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Journal articles on the topic 'Flow microreactor synthesis'

Author: Grafiati

Published: 4 June 2021

Last updated: 14 February 2022

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1

Takahashi, Yusuke, and Aiichiro Nagaki. "Anionic Polymerization Using Flow Microreactors." Molecules 24, no. 8 (2019): 1532. http://dx.doi.org/10.3390/molecules24081532.

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Flow microreactors are expected to make a revolutionary change in chemical synthesis involving various fields of polymer synthesis. In fact, extensive flow microreactor studies have opened up new possibilities in polymer chemistry including cationic polymerization, anionic polymerization, radical polymerization, coordination polymerization, polycondensation and ring-opening polymerization. This review provides an overview of flow microreactors in anionic polymerization and their various applications.

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2

Nakamura, Hiroyuki, Masato Uehara, and Hideaki Maeda. "Nanocrystals Synthesis by Microreactors." Advances in Science and Technology 45 (October 2006): 652–59. http://dx.doi.org/10.4028/www.scientific.net/ast.45.652.

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A microreactor is a continuous flow reactor, which can control reaction conditions precisely. We applied the microreactors to CdSe based nanocrystals synthesis and tuning particle size, optical properties. Furthermore, homogeneous coating of ZnS and its coating amount tuning was possible for optical properties improvement.

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3

Delville, Mariëlle M. E., Jan C. M. van Hest, and Floris P. J. T. Rutjes. "Ethyl diazoacetate synthesis in flow." Beilstein Journal of Organic Chemistry 9 (September 5, 2013): 1813–18. http://dx.doi.org/10.3762/bjoc.9.211.

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Ethyl diazoacetate is a versatile compound in organic chemistry and frequently used on lab scale. Its highly explosive nature, however, severely limits its use in industrial processes. The in-line coupling of microreactor synthesis and separation technology enables the synthesis of this compound in an inherently safe manner, thereby making it available on demand in sufficient quantities. Ethyl diazoacetate was prepared in a biphasic mixture comprising an aqueous solution of glycine ethyl ester, sodium nitrite and dichloromethane. Optimization of the reaction was focused on decreasing the resid

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4

Amii, Hideki, Aiichiro Nagaki, and Jun-ichi Yoshida. "Flow microreactor synthesis in organo-fluorine chemistry." Beilstein Journal of Organic Chemistry 9 (December 5, 2013): 2793–802. http://dx.doi.org/10.3762/bjoc.9.314.

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Organo-fluorine compounds are the substances of considerable interest in various industrial fields due to their unique physical and chemical properties. Despite increased demand in wide fields of science, synthesis of fluoro-organic compounds is still often faced with problems such as the difficulties in handling of fluorinating reagents and in controlling of chemical reactions. Recently, flow microreactor synthesis has emerged as a new methodology for producing chemical substances with high efficiency. This review outlines the successful examples of synthesis and reactions of fluorine-contain

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5

Maresz, Katarzyna, Agnieszka Ciemięga, and Julita Mrowiec-Białoń. "Selective Reduction of Ketones and Aldehydes in Continuous-Flow Microreactor—Kinetic Studies." Catalysts 8, no. 5 (2018): 221. http://dx.doi.org/10.3390/catal8050221.

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In this work, the kinetics of Meerwein–Ponndorf–Verley chemoselective reduction of carbonyl compounds was studied in monolithic continuous-flow microreactors. To the best of our knowledge, this is the first report on the MPV reaction kinetics performed in a flow process. The microreactors are a very attractive alternative to the batch reactors conventionally used in this process. The proposed micro-flow system for synthesis of unsaturated secondary alcohols proved to be very efficient and easily controlled. The microreactors had reactive cores made of zirconium-functionalized silica monoliths

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6

Zhang, Hong, Minjing Shang, Yuchao Zhao, and Yuanhai Su. "Process Intensification of 2,2′-(4-Nitrophenyl) Dipyrromethane Synthesis with a SO3H-Functionalized Ionic Liquid Catalyst in Pickering-Emulsion-Based Packed-Bed Microreactors." Micromachines 12, no. 7 (2021): 796. http://dx.doi.org/10.3390/mi12070796.

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A stable water-in-oil Pickering emulsion was fabricated with SO3H-functionalized ionic liquid and surface-modified silica nanoparticles and used for 2,2′-(4-nitrophenyl) dipyrromethane synthesis in a packed-bed microreactor, exhibiting high reaction activity and product selectivity. The compartmentalized water droplets of the Pickering emulsion had an excellent ability to confine the ionic liquid against loss under continuous-flow conditions, and the excellent durability of the catalytic system without a significant decrease in the reaction efficiency and selectivity was achieved. Compared wit

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7

Borovkov, Vladimir A., and Yury P. Yulenets. "ELECTROPHYSICAL METHOD TO IMPROVE BIODIESEL FUEL SYNTHESIS IN MICROREACTOR DEVICE." Bulletin of the Saint Petersburg State Institute of Technology (Technical University) 56 (2021): 38–43. http://dx.doi.org/10.36807/1998-9849-2020-56-82-38-43.

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An electrophysical method to increase the efficiency of biodiesel synthesis in flow-type microreactor device is considered. It’s shown that due to selective microwave reactants heating the process intensity may be significantly increased while creating through the microreactor cross-section the gradient of temperature and induced of its existence the gradient of surface tension. The flow-type microreactor regimes that provide maintaining of thermal capillary convection are determined

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8

Canty, Allan J., Jeremy A. Deverell, Anissa Gömann, Rosanne M. Guijt, Thomas Rodemann, and Jason A. Smith. "Microfluidic Devices for Flow-Through Supported Palladium Catalysis on Porous Organic Monolith." Australian Journal of Chemistry 61, no. 8 (2008): 630. http://dx.doi.org/10.1071/ch08160.

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Flow-through microreactors are described, constructed of fused silica capillaries with an internal diameter of 100 μm and glass microchips with a channel dimension of 150 μm and involving the in situ UV-initiated synthesis of a poly(glycidyl methacrylate-co-ethylene dimethacrylate) porous polymer monolith. The monolith is a continuous material covalently bonded to the capillary or chip walls, with good flow-through properties. Epoxide ring-opening through amine attack by 5-amino-1,10-phenanthroline and coordination to dichloropalladium(ii) allows use of the microreactors for Suzuki–Miyaura cat

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9

Nieuwland, Pieter J., Kaspar Koch, Jan C. M. van Hest, and Floris P. J. T. Rutjes. "Flow Markers in Microreactors: A Generally Applicable Chromatographic Method for Monitoring Flow Rates During Reactions." Open Chemical Engineering Journal 4, no. 1 (2010): 61–67. http://dx.doi.org/10.2174/1874123101004010061.

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Microreactors have found widespread use for continuous flow synthesis and reaction optimization. Flow rates are critical factors with respect to the latter application because they are used to set screening parameters such as reaction time and stoichiometric ratios. However, the set flow values of pumps for nanoliter to microliter volume reactors are quite often not sufficiently accurate. In this paper we present a generally applicable chromatographic method to analyze flow rates during microreactor reaction screening. By adding flow markers to all reactant and reagent flows and performing con

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10

Bojang, Adama A., and Ho-Shing Wu. "Design, Fundamental Principles of Fabrication and Applications of Microreactors." Processes 8, no. 8 (2020): 891. http://dx.doi.org/10.3390/pr8080891.

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This study highlights the development of small-scale reactors, in the form of microstructures with microchannel networking. Microreactors have achieved an impressive reputation, regarding chemical synthesis ability and their applications in the engineering, pharmaceutical, and biological fields. This review elaborates on the fabrication, construction, and schematic fundamentals in the design of the microreactors and microchannels. The materials used in the fabrication or construction of the microreactors include silicon, polymer, and glass. A general review of the application of microreactors

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11

Duan, Zhenya, Yan Wang, Ling Zhang, et al. "An application of continuous flow microreactor in the synthesis and extraction of rabeprazole." International Journal of Chemical Reactor Engineering 19, no. 3 (2021): 287–94. http://dx.doi.org/10.1515/ijcre-2020-0173.

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Abstract The oxidation of rabeprazole sulfide is a key step in the synthesis of rabeprazole, a drug for the treatment of stomach acid-related disorders. The current rabeprazole production process adopts one pot batch process, which has low reaction efficiency and poor stability. A continuous process can greatly improve the production efficiency and solve the above problems. Therefore, the reaction parameters of rabeprazole in microreactor were explored through laboratory experiments to explore the possibility of continuous production of rabeprazole. Rabeprazole sodium was synthesized by using

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12

Zhang, Guangcai, Xiongfu Zhang, Jing Lv, Haiou Liu, Jieshan Qiu, and King Lun Yeung. "Zeolite capillary microreactor by flow synthesis method." Catalysis Today 193, no. 1 (2012): 221–25. http://dx.doi.org/10.1016/j.cattod.2012.04.008.

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13

Watts, Kevin, William Gattrell, and Thomas Wirth. "A practical microreactor for electrochemistry in flow." Beilstein Journal of Organic Chemistry 7 (August 15, 2011): 1108–14. http://dx.doi.org/10.3762/bjoc.7.127.

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14

Tadic, Julijana, Marina Mihajlovic, Mica Jovanovic, and Dusan Mijin. "Continuous flow synthesis of some 6- and 1,6-substituted 3-cyano-4-methyl-2-pyridones." Journal of the Serbian Chemical Society 84, no. 6 (2019): 531–38. http://dx.doi.org/10.2298/jsc180703092t.

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In this study, six 6- and 1,6-substituted-3-cyano-4-methyl-2-pyridones were synthesized in a continuous flow microreactor system. The syntheses were realized at room temperature and the obtained results were compared to those achieved within classical syntheses. In order to optimize the continuous flow syntheses and increase the yield of the products, the retention time in the microreactor was varied by changing the flow rates of the reactant solutions. Furthermore, the reaction was optimized for 3-cyano-4,6-dimethyl-2- -pyridone and 3-cyano-6-hydroxy-4-methyl-2-pyridone, which are comercially

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15

Dong, Zhengya, David Fernandez Rivas, and Simon Kuhn. "Acoustophoretic focusing effects on particle synthesis and clogging in microreactors." Lab on a Chip 19, no. 2 (2019): 316–27. http://dx.doi.org/10.1039/c8lc00675j.

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16

Wen, Zhenghui, Mei Yang, Shuainan Zhao, Feng Zhou, and Guangwen Chen. "Kinetics study of heterogeneous continuous-flow nitration of trifluoromethoxybenzene." Reaction Chemistry & Engineering 3, no. 3 (2018): 379–87. http://dx.doi.org/10.1039/c7re00182g.

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17

Hardwick, Tomas, and Nisar Ahmed. "Advances in electro- and sono-microreactors for chemical synthesis." RSC Advances 8, no. 39 (2018): 22233–49. http://dx.doi.org/10.1039/c8ra03406k.

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18

Kreider, Peter B., Ki-Joong Kim, and Chih-Hung Chang. "Two-step continuous-flow synthesis of CuInSe2 nanoparticles in a solar microreactor." RSC Adv. 4, no. 27 (2014): 13827–30. http://dx.doi.org/10.1039/c4ra00467a.

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19

Nagaki, Aiichiro, Kana Akahori, Yusuke Takahashi, and Jun-ichi Yoshida. "Flow Microreactor Synthesis of Fluorine-Containing Block Copolymers." Journal of Flow Chemistry 4, no. 4 (2014): 168–72. http://dx.doi.org/10.1556/jfc-d-14-00017.

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20

Maw, San San, Satoshi Watanabe, and Minoru T. Miyahara. "Flow synthesis of silver nanoshells using a microreactor." Chemical Engineering Journal 374 (October 2019): 674–83. http://dx.doi.org/10.1016/j.cej.2019.05.210.

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21

Sharada, S., Prashant L. Suryawanshi, Rajesh Kumar P., Sarang P. Gumfekar, T. Bala Narsaiah, and Shirish H. Sonawane. "Synthesis of palladium nanoparticles using continuous flow microreactor." Colloids and Surfaces A: Physicochemical and Engineering Aspects 498 (June 2016): 297–304. http://dx.doi.org/10.1016/j.colsurfa.2016.03.068.

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22

Qu, Yang, Chiaki Tsuneishi, Hiroyuki Tateno, Yoshimasa Matsumura та Mahito Atobe. "Green synthesis of α-amino acids by electrochemical carboxylation of imines in a flow microreactor". Reaction Chemistry & Engineering 2, № 6 (2017): 871–75. http://dx.doi.org/10.1039/c7re00149e.

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23

Siraev, Ramil, Pavel Ilyushin, and Dmitry Bratsun. "Mixing control in a continuous-flow microreactor using electro-osmotic flow." Mathematical Modelling of Natural Phenomena 16 (2021): 49. http://dx.doi.org/10.1051/mmnp/2021043.

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In recent years, pharmaceutical production has been stimulating the gradual miniaturization of continuous-flow chemical reactors. This process eventually resulted in the emergence of a new generation of microreactors. The advantages of these new reactor types are the flexible production that allows us to quickly reconfigure the scheme, small reactant quantities used for the synthesis, the control of the main reaction parameters with high accuracy. Nevertheless, a decrease in the thickness of the channels where the species contact and react forces us to search for new non-mechanical mechanisms

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24

Amri, Nasser, Ryan A. Skilton, Duncan Guthrie, and Thomas Wirth. "Efficient Flow Electrochemical Alkoxylation of Pyrrolidine-1-carbaldehyde." Synlett 30, no. 10 (2019): 1183–86. http://dx.doi.org/10.1055/s-0037-1611774.

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We report on the optimization of the alkoxylation of pyrrolidine-1-carbaldehyde by using a new electrochemical microreactor. Precise control of the reaction conditions permits the synthesis of either mono- or dialkoxylated reaction products in high yields.

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25

Mizuno, Masatsugu, Hiroyuki Tateno, Yoshimasa Matsumura, and Mahito Atobe. "Synthesis and molecular weight control of poly(3-hexylthiophene) using electrochemical polymerization in a flow microreactor." Reaction Chemistry & Engineering 2, no. 5 (2017): 642–45. http://dx.doi.org/10.1039/c7re00089h.

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26

Matsuura, Shun-ichi, Manami Chiba, Emiko Tomon, and Tatsuo Tsunoda. "Synthesis of amino acid using a flow-type microreactor containing enzyme–mesoporous silica microsphere composites." RSC Adv. 4, no. 18 (2014): 9021–30. http://dx.doi.org/10.1039/c3ra45315d.

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A flow-type microreactor containing composites of the enzyme (glutaminase) and mesoporous silica microspheres with a 23.6 nm pore diameter (SBA23.6) exhibited precise, efficient, and continuous synthesis of theanine.

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27

Campbell, Zachary S., Daniel Jackson, Jacob Lustik, et al. "Continuous flow synthesis of phase transition-resistant titania microparticles with tunable morphologies." RSC Advances 10, no. 14 (2020): 8340–47. http://dx.doi.org/10.1039/d0ra01442g.

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A flow chemistry strategy for synthesis of anatase titania microparticles utilizing a flow-focusing microreactor integrated with a collimated UV LED is presented. The synthesized microparticles possess a wide variety of morphologies and high surface areas (up to 362 m<sup>2</sup> g<sup>−1</sup>).

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28

Lobry, Emeline, Florent Jasinski, Marta Penconi, et al. "Continuous-flow synthesis of polymer nanoparticles in a microreactor via miniemulsion photopolymerization." RSC Adv. 4, no. 82 (2014): 43756–59. http://dx.doi.org/10.1039/c4ra06814a.

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Water-based photopolymerization in microreactor using compact UV fluorescent lamps can create a breakthrough technology to produce polymer latexes in a safer, more environmental-friendly and energy-efficient way.

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29

Takizawa, Eiji, Aiichiro Nagaki, and Jun-ichi Yoshida. "Flow microreactor synthesis of tricyclic sulfonamides via N-tosylaziridinyllithiums." Tetrahedron Letters 53, no. 11 (2012): 1397–400. http://dx.doi.org/10.1016/j.tetlet.2012.01.019.

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30

Watanabe, Satoshi, Tatsumasa Hiratsuka, Yusuke Asahi, Asumi Tanaka, Kazuhiro Mae, and Minoru T. Miyahara. "Flow Synthesis of Plasmonic Gold Nanoshells via a Microreactor." Particle & Particle Systems Characterization 32, no. 2 (2014): 234–42. http://dx.doi.org/10.1002/ppsc.201400126.

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31

Amii, Hideki, Aiichiro Nagaki, and Jun-ichi Yoshida. "ChemInform Abstract: Flow Microreactor Synthesis in Organo-Fluorine Chemistry." ChemInform 45, no. 29 (2014): no. http://dx.doi.org/10.1002/chin.201429274.

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32

Wilms, D., J. Nieberle, J. Klos, H. Löwe, and H. Frey. "Synthesis of Hyperbranched Polyglycerol in a Continuous Flow Microreactor." Chemical Engineering & Technology 30, no. 11 (2007): 1519–24. http://dx.doi.org/10.1002/ceat.200700277.

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33

Bai‐cheng, Feng, Hou Xi‐chao, Wang Tie‐lin, Lu Jian‐qiang, and Jin Yan. "Synthesis of Bicyclic Esters in a Continuous‐Flow Microreactor." ChemistrySelect 5, no. 3 (2020): 952–56. http://dx.doi.org/10.1002/slct.201903919.

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34

Watanabe, Satoshi, Yusuke Asahi, Hideaki Omura, Kazuhiro Mae, and Minoru T. Miyahara. "Flow microreactor synthesis of gold nanoshells and patchy particles." Advanced Powder Technology 27, no. 6 (2016): 2335–41. http://dx.doi.org/10.1016/j.apt.2016.08.013.

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35

Li, Chong, Baojun Ding, Lijing Zhang, Kepeng Song, and Shengyang Tao. "3D-printed continuous flow reactor for high yield synthesis of CH3NH3PbX3 (X = Br, I) nanocrystals." Journal of Materials Chemistry C 7, no. 30 (2019): 9167–74. http://dx.doi.org/10.1039/c9tc02390a.

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36

Kornyushko, V. F., O. M. Nikolaeva, A. V. Panov, R. R. Biglov, and A. S. Kuznetsov. "Quality management of the chemical-technological process for continuous synthesis of pharmaceutical substances of medicinal compounds in flow microreactors." Fine Chemical Technologies 16, no. 3 (2021): 252–66. http://dx.doi.org/10.32362/2410-6593-2021-16-3-252-266.

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Objectives. The introduction of digital tools for the development of medicines, intelligent management systems, and quality control is stipulated not only by modern requirements for the chemical and pharmaceutical industry but also by strict regulatory requirements for manufactured products. This principle ensures the release of a quality product on the first attempt. The aim of this study is to develop information support for the intelligent quality management system for the production of active pharmaceutical substances (APSs) for medicines using a fundamentally new technology: continuous sy

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37

Moldavsky, A. L., A. M. Yurakov, B. Yu Lalaev, and I. A. Fridman. "New approaches to Improving Bendamustine Microractor Synthesis." Drug development & registration 9, no. 1 (2020): 13–17. http://dx.doi.org/10.33380/2305-2066-2020-9-1-13-17.

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Introduction. The chlorination reaction in the synthesis of the substance of bendamustine hydrochloride is a complex process. The presence of active adverse reactions makes scaling difficult.Aim. Improving the performance of the technology for producing bendamustine ethyl ester in a flow microreactor.Materials and methods. A series of experiments was carried out to carry out the chlorination stage in the synthesis of bendamustine hydrochloride in a flow microreactor with various concentrations in the initial reagent solutions.Results and discussion. Experimental work was carried out to increas

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38

Doyle, Brendon J., Frederic Morin, Jan B. Haelssig, Dominique M. Roberge, and Arturo Macchi. "Gas-Liquid Flow and Interphase Mass Transfer in LL Microreactors." Fluids 5, no. 4 (2020): 223. http://dx.doi.org/10.3390/fluids5040223.

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This work investigates the impact of fluid (CO2(g), water) flow rates, channel geometry, and the presence of a surfactant (ethanol) on the resulting gas–liquid flow regime (bubble, slug, annular), pressure drop, and interphase mass transfer coefficient (kla) in the FlowPlateTM LL (liquid-liquid) microreactor, which was originally designed for immiscible liquid systems. The flow regime map generated by the complex mixer geometry is compared to that obtained in straight channels of a similar characteristic length, while the pressure drop is fitted to the separated flows model of Lockhart–Martine

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39

Lei, Ming, Peiyuan Gao, Xuan Sun, and Hong Zhang. "Synthesis of Hantzsch 1,4-Dihydropyridines in a Continuous Flow Microreactor." HETEROCYCLES 93, no. 2 (2016): 755. http://dx.doi.org/10.3987/com-15-s(t)29.

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40

Xu, Lei, Jinhui Peng, C. Srinivasakannan, Guo Chen, and Amy Q. Shen. "Synthesis of copper nanocolloids using a continuous flow based microreactor." Applied Surface Science 355 (November 2015): 1–6. http://dx.doi.org/10.1016/j.apsusc.2015.07.070.

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41

LIU, S., C. CHANG, B. PAUL, and V. REMCHO. "Convergent synthesis of polyamide dendrimer using a continuous flow microreactor." Chemical Engineering Journal 135 (January 15, 2008): S333—S337. http://dx.doi.org/10.1016/j.cej.2007.07.022.

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42

Palde, Prakash B., and Timothy F. Jamison. "Safe and Efficient Tetrazole Synthesis in a Continuous-Flow Microreactor." Angewandte Chemie 123, no. 15 (2011): 3587–90. http://dx.doi.org/10.1002/ange.201006272.

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43

Palde, Prakash B., and Timothy F. Jamison. "Safe and Efficient Tetrazole Synthesis in a Continuous-Flow Microreactor." Angewandte Chemie International Edition 50, no. 15 (2011): 3525–28. http://dx.doi.org/10.1002/anie.201006272.

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44

Asai, Tatsuro, Atsushi Takata, Aiichiro Nagaki, and Jun-ichi Yoshida. "Practical Synthesis of Photochromic Diarylethenes in Integrated Flow Microreactor Systems." ChemSusChem 5, no. 2 (2011): 339–50. http://dx.doi.org/10.1002/cssc.201100376.

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45

Wang, Fajun, Jinpei Huang, and Jianhong Xu. "Continuous-flow synthesis of azo dyes in a microreactor system." Chemical Engineering and Processing - Process Intensification 127 (May 2018): 43–49. http://dx.doi.org/10.1016/j.cep.2018.03.014.

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46

Comer, Eamon, and Michael G. Organ. "A Microreactor for Microwave-Assisted Capillary (Continuous Flow) Organic Synthesis." Journal of the American Chemical Society 127, no. 22 (2005): 8160–67. http://dx.doi.org/10.1021/ja0512069.

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47

Lin, Xue Zhang, Alexander D. Terepka, and Hong Yang. "Synthesis of Silver Nanoparticles in a Continuous Flow Tubular Microreactor." Nano Letters 4, no. 11 (2004): 2227–32. http://dx.doi.org/10.1021/nl0485859.

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48

Génot, Valérie, Serge Desportes, Callie Croushore, et al. "Synthesis of organic nanoparticles in a 3D flow focusing microreactor." Chemical Engineering Journal 161, no. 1-2 (2010): 234–39. http://dx.doi.org/10.1016/j.cej.2010.04.029.

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49

Sen, Nirvik, K. K. Singh, S. Mukhopadhyay, and K. T. Shenoy. "Solvent-free flow synthesis of [OMIM]Br in a microreactor." Chemical Engineering and Processing - Process Intensification 166 (September 2021): 108431. http://dx.doi.org/10.1016/j.cep.2021.108431.

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50

Nishiyama, Yasuhiro, Akira Fujii, and Hajime Mori. "Highly Selective Organic Synthesis by Efficient Mixing in Flow Microreactor." Journal of Synthetic Organic Chemistry, Japan 79, no. 3 (2021): 234–42. http://dx.doi.org/10.5059/yukigoseikyokaishi.79.234.

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