tested inhibitor. Thiourea is an anodic type inhibitor and its inhibition efficiencies up to 99.88% can be obtaine

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46

Bandookwala, Maria, Kavya Sri Nemani, Bappaditya Chatterjee, and Pinaki Sengupta. "Reactive Metabolites: Generation and Estimation with Electrochemistry Based Analytical Strategy as an Emerging Screening Tool." Current Analytical Chemistry 16, no. 7 (2020): 811–25. http://dx.doi.org/10.2174/1573411016666200131154202.

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Background: Analytical scientists have constantly been in search for more efficient and economical methods for drug simulation studies. Owing to great progress in this field, there are various techniques available nowadays that mimic drug metabolism in the hepatic microenvironment. The conventional in vitro and in vivo studies pose inherent methodological drawbacks due to which alternative analytical approaches are devised for different drug metabolism experiments. Methods: Electrochemistry has gained attention due to its benefits over conventional metabolism studies. Because of the protein bi

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47

Spring, Sam A., Sean Goggins, and Christopher G. Frost. "Ratiometric Electrochemistry: Improving the Robustness, Reproducibility and Reliability of Biosensors." Molecules 26, no. 8 (2021): 2130. http://dx.doi.org/10.3390/molecules26082130.

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Electrochemical biosensors are an increasingly attractive option for the development of a novel analyte detection method, especially when integration within a point-of-use device is the overall objective. In this context, accuracy and sensitivity are not compromised when working with opaque samples as the electrical readout signal can be directly read by a device without the need for any signal transduction. However, electrochemical detection can be susceptible to substantial signal drift and increased signal error. This is most apparent when analysing complex mixtures and when using small, si

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48

Barbero, C., M. C. Miras, and R. Kötz. "Electrochemical mass transport studied by probe beam deflection: potential step experiments." Electrochimica Acta 37, no. 3 (1992): 429–37. http://dx.doi.org/10.1016/0013-4686(92)87032-u.

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49

Hodgetts, Rebecca Y., Hoang‐Long Du, Douglas R. MacFarlane, and Alexandr N. Simonov. "Electrochemically Induced Generation of Extraneous Nitrite and Ammonia in Organic Electrolyte Solutions During Nitrogen Reduction Experiments." ChemElectroChem 8, no. 9 (2021): 1596–604. http://dx.doi.org/10.1002/celc.202100251.

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50

Palleschi, G., M. Mascini, L. Bernardi, G. Bombardieri, and A. M. De Luca. "Glucose Clamp Experiments With Electrochemical Biosensors." Analytical Letters 22, no. 5 (1989): 1209–20. http://dx.doi.org/10.1080/00032718908051401.

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