Dissertations / Theses on the topic 'Experimental Stress Analysis'
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URURAHY, MARCELO FERREIRA PINTO. "THEORETICAL-EXPERIMENTAL THERMAL STRESS ANALYSIS IN VISCOELASTIC CYLINDERS." PONTIFÍCIA UNIVERSIDADE CATÓLICA DO RIO DE JANEIRO, 1991. http://www.maxwell.vrac.puc-rio.br/Busca_etds.php?strSecao=resultado&nrSeq=19375@1.
Full textApresenta-se neste trabalho o desenvolvimento de um modelo teórico-numérico baseado na Teoria da Viscoelasticidade Linear capaz de prever as distribuições transientes e residuais das componentes de tensão e de deformação de um cilindro polimérico longo submetido a resfriamento brusco. Descrevem-se, ainda, os procedimentos experimentais adotados como intuito de se determinarem algumas propriedades térmicas e mecânicas do sistema epóxi DER331/XG0103/XB81215. Finalmente, comparam-se os resultados fornecidos pelo modelo teórico-numérico com resultados experimentais obtidos através da utilização de uma técnica extensométrica conhecida como Método de Sachs.
This work presents the development of a theoretical and numerical model based on the Linear Viscoelastic Theory able to predict the transient and residual stress and deformation distributions in a long polymeric cylinder subject to a rapid cooling. The work describes the experimental procedures adopted aiming to determine some thermal and mechanical properties of the epoxy system DER331/XG0103/XB81215. Finally, the results from the theoretical numerical model are compared to the ones obtained experimentally by na extensometric technique known as Sachs’ Method.
Schepers, Scott Timothy. "Renewal In The Context Of Stress: A Potential Mechanism Of Stress-Induced Reinstatement." ScholarWorks @ UVM, 2017. http://scholarworks.uvm.edu/graddis/780.
Full textWard, David. "Hydrodynamic effects on soiled surfaces : an experimental study and theoretical analysis." Thesis, Open University, 2000. http://oro.open.ac.uk/58091/.
Full textChaparala, Satish Chandra. "Die stress analysis in plastic encapsulated electronic packages an experimental and numerical approach /." Diss., Online access via UMI:, 2006.
Find full textPark, Hyuen Me (Mia) Park. "Numerical and experimental analysis of stress behavior of plasma-sprayed Bioglass on titanium /." Full text open access at:, 1996. http://content.ohsu.edu/u?/etd,587.
Full textWei, Ling. "Experimental study of growth and protein dynamics in yeast Hog1 mutants under osmotic stress." HKBU Institutional Repository, 2011. http://repository.hkbu.edu.hk/etd_ra/1282.
Full textJohnson, Shane Miguel. "Computational modeling, stochastic and experimental analysis with thermoelastic stress analysis for fiber reinforced polymeric composite material systems." Diss., Georgia Institute of Technology, 2010. http://hdl.handle.net/1853/34668.
Full textJavidinejad, Amir. "An experimental stress analysis approach for pure shear testing and analysis of a fiber reinforced plastic composite." Thesis, Georgia Institute of Technology, 1994. http://hdl.handle.net/1853/20706.
Full textPark, Joon Boo. "Theoretical and Experimental Analysis of Residual Stress Formation after Implant Resistance Welding of Polycarbonate." The Ohio State University, 1992. http://rave.ohiolink.edu/etdc/view?acc_num=osu1392653414.
Full text鈴木, 賢治, Kenji SUZUKI, 啓介 田中, Keisuke TANAKA, 義明 秋庭, Yoshiaki AKINIWA, 昌志 川村, et al. "放射光高エネルギーX線による遮熱コーティングのはく離応力の評価." 日本機械学会, 2004. http://hdl.handle.net/2237/9140.
Full textLiu, Zhiqiang. "Modelling and experimental studies of contact and friction of metallic rough surfaces in initial sliding." Thesis, Heriot-Watt University, 2001. http://hdl.handle.net/10399/542.
Full textAlbakri, Mohammad Ismail. "Modeling and Experimental Analysis of Piezoelectric Augmented Systems for Structural Health and Stress Monitoring Applications." Diss., Virginia Tech, 2017. http://hdl.handle.net/10919/84513.
Full textPh. D.
Ragab, Adham Ezzat. "Sensitivity Analysis of Casting Distortion and Residual Stress Prediction Through Simulation Modeling and Experimental Verification." The Ohio State University, 2003. http://rave.ohiolink.edu/etdc/view?acc_num=osu1052493015.
Full textMarsh, Richard. "Experimental analysis of oil based cavitation peening in air." Thesis, Georgia Institute of Technology, 2011. http://hdl.handle.net/1853/43602.
Full textDallmeier, Johannes. "Experimental analysis and numerical fatigue modeling for magnesium sheet metals." Doctoral thesis, Technische Universitaet Bergakademie Freiberg Universitaetsbibliothek "Georgius Agricola", 2016. http://nbn-resolving.de/urn:nbn:de:bsz:105-qucosa-209124.
Full textZhang, Chao. "Random delamination of graphite/epoxy laminated composites : stress analysis, failure criteria, experimental characterization and stochastic modeling." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 2001. http://www.collectionscanada.ca/obj/s4/f2/dsk3/ftp05/NQ63992.pdf.
Full textAlmeida, Camila de. "Modelling of the protection mechanisms against methylgyoxal stress in Escherichia coli : dynamical analysis and experimental validation." Thesis, University of Aberdeen, 2009. http://digitool.abdn.ac.uk:80/webclient/DeliveryManager?pid=103942.
Full textOlden, Elizabeth Jane. "The application of experimental stress analysis techniques to the study of cracks around cold-expanded holes." Thesis, University of Sheffield, 1998. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.286604.
Full textJain, Anurag. "Experimental study and numerical analysis of compression molding process for manufacturing precision aspherical glass lenses." Columbus, Ohio : Ohio State University, 2006. http://rave.ohiolink.edu/etdc/view?acc%5Fnum=osu1148650470.
Full textSutherland, Brandy. "Experimental and analytical analysis of the stress-strain diagram of FRP-confined concrete with different loading rates." Thesis, Manhattan, Kan. : Kansas State University, 2007. http://hdl.handle.net/2097/420.
Full textLai, Chun Hon. "Experimental study of stress-dependent soil-water characteristics and their applications on numerical analysis of slope stability /." View abstract or full-text, 2004. http://library.ust.hk/cgi/db/thesis.pl?CIVL%202004%20LAIC.
Full textSUZUKI, Kenji, Keisuke TANAKA, and Yoshiaki AKINIWA. "Estimation of Spalling Stress in Thermal Barrier Coatings Using Hard Synchrotron X-Rays." The Japan Society of Mechanical Engineers, 2004. http://hdl.handle.net/2237/9176.
Full textOzsoy, Serhan. "Vibration Induced Stress And Accelerated Life Analyses Of An Aerospace Structure." Master's thesis, METU, 2006. http://etd.lib.metu.edu.tr/upload/2/12606966/index.pdf.
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s dynamic characteristics and varying loadings. Therefore, experimental, numerical or a combination of both methods are used for fatigue evaluations. Fatigue failure can occur on systems and platforms as well as components to be mounted on the platform. In this thesis, a helicopter&
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s Missile Warning Sensor - Cowling assembly is analyzed. Analytical, numerical and experimental approaches are used wherever necessary to perform stress and fatigue analyses. Operational flight tests are used for obtaining the loading history at the analyzed location by using sensors. Operational vibration profiles are created by synthesizing the data (LMS Mission Synthesis). Numerical fatigue analysis of the assembly is done for determining the natural modes and the critical locations on the assembly by using a finite element model (MSC Fatigue). In addition, numerical multiaxial PSD analysis is performed for relating the experimental results (Ansys). Residual stresses due to riveting are determined (MSC Marc) and included in experimental analysis as mean stresses. Bolt analysis is performed analytically (Hexagon) for keeping the v assembly stresses in safe levels while mounting the experimental prototype to the test fixture. Fatigue tests for determining the accelerated life parameters are done by an electromagnetic shaker and stress data is collected. Afterwards, fatigue test is performed for determining whether the assembly satisfies the required operational life. Resonance test is performed at the frequency in which the critical location is at resonance, since there was no failure observed after fatigue testing. A failure is obtained during resonance test. At the end of the study, an analytical equation is brought up which relates accelerated life test durations with equivalent alternating stresses. Therefore, optimization of the accelerated life test duration can be done, especially in military applications, by avoiding the maximum stress level to reach or exceed the yield limit.
Farukh, Farukh. "Experimental and numerical analysis of deformation and damage in thermally bonded nonwoven material." Thesis, Loughborough University, 2013. https://dspace.lboro.ac.uk/2134/12812.
Full textAdeleke, Bukola. "Experimental and Finite Element Analysis of Wind Induced Displacement of a Dual Axis Photovoltaic Solar Trackers." Thesis, Université d'Ottawa / University of Ottawa, 2016. http://hdl.handle.net/10393/34310.
Full text鈴木, 賢治, Kenji SUZUKI, 一秀 松本, Kazuhide MATSUMOTO, 貴博 久保, Takahiro KUBO, 修太郎 町屋, et al. "高エネルギー反射光によるEB-PVD遮熱コーティングの残留応力分布の解析." 日本機械学会, 2005. http://hdl.handle.net/2237/9130.
Full text鈴木, 賢治, Kenji SUZUKI, 修太郎 町屋, Shutaro MACHIYA, 啓介 田中, Keisuke TANAKA, 喜久 坂井田, and Yoshihisa SAKAIDA. "熱遮へいコーティング膜の変形特性のX線的研究." 日本機械学会, 2001. http://hdl.handle.net/2237/9163.
Full textCantrell, Ashley M. "Understanding Posttraumatic Stress and Academic Achievement: Exploring Attentional Control, Self-Efficacy, and Coping Among College Students." TopSCHOLAR®, 2016. http://digitalcommons.wku.edu/theses/1618.
Full textChekkilla, Avinash Goud. "Monitoring and Analysis of CPU Utilization, Disk Throughput and Latency in servers running Cassandra database : An Experimental Investigation." Thesis, Blekinge Tekniska Högskola, Institutionen för tillämpad signalbehandling, 2017. http://urn.kb.se/resolve?urn=urn:nbn:se:bth-13706.
Full textCrammond, G. "Development of optical techniques for the experimental analysis of local stress and strain distributions in adhesively bonded composite joints." Thesis, University of Southampton, 2013. https://eprints.soton.ac.uk/355981/.
Full textVanDenBosch, Leah M. "Investigating the effect of fluid shear stress on the failure of cancer cell membranes: an experimental and computational analysis." Thesis, University of Iowa, 2018. https://ir.uiowa.edu/etd/6318.
Full textKelly, Brennan James. "Experimental and Simulated Analysis of Voltage Stress Within a Bar-Wound Synchronous Machine Excited by a Silicon Carbide Inverter." The Ohio State University, 2021. http://rave.ohiolink.edu/etdc/view?acc_num=osu1619111736344023.
Full text田中, 啓介, Keisuke TANAKA, 賢一 水野, Kenichi MIZUNO, 修太郎 町屋, Shutaro MACHIYA, 義明 秋庭, and Yoshiaki AKINIWA. "シリコン単結晶の重回帰分析を用いたX線応力測定." 日本機械学会, 2006. http://hdl.handle.net/2237/9153.
Full textLacerda, Larissa Gomes. "Chronic Mild Stress (CMS): um estudo sobre a interação entre manipulação neonatal e submissão ao protocolo de estressores na vida adulta." Pontifícia Universidade Católica de São Paulo, 2013. https://tede2.pucsp.br/handle/handle/16705.
Full textConselho Nacional de Desenvolvimento Científico e Tecnológico
Chronic Mild Stress (CMS) an experimental animal model of anhedonia induced by exposing the rats to a protocol of chronic stress for a long period of time. At the Laboratório do Programa de Pós Graduação em Psicologia Experimental: Análise do Comportamento, a research line about CMS and its relation with the operant behavior has been developed since 2001, as in Pereira (2009). Unlike other studies conducted in this laboratory, Pereira (2009) did not observe sucrose intake and preference reducing (anhedonia) along stressors. One pointed hypothesis was the neonatal handling was a responsible variable for that. The goal of this study was to investigate whether the neonatal handling alters the fluid intake and preference on rats that were submitted to the stressors protocol (CMS) during the adult phase. Three groups were divided among experimental conditions: 1) neonatal handling, 2) protocol and 3) neonatal handling and protocol. The used measures were: weight, ration and water intake and weekly tests over intake and fluid preference. Results found show that stressors protocol reduced weight of subjects from the manipulation group (MP) as for the ones from only stressors protocol group (P). Food and water intake also presented similar results for Groups P and MP: all subjects presented water intake enhance and ration intake reducing during protocol. For fluid intake and preference tests, both Group P and MP presented preference oscillation at no stressors period and sucrose intake enhance during protocol submission weeks, that means, they did not produced anhedonia. Results allow to assure that the group submitted to maternal manipulation with 15min mother s separation did not show any difference in comparison to the nohandling group, specially related to preference and intake tests, when submitted to CMS
Chronic Mild Stress (CMS) um modelo animal experimental de anedonia induzida através da exposição de ratos a um protocolo de estressores crônicos por um longo período de tempo. No Laboratório do Programa de Pós Graduação em Psicologia Experimental: Análise do Comportamento, uma linha de pesquisa sobre o CMS e a relação com o comportamento operante tem sido desenvolvida desde 2001, como em Pereira, 2009. Diferente de outros estudos realizados nesse laboratório, Pereira (2009) não observou redução da ingestão e preferência de sacarose (anedonia) durante os estressores. Uma das hipóteses levantadas foi que a manipulação neonatal tenha sido uma variável responsável por isso. O objetivo do presente estudo foi investigar se a manipulação neonatal, altera a ingestão e preferência de líquidos em ratos que passaram pelo protocolo de estressores (CMS) durante a fase adulta. Três grupos foram divididos entre as condições experimentais: 1) manipulação neonatal, 2) protocolo e 3) manipulação neonatal e protocolo. As medidas utilizadas foram: peso, consumo de ração e de água e testes semanais de ingestão e preferência de líquido. Os resultados encontrados mostram que o protocolo de estressores diminuiu o peso dos sujeitos tanto para o grupo que passou pela manipulação (MP) quanto para o que passou apenas pelo protocolo de estressores (P). O consumo de alimento e água também apresentou resultados semelhantes para os Grupos P e MP: todos apresentaram aumento na ingestão de água e diminuição do consumo de ração durante o protocolo. Para os testes de consumo e preferência de líquido, tanto o Grupo P quanto o MP apresentaram oscilação de preferência no período sem estressores e aumento da ingestão de sacarose durante as semanas de submissão ao protocolo, ou seja, não produziram anedonia. Os resultados permitem afirmar que o grupo que passou pelo procedimento de manipulação neonatal separados da mãe por 15min não apresentou diferença em comparação com o grupo que não foi manipulado, principalmente em relação aos testes de ingestão e preferência, quando submetidos ao CMS
Kreamelmeyer, Fred Dennis. "Teacher burnout : an analysis of the relationship between participation in an experimental undergraduate program and longevity of career." Virtual Press, 1985. http://liblink.bsu.edu/uhtbin/catkey/436969.
Full textKulkarni, Kanchan Avinash. "Experimental Characterization and Finite Element Simulation of Laser Shock Peening Induced Surface Residual Stresses using Nanoindentation." University of Cincinnati / OhioLINK, 2012. http://rave.ohiolink.edu/etdc/view?acc_num=ucin1352489043.
Full textXiao, Kewei. "A diffusion-viscous analysis and experimental verification of the drying behavior in nanosilver-enabled low-temperature joining technique." Diss., Virginia Tech, 2014. http://hdl.handle.net/10919/25137.
Full textPh. D.
Sahoo, Dipankar. "Experimental analysis of the vorticity and turbulent flow dynamics of a pitching airfoil at realistic flight (helicopter) conditions." Diss., Texas A&M University, 2008. http://hdl.handle.net/1969.1/85893.
Full textMercimek, Umit. "Shock Failure Analysis Of Military Equipments By Using Strain Energy Density." Master's thesis, METU, 2010. http://etd.lib.metu.edu.tr/upload/12612721/index.pdf.
Full texts dynamic characteristics and varying loadings. Therefore, experimental, numerical or a combination of both methods are used for evaluations. The experimental analysis of the shocks due to firing is done for 12.7mm Gatling gun and 25mm cannon. During the tests, the Gatling gun and the cannon are located on military Stabilized Machine Gun Platform and Stabilized Cannon Platform respectively. For the firing tests, ICP (integrated circuit piezoelectric) accelerometers are attached to obtain the loading history for corresponding points. Shock Response Spectrum (SRS) analysis (nCode Glypworks) is done to define the equivalent shock profiles created on test pieces and the mount of 25mm cannon by means of the gun and the cannon firing. Transient shock analysis of the test pieces and the mount are done by applying the obtained shock profiles on the parts in a finite element model (ANSYS). Furthermore, experimental stress analysis due to shock loading is performed for two different types of material and different thicknesses of the test pieces. The input data for the analysis is obtained through measurements from strain rosette precisely located at the critical location of the test pieces. As a result of the thesis, a proposal is tried to be introduced where strain energy density theory is applied to predict the shock failure at military structures.
Charonko, John James. "Studies of Stented Arteries and Left Ventricular Diastolic Dysfunction Using Experimental and Clinical Analysis with Data Augmentation." Diss., Virginia Tech, 2009. http://hdl.handle.net/10919/26875.
Full textPh. D.
TANAKA, Keisuke, Yoshiaki AKINIWA, Yoshihisa SAKAIDA, and Hirohisa KIMACHI. "Lattice Strain and Domain Switching Induced in Tetragonal PZT by Poling and Mechanical Loading." The Japan Society of Mechanical Engineers, 2000. http://hdl.handle.net/2237/9183.
Full textAndraéy, Erik. "Development of verified FE simulation method on crimp joint with gasket : A combined experimental and numerical study." Thesis, Blekinge Tekniska Högskola, Institutionen för maskinteknik, 2021. http://urn.kb.se/resolve?urn=urn:nbn:se:bth-21924.
Full textVid utveckling av kylarmoduler för drivlinor som appliceras i kommersiella fordon, är högsta prioritet att säkerhetsställa hållfastheten hos produkterna. Anledningen ligger kring den strukturomvandling som företag genomgår där storleken på lagerlokaler minskar och företagen väljer att förlita sig på transporterna som utförs av kommersiella fordon istället. Ifall en kylarmodul inte skulle klara av att bibehålla ett bestämt temperaturintervall hos drivlinan så dröjer det inte länge förens fordonet tvingas att stanna. I värsta fall kan fordonets stillestånd påverka ett företag att tvingas stanna i väntan. Därför är utveckling av FE simuleringsmetoder tillsammans med utmattningstest, några av de kärnaktiviteter som utförs för att säkerhetsställa hållfastheten av kylarmodulerna innan de implementeras i fordon. En av de metoder som ännu inte blivit tillräckligt verifierat gäller hur man utför FEA på ett falsförband med packning. Falsförbandet skapas genom en falsningsprocess där ändplåten av aluminium falsas över polyamidtanken, vilket skapar ett vattentätt förband med hjälp av packningen. Omfattningen av detta examensarbete gäller att verifiera de existerande simuleringsmetoderna av falsförbandet och bestämma felmarginalen med avseende på töjningar. Omfattningen av examensarbetet innefattar även ett utvecklingsarbete av en ny FE simuleringsmetod med en lägre felmarginal jämfört med de existerande metoderna. Verifieringen av metoderna sker genom en jämförelse mellan de numeriska resultaten och en experimentell spänningsanalys där töjningen på ändplåten är uppmätt med hjälp av trådtöjningsgivare i en tryckpulsationsrigg. Den genomsnittliga felmarginalen av de tre existerande metoderna för att simulera falsförbandet var 37,9%, 13,4%, och 11,5% vid den nedre dimensionerande yttre radien på falsförbandet vid ett tryck på 100 kPa. Den använda metoden för att bestämma felmarginalen upptäcktes senare vara felaktig, men det resulterar endast i små förändringar av den bestämda felmarginalen, de existerande simuleringsmetoderna är fortfarande sedda som otillräckliga. Metoden för att bestämma felmarginalen korrigerades sedan inför utvecklandet av den nya FE simuleringsmetoden av falsförbandet. Den utvecklade metoden i detta examensarbete har en genomsnittlig felmarginal på 6,9% vid 100, 160, 220 och 260 kPa.
Chivante, Maurício Roberto de Pinho. "Avaliação experimental das relações tensão-deformação de um tecido de fibra de vidro recoberto com PTFE." Universidade de São Paulo, 2009. http://www.teses.usp.br/teses/disponiveis/3/3144/tde-18122009-134136/.
Full textConsidering the growing use of tensioned membrane structures, the stress-strain relation of the fabric used on its construction must be well understood. This dissertation presents a study of the mechanical behavior of a PTFE coated fiberglass fabric, emphasizing its complex strain mechanism which is influenced by the material anisotropy, physical non-linearity, crimp interchange, hysteresis, removal of yarn spacing and changes in temperature. Different material models were studied, focusing on an orthotropic material model represented by a hyperelastic strain energy function. Also, different test protocols were reviewed and a series of biaxial tests on cruciform samples were performed at the Birdair, Inc.s Research and Development Center. A strain energy function was adjusted to the collected data and than its results compared to the data itself and to another stress-strain function directly adjusted to the data. The performance of the strain-energy function chosen is not on a level of industrial application; however this study gives a global understanding of the PTFE coated fiberglass strain mechanism and also provides a consistent database that may be used on real situations.
TANAKA, Keisuke, and Yoshiaki AKINIWA. "Diffraction Measurements of Residual Macrostress and Microstress Using X-Rays, Synchrotron and Neutrons." The Japan Society of Mechanical Engineers, 2004. http://hdl.handle.net/2237/9178.
Full textAzzabou-Kacem, Soundess. "Stress shift in English rhythm rule environments : effects of prosodic boundary strength and stress clash types." Thesis, University of Edinburgh, 2018. http://hdl.handle.net/1842/33200.
Full textEl-Hajjar, Rani Fayez. "Experimental study and analytical modeling of translayer fracture in pultruded FRP composites." Diss., Available online, Georgia Institute of Technology, 2004:, 2004. http://etd.gatech.edu/theses/available/etd-03152004-230942/unrestricted/elhajjar%5Frani%5Ff%5F200405%5Fphd.pdf.
Full textDr. Zureick, Abdul-Hamid, Committee Member; Dr. White, Donald, Committee Member; Dr. Saxena, Ashok, Committee Member; Dr. Jacobs, Laurence, Committee Member; Dr. Haj-Ali, Rami, Committee Chair; Dr. Armanios, Erian, Committee Member. Vita. Includes bibliographical references (leaves 164-172).
Stamatialis, Dimitrios F., Dimitrios N. Soulas, and Merope Sanopouloua. "Mechanisms of non-fickian micromolecular diffusion in glassy polymer films: analysis of experimental sorption and concurrent dilation kinetics in the light of a differential swelling stress model." Diffusion fundamentals 11 (2009) 10, S. 1-2, 2009. https://ul.qucosa.de/id/qucosa%3A13930.
Full textJob, Sarah. "Identity-Specific Positive Psychology Intervention for Sexual Minorities: A Randomized Control Trial." Digital Commons @ East Tennessee State University, 2021. https://dc.etsu.edu/etd/3891.
Full textDominguez, John Alexis. "INFLUÊNCIA DA INCORPORAÇÃO DE UM PLASTIFICANTE E UM POLIETILENO DE ALTO PESO MOLECULAR NAS PROPRIEDADES DE UMA RESINA EXPERIMENTAL E DIMINUIÇÃO DO ESTRESSE DE CONTRAÇÃO." UNIVERSIDADE ESTADUAL DE PONTA GROSSA, 2015. http://tede2.uepg.br/jspui/handle/prefix/1722.
Full textThe objectives of this study were: 1) to evaluate the degree of conversion, shrinkage stress, flexural and compressive strength of an experimental resin with a lactic polyacid and castor oil; 2) to evaluate the cytotoxicity of an experimental resin with a lactic polyacid, and castor oil; 3) evaluate, degree of conversion, shrinkage stress, flexural and compressive strength an experimental resin with addition of a high molecular weight polyethylene; 4) to assess the cytotoxicity of an experimental resin with addition of a high molecular weight polyethylene. Initially, it was synthesized a poly (lactic acid) (PLA) via a polycondensation process. After 24 hours, the castor oil (OR) was incorporated by an esterification process with N, N-Dicyclonecylcarbodimide and 99% 4-Dimethylamino-Pyridine in 40 mL of tetrahydrofuran. After this, the blend was characterized by X-ray diffraction (XRPD), Raman spectroscopy, scanning electron microscopy (SEM) and shrinkage stress, where was proven the incorporation of PLA + OR in the experimental composite resin. In the third chapter, PLA + OR were manipulated in two concentrations (1.5% and 3%) in an experimental composite: (2,2 bis [4- (2-hydroxy-3-metacrilatoxypropoxy) phenol] (BisGMA) Triethylene glycol dimethacrylate (TEGDMA), camphorquinone (CQ), N, N-dimethylaminoethyl methacrylate (DEMA-EMA), butylated hydroxytoluene (BHT), silanated barium borosilicate glass, and the tests of degree of conversion, compressive and flexural strength and shrinkage stress were made. The cytotoxicity assay was done; a suspension of 3 x 103 cells/mL of culture medium was prepared. For this, the cells were detached from the bottom of the bottle by the addition of trypsin with EDTA, after incubation in 5% CO2 with 3 mL Eagle's medium supplemented culture. After 24 h incubation period, the culture medium was removed and 200 uL of a solution of culture medium and methylltetrazolium salt (MTT). Subsequently, the analysis of mitochondrial activity was performed in a spectrophotometer (Biotek EL 800, Biotek, Winooski, VT, USA) with a 10 wavelength of 570 nm. The data from each test were analyzed by one-way ANOVA. No significant differences were found (p <0.005) in compressive and degree of conversion tests, and significant differences in shrinkage stress where obtained, up to 69% decrease. and flexion, statistically significant . In the fourth chapter, it was incorporated a high molecular weight polyethylene and polypropiylene, in the experimental resin proposed in chapter two, at two concentrations (1.5% and 3%), and tested by degree of conversion, compressive and flexural strength and shrinkage stress. The data from each test were analyzed by one way ANOVA, finding no significant difference (p> 0.005) in degree of conversion, compressive and flexural strength, and the contraction stress showed a significant reduction of up to 40%. Conclusion: PLA + castor oil and the high molecular weight polyethylene decreases the shrinkage stress and properties like flexural and compressive strength and degree of conversion were not influenced.
Os objetivos deste estudo foram: 1) avaliar o grau de conversão, tensão de contração, resistência à flexão e compressão de uma resina experimental com um poliácido lático e óleo de rícino; 2) avaliar a citotoxicidade de uma resina experimental com um poliácido lático e óleo de rícino; 3) avaliar o grau de conversão, tensão de contração, resistência à flexão e compressão de uma resina experimental com adição de um polietileno de alto peso molecular e 4) avaliar a citotoxicidade de uma resina experimental com adição de um polietileno de alto peso molecular. Previamente realizou-se a síntese de um Poli-ácido lático (PLA) por meio de um processo de policondensação. Após 24 horas, foi incorporado o óleo de rícino (OR) por meio de um processo de esterificação junto a N,N-Diciclonecilcarbodimida e 4-Dimetilamino-Piridina a 99% em 40 mL de tetrahidrofeurano. Em seguida, o conjunto foi caracterizado por difração de espectroscopia Raman, microscopia eletrônica de varredura (MEV) e estresse de contração, onde foi comprovada a incorporação do PLA+OR numa resina composta experimental. No terceiro capítulo foi feita a incorporação do PLA+OR em duas concentrações (1,5% e 3%) numa resina composta experimental: (2,2 bis[4-(2-hidroxi-3-metacrilatoxipropoxi)fenol](BisGMA), Trietilglicoldimetacrilato (TEGDMA), canforoquinona (CQ), N,N– dimetilaminoetil metacrilato (DMAEMA), hidroxitolueno butilado (BHT), vidro de borossilicato de bário silanizado e foram realizados os testes de flexão, compressão, grau de conversão e estresse de contração. Foi feito o teste de citotoxicidade, uma suspensão de 3 x 103 células/mL de meio de cultura foi preparada. Para isso, as células foram descoladas do fundo da garrafa por meio da adição de tripsina com EDTA, após incubação em estufa com 5% de CO2 e 3 mL de meio de cultura Eagle suplementado. Após o período de incubação de 24 h, o meio de cultura foi removido e 200 μL de uma solução de meio de cultura e sal metiltetrazólio (MTT).Posteriormente, a análise da atividade mitocondrial foi realizada em espectrofotômetro (Biotek EL 800, Biotek, Winooski, VT, EUA) com comprimento de onda de 570 nm. Os dados obtidos de cada teste foram analisados com ANOVA um fator. Não encontrou-se diferença significativa (p> 0.005) nos testes de compressão e grau de conversão; já para o teste de estresse de contração, houve diminuição estatisticamente significativa de até 69% e no teste de resistência à flexão . No quarto capítulo foi feita a incorporação de um polipropileno (PP) e o polietileno de ultra-alto peso molecular (UTEC) a uma resina experimental com os mesmos materiais manipulados no capítulo dois, em duas concentrações (1,5% e 3%), e realizados os testes de compressão, flexão, grau de conversão e estresse de contração. Os dados de cada teste foram analisados com ANOVA um fator. Não houve diferença significativa (p> 0.005) nos testes de compressão, flexão e grau de conversão; já para o teste de estresse de contração houve diminuição estatisticamente significativa de até 40%. Conclusão: OPLA+óleo de rícino e o polietileno de ultra alto peso molecular em 1,5%, diminuíram o estresse de contração e propriedades como resistência à flexão, compressão e grau de conversão não foram influenciadas.
Hurley, Caitlin Mae. "Kinetic study of hydrogen-material interactions in nickel base alloy 600 and stainless steel 316L through coupled experimental and numerical analysis." Phd thesis, Toulouse, INPT, 2015. http://oatao.univ-toulouse.fr/14454/1/hurley.pdf.
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