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Dissertations / Theses on the topic 'Fourier transform ion cyclotron resonance mass spectrometry'

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Published: 4 June 2021

Last updated: 3 February 2022

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1

Hauschild, Jennifer M. "Fourier transform ion cyclotron resonance mass spectrometry for petroleomics." Thesis, University of Oxford, 2012. http://ora.ox.ac.uk/objects/uuid:8604a373-fb6b-4bc0-8dc1-464a191b1fac.

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The past two decades have witnessed tremendous advances in the field of high accuracy, high mass resolution data acquisition of complex samples such as crude oils and the human proteome. With the development of Fourier transform ion cyclotron resonance mass spectrometry, the rapidly growing field of petroleomics has emerged, whose goal is to process and analyse the large volumes of complex and often poorly understood data on crude oils generated by mass spectrometry. As global oil resources deplete, oil companies are increasingly moving towards the extraction and refining of the still plentifu

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2

Lin, Tzu-Yung. "Advanced electronics for Fourier-transform ion cyclotron resonance mass spectrometry." Thesis, University of Warwick, 2012. http://wrap.warwick.ac.uk/55048/.

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With the development of mass spectrometry (MS) instruments starting in the late 19th century, more and more research emphasis has been put on MS related subjects, especially the instrumentation and its applications. Instrumentation research has led modern mass spectrometers into a new era where the MS performance, such as resolving power and mass accuracy, is close to its theoretical limit. Such advanced performance releases more opportunities for scientists to conduct analytical research that could not be performed before. This thesis reviews general MS history and some of the important miles

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3

Qi, Yulin. "Advanced methods in Fourier transform ion cyclotron resonance mass spectrometry." Thesis, University of Warwick, 2013. http://wrap.warwick.ac.uk/57931/.

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Mass spectrometry (MS) is a powerful analytical technique used to characterize various compounds by measuring the mass-to-charge ratio (m/z). Among different types of mass analyzers, Fourier transform ion cyclotron resonance mass spectrometer (FT-ICR MS) is the instrument of choice for those working at the forefront of research, as it offers incomparable mass accuracy, resolving power, and the highest flexibility for hybrid instrumentation and fragmentation techniques. The FT-ICR MS requires professional and careful tuning to achieve its superior performance. Our work aims to review, develop a

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4

Mullen, Steven Lawrence. "Fourier transform ion cyclotron resonance mass spectrometry of organometallic compounds /." The Ohio State University, 1987. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487325740718905.

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5

Weisbrod, Chad Randal. "Improvement of Fourier transform ion cyclotron resonance mass spectrometry detection technology." Pullman, Wash. : Washington State University, 2010. http://www.dissertations.wsu.edu/Thesis/Spring2010/c_weisbrod_060210.pdf.

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6

Gates, Paul Jonathan. "Fourier-transform ion cyclotron resonance mass spectrometry : analysis of natural products." Thesis, University of Cambridge, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.621612.

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7

Wills, Rebecca Helen. "High mass accuracy analytical applications of Fourier transform ion cyclotron resonance mass spectrometry." Thesis, University of Warwick, 2014. http://wrap.warwick.ac.uk/60050/.

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The performance capabilities of Fourier transform ion cyclotron resonance (FTICR) mass spectrometry are higher than any other type of mass spectrometer, making this technique suitable for a range of analytical applications. Here, FTICR mass spectrometry has been used for the structural analysis of polyketides and nonribosomal peptides, and in the identification of peptide binding sites of ruthenium(II) arene anticancer complexes. In both these applications, methods have been developed involving complementary tandem mass spectrometry techniques, specifically collision activated dissociation (CA

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8

Schmidt, Eric Grayson. "Observation and control of ion motion in fourier transform ion cyclotron resonance mass spectrometry /." Digital version accessible at:, 1999. http://wwwlib.umi.com/cr/utexas/main.

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9

Tsybin, Youri. "High Rate Electron Capture Dissociation Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." Doctoral thesis, Uppsala universitet, Jonfysik, 2004. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-4136.

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Advances in science and technology during the past decade have greatly enhanced the level of the structural investigation of macromolecules – peptides and proteins. Biological mass spectrometry has become one of the most precise and sensitive techniques in peptide and protein analysis. However, increasing demands of biotechnological applications require further progress to be made. In the present thesis the development and improvement of peptide and protein characterization methods and techniques based on ion-electron and ion-photon reactions in electrospray ionization Fourier transform ion cy

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10

Anupriya, Anupriya. "Gas Phase Structure Characterization Using Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." BYU ScholarsArchive, 2016. https://scholarsarchive.byu.edu/etd/6447.

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This dissertation investigates Fourier transform ion cyclotron resonance mass spectrometry (FTICR-MS) based techniques to study the impact of molecular structure on conformation and binding energetics. A novel method to determine collison cross sectional areas using FTICR (CRAFTI), initially developed by the Dearden lab, was applied to study the conformations of molecular systems with unique structural attributes in an attempt to explore the molecular range of CRAFTI. The systems chosen for CRAFTI studies include crown-ether alkylammonium complexes and biogenic amino acids. The results were fo

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11

Wei, Juan. "Advanced applications of high performance Fourier transform ion cyclotron resonance mass spectrometry." Thesis, University of Warwick, 2014. http://wrap.warwick.ac.uk/66290/.

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Fourier transform ion cyclotron resonance mass spectrometry (FTICR MS) displays its advances in obtaining high resolving power, high mass accuracy, and coupling with many different tandem mass spectrometry (MS/MS) techniques. In this thesis, the superior performance of FTICR MS was demonstrated by several different applications. The peak separation limit of the 12 T solariX FTICR instrument was challenged by measuring the isotopic fine structures of several 17O enriched amyloid-β (Aβ) peptides (Chapter 2 and 3). A resolving power as high as 6 M was achieved at m/z 880, and peaks were assigned

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12

Williams, Christopher Paul. "Application of Hartley and Hilbert transforms in Fourier transform ion cyclotron resonance mass spectrometry /." The Ohio State University, 1992. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487760357822985.

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13

Ross, Charles William. "Gas phase ion - molecule reactions studied by Fourier transform ion cyclotron resonance mass spectrometry /." The Ohio State University, 1993. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487846885778077.

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14

Shomo, Ronald Edward II. "Soft ionization techniques for Fourier transform ion cyclotron resonance and quadrupole mass spectrometry /." The Ohio State University, 1988. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487597424138083.

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15

Grosshans, Peter Byron. "Improvements in our basic understanding of Fourier transform ion cyclotron resonance mass spectrometry /." The Ohio State University, 1990. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487683756126656.

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16

Limbach, Patrick Alan. "Improvements to the analytical capabilities of fourier transform ion cyclotron resonance mass spectrometry /." The Ohio State University, 1992. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487780393267365.

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17

Wood, Troy Dale. "Laser desorption Fourier transform ion cyclotron resonance (LD/FT/ICR) mass spectrometry for high mass ions /." The Ohio State University, 1993. http://rave.ohiolink.edu/etdc/view?acc_num=osu148784730905092.

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18

Wang, Mingda. "New and improved ion traps for high resolution Fourier transform ion cyclotron resonance mass spectrometry /." The Ohio State University, 1990. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487681788254101.

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19

Chen, Ruidan. "Theory and practice of ion trap design in fourier transform ion cyclotron resonance mass spectrometry /." The Ohio State University, 1993. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487847309053468.

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20

Torres, Theresa Ann. "Development of Fourier transform ion cyclotron resonance mass spectrometry for the study of ion-ion reactions /." Digital version accessible at:, 1998. http://wwwlib.umi.com/cr/utexas/main.

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21

Marto, Jarrod A. "External Ion Injection and Applications of Ion Axialization in Fourier Transform Ion Cyclotron Resonance Mass Spectrometry /." The Ohio State University, 1995. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487868114113087.

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22

Craig, Edward Clayton. "Application of dispersion versus absorption (DISPA) in Fourier transform nuclear magnetic resonance and Fourier transform ion cyclotron mass spectrometry /." The Ohio State University, 1987. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487324944214076.

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23

McDonnell, Liam Andrew. "Characterisation of macromolecules using electrospray ionization and Fourier transform ion cyclotron resonance mass spectrometry." Thesis, University of Warwick, 2001. http://wrap.warwick.ac.uk/67794/.

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Multipole storage-assisted dissociation (MSAD), in which ions are stored for extended periods of time in a multipole ion-trap, represents one of the most recent and simplest methods by which structurally informative fragments can be obtained. A potential array investigation of MSAD is reported. It was found that the average kinetic energy of the ion was similar to the energy of a single IR photon and the average kinetic energy of an ion during sustained off-resonance irradiation collision-induced dissociation (SORICID), thus explaining the similar fragments that have been obtained using these

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24

Polfer, Nicolas Camille. "Structural elucidation of peptides and proteins by Fourier transform ion cyclotron resonance mass spectrometry." Thesis, University of Edinburgh, 2003. http://hdl.handle.net/1842/11267.

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Two unique features of FT-ICR mass spectrometry are high mass resolution and mass accuracy. These features have been exploited in a novel approach to the study of metal exchange reactions in metallo-proteins using stable isotope labelling. The system chosen, Zn<sub>4</sub>-SmtA, is a cyanobacterial metallothionein (MT) Deconvoluted ESI-FT-ICR spectra for Zn<sub>4</sub>-FT-ICR spectra for Zn<sub>4</sub>-Smt containing Zn isotopes in natural abundance as well as enriched with 93% <sup>67</sup>Zn show that the Zn<sub>4</sub> cluster of SmtA, in contrast to the structurally-analogous cluster of ma

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25

Green, Philip Spencer. "Biochemical applications of electrospray ionization coupled with Fourier transform ion cyclotron resonance mass spectrometry." Thesis, University of Warwick, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.250112.

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26

May, Michael Alan. "Theoretical advances and laser desorption applications in Fourier transform ion cyclotron resonance mass spectrometry /." The Ohio State University, 1994. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487849377294552.

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27

Van, Orden Steven Lee. "Mechanistic investigations of gas phase ion-molecule reactions using Fourier transform ion cyclotron resonance mass spectrometry." Diss., The University of Arizona, 1993. http://hdl.handle.net/10150/186137.

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Studies of the mechanisms and energetics of a variety ion-molecule reactions involving organometallic and organic ions, have been performed using Fourier transform ion cyclotron resonance mass spectrometry (FTMS). The bond activation processes of V⁺, VO⁺, VOH⁺, and VOCH₃⁺ with water and methanol were investigated in detail. All ions are observed to preferentially activate the C-O bond in methanol, however C-H and O-H bond cleavage are also observed. The addition of the oxo, hydroxo, and methoxo ligands is found to significantly effect the intrinsic reactivity of the ions, relative to V⁺. The r

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28

Kaiser, Nathan Kenneth. "Fourier transform ion cyclotron resonance mass spectrometry instrumentation design and development reduction of ion cloud de-phasing and time-of-flight discrimination /." Online access for everyone, 2007. http://www.dissertations.wsu.edu/Dissertations/Fall2007/n_kaiser_120207.pdf.

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29

Ostrander, Chad Michael. "Development and evaluation of the central trapping electrode trapped-ion cell for Fourier transform mass spectrometry /." Full text (PDF) from UMI/Dissertation Abstracts International, 2000. http://wwwlib.umi.com/cr/utexas/fullcit?p3004351.

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30

Robinson, Jessica Marie. "Examination of gas-phase conformations of oligonucleotides using electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry /." Digital version accessible at:, 1998. http://wwwlib.umi.com/cr/utexas/main.

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31

Benigni, Paolo. "Trapped Ion Mobility Spectrometry coupled to Fourier Transform Ion Cyclotron Resonance Mass Spectrometry for the analysis of Complex Mixtures." FIU Digital Commons, 2017. https://digitalcommons.fiu.edu/etd/3547.

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Analytical Characterization of complex mixtures, such as crude oil, environmental samples, and biological mixtures, is challenging because of the large diversity of molecular components. Mass spectrometry based techniques are among the most powerful tools for the separation of molecules based on their molecular composition, and the coupling of ion mobility spectrometry has enabled the separation and structural elucidation using the tridimensional structure of the molecule. The present work expands the ability of analytical chemists by furthering the development of IMS-MS instrumentation by cou

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32

Hagman, Charlotte. "Method Development in Quantitative and Structural Proteomics using Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." Doctoral thesis, Uppsala University, Department of Engineering Sciences, 2005. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-4761.

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<p>In this thesis, methods for studying different aspects of proteomics were developed with Fourier Transform Ion Cyclotron Resonance, (FTICR), mass spectrometry. The FTICR technique provides ultra-high mass resolving power, mass accuracy at sub ppm level and sensitivity in the attomole region.</p><p>Methods for quantifying biomarkers in body fluids such as cerebrospinal fluid, (CSF), and plasma were developed. Two sets of global markers with different properties were used for quantitative analysis; S-Methyl Thioacetimidate, (SMTA), and S-Methyl Thiopropionimidate, (SMTP), and [H<sub>4</sub>]-

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33

Ramström, Margareta. "Analysis of Complex Biological Samples using Liquid Chromatography-Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." Doctoral thesis, Uppsala University, Analytical Chemistry, 2005. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-5729.

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<p>Studies of protein and peptide expression are vital in order to understand complex biological systems. As demonstrated in this thesis, on-line packed capillary liquid chromatography-Fourier transform ion cyclotron resonance mass spectrometry (LC-FTICR MS) is a useful analytical tool for such studies.</p><p>A proteomics method, based on global tryptic digestion and subsequent separation and detection of the peptides by LC-FTICR MS, was developed for qualitative analysis of body fluids. Initial experiments on cerebrospinal fluid (CSF) provided results that were comparable or superior to those

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34

Palmblad, Magnus. "Identification and Characterization of Peptides and Proteins using Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." Doctoral thesis, Uppsala universitet, Institutionen för materialvetenskap, 2002. http://urn.kb.se/resolve?urn=urn:nbn:se:uu:diva-1999.

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Mass spectrometry has in recent years been established as the standard method for protein identification and characterization in proteomics with excellent intrinsic sensitivity and specificity. Fourier transform ion cyclotron resonance is the mass spectrometric technique that provides the highest resolving power and mass accuracy, increasing the amount of information that can be obtained from complex samples. This thesis concerns how useful information on proteins of interest can be extracted from mass spectrometric data on different levels of protein structure and how to obtain this data expe

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35

Woodling, Kellie Ann. "Using electron capture dissociation Fourier transform ion cyclotron resonance mass spectrometry to study modified polypeptides." [Gainesville, Fla.] : University of Florida, 2005. http://purl.fcla.edu/fcla/etd/UFE0012801.

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36

Guan, Shenheng. "Fourier transform ion cyclotron resonance mass spectrometry: Personal computer-based instrument and two-dimensional spectroscopy." Scholarly Commons, 1989. https://scholarlycommons.pacific.edu/uop_etds/3367.

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A personal computer based Fourier transform ion cyclotron resonance mass spectrometer has been designed and constructed. An IBM PC AT compatible computer is used to host the interface of the instrument. The advantages of using a personal computer to host the FT-ICR instrument include: (1) very low cost of the computer; (2) extensive graphic and mathematic capabilities; (3) easy performance alteration or expansion; (4) an abundance of application software; and (5) support for a wide range of output devices. A dedicated digital hardware interface, which provides high speed data transfer and accu

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37

Xiang, Xinzhen Jane. "Improvements in the analytical capabilities and understanding of Fourier transform ion cyclotron resonance mass spectrometry /." The Ohio State University, 1994. http://rave.ohiolink.edu/etdc/view?acc_num=osu148784969696617.

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38

Blackburn, John William Teasdale. "High-resolution Fourier transform ion cyclotron resonance mass spectrometry and nuclear magnetic resonance spectroscopy of humic substances." Thesis, University of Edinburgh, 2018. http://hdl.handle.net/1842/31149.

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Humic substances (HS) are described as a complex mixture of organic molecules formed by incomplete decomposition of plant, animal and microbial matter. They are found in soil, water and air and have many environmental roles, e.g. water retention and metal ion binding in soil. Despite their importance, the molecular composition of HS is poorly understood. This is mostly because of an inability to separate individual molecules from these complex mixtures and then characterise them by standard analytical methods such as NMR and MS. In order improve the understanding of these important mixtures I

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39

Sarowar, Chowdhury Hasan Chemistry Faculty of Science UNSW. "Electrospray ionisation fourier transform ion cyclotron resonance and quadrupole ion trap mass spectrometry of metal-flavonoid complexes." Publisher:University of New South Wales. Chemistry, 2009. http://handle.unsw.edu.au/1959.4/43658.

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Positive-ion electrospray ionisation Fourier transform ion cyclotron resonance and ion trap mass spectrometry have been used to investigate the reactions of the flavonoids 3-hydroxyflavone, 5-hydroxyflavone, 5-methoxyflavoe, quercetin, quercitrin and rutin with monovalent Li+, Na+, K+ and Cs+, divalent Cu2+, Zn2+ and Pb2+ and trivalent La3+ and Eu3+ metal cations. The effect of capillary-skimmer potential difference and the ion residence time in the hexapole ion trap of the Fourier transform ion cyclotron resonance mass spectrometer are systematically investigated for the flavonoid-alkali and

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40

Yin, Winnie Weixin. "Fourier transform ion cyclotron resonance mass spectrometric study of gas-phase ion-molecule reactions /." The Ohio State University, 1993. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487847309051562.

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41

Arkin, C. Richard. "Theoretical treatment of ion motion in an open trapped-ion cell for use in Fourier transform ion cyclotron resonance mass spectrometry." Digital version:, 2000. http://wwwlib.umi.com/cr/utexas/fullcit?p9992745.

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42

Karim, Muhammed. "Study of the post-translational modifications of histone H4 by Fourier transform ion cyclotron resonance mass spectrometry." Thesis, University of Edinburgh, 2014. http://hdl.handle.net/1842/9780.

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Post-translational modification (PTM) of proteins is known to be a method by which protein function can be regulated. The addition of selected chemical groups at specific amino acid residues can act as a switch by which the function of a modified protein can be attenuated. Histones are a group of proteins which are found in the nucleus of eukaryotic cells and interact with DNA, providing it with a structural foundation upon which the chromosome is built. Histone proteins have numerous sequence variants and are known to be extensively post-translationally modified in a dynamic manner. These mod

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43

Wallace, James Ian. "The analysis of biological molecules by electrospray ionisation Fourier transform ion cyclotron resonance (ESIFTICR) mass spectrometry." Thesis, University of Warwick, 1999. http://wrap.warwick.ac.uk/73491/.

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44

Alber, George Miles. "Theory and instrumentation for precise mass measurement by Fourier transform Ion Cyclotron Resonance Mass Spectrometry (FT/ICR/MS) /." The Ohio State University, 1992. http://rave.ohiolink.edu/etdc/view?acc_num=osu1487777170408073.

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45

Uechi, Guy Takeo. "Infrared photophysics of gas phase ions in a Fourier transform ion cyclotron resonance mass spectrometer." Case Western Reserve University School of Graduate Studies / OhioLINK, 1993. http://rave.ohiolink.edu/etdc/view?acc_num=case1056650065.

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46

Scotcher, Jenna. "Study of the molecular details of p53 redox-regulation using Fourier transform ion cyclotron resonance mass spectrometry." Thesis, University of Edinburgh, 2011. http://hdl.handle.net/1842/8088.

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Reactive oxygen species (ROS) such as hydrogen peroxide (H2O2) and superoxide (O2 • −) have been shown to serve as messengers in biological signal transduction, and many prokaryotic and eukaryotic proteins are now known to have their function controlled via ROS-mediated oxidation reactions occurring on critical cysteine residues. The tumour-suppressor protein p53 is involved in the regulation of a diverse range of cellular processes including apoptosis, differentiation, senescence, DNArepair, cell-cycle arrest, autophagy, glycolysis and oxidative stress. However, little is understood about the

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47

Silwal, Indira K. C. "Characterization of Unknown Chemicals Using Gas Chromatography/Fourier Transform Ion Cyclotron Resonance Mass Spectrometry and AB-Initio Calculations." Fogler Library, University of Maine, 2008. http://www.library.umaine.edu/theses/pdf/SilwalIKC2008.pdf.

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48

Zhang, Haizhen. "Characterization of Cucurbituril Complex Ions in the Gas Phase Using Electrospray Ionization Fourier Transform Ion Cyclotron Resonance Mass Spectrometry." Diss., CLICK HERE for online access, 2006. http://contentdm.lib.byu.edu/ETD/image/etd1582.pdf.

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49

Proschogo, Nicholas William Chemistry Faculty of Science UNSW. "Identification of mammalian lipid material by high performance liquid chromatography and fourier transform ion cyclotron resonance mass spectrometry." Publisher:University of New South Wales. Chemistry, 2008. http://handle.unsw.edu.au/1959.4/42914.

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The analysis of the exact compositions of human lipids is of great importance and can lead to a better understanding of the role of lipids in heart diseases and diabetes. Reverse phase and normal phase high performance liquid chromatography has been used for the analysis of lipid material and applied to beef dripping. Electrospray ionization Fourier transform ion cyclotron resonance mass spectrometry has been used to investigate the free fatty acids, monoacylglycerides, diacylglycerides and triacylglycerides present in lard and beef dripping with the general conclusion that this is a semi quan

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50

Burkitt, William Ian. "Metal-binding non-covalent protein complexes studied by electrospray ionisation and Fourier transform ion cyclotron resonance mass spectrometry." Thesis, University of Warwick, 2005. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.429814.

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