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Relevant bibliographies by topics / Flow synthesis, Precipitation, Microwave, Reactors

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Journal articles
Dissertations / Theses
Book chapters
Conference papers

Academic literature on the topic 'Flow synthesis, Precipitation, Microwave, Reactors'

Author: Grafiati

Published: 6 September 2023

Last updated: 31 July 2025

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Journal articles on the topic "Flow synthesis, Precipitation, Microwave, Reactors"

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Aimable, Anne, Tomasz Strachowski, Ewelina Wolska, Witold Lojkowski, and Paul Bowen. "Comparison of two innovative precipitation systems for ZnO and Al-doped ZnO nanoparticle synthesis." Processing and Application of Ceramics 4, no. 3 (2010): 107–14. http://dx.doi.org/10.2298/pac1003107a.

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This study presents a comparative approach to investigate the potentials of two innovative methods for the synthesis of ZnO and Al-doped ZnO. The first method is a precipitation system working in mild hydrothermal conditions (90?C) using a tubular reactor (Segmented Flow Tubular Reactor, SFTR). The second method is a microwave-assisted hydrothermal process working at 250?C - 38 atmospheres. Nanocrystalline ZnO with a high specific surface area (49-68 m2/g) was obtained with both systems. Smaller equiaxed particles (50-70 nm) were obtained with the SFTR, with an excellent homogeneity in size an

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Dvoeglazov, Konstantin, Yury Kulyako, Sergey Vinokurov, et al. "Synthesis of Mixed Actinide Oxides Using Microwave Radiation." Energies 15, no. 18 (2022): 6618. http://dx.doi.org/10.3390/en15186618.

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A method has been developed for producing mixed actinide oxides suitable for fabricating mixed nitride uranium plutonium fuel for fast neutron reactors. The method is based on the use of microwave radiation for the direct denitration of actinide nitrate solutions. The possibility of producing uranium, plutonium, and neptunium-mixed oxides was shown. A pilot installation for preparing actinide oxides by microwave denitration was designed and tested. Mixed oxides of uranium and cerium (for plutonium imitation) were successfully used to synthesize uranium cerium nitrides and produce fuel pellets.

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Sharma, Gaurav, and Guennadi A. Kouzaev. "Miniature glass-metal coaxial waveguide reactors for microwave-assisted liquid heating." AIMS Electronics and Electrical Engineering 7, no. 1 (2023): 100–120. http://dx.doi.org/10.3934/electreng.2023006.

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<abstract> <p>Microwave (MW) irradiation is recognized as an effective tool in industries related to pharmaceuticals, chemistry, nanoparticle synthesis, food, etc. In the hardware field, some research efforts are concentrated on creating miniature reactors using low-cost technologies aimed at on-demand chemistry or parallel synthesis of many drugs.</p> <p>This paper reports on the development and characterization of novel miniature chemical-resistant glass-metal coaxial reactors based on a modified Liebig condenser. It is composed of two concentric glass tubes, one for

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Erdmenger, Tina, Renzo M. Paulus, Richard Hoogenboom, and Ulrich S. Schubert. "Scaling-up the Synthesis of 1-Butyl-3-methylimidazolium Chloride under Microwave Irradiation." Australian Journal of Chemistry 61, no. 3 (2008): 197. http://dx.doi.org/10.1071/ch07345.

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Ionic liquids are considered to be ‘green’ solvents on account of their non-volatility and non-flammability – which are results of their negligible vapour pressures – as well as reusability. On the basis of ecological concerns, ionic liquids seem to be an attractive alternative to conventional volatile organic solvents. In the present work, the reaction conditions for the synthesis of 1-butyl-3-methylimidazolium chloride were optimized on a small scale (~2 mL, 10 mmol) using a single-mode microwave system. The conditions obtained were subsequently transferred to various microwave reactors, bot

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Wojnarowicz, Jacek, Sylwia Kusnieruk, Tadeusz Chudoba, et al. "Paramagnetism of cobalt-doped ZnO nanoparticles obtained by microwave solvothermal synthesis." Beilstein Journal of Nanotechnology 6 (September 30, 2015): 1957–69. http://dx.doi.org/10.3762/bjnano.6.200.

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Zinc oxide nanopowders doped with 1–15 mol % cobalt were produced by the microwave solvothermal synthesis (MSS) technique. The obtained nanoparticles were annealed at 800 °C in nitrogen (99.999%) and in synthetic air. The material nanostructure was investigated by means of the following techniques: X-ray diffraction (XRD), helium pycnometry density, specific surface area (SSA), inductively coupled plasma optical emission spectrometry (ICP-OES), extended X-ray absorption fine structure (EXAFS) spectroscopy, scanning electron microscopy (SEM), energy dispersive X-ray spectroscopy (EDS) and with

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Laybourn, Andrea, Ana María López-Fernández, Ieuan Thomas-Hillman, et al. "Combining continuous flow oscillatory baffled reactors and microwave heating: Process intensification and accelerated synthesis of metal-organic frameworks." Chemical Engineering Journal 356 (January 2019): 170–77. http://dx.doi.org/10.1016/j.cej.2018.09.011.

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Wu, Shuai, Qiang Wang, Kesheng Guo, et al. "Synthesis and Mechanism Study of Carbon Nanowires, Carbon Nanotubes, and Carbon Pompons on Single-Crystal Diamonds." Crystals 14, no. 6 (2024): 481. http://dx.doi.org/10.3390/cryst14060481.

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Carbon nanomaterials are in high demand owing to their exceptional physical and chemical properties. This study employed a mixture of CH4, H2, and N2 to create carbon nanostructures on a single-crystal diamond using microwave plasma chemical vapor deposition (MPCVD) under high-power conditions. By controlling the substrate surface and nitrogen flow rate, carbon nanowires, carbon nanotubes, and carbon pompons could be selectively deposited. The results obtained from OES, SEM, TEM, and Raman spectroscopy revealed that the nitrogen flow rate and substrate surface conditions were crucial for the g

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Kamaruddin, Mohd Johari, Muhammad Abbas Ahmad Zaini, Anwar Johari та Tuan Amran Tuan Abdullah. "Dielectric Properties for the Ring Opening Polymerisation of ε-Caprolactone". Applied Mechanics and Materials 493 (січень 2014): 621–27. http://dx.doi.org/10.4028/www.scientific.net/amm.493.621.

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A dielectric property study was performed across a wide range of frequencies and temperatures onring opening polymerisation of ε-caprolactone system in order to relate quantitatively their dielectric properties to microwave heating mechanisms. An analysis of the results concluded that heating mechanism of the polymerisation mixtures in a microwave field was controlled by the dielectric properties of monomer, where the monomer was the major component (>90 % volume/volume) as well as the component with highest dielectric loss and dissipation factor. The penetration depth of mixtures at 2.45 G

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Akay, Galip. "Hydrogen, Ammonia and Symbiotic/Smart Fertilizer Production Using Renewable Feedstock and CO2 Utilization through Catalytic Processes and Nonthermal Plasma with Novel Catalysts and In Situ Reactive Separation: A Roadmap for Sustainable and Innovation-Based Technology." Catalysts 13, no. 9 (2023): 1287. http://dx.doi.org/10.3390/catal13091287.

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This multi-disciplinary paper aims to provide a roadmap for the development of an integrated, process-intensified technology for the production of H2, NH3 and NH3-based symbiotic/smart fertilizers (referred to as target products) from renewable feedstock with CO2 sequestration and utilization while addressing environmental issues relating to the emerging Food, Energy and Water shortages as a result of global warming. The paper also discloses several novel processes, reactors and catalysts. In addition to the process intensification character of the processes used and reactors designed in this

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Horikoshi, Satoshi, Hideki Abe, Kanjiro Torigoe, Masahiko Abe, and Nick Serpone. "Access to small size distributions of nanoparticles by microwave-assisted synthesis. Formation of Ag nanoparticles in aqueous carboxymethylcellulose solutions in batch and continuous-flow reactors." Nanoscale 2, no. 8 (2010): 1441. http://dx.doi.org/10.1039/c0nr00141d.

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Dissertations / Theses on the topic "Flow synthesis, Precipitation, Microwave, Reactors"

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Nikam, A. V. "Batch and flow synthesis of inorganic nanoparticles and organic particles." Thesis(Ph.D.), CSIR-National CHemical Laboratory, Pune, 2017. http://dspace.ncl.res.in:8080/xmlui/handle/20.500.12252/4265.

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Wang, Yantao. "Synthesis and conversion of furfural-batch versus continuous flow." Thesis, Compiègne, 2019. http://www.theses.fr/2019COMP2474/document.

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Le furfural, identifié comme l'un des 30 principaux produits chimiques biologiques, est une molécule importante en terme de chimie verte et développement durable. L'objectif de ce travail de doctorat est de réaliser la synthèse et la conversion du furfural en flux continu et par lots. Ici, nous avons développé des méthodes plus éco-efficiente pour la synthèse du furfural, et valorisé le furfural en produits à haute valeur ajoutée, tels que le 2-furonitrile, l'alcool furfurylique, etc... Plusieurs questions clés ont été identifiées afin de concevoir des processus plus écologiques que les proces

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Book chapters on the topic "Flow synthesis, Precipitation, Microwave, Reactors"

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Carlucci, Claudia, and Ana Melisa Jiménez-Ramirez. "Biofuel from seeds, extraction oil and its efficiency." In PLANTS: Physiology, crop production, and stress responses. Editora Científica Digital, 2025. https://doi.org/10.37885/250419151.

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The increasing global demand for renewable energy has stimulated extensive research into biodiesel production from vegetable oils via continuous flow methodologies, due to their superior efficiency, safety, and scalability compared to conventional batch processes. This study explores the synthesis of biodiesel from various oil sources—such as palm, soybean, jatropha, canola, sunflower, rapeseed, and cottonseed—employing a wide range of reactors including microtube, bubble column, fixed-bed, membrane, slit-channel, vortex, and reactive distillation systems. The research aimed to compare the con

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Conference papers on the topic "Flow synthesis, Precipitation, Microwave, Reactors"

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Barham, Joshua Philip, Yasuo Norikane, Hiromichi Egami, and Yoshitaka Hamashima. "High Efficiency Microwave Flow Chemistry Towards Synthesis of Functional Materials and Pharmaceutical Cores." In Ampere 2019. Universitat Politècnica de València, 2019. http://dx.doi.org/10.4995/ampere2019.2019.9860.

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Microwave (MW) heating benefits organic synthesis by affording higher product yields in shorter time periods than conventional heating, yet it suffers from poor scalability and is limited to polar solvents in typical batch mode reactors. Herein, we report a microwave flow reactor using a solid-state semiconductor MW generator. The tunable, single-mode MW heating allows high efficiency, scalable organic synthesis, rapid reaction optimization and is applicable to non-polar solvents (o-Xylene and CPME can be rapidly heated to ca. 260 oC). Auto-frequency tuning compensates for changes in the micro

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