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Dissertations / Theses on the topic 'Enantiomere'

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Published: 4 June 2021

Last updated: 4 May 2024

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1

Lavé, Thierry. "Pharmacocinetique et methodes d'analyse chromatographique des enantiomeres." Strasbourg 1, 1992. http://www.theses.fr/1992STR15092.

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2

Würthner, Stefan. "Diskriminierung von Enantiomeren mit chiralen Selektoren." [S.l. : s.n.], 2007.

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3

Lavé, Thierry. "Etude de la pharmacocinetique et du metabolisme des enantiomeres du tertatolol chez le rat et chez l'homme." Strasbourg 1, 1993. http://www.theses.fr/1993STR15093.

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4

Frihmat, Rachid. "Stéréoisomérie et biopharmacie : méthodes analytiques par HPLC et étude pharmacocinétique des énantiomères de l'ibuprofène après administration chez le chien." Clermont-Ferrand 1, 1993. http://www.theses.fr/1993CLF1PP08.

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5

BUI, TUNG HIEP. "Etude de la stereoselectivite de la pharmacocinetique de la chlorpheniramine : influence sur les etudes de bioequivalence (doctorat : pharmacotechnie et biopharmacie)." Paris 11, 1999. http://www.theses.fr/1999PA114819.

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6

Driehsen, Carina. ""Zur Wirkung von Mirtazapin und seiner Enantiomere auf chronisch neuropathische Schmerzen der Ratte"." Diss., lmu, 2008. http://nbn-resolving.de/urn:nbn:de:bvb:19-90461.

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7

Leynadier, Daniel. "Interactions de deux enantiomeres 1-deaza-7,8-dihydropteridiques avec le systeme microtubulaire." Aix-Marseille 2, 1993. http://www.theses.fr/1993AIX22954.

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8

Munkelt, Thomas [Verfasser], and Andreas [Gutachter] Seidel-Morgenstern. "Separation, Speicherung und Gewinnung der Enantiomere chiraler Anästhetika / Thomas Munkelt ; Gutachter: Andreas Seidel-Morgenstern." Magdeburg : Universitätsbibliothek Otto-von-Guericke-Universität, 2019. http://d-nb.info/1219937061/34.

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9

Chimier, Sylvie. "Etude "in vitro" de la distribution érythrocytaire de la méfloquine et de ses énantiomères." Paris 5, 1996. http://www.theses.fr/1996PA05P143.

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10

Song, Karine. "Etudes pharmacotoxicologiques du propranolol et de ses enantiomères." Paris 5, 1997. http://www.theses.fr/1997PA05P126.

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11

Menzel, Anne. "Gentechnisch veränderte Escherichia coli-Zellen zur biokatalytischen Herstellung enantiomerenreiner Aminosäuren und sekundärer Alkohole." [Lautertal] Stephan, 2006. http://deposit.d-nb.de/cgi-bin/dokserv?id=2832160&prov=M&dok_var=1&dok_ext=htm.

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12

Menard, Christophe. "Identification et caractérisation des voies enzymatiques hépatiques impliquées dans le métabolisme d'un antihypertenseur : le ciclétanine (Doctorat : sciences de la vie et de la santé)." Brest, 1999. http://www.theses.fr/1999BRES3101.

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13

Teves, Harald. "Modellgestützte Entwicklung eines mehrstufigen Verfahrens zur enzymatischen Synthese enantiomerenreiner Aminosäuren." [S.l. : s.n.], 2008. http://nbn-resolving.de/urn:nbn:de:bsz:93-opus-34117.

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14

Martin, Corinne. "Etude de la stéréosélectivité de la pharmacocinétique de la méfloquine après administration de la forme racémique et de ses isomères séparés." Paris 5, 1994. http://www.theses.fr/1994PA05P115.

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15

Cannes, Mélanie. "Séparation énantiomérique : utilisation des cyclodextrines en chromatographie liquide chirale." Paris 5, 1996. http://www.theses.fr/1996PA05P195.

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16

Eßer, Simon. "Von Chorismat abgeleitete funktionalisierte Cyclohexadien-trans-diole Optimierung der mikrobiellen Produktion, Untersuchungen zur Reaktivität und Synthese beider Enantiomere des Naturstoffs Valienon /." [S.l. : s.n.], 2006.

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17

Zheng, Hui. "Stereoselective pharmacokinetics and metabolism of XK469, a new quinoxaline topoisomerase II beta poison, in the rat." Columbus, Ohio : Ohio State University, 2004. http://rave.ohiolink.edu/etdc/view?acc%5Fnum=osu1080257372.

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Thesis (Ph. D.)--Ohio State University, 2004.<br>Title from first page of PDF file. Document formatted into pages; contains xxi, 190 p.; also includes graphics. Includes abstract and vita. Advisor: Kenneth K. Chan, Dept. of Pharmacy. Includes bibliographical references (p. 182-190).

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18

Kröner, Dominik. "Theory of selective preparation of enantiomers by laser pulses Theorie zur selektiven Präparation von Enantiomeren durch Laserpulse /." [S.l. : s.n.], 2003. http://www.diss.fu-berlin.de/2003/141/index.html.

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19

Pelletier, Véronique. "Les médicaments racémiques : importance pharmacologique, analyse par chromatographie en phase liquide chirale." Paris 5, 1990. http://www.theses.fr/1990PA05P029.

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20

Barros, Georgia de Oliveira Figueiredo. "Resolução de misturas racemicas por acoplamento de cristalização a cromatografia em leito movel simulado : estudos fundamentais para a produção de S-cetamina." [s.n.], 2005. http://repositorio.unicamp.br/jspui/handle/REPOSIP/267314.

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Orientador: Everson Alves Miranda<br>Dissertação (mestrado) - Universidade Estadual de Campinas, Faculdade de Engenharia Quimica<br>Made available in DSpace on 2018-08-04T07:13:28Z (GMT). No. of bitstreams: 1 Barros_GeorgiadeOliveiraFigueiredo_M.pdf: 2282903 bytes, checksum: b104323f697a813ec6af57b15ba7b95b (MD5) Previous issue date: 2005<br>Resumo: A separação de enantiômetros em altos níveis de pureza enantiomérica é atualmente um requerimento da industria farmacêutica. No entanto, altas purezas estão sendo alcançadas neste sistema com comprometimento da produtividade. O acoplamento do lei

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21

Coeuille, Jean-Yves. "Séparation chirale et chromatographie en Lit Mobile Simulé." Paris 5, 1997. http://www.theses.fr/1997PA05P030.

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22

Grisoni, Serge. "Synthese biomimetique du cycle c des alcaloides de l'ergot : application, premiere synthese enantioselective de la (-) chanoclavine i." Paris 6, 1987. http://www.theses.fr/1987PA066408.

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Synthese de benzo (cd) indoles a partir de l'indolecarbaldehyde-4 par cyclisation intramoleculaire en presence de pd(o); l'utilisation de bases solides (alumine-kf ou k::(2)co::(3)) permet des conditions operationnelles douces

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23

Lindner, Susann [Verfasser], Gabriele [Akademischer Betreuer] Nöldge-Schomburg, Michael [Akademischer Betreuer] Bauer та Amelie [Akademischer Betreuer] Lupp. "Einfluss der Anästhetika Propofol und Ketamin sowie der Enantiomere Ketamin "r" und "s" auf die bakterienstimulierte TNFα-Antwort in Leukozyten / Susann Lindner. Gutachter: Gabriele Nöldge-Schomburg ; Michael Bauer ; Amelie Lupp". Jena : Thüringer Universitäts- und Landesbibliothek Jena, 2012. http://d-nb.info/1019969520/34.

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24

Peyrin, Eric. "Mécanisme de fixation et de reconnaissance chirale des acides aminés dansyles sur la sérum albumine humaine : approche chromatographique et thermodynamique." Besançon, 1998. http://www.theses.fr/1998BESA2073.

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La separation de molecules chirales biologiques ou medicamenteuses suscite, depuis quelques annees, un grand interet de la part des analystes. Cet interet est bien comprehensible des lors qu'il est reconnu que la majorite des processus biochimiques sont enantioselectifs. Il est donc fondamental d'obtenir des enantiomeres purs des molecules chirales actives afin d'apprehender au mieux leurs activites et/ou leurs toxicites respectives. Parmi les diverses techniques de resolution chirale, la chromatographie en phase liquide occupe une place de choix. Les phases stationnaires chirales proteiques,

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25

Speybrouck, David. "Impact de l'additif en chromatographie en phase supercritique sur phases stationnaires énantiosélectives." Thesis, Normandie, 2018. http://www.theses.fr/2018NORMR052/document.

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Le développement de molécules chirales est devenu un enjeu majeur pour l’industrie pharmaceutique. Lors de la mise au point d’un nouveau principe actif, la chromatographie en phase supercritique (CPS) sur phases stationnaires énantiosélectives, est devenue une méthode incontournable pour l’analyse ou la purification d’énantiomères. Il n’en demeure pas moins que certains composés tels que les composés basiques restent délicats à analyser par cette technique et que l’ajout d’un additif basique dans la phase mobile est très souvent nécessaire. La quantité d’additif ajoutée dans la phase mobile es

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26

Henrot, Serge. "Synthese stereo et enantioselective de beta-hydroxy esters fonctionnalises par voie chimique et par voie microbiologique : application a la preparation de la (-) alpha multistriatine et du r (-) gabob." Paris 6, 1987. http://www.theses.fr/1987PA066428.

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27

TCHERTCHI, AN SYLVIE. "Controle de la stéréochimie en série acyclique : application à la synthèse de la zwittermycine A." Université Joseph Fourier (Grenoble), 1997. http://www.theses.fr/1997GRE10267.

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La zwittermycine a est un aminopolyol possedant d'importantes proprietes antibiotiques et antifongiques. Elle est composee d'une partie uree-amide derivee d'un aminoacide non naturel proteique, l'albizziine, et d'une partie diaminopentol. L'approche synthetique convergente envisagee utilise un synthon chiral commun derive de la l-serine, l'aldehyde de garner. Au cours de ce travail, nous avons realise la synthese des deux enantiomeres de la partie uree-amide sous une forme protegee. Dans un deuxieme temps, deux strategies pour la synthese de la partie diaminopentol ont ete mises en oeuvre. La

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28

Sayah, Ghassemi Babak. "Chimie et réactivité des hexahydropyrroloindolizines : application à la synthèse des myrmicarines." Université Joseph Fourier (Grenoble), 2001. http://www.theses.fr/2001GRE10114.

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Parmi les composes naturels ou synthetiques possedant des activites biologiques interessantes, les alcaloides tiennent une part importante. Recemment une nouvelle famille d'alcaloides bicycliques et oligocycliques, nommee myrmicarine, a ete isolee de glandes a poisons de fourmis d'afrique de type mirmicinae. La plupart de ces composes possedent en totalite ou en partie un motif hexahydropyrroloindolizine contenant un centre stereogene dont la configuration absolue n'est pas connue. Nous avons entrepris la synthese de ces alcaloides sous forme enantiopure. Dans un premier temps, suivant une str

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29

Wildervanck, Alexander Franciscus. "Separation of enantiomers of Baclofen." Master's thesis, University of Cape Town, 1996. http://hdl.handle.net/11427/20462.

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(3-(Aminomethyl)-4-chlorobenzenepropanoic acid (Baclofen), 3-(p-chlorophenyl)pyrrolidone (Baclofen lactam) and 3-(p-Chlorophenyl)glutaramide (baclofen's synthetic precursor) were individually used as substrates in co-crystallisation experiments with several resolving agents. Experiments were conducted in the solid state and in solution. The (-) enantiomer of the lactam and the ( +) enantiomer of the glutaramide were found to cocrystallise selectively with (2R,3R)-( +)-tartaric acid and (S)-(-)-a.-Methylbenzylamine respectively. Both these dissociable diastereomers Vere analysed by X-ray crysta

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30

Bates, Paul Stephen. "Enantiomer discrimination and ion receptors." Thesis, Durham University, 1993. http://etheses.dur.ac.uk/5689/.

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Highly lipophilic α-, β- and γ- cyclodextrin derivatives were prepared in order to obtain enantiomer selective ionophores for β-aryl ammonium ions and selective ionophores for tetrahedral ammonium ions. The extent of cyclodextrin functionalisation and the homogeneity of the products was investigated by chemical depolymerisation, (^1)H and (^13)C NMR and (+)-FAB-, FD- and ES- mass spectral analysis. For each cyclodextrin, the products of alkylation were found to consist of several constitutional isomers and homologues. These highly lipophilic molecules were incorporated into solvent polymeric m

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31

Schulz, Harald [Verfasser]. "Hochempfindlicher lasergestützter Enantiomeren-Detektor / Harald Schulz." Aachen : Shaker, 2005. http://d-nb.info/1181620457/34.

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32

Bromley, Graham. "Approaches to single enantiomers of cyclopropanes." Thesis, Cardiff Metropolitan University, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.409442.

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33

Anandamanoharan, P. "Isolation of enantiomers via diastereomer crystallisation." Thesis, University College London (University of London), 2010. http://discovery.ucl.ac.uk/19315/.

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Enantiomer separation remains an important technique for obtaining optically active materials. Even though the enantiomers have identical physical properties, the difference in their biological activities make it important to separate them, in order to use single enantiomer products in the pharmaceutical and fine chemical industries. In this project, the separations of three pairs of diastereomer salts (Fig1) by crystallisation are studied, as examples of the ‘classical’ resolution of enantiomers via conversion to diastereomers. The lattice energies of these diastereomer compounds are calculat

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34

Vandenbussche, Sophie. "Origin of homochirality on Earth: experimental and theoretical investigations." Doctoral thesis, Universite Libre de Bruxelles, 2009. http://hdl.handle.net/2013/ULB-DIPOT:oai:dipot.ulb.ac.be:2013/210362.

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Chirality is the property of objects, including molecules, which are not superimposable on their materialized mirror image. Chiral molecules are omnipresent in living organisms and the constituents of biological macromolecules (proteins and nucleic acids) are chiral. Amino-acids (constituting proteins), ribose and 2-deoxy-ribose (the only chiral constituent of RNA and DNA nucleotides respectively) are furthermore generally present in living organisms only under one of their enantiomeric forms. This is referred to as the homochirality of the living world. The origin of this homochirality is sti

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35

Koza, Gani. "Synthesis of single enantiomers of ketomycolic acids." Thesis, Bangor University, 2007. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.488849.

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36

Zu, Chengli. "Enantiomer analysis using electrospray ionization mass spectrometry." Diss., Mississippi State : Mississippi State University, 2007. http://library.msstate.edu/etd/show.asp?etd=etd-04092007-103342.

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37

Taylor, Richard John. "NMR assay of enantiomeric excess." Thesis, Durham University, 1987. http://etheses.dur.ac.uk/9530/.

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The use of (S)-methylmandelate as a Chiral Derivatising Agent for chiral acids is described. The diastereoisomers obtained by esterification are studied by (^1)H.N.M.R. Assignment of absolute configuration in these systems is made using models proposed to explain the origin of diastereotopic methylene proton non-equivalence in camphanamides. The development and application of chiral phosphine platinum (O) and palladium (O) ethene complexes as Chiral Derivatising Agents for chiral alkenes and allenes is reported. The (^31)P N.M.R. spectra recorded for the mixtures of diastereo isomers obtained

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38

Castrignanò, Erika. "Enantiomeric profiling of chiral biomarkers." Thesis, University of Bath, 2016. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.715278.

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Wastewater-based epidemiology (WBE) is an innovative tool that, unlike traditional epidemiological approaches, is capable of providing real-time profiling of community health and lifestyle along with emerging trends and changes in pattern usage of drugs in wastewater. By using human urinary excreted indicators, so-called “biomarkers”, WBE provides estimates at population level. Therefore, the choice and the evaluation of suitable biomarkers of exposure to drugs is of fundamental importance for the public health monitoring. Moreover, since many drugs are chiral, the investigation on enantiomeri

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39

Toschi, Gianna. "Synthetic approaches to single enantiomers of mycolic acids." Thesis, Bangor University, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.429853.

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40

Brookes, Michael H. "The synthesis of the enantiomers of lipoic acid." Thesis, University of Warwick, 1985. http://wrap.warwick.ac.uk/55428/.

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Lipoic acid is a biologically important molecule. Whilst the racemate has been available by a number of syntheses for many years, no convenient preparation of the pure enantiomers has so far been described. All the evidence so far presented indicates that only the dextrorotatory isomer is active in vivo, the absolute configuration of which has not been established with certainty. To further elucidate the biochemical role(s) and biosynthesis of this compound, a convenient EPC synthesis would be beneficial. This thesis describes the development of a route to the (R)- and (S)- forms of the target

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41

McBride, John Joseph. "Development of biosensors for the determination of enantiomers." Thesis, University of Brighton, 1993. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.359142.

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42

Thome, Brian Matthew. "Increasing the scale of electrophoretic true moving bed enantiomer separations using voltage gradients and filtration enhancement." Online access for everyone, 2006. http://www.dissertations.wsu.edu/Dissertations/Fall2006/b_thome_110706.pdf.

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43

Nhujak, Thumnoon. "Quantitative aspects of capillary electrophoresis and chiral analysis." Thesis, University of York, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.270036.

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44

Haglöf, Jakob. "Enantiomeric Separations using Chiral Counter-Ions." Doctoral thesis, Uppsala universitet, Avdelningen för analytisk farmaceutisk kemi, 2010. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-130049.

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This thesis describes the use of chiral counter-ions for the enantiomeric separation of amines in non-aqueous capillary electrophoresis. The investigations have been concentrated on studies of the influence, of the chiral counter-ion, the solvent, the electrolyte and the analyte, on the enantioselective separation. Modified divalent dipeptides have been introduced in capillary electrophoresis for the separation of amino alcohols and chiral resolution of amines. Association constants for the ion-pair between dipeptide and amino alcohol could be utilized for development of separation systems wit

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45

Nzeadibe, Kingsley C. I. "Synthesis of new, single-isomer quaternary ammonium derivatives of beta-cyclodextrin for electrophoretic enantiomer separations." Texas A&M University, 2003. http://hdl.handle.net/1969.1/5833.

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The isolation of individual enantiomers of drugs is an important subject of interest in the pharmaceutical and medical fields, because stereochemistry can have a significant effect on the biological activity of the drug. Therefore, it is important to develop enantiomeric separation methods for the determination of the optical purity of drugs, since the undesired enantiomer is regarded as one of the impurities. The available single isomer anionic cyclodextrins (CD) can resolve the enantiomers of only a few weakly acidic analytes. To rectify this problem, the chloride salts of heptakis(6-deoxy-6

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46

Thvedt, Thor Håkon Krane. "Syntese av α-fluorketoner, ograsemiske og enantiomert rene2-fluoraminer". Thesis, Norges teknisk-naturvitenskapelige universitet, Institutt for kjemi, 2009. http://urn.kb.se/resolve?urn=urn:nbn:no:ntnu:diva-6854.

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47

Elgarhy, Karim. "The separation of the enantiomers of asparagine by crystallization /." Thesis, McGill University, 2005. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=100356.

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Enantiomers are chiral molecules (i.e. they are mirror-images of each other). They have identical physical properties except for the rotation of polarized light. However their chemical properties are different when reacting with other chiral molecules. The majority of biological processes involve the reaction of two or more chiral molecules. There is therefore a strong interest coming from the pharmaceutical, food and agricultural industry for the separation of enantiomers.<br>Separation methods such as chromatography exist but are generally expensive and limited in scale. Stereosynthesis ofte

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48

Meeson, Stephen Russell. "The separation of enantiomers by high performance liquid chromatography." Thesis, University of Newcastle Upon Tyne, 1990. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.278414.

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49

Rocco, Anna. "Separation of Enantiomers by Means of NanoO-Liquid Chromatography." Doctoral thesis, Lithuanian Academic Libraries Network (LABT), 2013. http://vddb.library.lt/obj/LT-eLABa-0001:E.02~2013~D_20130122_144808-59559.

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Nano-liquid chromatography (nano-LC) was selected as analytical tool to develop different methods for chiral separations. Nano-LC offers several advantages over conventional LC, e.g., low sample requirement, short analysis time, easy coupling with mass spectrometer, and use of small amount of reagents, with a consequent low environmental pollution. In case of chiral separations, where expensive chiral stationary phases or chiral mobile phase additives (CMPA) have to be employed, nano-LC results very useful since it allows to perform analysis with small amount of this costly material. Initiall

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50

Cooper, Andrew Donovan. "Resolution of enantiomers using cyclodextrins in NMR and HPLC." Thesis, University of Bath, 1991. https://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.292808.

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