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Journal articles on the topic 'Flame photometric detector'

Author: Grafiati

Published: 4 June 2021

Last updated: 1 February 2022

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1

Sun, Xun-Yun, and Walter A. Aue. "Detection at the picogram level of bis(cyclopentadienyl)ruthenium by gas chromatography – flame photometry." Canadian Journal of Chemistry 67, no. 5 (May 1, 1989): 897–901. http://dx.doi.org/10.1139/v89-138.

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Ruthenocene — bis(cyclopentadienyl)ruthenium — can be determined with surprisingly high sensitivity and selectivity by gas chromatography – flame photometry. The detector's response relies mainly on an unidentified emission system (RuH?) with major peaks at 484 and 528 nm, while some familiar atomic lines show up as well. Without interference filter, the minimum detectable amount of ruthenocene, at S/N = 2, is approximately 2 pg (or 2 × 10−13 g/s or 1 × 10−15 mol/s), the elemental selectivity ruthenium/carbon 4 × 105, and the linear range 1:4 × 104. These calibration characteristics place ruthenium among the strongest luminescing and best performing species in the flame photometric detector. In fact, under conditions optimized for ruthenocene, ruthenium responds stronger than other FPD-active atoms (Sn, P, Cr, S, B). Fortunately, quenching effects are very weak: for instance, it takes about 1600 ppm (v/v) of methane in the detector to reduce the ruthenocene peak height by 50%.Keywords: ruthenocene, gas chromatography, flame photometric detector, ruthenium hydride.

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2

Tzanani, Nitzan, and Aviv Amirav. "Combined Pulsed Flame Photometric Ionization Detector." Analytical Chemistry 67, no. 1 (January 1995): 167–73. http://dx.doi.org/10.1021/ac00097a026.

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3

Aue, Walter A., and Xun-yun Sun. "Quenching in the flame photometric detector." Journal of Chromatography A 641, no. 2 (July 1993): 291–99. http://dx.doi.org/10.1016/0021-9673(93)80145-x.

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4

Ogasawara, Minoru, Kyoko Tsuruta, and Shinsuke Arao. "Flame photometric detector for thin-layer chromatography." Journal of Chromatography A 973, no. 1-2 (October 2002): 151–58. http://dx.doi.org/10.1016/s0021-9673(02)01117-2.

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5

Singh, Hameraj, and Walter A. Aue. "Analyte noise in the flame photometric detector." Journal of Chromatography A 724, no. 1-2 (February 1996): 251–54. http://dx.doi.org/10.1016/0021-9673(95)00916-7.

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6

Kilany, A. Y., Mohamed A. Elsayed, M. K. Abd El Megid, and M. S. Fayed. "Study of the Effect of Air to Fuel Ratio Parameter on the Organophosphorus – Pesticide Analysis by GC-FPD." International Letters of Chemistry, Physics and Astronomy 36 (July 2014): 236–48. http://dx.doi.org/10.18052/www.scipress.com/ilcpa.36.236.

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In the present contribution, sensitive and precise method for the quantification of Organophosphorus / Pesticides (Malathion and Dimethoate) in nanograms range has been developed. The performance of flame photometric detector (FPD), a selective detector (P&S-mode) that can be used in the analysis of organophosphorus compound, is evaluated in terms of sensitivity, selectivity and reproducibility. The performance of flame photometric detector was strongly depending on the absolute and relative flow rate of air and hydrogen gases. The optimum air-to-fuel ratio for detection of Malathion and Dimethoate was 0.4 and 0.3 (FPD-P mode). At this ratio, low picogram amounts of phosphor can be detected accurately (0.18 pgP) with a wide linear dynamic range of 0.18 pgP to 298 ngP. While, the optimum air-to-fuel ratio, for detection of Malathion and Dimethoate was 0.6 (FPD-S mode). In addition to, the method is precise with 4.5 % relative standard deviation (RSD). In conclusion, it could be proposed that this procedure can be recommended as a suitable method for the quantification of Malathion and Dimethoate in cases of acute poisoning.

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7

Fowler, William K. "Response of the flame-photometric detector to ammonia." Analytical Chemistry 63, no. 23 (December 1991): 2798–800. http://dx.doi.org/10.1021/ac00023a024.

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8

Singh, Hameraj, Brian Millier, and Walter A. Aue. "Time-integrated spectra from a flame photometric detector." Journal of Chromatography A 724, no. 1-2 (February 1996): 255–64. http://dx.doi.org/10.1016/0021-9673(95)00926-4.

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9

Thurbide, Kevin B., and Walter A. Aue. "High-throughput reactor for simulating the flame photometric detector." Journal of Chromatography A 905, no. 1-2 (January 2001): 241–50. http://dx.doi.org/10.1016/s0021-9673(00)00991-2.

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10

Barinaga, C. J., and S. O. Farwell. "Dead volume reduction in a commercial flame photometric detector." Journal of High Resolution Chromatography 9, no. 8 (August 1986): 474–76. http://dx.doi.org/10.1002/jhrc.1240090815.

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11

Clark, Adrian G., and Kevin B. Thurbide. "An improved multiple flame photometric detector for gas chromatography." Journal of Chromatography A 1421 (November 2015): 154–61. http://dx.doi.org/10.1016/j.chroma.2015.04.007.

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12

McKelvie, Kaylan H., and Kevin B. Thurbide. "Analysis of sulfur compounds using a water stationary phase in gas chromatography with flame photometric detection." Analytical Methods 9, no. 7 (2017): 1097–104. http://dx.doi.org/10.1039/c6ay03017c.

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13

Clark, Adrian G., and Kevin B. Thurbide. "Spectral examination of a multiple-flame photometric detector for use in chromatography." Canadian Journal of Chemistry 92, no. 7 (July 2014): 629–34. http://dx.doi.org/10.1139/cjc-2014-0159.

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An examination of the emission spectra produced in a novel multiple-flame photometric detector (mFPD) was performed and directly compared to spectra obtained from a conventional single-flame FPD mode. Through monitoring a broad spectral range from 250 to 850 nm, it was found that the mFPD produces sulfur emission predominantly as S2*, but HSO* can also be isolated in the red spectral region. Further, phosphorus emission in the mFPD was found to stem from HPO*, while carbon emission was attributed to CH* and C2*. Finally, background emission in the mFPD was determined to be from OH*. Qualitatively, these finding agree very well with the species found in a conventional single-flame FPD. However, quantitatively, the mFPD spectra consistently produced analyte emission bands that were relatively more intense, by as much as a factor of 3. In contrast with this, hydrocarbon spectra in the mFPD yielded significantly reduced relative intensities, owing to decreased C2* emission. As well, aromatic and aliphatic hydrocarbons produced much more similar distributions of CH* and C2* emission in the mFPD than in the conventional single-flame FPD mode. The results indicate that a relative reduction of C2 radical and an increase of oxidized carbon in the analytical flame of the mFPD could play a central role in the observed quenching-resistant behavior of this detector.

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14

Jing, Hongwu, and Aviv Amirav. "Pulsed flame photometric detector – a step forward towards universal heteroatom selective detection." Journal of Chromatography A 805, no. 1-2 (May 1998): 177–215. http://dx.doi.org/10.1016/s0021-9673(97)01306-x.

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15

Ni, Lanxiu, Xuhui Geng, Shenghong Li, Haijing Ning, Yan Gao, and Yafeng Guan. "A flame photometric detector with a silicon photodiode assembly for sulfur detection." Talanta 207 (January 2020): 120283. http://dx.doi.org/10.1016/j.talanta.2019.120283.

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16

Hayward, Taylor C., and Kevin B. Thurbide. "Quenching-Resistant Multiple Micro-Flame Photometric Detector for Gas Chromatography." Analytical Chemistry 81, no. 21 (November 2009): 8858–67. http://dx.doi.org/10.1021/ac901421s.

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17

Quincoces, C. E., and M. G. González. "Characterization of the flame photometric detector in the sulphur mode." Chromatographia 20, no. 6 (June 1985): 371–75. http://dx.doi.org/10.1007/bf02269065.

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18

Sun, Xun-Yun, and Walter A. Aue. "Constancy of spectral response ratios in the flame photometric detector." Journal of Chromatography A 667, no. 1-2 (April 1994): 191–203. http://dx.doi.org/10.1016/0021-9673(94)89067-6.

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19

Aue, Walter A., Cecil G. Eisener, Jennifer A. Gebhardt, and Nancy B. Lowery. "Second-channel designs for a single-channel flame photometric detector." Journal of Chromatography A 699, no. 1-2 (May 1995): 195–201. http://dx.doi.org/10.1016/0021-9673(95)00093-3.

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20

Hayward, Taylor C., and Kevin B. Thurbide. "Characteristics of sulfur response in a micro-flame photometric detector." Journal of Chromatography A 1105, no. 1-2 (February 2006): 66–70. http://dx.doi.org/10.1016/j.chroma.2005.09.031.

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21

Sun, Xun-Yun, Brian Millier, and Walter A. Aue. "Flame photometric detection of some transition metals. I. Calibrations and spectra." Canadian Journal of Chemistry 70, no. 4 (April 1, 1992): 1129–42. http://dx.doi.org/10.1139/v92-149.

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After gas-chromatographic separation as volatile organometallics, some transition elements were found to respond with analytically relevant sensitivities in the flame photometric detector. Their minimum detectable amounts, in mole of metal per second at an S/Np-t-p ratio of 2, were 1 × 10−14 for nickel and 6 × 10−13 for rhenium, as well as a less sensitive 2 × 10−12 for molybdenum and 3 × 10−12 for cobalt. (When divided by 3.7, these values yield the S/σ = 3 limit of detection as recommended by IUPAC.) Calibration curves were established for these elements in comparison with transition metals already known to respond in the flame photometric detector. Their chemiluminescent spectra, together with that of chromium, were measured in the detector at analytically (as opposed to spectroscopically) optimized conditions. Atomic lines, molecular bands, and continua were all present. Also, the spectra produced by several types of carbon compounds were recorded for a definition of potential spectral interferences from hydrocarbonaceous sample matrices. The atomic lines and the massive continua displayed by certain metals are discussed in some detail. Atomic lines appear up to a limiting energy level of 3.6 eV above ground state. It is suggested that continua could arise from small, perhaps catalytically active particles. Also discussed, in accordance with a reviewer's request, are the analytical performance of the FPD compared to ICP and MIP sources, and the definition and influence of noise on measured performance criteria.

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22

Millier, Brian, Xun-Yun Sun, and Walter A. Aue. "Multichannel chromatography and on-line spectra from a flame photometric detector." Journal of Chromatography A 675, no. 1-2 (July 1994): 155–75. http://dx.doi.org/10.1016/0021-9673(94)85270-7.

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23

Gebhardt, Jennifer A., and Walter A. Aue. "Converting a single-channel flame photometric detector to triple-channel operation." Journal of Chromatography A 721, no. 2 (January 1996): 365–68. http://dx.doi.org/10.1016/0021-9673(95)00799-7.

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24

Aue, Walter A., Brian Millier, and Xun-Yun Sun. "Flame photometric detection of some transition metals. II. Enhancement of selectivity." Canadian Journal of Chemistry 70, no. 4 (April 1, 1992): 1143–55. http://dx.doi.org/10.1139/v92-150.

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A flame photometric detector was used in single-channel and in differential dual-channel modes to characterize and control its selectivity for various transition elements against a hydrocarbon background. The experiments included gas-chromatographable compounds of Cr, Mn, Fe, Co, Ni, Ru, Re, and Os. Single-channel dispersive modes brought only modest gains in selectivity vis-a-vis the non-dispersive (no optical filter) mode. In dual-channel differential modes, however, metal–carbon selectivities could be improved by factors of one to two orders of magnitude. The highest still measurable selectivity ratios are now in excess of 107. The differential dual-channel operation of the detector also made it possible to increase the selectivity of one hetero-element vis-a-vis another; and to distinguish between two hetero-elements, by oppositely directed peaks, in a (spectrally suppressed) matrix of carbon compounds. Metal–metal selectivities could be improved by factors of one to three orders of magnitude over the best dispersive single-channel modes.

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25

Karnicky, J. F., L. T. Zitelli, and S. Van der Wal. "Ultrasonic micronebulizer inferface for high-performance liquid chromatography with flame photometric detector." Analytical Chemistry 59, no. 2 (January 15, 1987): 327–33. http://dx.doi.org/10.1021/ac00129a023.

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26

Ming-de, Xu, and Jiang Gui-bin. "Determination of butyltin in seawater by gas chromatography with flame photometric detector." Chinese Journal of Oceanology and Limnology 17, no. 4 (December 1999): 385–88. http://dx.doi.org/10.1007/bf02842835.

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27

Satto, Isao, Sadaji Yamada, Harumi Oshtma, Yoshttomo Ikai, Hisao Oka, and Junko Hayakawa. "Analysis of Methyl Isothiocyanate in Wine by Gas Chromatography with Dual Detection." Journal of AOAC INTERNATIONAL 77, no. 5 (September 1, 1994): 1296–99. http://dx.doi.org/10.1093/jaoac/77.5.1296.

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Abstract Methyl isothiocyanate (MITC) was extracted from a 5 mL wine sample with 2 mL dichloromethane, and the extract was washed with 5% sodium chloride solution. MITC was determined by gas chromatography with a dual nitrogen-phosphorus detector (NPD) and a flame photometric detector (FPD, S mode) (DB-210 column, 30 m × 0.53 mm id, column temperature, 70°C). The limit of detection and quantitation of MITC with NPD–GC were 0.003 and 0.01 ppm, respectively. Average recoveries of MITC added to wine at 1 and 0.1 ppm were over 95%. This method is simple and rapid for routine analysis of MITC in wine.

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28

Aue, Walter A., Bernard J. Flinn, Christopher G. Flinn, Veluppillai Paramasigamani, and Kathleen A. Russell. "Transformation and transmission of organotin compounds inside a gas chromatograph." Canadian Journal of Chemistry 67, no. 3 (March 1, 1989): 402–10. http://dx.doi.org/10.1139/v89-063.

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A wide variety of mono-, di-, and tri-substituted tin compounds are transformed to, and transmitted as, chlorides, bromides, or iodides on injection into a gas chromatographic system doped with HCl, HBr, or HI, respectively. This transformation occurs directly from some thirty-odd analytes such as organotin oxides, hydroxides, organic esters, and other halides including fluorides. Three germanium compounds appear to behave similarly. A conventional, packed-column gas chromatographic set-up with flame photometric or flame ionization detector can tolerate the necessary acid doping. Compounds such as bis(tributyltin) oxide will elute, as halides, in subpicogram amounts. If the dopant flow is turned off, the packed column can act as a hydrogen halide reservoir for several days of operation. The transformations of tributyltin species into the halide form are generally fast on the timescale of chromatographic processes, i.e. sharp peaks result from the use of mixed hydrogen halides, and the retention time of mixed-halide peaks can be adjusted by varying the dopant composition. Keywords: organotins, gas chromatography, derivatization, acid doping, photometric detection.

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29

Kientz, Charles E., and Albert Verweij. "The Application of a Flame Photometric Detector in Packed Microcapillary Liquid Chromatography: Detection of Organophosphates." International Journal of Environmental Analytical Chemistry 30, no. 4 (August 1987): 255–63. http://dx.doi.org/10.1080/03067318708075474.

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30

Kilany, A., M. Elsayed, M. Fayed, and M. Abd ElMegid. "APPLICATION OF GAS CHROMATOGRAPHY FOR THE ANALYSIS OF MALATHION BY FLAME PHOTOMETRIC DETECTOR." International Conference on Chemical and Environmental Engineering 6, no. 6 (May 1, 2012): 1–12. http://dx.doi.org/10.21608/iccee.2012.35848.

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31

Driscoll, J. N., and A. W. Berger. "Improved flame photometric detector for the analysis of sulfur compounds by gas chromatography." Journal of Chromatography A 468 (May 1989): 303–8. http://dx.doi.org/10.1016/s0021-9673(00)96324-6.

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32

OKAZAKI, Shigemitu, and Yoshihito SUZUKI. "Flame photometric detector of micro liquid chromatography by means of electrospray of eluent." NIPPON KAGAKU KAISHI, no. 9 (1988): 1583–86. http://dx.doi.org/10.1246/nikkashi.1988.1583.

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33

Liu, G. H., and P. R. Fu. "Effects of hydrocarbon quenching in gas chromatography when using the flame photometric detector." Chromatographia 27, no. 3-4 (February 1989): 159–63. http://dx.doi.org/10.1007/bf02265869.

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34

Dachs, J., and J. M. Bayona. "Optimization of a flame photometric detector for supercritical fluid chromatography of organotin compounds." Journal of Chromatography A 636, no. 2 (April 1993): 277–83. http://dx.doi.org/10.1016/0021-9673(93)80242-z.

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35

Thurbide, Kevin B., Brad W. Cooke, and Walter A. Aue. "Novel flame photometric detector for gas chromatography based on counter-current gas flows." Journal of Chromatography A 1029, no. 1-2 (March 2004): 193–203. http://dx.doi.org/10.1016/j.chroma.2003.12.020.

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36

Singh, Hameraj, Cecil G. Eisener, and Walter A. Aue. "Dual-channel flame photometric detector for sensitive spectrum acquisition and variable-wavelength operation." Journal of Chromatography A 734, no. 2 (May 1996): 405–9. http://dx.doi.org/10.1016/0021-9673(95)01295-8.

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37

Zalat, O. A., Mohamed A. Elsayed, M. S. Fayed, and M. K. Abd El Megid Megid. "Sources of Uncertainty for the Determination of Chlorpyrifos by Gas Chromatography Equipped with Flame Photometric Detector." International Letters of Chemistry, Physics and Astronomy 25 (January 2014): 48–55. http://dx.doi.org/10.18052/www.scipress.com/ilcpa.25.48.

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Analysts are increasingly being required to evaluate the uncertainty associated with methods. Estimating the uncertainty of an analytical result is an essential part of quantitative analysis. This paper discusses the sources of uncertainty of chlorpyrifos determination by gas chromatography equipped with flame photometric detector (GC-FPD). The analysis was performed on HP-5 MS, 30 m x 0.32 mm capillary column with a 0.25 μm stationary film thickness using ultra pure nitrogen (99.9999%) as a carrier gas at 25 psi constant pressure. The method has been optimized. Factors affecting quantization of chlorpyrifos such as injector temperature, carrier gas inlet pressure, air to hydrogen ratios and initial temperature program have been studied to get the best sensitivity, minimum delectability. The liner range of the detector was from 0.15 ng/ml to 1200 ppm, the minimum detection limit was 0.15 ng/ml and the relative standard deviation was 0.839.

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38

Frishman, Gad, Aviv Amirav, and Haim Barak. "Pressure and gas composition effects on the operation of the pulsed flame photometric detector." Israel Journal of Chemistry 41, no. 2 (November 2001): 91–98. http://dx.doi.org/10.1560/r5t2-v8hm-wyjj-41tv.

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39

Clark, Adrian G., and Kevin B. Thurbide. "Properties of a novel linear sulfur response mode in a multiple flame photometric detector." Journal of Chromatography A 1326 (January 2014): 103–9. http://dx.doi.org/10.1016/j.chroma.2013.12.050.

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40

Le Harle, Jean-Pierre, and Bruno Bellier. "Optimisation of the selectivity of a pulsed flame photometric detector for unknown compound screening." Journal of Chromatography A 1087, no. 1-2 (September 2005): 124–30. http://dx.doi.org/10.1016/j.chroma.2005.02.045.

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41

Wu, Shijian, Huanyan Zhang, Beibei Chen, Ming Liu, Yanjun Shen, Qichao Sha, Yuee Zhi, and Pei Zhou. "Multiresidue Determination of Organophosphorus Pesticides in Solid Waste Environmental Samples by Gas Chromatography." Journal of AOAC INTERNATIONAL 97, no. 5 (September 1, 2014): 1463–69. http://dx.doi.org/10.5740/jaoacint.12-185.

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Abstract The method for the determination of 12 organophosphorus pesticides in solid waste was established. The organophosphorus pesticides were analyzed by Soxhlet extraction or accelerated solvent extraction (ASE)-SPE cartridge-flame photometric detector (FPD), and leaching solution by rotary oscillation-positive pressure filtration-liquid–liquid extraction-SPE cartridge-FPD. The differences of extraction efficiencies between Soxhlet and ASE were compared. Solvent of Soxhlet extraction, purification and recovery of organophosphorus pesticides in leaching conditions were also studied. The recoveries were 54.2–119.8%, and the average recovery was 87.7%. The RSD was 1.89–9.10% (n = 6), the average RSD was 6.88%, and the detection limit was 0.27–0.69 μg/kg.

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42

Yang, Qiuhong, Yibin Yang, Ning Xu, Yongtao Liu, Jing Dong, and Xiaohui Ai. "Determination of methylene bisthiocyanate in aquatic products by gas chromatography with pulsed-flame photometric detector." Chinese Journal of Chromatography 35, no. 8 (2017): 881. http://dx.doi.org/10.3724/sp.j.1123.2017.04016.

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43

Kendler, Shai, Shaelah M. Reidy, Gordon R. Lambertus, and Richard D. Sacks. "Ultrafast Gas Chromatographic Separation of Organophosphor and Organosulfur Compounds Utilizing a Microcountercurrent Flame Photometric Detector." Analytical Chemistry 78, no. 19 (October 2006): 6765–73. http://dx.doi.org/10.1021/ac060851a.

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44

Bradley, Cherlynlavaughn, and Douglas J. Schiller. "Determination of sulfur compound distribution in petroleum by gas chromatography with a flame photometric detector." Analytical Chemistry 58, no. 14 (December 1986): 3017–21. http://dx.doi.org/10.1021/ac00127a026.

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45

Cho, Yung Hyun, and Man Ki Park. "Determination of barbiturates in plasma by gas chromatography-flame photometric detector after N,N′-dimethylthiomethyl derivatization." Archives of Pharmacal Research 9, no. 3 (September 1986): 131–38. http://dx.doi.org/10.1007/bf02899996.

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46

Tang, You-Zhi, and Walter A. Aue. "Spectra and response linearization of chlorine and bromine compounds in a copper-sensitized flame photometric detector." Journal of Chromatography A 408 (January 1987): 69–79. http://dx.doi.org/10.1016/s0021-9673(01)81791-x.

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47

Chambers, L., and M. L. Duffy. "Determination of Total and Speciated Sulfur Content in Petrochemical Samples Using a Pulsed Flame Photometric Detector." Journal of Chromatographic Science 41, no. 10 (November 1, 2003): 528–34. http://dx.doi.org/10.1093/chromsci/41.10.528.

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48

SHIGA, Naofumi, Yuji SHIMAMURA, Osami MATANO, and Shinko GOTO. "Residue analysis of cyhexatin and its metabolites in crops by gas chromatography with flame photometric detector." Bunseki kagaku 35, no. 1 (1986): T1—T6. http://dx.doi.org/10.2116/bunsekikagaku.35.t1.

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49

MATSUMURA, Toshiro, Katsuaki KAMETANI, Hitoshi TODORIKI, Tadanori TAKEMURA, Mariko TODOME, and Mitsuharu TAKEDA. "Determination of sulfuric acid particles in the atmosphere by a gas chromatograph with flame photometric detector." NIPPON KAGAKU KAISHI, no. 1 (1986): 100–104. http://dx.doi.org/10.1246/nikkashi.1986.100.

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50

Ni, Lanxiu, Shenghong Li, Kun Ding, Xuhui Geng, Chunfeng Duan, and Yafeng Guan. "Enhancement of Chemiluminescence Intensity of S2* in Non-premixed Hydrogen Microjet Flame in the Photometric Detector for Sulfur Detection." Analytical Chemistry 93, no. 4 (January 11, 2021): 1969–75. http://dx.doi.org/10.1021/acs.analchem.0c02825.

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