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Journal articles on the topic 'Electrosynthesis'

Author: Grafiati

Published: 4 June 2021

Last updated: 25 July 2025

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1

Chen, Po-Yu, Meng-Yang Chang, Chieh-Kai Chan та Nai-Chang Lo. "An Efficient Organic Electrosynthesis of β-Hydroxysulfones". Synthesis 28, № 19 (2017): 4469–77. http://dx.doi.org/10.1055/s-0036-1589051.

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An efficient organic electrosynthesis of tertiary β-hydroxysulfones from functionalized α-methylstyrenes with substituted sodium sulfinates has been established. The novel electrosynthetic method provided the desired products in excellent yields, and the key structure was confirmed by X-ray single-crystal diffraction analysis.

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2

Waldvogel, Siegfried R. "Cathodic Oxidation of Alkanes Using Molecular Oxygen." ECS Meeting Abstracts MA2023-01, no. 41 (2023): 2331. http://dx.doi.org/10.1149/ma2023-01412331mtgabs.

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The electrochemical conversion of less activated substrates provides an attractive approach to convert such substances into valuable intermediates. Electrosynthesis represents a future technology, which is characterized by its outstanding sustainability.[1] A new way is presented to electrochemically convert alkanes and alkenes into the oxygenated species by cathodically activated molecular oxygen. This method allows the use to side streams in industry and substitutes conventional techniques which rely on the use of fuming nitric acid. Consequently, electrosynthesis will contribute to less cli

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3

Lin, Song. "Reductive Electrosynthesis." ECS Meeting Abstracts MA2021-01, no. 42 (2021): 1735. http://dx.doi.org/10.1149/ma2021-01421735mtgabs.

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4

Debabov, V. G. "Microbial Electrosynthesis." Biotekhnologiya, no. 3 (2017): 9–28. http://dx.doi.org/10.21519/0234-2758-2017-33-3-9-28.

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5

Debabov, V. G. "Microbial Electrosynthesis." Applied Biochemistry and Microbiology 53, no. 9 (2017): 842–58. http://dx.doi.org/10.1134/s0003683817090034.

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6

Francke, Robert, R. Daniel Little, and Shinsuke Inagi. "Organic Electrosynthesis." ChemElectroChem 6, no. 16 (2019): 4065–66. http://dx.doi.org/10.1002/celc.201901175.

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7

Minteer, Shelley D. "Enzymatic Bioelectrocatalysis for Organic Electrosynthesis." ECS Meeting Abstracts MA2023-02, no. 52 (2023): 2484. http://dx.doi.org/10.1149/ma2023-02522484mtgabs.

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Organic electrosynthesis has become a popular research area in the last decade due to a desire for more sustainable and greener organic synthesis methods. However, electrosynthesis frequently has challenges with selectivity. This talk will detail the design of bioelectrocatalytic systems for organic electrosynthesis with a focus on improving the selectivity and efficiency of electrosynthesis systems. Specifically, the talk will describe bioelectrocatalytic systems for C-H activation and chiral synthesis. It will discuss both materials design of electrodes and enzyme design for electrochemistry

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8

Blanco, Daniela E., Bryan Lee, and Miguel A. Modestino. "Optimizing organic electrosynthesis through controlled voltage dosing and artificial intelligence." Proceedings of the National Academy of Sciences 116, no. 36 (2019): 17683–89. http://dx.doi.org/10.1073/pnas.1909985116.

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Organic electrosynthesis can transform the chemical industry by introducing electricity-driven processes that are more energy efficient and that can be easily integrated with renewable energy sources. However, their deployment is severely hindered by the difficulties of controlling selectivity and achieving a large energy conversion efficiency at high current density due to the low solubility of organic reactants in practical electrolytes. This control can be improved by carefully balancing the mass transport processes and electrocatalytic reaction rates at the electrode diffusion layer throug

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9

Nur, Adrian, Arif Jumari, Anatta W. Budiman, et al. "The Current Density on Electrosynthesis of Hydroxyapatite with Bipolar Membrane." MATEC Web of Conferences 156 (2018): 05015. http://dx.doi.org/10.1051/matecconf/201815605015.

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Synthesis of hydroxyapatite by electrochemical method was has been successfully done. The novelty of this research is used of the bipolar membrane to separate electrolysis chamber. The bipolar membrane is used to keep the cations still around the cathode and react to form hydroxyapatite. The aim of this paper was to compare the current density on electrosynthesis of hydroxyapatite with and without bipolar membrane and the effect of current density on electrosynthesis. The electrosynthesis was performed at 2 hours at 400 to 600 mA/cm2 at room temperature. The bigger the current density, the mor

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10

Tran Thi, Luyen, Benjamin Schille, and Robert Francke. "PolyTEMPO electrocatalyst for organic electrosynthesis of benzonitrile from benzyl alcohol." Vietnam Journal of Catalysis and Adsorption 10, no. 1 (2021): 93–97. http://dx.doi.org/10.51316/jca.2021.015.

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Requirements for using Poly (2,2,6,6-tetramethylpiperidinyloxy-4-yl methacrylate) (PolyTEMPO) as an electrocatalyst for the organic electrosynthesis of benzonitrile from benzyl alcohol were investigated. The research results indicated that PolyTEMPO expressed catalytic activity in the electrosynthesis of benzonitrile from benzyl alcohol in the presence of ammonium acetate. The electrosynthesis yield of benzonitrile from benzyl alcohol with PolyTEMPO catalyst reached the maximum value at 35 °C after 18 hours.

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11

Marshall, Christopher W., Daniel E. Ross, Erin B. Fichot, R. Sean Norman, and Harold D. May. "Electrosynthesis of Commodity Chemicals by an Autotrophic Microbial Community." Applied and Environmental Microbiology 78, no. 23 (2012): 8412–20. http://dx.doi.org/10.1128/aem.02401-12.

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ABSTRACTA microbial community originating from brewery waste produced methane, acetate, and hydrogen when selected on a granular graphite cathode poised at −590 mV versus the standard hydrogen electrode (SHE) with CO2as the only carbon source. This is the first report on the simultaneous electrosynthesis of these commodity chemicals and the first description of electroacetogenesis by a microbial community. Deep sequencing of the active community 16S rRNA revealed a dynamic microbial community composed of an invariantArchaeapopulation ofMethanobacteriumspp. and a shiftingBacteriapopulation.Acet

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12

Ahumada, Guillermo, Malin Lill, Julius Kuzmin, Ellymay Goossens, Astrid Steffensen, and Helena Lundberg. "Tetrabutylammonium Borohydride: A Sacrificial Reductant in Organic Electrosynthesis." ECS Meeting Abstracts MA2023-02, no. 53 (2023): 3368. http://dx.doi.org/10.1149/ma2023-02533368mtgabs.

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In this work, tetrabutylammonium borohydride (TBAB) is investigated as a terminal reductant in reductive organic electrosynthesis as replacement for sacrificial anodes. Sacrificial anodes are typically based on easily oxidized metals, such as Mg, Zn, or Al, and are consumed during the reaction, resulting in stoichiometric metal waste. In contrast, oxidation of TBAB enables the use of inert anodes and results in anodic H2 formation, effectively serving as the inverse of cathodic proton reduction. Our results indicate that TBAB oxidation at carbon-based electrodes can replace the use of sacrific

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13

Atobe, Mahito, and Naoki Shida. "Novel Electrocatalytic Hydrogenation Using a Solid Polymer Electrolyte (SPE) Reactor." ECS Meeting Abstracts MA2024-01, no. 41 (2024): 2343. http://dx.doi.org/10.1149/ma2024-01412343mtgabs.

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Organic electrosynthetic reactions, which are driven by electricity, can generally be carried out under mild conditions (room temperature and ambient pressure). In addition, they do not require any hazardous reagents and produce less waste than other conventional chemical syntheses. Therefore, electrosynthesis is known to be a mild and clean method for organic synthesis and there has recently been renewed interest in its development. However, electrosynthesis also has some disadvantages. Ordinary chemical reactions are homogeneous, while the reaction field of electrolysis is a heterogeneous in

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14

Babayev, Aziz, Giyosbek Xasanov, and Orifjon Kilichov. "Method for increasing the efficiency of ozone electrosynthesis process with periodic voltage pulses." E3S Web of Conferences 377 (2023): 01003. http://dx.doi.org/10.1051/e3sconf/202337701003.

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This article presents the results of a scientific study to improve the efficiency of ozone electrosynthesis. The issues of applying another voltage as a periodic voltage pulse are considered. The analysis of the process of electrosynthesis of ozone when fed with periodic high-voltage pulses is given, as a result of which the stability of discharges in the discharge gap was achieved. Transient processes in the discharge gap in the pause between voltage pulses are considered. The results of studies of the energy indicators of pulsed and sinusoidal voltages are also presented. Where the analysis

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15

Hacku, Robert, James McKone, Tyler Petek, Glenn Cormack, and Elisa Seddon. "Building Electrochemical Roadmaps for Decarbonization in the Specialty Chemical Sector." ECS Meeting Abstracts MA2024-01, no. 56 (2024): 2976. http://dx.doi.org/10.1149/ma2024-01562976mtgabs.

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Greenhouse gas emissions from the chemical manufacturing industry are enormous, by some estimates they amount to 5% percent of the global total.1,2 Moreover, chemical manufacturing is widely considered as a “difficult-to-decarbonize” sector due to the deeply entrenched reliance on crude-based hydrocarbons as fuels and feedstocks.3 The ultimate goal of eliminating anthropogenic greenhouse gas emissions, clearly demands a wholesale reconsideration of energy and material flows in chemical manufacturing. One area of research that has gained momentum in the past decade is the use of electrochemistr

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16

Lin, Honghong, Kecheng Wei, Zhouyang Yin, and Shouheng Sun. "Nanocatalysts in electrosynthesis." iScience 24, no. 3 (2021): 102172. http://dx.doi.org/10.1016/j.isci.2021.102172.

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17

Waldvogel, Siegfried R. "Electrosynthesis and electrochemistry." Beilstein Journal of Organic Chemistry 11 (June 2, 2015): 949–50. http://dx.doi.org/10.3762/bjoc.11.105.

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18

Pickett, Christopher J., and Jean Talarmin. "Electrosynthesis of ammonia." Nature 317, no. 6038 (1985): 652–53. http://dx.doi.org/10.1038/317652a0.

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19

Batanero, Belen, and Fructuoso Barba. "Electrosynthesis of tryptanthrin." Tetrahedron Letters 47, no. 47 (2006): 8201–3. http://dx.doi.org/10.1016/j.tetlet.2006.09.130.

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20

Rahman, Muhammad H., Mandeep K. Bal, and Alan M. Jones. "Metabolism‐Inspired Electrosynthesis." ChemElectroChem 6, no. 16 (2019): 4093–104. http://dx.doi.org/10.1002/celc.201900117.

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21

Cuesta, Angel. "Understanding organic electrosynthesis." Nature Catalysis 7, no. 2 (2024): 115–16. http://dx.doi.org/10.1038/s41929-023-01101-4.

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22

Osterloh, William Ryan, and Karl Kadish. "Electrosynthesis and Electrochemistry of Porphyrins with Redox Active Substituents." ECS Meeting Abstracts MA2022-01, no. 14 (2022): 962. http://dx.doi.org/10.1149/ma2022-0114962mtgabs.

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Electrosynthesis, when combined with classical electrochemical measurements, can often provide unique insights into the mechanism and intermediates involved in formation of the desired product. This is described in the current work which investigates the redox properties of electrosynthesis and electrochemistry of porphyrins with redox active substituents.

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23

Zeng, Li, Qinghong Yang, Jianxing Wang, et al. "Programmed alternating current optimization of Cu-catalyzed C-H bond transformations." Science 385, no. 6705 (2024): 216–23. http://dx.doi.org/10.1126/science.ado0875.

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Direct current (DC) electrosynthesis, which has undergone optimization over the past century, plays a pivotal role in a variety of industrial processes. Alternating current (AC) electrosynthesis, characterized by polarity reversal and periodic fluctuations, may be advantageous for multiple chemical reactions, but apparatus, principles, and application scenarios remain underdeveloped. In this work, we introduce a protocol for programmed AC (pAC) electrosynthesis that systematically adjusts currents, frequencies, and duty ratios. The application of representative pAC waveforms facilitates copper

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24

Mirzaie, Farzad, and Marc-Antoni Goulet. "Electrosynthesis of Glyoxylic Acid By Electrochemical Reduction of Oxalic Acid and Oxidation of Glyoxal inside Co-Laminar Flow Cells." ECS Meeting Abstracts MA2024-01, no. 44 (2024): 2422. http://dx.doi.org/10.1149/ma2024-01442422mtgabs.

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This study investigates the simultaneous electrosynthesis of glyoxylic acid through electrochemical reduction of oxalic acid and oxidation of glyoxal inside a co-laminar flow reactor. This system offers specific advantages over traditional beaker cells including: continuous operation and controlled mixing of products. This study involves a systematic exploration of operating conditions such as flow rate, applied potential, current density, electrode gap and influence of specific electrocatalysts. These operating conditions are varied while the yield and current efficiency of the cell are measu

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25

Nevin, Kelly P., Sarah A. Hensley, Ashley E. Franks, et al. "Electrosynthesis of Organic Compounds from Carbon Dioxide Is Catalyzed by a Diversity of Acetogenic Microorganisms." Applied and Environmental Microbiology 77, no. 9 (2011): 2882–86. http://dx.doi.org/10.1128/aem.02642-10.

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ABSTRACTMicrobial electrosynthesis, a process in which microorganisms use electrons derived from electrodes to reduce carbon dioxide to multicarbon, extracellular organic compounds, is a potential strategy for capturing electrical energy in carbon-carbon bonds of readily stored and easily distributed products, such as transportation fuels. To date, only one organism, the acetogenSporomusa ovata, has been shown to be capable of electrosynthesis. The purpose of this study was to determine if a wider range of microorganisms is capable of this process. Several other acetogenic bacteria, including

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26

Dörr, Maurice, Maximilian M. Hielscher, Jonny Proppe, and Siegfried R. Waldvogel. "Electrosynthetic Screening and Modern Optimization Strategies for Electrosynthesis of Highly Value‐added Products." ChemElectroChem 8, no. 14 (2021): 2621–29. http://dx.doi.org/10.1002/celc.202100318.

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27

Dörr, Maurice, Maximilian M. Hielscher, Jonny Proppe, and Siegfried R. Waldvogel. "Electrosynthetic Screening and Modern Optimization Strategies for Electrosynthesis of Highly Value‐added Products." ChemElectroChem 8, no. 14 (2021): 2620. http://dx.doi.org/10.1002/celc.202100726.

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28

Homma, Haruka, Ruka Hasegawa, Tomohiro Yokoyama та Toshiki Tajima. "Convergent Paired Electrosynthesis of β-Nitroalcohols Using an Electrogenerated Base". ECS Meeting Abstracts MA2024-02, № 53 (2024): 3635. https://doi.org/10.1149/ma2024-02533635mtgabs.

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Organic electrosynthesis has attracted much attention as an environmentally benign organic synthesis process, because it is a redox process that does not use oxidizing or reducing agents. In organic electrosynthesis, only one of the reactions, oxidation at the anode or reduction at the cathode, is often targeted, and the counter electrode is mostly used only to conduct electric current. In contrast, paired electrosynthesis targets both anodic and cathodic reactions and is attractive from the viewpoint of current efficiency. Furthermore, convergent paired electrosynthesis, which yields a single

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29

Chakravorti, M. C., and Gampa V. B. Subrahmanyam. "Electrosynthesis of thiocyanato and mixed ligand thiocyanato complexes of transition metals by the sacrificial dissolution of metal anodes." Canadian Journal of Chemistry 70, no. 3 (1992): 836–38. http://dx.doi.org/10.1139/v92-110.

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A general method for the electrosynthesis of anionic and mixed ligand nonelectrolytic thiocyanato complexes of transition metals has been developed by the oxidation of sacrificial metal anodes in aqueous, or aqueous ethanolic, medium containing ammonium thiocyanate at room temperature and at an applied potential of 2–7 V. The method is rapid and gives good yield with high purity. Keywords: electrosynthesis, thiocyanato complexes, mixed ligand thiocyanato complexes.

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30

Jones, Alan M., and Craig E. Banks. "The Shono-type electroorganic oxidation of unfunctionalised amides. Carbon–carbon bond formation via electrogenerated N-acyliminium ions." Beilstein Journal of Organic Chemistry 10 (December 18, 2014): 3056–72. http://dx.doi.org/10.3762/bjoc.10.323.

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N-acyliminium ions are useful reactive synthetic intermediates in a variety of important carbon–carbon bond forming and cyclisation strategies in organic chemistry. The advent of an electrochemical anodic oxidation of unfunctionalised amides, more commonly known as the Shono oxidation, has provided a complementary route to the C–H activation of low reactivity intermediates. In this article, containing over 100 references, we highlight the development of the Shono-type oxidations from the original direct electrolysis methods, to the use of electroauxiliaries before arriving at indirect electrol

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31

Li, Nian, Ruzal Sitdikov, Ajit Prabhakar Kale, Joost Steverlynck, Bo Li, and Magnus Rueping. "A review of recent advances in electrochemical and photoelectrochemical late-stage functionalization classified by anodic oxidation, cathodic reduction, and paired electrolysis." Beilstein Journal of Organic Chemistry 20 (October 9, 2024): 2500–2566. http://dx.doi.org/10.3762/bjoc.20.214.

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With the resurgence of electrosynthesis in organic chemistry, there is a significant increase in the number of routes available for late-stage functionalization (LSF) of drugs. Electrosynthetic methods, which obviate the need for hazardous chemical oxidants or reductants, offer unprecedented control of reactions through the continuous variation of the applied potential and the possibility of combination with photochemical processes. This capability is a substantial advantage for performing electrochemical or photoelectrochemical LSF. Ultimately, these protocols are poised to become a vital com

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32

Beeler, Joshua A., and Henry S. White. "Reductive Electrosynthesis Initiated By Mediated Oxalate Oxidation." ECS Meeting Abstracts MA2024-02, no. 53 (2024): 3639. https://doi.org/10.1149/ma2024-02533639mtgabs.

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Reductive electrosynthesis often requires large negative potentials, air-sensitive electrocatalysts, precious metal electrode surfaces, dry solvent, and/or a sacrificial anode. As a result, electroorganic reduction reactions remain relatively underdeveloped compared to oxidative electroorganic methods. This work introduces a novel reductive electrosynthetic method, wherein the mediated oxidation of oxalate (C2O4 2–) at a carbon electrode facilitates the homogeneous reduction of aryl halides. Specifically, the homogeneous oxidation of C2O4 2– in mixed organic/aqueous solutions by electrochemica

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33

Jiang, Jun, Zheng Wang, and Wei-Min He. "Electrosynthesis of 1-indanones." Chinese Chemical Letters 32, no. 5 (2021): 1591–92. http://dx.doi.org/10.1016/j.cclet.2021.02.067.

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34

Inguanta, Rosalinda, Salvatore Piazza, and Carmelo Sunseri. "Template electrosynthesis of CeO2nanotubes." Nanotechnology 18, no. 48 (2007): 485605. http://dx.doi.org/10.1088/0957-4484/18/48/485605.

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35

Zagumennov, V. A., and I. P. Kosachev. "Diaphragmless Electrosynthesis of Diphenylphosphate." Russian Journal of Electrochemistry 56, no. 9 (2020): 760–65. http://dx.doi.org/10.1134/s1023193520090104.

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36

Gong, Yanming, Ali Ebrahim, Adam M. Feist, et al. "Sulfide-Driven Microbial Electrosynthesis." Environmental Science & Technology 47, no. 1 (2012): 568–73. http://dx.doi.org/10.1021/es303837j.

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37

Couper, A. Mottram, Derek Pletcher, and Frank C. Walsh. "Electrode materials for electrosynthesis." Chemical Reviews 90, no. 5 (1990): 837–65. http://dx.doi.org/10.1021/cr00103a010.

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38

Fedoroňko, Michal, Tibor Stach, Peter Capek, and Vladimı́r Farkaš. "Electrosynthesis of oligosaccharide glycamines." Carbohydrate Research 306, no. 3 (1998): 457–61. http://dx.doi.org/10.1016/s0008-6215(97)10072-6.

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39

Cognet, P., A. M. Wilhelm, H. Delmas, H. Aı̈t Lyazidi, and P. L. Fabre. "Ultrasound in organic electrosynthesis." Ultrasonics Sonochemistry 7, no. 4 (2000): 163–67. http://dx.doi.org/10.1016/s1350-4177(00)00036-5.

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40

Golabi, S. M., F. Nourmohammadi, and A. Saadnia. "Electrosynthesis of organic compounds." Journal of Electroanalytical Chemistry 548 (May 2003): 41–47. http://dx.doi.org/10.1016/s0022-0728(03)00218-3.

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41

Vargas, R. R., V. L. Pardini та H. Viertler. "Electrosynthesis of γ-asarone". Tetrahedron Letters 30, № 31 (1989): 4037–40. http://dx.doi.org/10.1016/s0040-4039(00)99315-8.

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42

Nguyen, Tu N., and Hans-Conrad zur Loye. "Electrosynthesis in hydroxide melts." Journal of Crystal Growth 172, no. 1-2 (1997): 183–89. http://dx.doi.org/10.1016/s0022-0248(96)00726-9.

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43

Radmannia, Sepideh, and Milad Naderzad. "IoT-based electrosynthesis ecosystem." Internet of Things 3-4 (October 2018): 46–51. http://dx.doi.org/10.1016/j.iot.2018.08.001.

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44

Kreysa, G., and H. Medin. "Indirect electrosynthesis ofp-methoxybenzaldehyde." Journal of Applied Electrochemistry 16, no. 5 (1986): 757–67. http://dx.doi.org/10.1007/bf01006929.

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45

Martínez Suárez, Jaime F., José A. Caram, Gustavo A. Echeverría, Oscar E. Piro, Ana M. Gennaro, and María V. Mirífico. "Electrosynthesis of N-Methylisatin." Journal of Organic Chemistry 84, no. 11 (2019): 6879–85. http://dx.doi.org/10.1021/acs.joc.9b00690.

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46

Utley, James. "Trends in organic electrosynthesis." Chemical Society Reviews 26, no. 3 (1997): 157. http://dx.doi.org/10.1039/cs9972600157.

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47

Smith, Allen A. "Electrosynthesis of a Macrocycle." Journal of The Electrochemical Society 139, no. 11 (1992): L103. http://dx.doi.org/10.1149/1.2069082.

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48

de Robillard, Guillaume, Charles H. Devillers, Doris Kunz, Hélène Cattey, Eric Digard, and Jacques Andrieu. "Electrosynthesis of Imidazolium Carboxylates." Organic Letters 15, no. 17 (2013): 4410–13. http://dx.doi.org/10.1021/ol401949f.

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49

Gomez, J. R. Ochoa. "Electrosynthesis of N-methylhydroxylamine." Journal of Applied Electrochemistry 21, no. 4 (1991): 331–34. http://dx.doi.org/10.1007/bf01020218.

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50

Jundale, S. B., and C. D. Lokhande. "Electrosynthesis of SmTe films." Materials Chemistry and Physics 37, no. 4 (1994): 333–37. http://dx.doi.org/10.1016/0254-0584(94)90171-6.

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