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Relevant bibliographies by topics / Flame photometric detector

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Academic literature on the topic 'Flame photometric detector'

Author: Grafiati

Published: 4 June 2021

Last updated: 1 February 2022

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Journal articles on the topic "Flame photometric detector"

1

Sun, Xun-Yun, and Walter A. Aue. "Detection at the picogram level of bis(cyclopentadienyl)ruthenium by gas chromatography – flame photometry." Canadian Journal of Chemistry 67, no. 5 (May 1, 1989): 897–901. http://dx.doi.org/10.1139/v89-138.

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Ruthenocene — bis(cyclopentadienyl)ruthenium — can be determined with surprisingly high sensitivity and selectivity by gas chromatography – flame photometry. The detector's response relies mainly on an unidentified emission system (RuH?) with major peaks at 484 and 528 nm, while some familiar atomic lines show up as well. Without interference filter, the minimum detectable amount of ruthenocene, at S/N = 2, is approximately 2 pg (or 2 × 10−13 g/s or 1 × 10−15 mol/s), the elemental selectivity ruthenium/carbon 4 × 105, and the linear range 1:4 × 104. These calibration characteristics place ruthenium among the strongest luminescing and best performing species in the flame photometric detector. In fact, under conditions optimized for ruthenocene, ruthenium responds stronger than other FPD-active atoms (Sn, P, Cr, S, B). Fortunately, quenching effects are very weak: for instance, it takes about 1600 ppm (v/v) of methane in the detector to reduce the ruthenocene peak height by 50%.Keywords: ruthenocene, gas chromatography, flame photometric detector, ruthenium hydride.

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2

Tzanani, Nitzan, and Aviv Amirav. "Combined Pulsed Flame Photometric Ionization Detector." Analytical Chemistry 67, no. 1 (January 1995): 167–73. http://dx.doi.org/10.1021/ac00097a026.

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3

Aue, Walter A., and Xun-yun Sun. "Quenching in the flame photometric detector." Journal of Chromatography A 641, no. 2 (July 1993): 291–99. http://dx.doi.org/10.1016/0021-9673(93)80145-x.

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4

Ogasawara, Minoru, Kyoko Tsuruta, and Shinsuke Arao. "Flame photometric detector for thin-layer chromatography." Journal of Chromatography A 973, no. 1-2 (October 2002): 151–58. http://dx.doi.org/10.1016/s0021-9673(02)01117-2.

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Singh, Hameraj, and Walter A. Aue. "Analyte noise in the flame photometric detector." Journal of Chromatography A 724, no. 1-2 (February 1996): 251–54. http://dx.doi.org/10.1016/0021-9673(95)00916-7.

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6

Kilany, A. Y., Mohamed A. Elsayed, M. K. Abd El Megid, and M. S. Fayed. "Study of the Effect of Air to Fuel Ratio Parameter on the Organophosphorus – Pesticide Analysis by GC-FPD." International Letters of Chemistry, Physics and Astronomy 36 (July 2014): 236–48. http://dx.doi.org/10.18052/www.scipress.com/ilcpa.36.236.

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In the present contribution, sensitive and precise method for the quantification of Organophosphorus / Pesticides (Malathion and Dimethoate) in nanograms range has been developed. The performance of flame photometric detector (FPD), a selective detector (P&S-mode) that can be used in the analysis of organophosphorus compound, is evaluated in terms of sensitivity, selectivity and reproducibility. The performance of flame photometric detector was strongly depending on the absolute and relative flow rate of air and hydrogen gases. The optimum air-to-fuel ratio for detection of Malathion and Dimethoate was 0.4 and 0.3 (FPD-P mode). At this ratio, low picogram amounts of phosphor can be detected accurately (0.18 pgP) with a wide linear dynamic range of 0.18 pgP to 298 ngP. While, the optimum air-to-fuel ratio, for detection of Malathion and Dimethoate was 0.6 (FPD-S mode). In addition to, the method is precise with 4.5 % relative standard deviation (RSD). In conclusion, it could be proposed that this procedure can be recommended as a suitable method for the quantification of Malathion and Dimethoate in cases of acute poisoning.

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Fowler, William K. "Response of the flame-photometric detector to ammonia." Analytical Chemistry 63, no. 23 (December 1991): 2798–800. http://dx.doi.org/10.1021/ac00023a024.

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Singh, Hameraj, Brian Millier, and Walter A. Aue. "Time-integrated spectra from a flame photometric detector." Journal of Chromatography A 724, no. 1-2 (February 1996): 255–64. http://dx.doi.org/10.1016/0021-9673(95)00926-4.

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Thurbide, Kevin B., and Walter A. Aue. "High-throughput reactor for simulating the flame photometric detector." Journal of Chromatography A 905, no. 1-2 (January 2001): 241–50. http://dx.doi.org/10.1016/s0021-9673(00)00991-2.

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10

Barinaga, C. J., and S. O. Farwell. "Dead volume reduction in a commercial flame photometric detector." Journal of High Resolution Chromatography 9, no. 8 (August 1986): 474–76. http://dx.doi.org/10.1002/jhrc.1240090815.

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Dissertations / Theses on the topic "Flame photometric detector"

1

Khayamian, Taghi. "Electrospray as a new sample introduction technique for the flame photometric detector." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1997. http://www.collectionscanada.ca/obj/s4/f2/dsk3/ftp04/nq24775.pdf.

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Bernard, Joël. "Design and characterization of a thermochemical high performance liquid chromatography flame photometric detector for the detection of non-volatile andor thermolabile sulfur compounds." Thesis, McGill University, 1999. http://digitool.Library.McGill.CA:80/R/?func=dbin-jump-full&object_id=35982.

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The need for selective and inexpensive detectors in liquid chromatography is of considerable interest in the determination of sulfur compounds. Of the available-selective sulfur methodologies, flame photometric detector coupled to gas chromatography is the most widely used. It has proven to be a sensitive and selective method for detection of heat stable and volatile sulfur compounds. Fundamentally, this technique is not applicable to high boiling and/or thermolabile sulfur compounds. More recently, hyphenated flame photometric detector has been utilized, with limited success, to monitor sulfur species in liquid chromatography. However, existing HPLC-FPD methodologies have never been applied to real samples, due to the low population of S 2, the emitting species, and the quenching effects of the other species present in the flame.
In this work, two total consumption high-performance liquid chromatography flame photometric (HPLC-FPD) interfaces compatible with either methanolic or aqueous mobile phases are described and optimized for monitoring low volatile and thermally fragile sulfur compounds in biological samples. Each interface was fuelled either by methanol or by hydrogen. The all quartz interfaces enclosed four consecutive thermal processes: (a) thermovaporization of the HPLC effluent; (b) pyrolysis of the organic matrix (including sulfur species) in a kinetic H2/O2 flame; (c) conversion of the oxidized sulfur compounds to H2S in a reducing post-combustion stage fuelled by hydrogen; and (d) transport of the generated hydrides towards a hydrogen radical rich surrounding of an inverted hydrogen-oxygen diffusion flame. Chemiluminescence induced in the last step was integrated as a narrow beam in a light-guide positioned remotely from the analytical cool flame and oriented towards a photomultiplier unit. Radioisotopic assays demonstrated that sulfur (as H235SO4) was transferred quantitatively to the analytical flame. Indirect evidence suggested that sulfur was hydrogenated in the post-combustion step via a thermochemical hydride generation process to mediate the formation of S2. The linearity of calibration graphs (0.9950 < r < 0.9986), where r is the correlation coefficient) and unprecedented HPLC-FPD limits of detection for sulfur compounds (1.5 etag/s for 2-methylthiophene, 2.25 etag/s for carbon disulfide, and 4.5 etag/s for ethanesulfonic acid) allowed for the speciation of sulfur species in garlic extracts. Alternatively, modification of the methanol fuelled interface to a hydrogen fuelled reactor allowed detection of thiosulfinates and high molecular weight sulfur compounds in horse kidney and garlic extracts, respectively.

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Bernard, Joel. "Design and characterization of a thermochemical high performance liquid chromatography flame photometric detector for the detection of non-volatile and/or thermolabile sulfur compounds." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1999. http://www.collectionscanada.ca/obj/s4/f2/dsk1/tape7/PQDD_0015/NQ55302.pdf.

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Daphney, Cedrick M. "The Fate and Transport of Chemical Warfare Agent Simulants in Complex Matrices." Digital Archive @ GSU, 2008. http://digitalarchive.gsu.edu/chemistry_theses/13.

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Experiments to determine the fate and transport of the chemical warfare agent (CWA) simulants diisopropyl fluorophosphate (DIFP), O,S-diethyl methylphosphonothioate (OSDEMP), and 2-Chloroethyl ethyl sulfide (CEES) exposed to complex matrix systems are reported here. The aforementioned simulants were used in place of O-isopropyl methylphosphonofluoridate (GB), O-Ethyl S-(2-diisopropylaminoethyl) methylphosphonothiolate (VX), and Bis (2-chloroethyl) sulfide (HD), respectively. At ambient temperature, simulant pH (2.63 to 12.01) and reaction time (1 minute to 24 hours) were found to have significant influence on the recovery of simulants from charcoal, plastic, and TAP (butyl rubber gloves) in aqueous media. Buffer systems used included, phosphate, acetate, borate, and disodium tetraborate. Organic extractions were carried out using a 90:10 (v/v) dichloromethane / 2-propanol solution. All extracts were analyzed with a gas chromatograph equipped with flame ionization and flame photometric detectors (GC-FID-FPD). The FPD was used to determine the amount of simulant recovery.

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Russell, Duncan William. "The measurement of dimethylsulphide precursors in marine and terrestrial flora." Thesis, University of Southampton, 1996. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.242458.

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6

Shi, Changhong. "Simultaneous derivatization and flame photometric detection of some elements from Groups 8 and 14." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1998. http://www.collectionscanada.ca/obj/s4/f2/dsk2/ftp03/MQ36375.pdf.

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Lin, Huang-Hui, and 林晃暉. "Determination of Chromium by Gas Chromatography/Flame Photometric Detection Method." Thesis, 1997. http://ndltd.ncl.edu.tw/handle/86015882044679246285.

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Ting, Tsou-Hui, and 丁佐蕙. "Determination of Chromium by Solid-Phase Microextraction and Gas Chromatography/Flame Photometric Detection Method." Thesis, 2002. http://ndltd.ncl.edu.tw/handle/61185494692913918224.

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Li, Jen-Yi, and 李貞儀. "Analysis of Aluminum by Single-Drop Microextraction Coupled with Gas Chromatography/Flame Photometric Detection." Thesis, 2008. http://ndltd.ncl.edu.tw/handle/57239839434059685316.

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Yeh, Chun-Hung, and 葉俊宏. "The Analysis of Ordorous Sulfur Compounds in Air by Gas Ciromatography with Flame Photometric Detection." Thesis, 1997. http://ndltd.ncl.edu.tw/handle/61987714116995535154.

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碩士
淡江大學
化學學系
85
The thesis is according to "Programmed Temperature Vaporization injection" and " Programmed Temperature Thermal Desorption injection " for analyzing the sulfur compounds in air with solid adsorbent preconcentration. Packing adsorbent into the glass liner to be a adsorbent tube , then sampling the air from polluted area. After sampling, the adsorbent tube was put into the injection port of the GC for thermal desorption , then the sulfur gases were thermally released according to programmed temperature from the adsorbent trap . At the same time , cooling front section of the column with liquid nitrogen . The flame photometric detector ( FPD ) was uesd . The FPD has good response to sulfur compounds, but the disadventages are non-liner response andquenched by non-sulfur compound. Volatile and non-volatile sulfur compoundwere compared on FPD and Flameless SCD. We found the Flameless SCD has highseletivity for sulfur compounds. The detection limit of FPD for dimethylsulfide and dimethyl disulfide are 11.63 pgS and 18.58 pgS respectively . The ability of adsorption for Tenax-TA and Tenax-GR are compared . Tenax-GR has better adsorption ability than Tenax-TA. In addition,we also build the profileof sulfide compounds from Taiwan's petrochemistry company. For the surrounding air of pigsty , sulfur dioxide , dimethyl sulfide and dimethyl disulfide were detected.

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Books on the topic "Flame photometric detector"

1

Jha, Virendra K. Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory: Determination of organophosphate pesticides in bottom sediment by gas chromatography with flame photometric detection. Denver, Colo: U.S. Dept. of the Interior, U.S. Geological Survey, 2003.

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2

Jha, Virendra K. Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory: Determination of organophosphate pesticides in bottom sediment by gas chromatography with flame photometric detection. Denver, Colo: U.S. Dept. of the Interior, U.S. Geological Survey, 2003.

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3

Jha, Virendra K. Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory: Determination of organophosphate pesticides in whole water by continuous liquid-liquid extraction and capillary-column gas chromatography with flame photometric detection. Denver, Colo: U.S. Dept. of the Interior, U.S. Geological Survey, 2003.

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Jha, Virendra K. Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory: Determination of organophosphate pesticides in whole water by continuous liquid-liquid extraction and capillary-column gas chromatography with flame photometric detection. Denver, Colo: U.S. Dept. of the Interior, U.S. Geological Survey, 2003.

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5

S, Wydoski Duane, and Geological Survey (U.S.), eds. Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory: Determination of organophosphate pesticides in filtered water by gas chromatography with flame photometric detection. Denver, Colo: U.S. Dept. of the Interior, U.S. Geological Survey, 2002.

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Book chapters on the topic "Flame photometric detector"

1

Muccio, Alfonso, Anna M. Cicero, Antonella Ausili, and Stefano Muccio. "Determination of Organophosphorus Pesticide Residues in Vegetable Oils by Single-Step Multicartridge Extraction and Cleanup and by Gas Chromatography With Flame Photometric Detector." In Pesticide Protocols, 263–71. Totowa, NJ: Humana Press, 2006. http://dx.doi.org/10.1385/1-59259-929-x:263.

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2

"Flame Photometry." In Detection Technologies for Chemical Warfare Agents and Toxic Vapors, 135–52. CRC Press, 2004. http://dx.doi.org/10.1201/9780203485705.ch7.

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3

Kataoka, Hiroyuki, Noritoshi Hirabayashi, and Masami Makita. "[18] Analysis of lipoic acid by gas chromatography with flame photometric detection." In Methods in Enzymology, 166–76. Elsevier, 1997. http://dx.doi.org/10.1016/s0076-6879(97)79020-7.

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4

Lodge, James P. "Determination of Sulfur-Containing Gases in the Atmosphere (Continuous Method with Flame Photometric Detector): Determination of Sulfur-Containing Gases in the Atmosphere (Following Chromatographic Separation, with the FPD), Determination of Sulfur-Containing Gases in the Atmosphere (Total Gaseous Sulfur with the FPD)." In Methods of Air Sampling and Analysis, 512–22. Routledge, 2017. http://dx.doi.org/10.1201/9780203747407-94.

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Conference papers on the topic "Flame photometric detector"

1

Zhang, Daoshan, Zhaohui Zhang, and Zhijun Li. "The P, S, CI Flame Photometric Sensors Fusion and Intelligent Detection." In 2012 International Conference on Computer Distributed Control and Intelligent Environmental Monitoring (CDCIEM). IEEE, 2012. http://dx.doi.org/10.1109/cdciem.2012.188.

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Reports on the topic "Flame photometric detector"

1

Longworth, Terri L., John M. Baranoski, and Kwok Y. Ong. Domestic Preparedness Program: Evaluation of the Agilent Gas Chromatograph - Flame Photometric Detector/Mass Selective Detector (GC-FPD/MSD) System Against Chemical Warfare Agents Summary Report. Fort Belvoir, VA: Defense Technical Information Center, May 2003. http://dx.doi.org/10.21236/ada416884.

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Logan, Thomas P., Edward D. Allen, Mark R. Way, Austin T. Swift, and Sunil-Datta Soni. A Method for the Analysis of Tabun in Multisol Using Gas Chromatographic Flame Photometric Detection. Fort Belvoir, VA: Defense Technical Information Center, May 2006. http://dx.doi.org/10.21236/ada469216.

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Mayer, B. P., A. M. Williams, R. N. Leif, and A. K. Vu. Extraction of Phosphonic Acids from Urine Samples and Analysis by Gas Chromatography with Detection by Mass Spectrometryand Flame Photometric Detection. Office of Scientific and Technical Information (OSTI), December 2013. http://dx.doi.org/10.2172/1116967.

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4

Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory : determination of organophosphate pesticides in bottom sediment by gas chromatography with flame photometric detection. US Geological Survey, 2003. http://dx.doi.org/10.3133/wri024222.

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5

Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory; determination of organophosphate pesticides in filtered water by gas chromatography with flame photometric detection. US Geological Survey, 2002. http://dx.doi.org/10.3133/wri024071.

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6

Methods of analysis by the U.S. Geological Survey National Water Quality Laboratory : determination of organophosphate pesticides in whole water by continuous liquid-liquid extraction and capillary-column gas chromatography with flame photometric detection. US Geological Survey, 2003. http://dx.doi.org/10.3133/wri034139.

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