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Journal articles on the topic 'Gas solid chromatography'

Author: Grafiati
Published: 4 June 2021
Last updated: 16 February 2022

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1

Berezkin, Viktor G. "Capillary gas-solid chromatography." Russian Chemical Reviews 65, no. 11 (November 30, 1996): 915–34. http://dx.doi.org/10.1070/rc1996v065n11abeh000237.

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2

Shen, Yufeng, and Milton L. Lee. "Solvating gas-solid chromatography." Journal of Microcolumn Separations 11, no. 5 (1999): 359–65. http://dx.doi.org/10.1002/(sici)1520-667x(1999)11:5<359::aid-mcs6>3.0.co;2-2.

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3

Green, JohnD. "Gas-Liquid-Solid Chromatography." Analytica Chimica Acta 264, no. 2 (July 1992): 370. http://dx.doi.org/10.1016/0003-2670(92)87029-k.

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4

Barry, Eugene F. "Gas-liquid-solid chromatography." Microchemical Journal 45, no. 1 (February 1992): 111. http://dx.doi.org/10.1016/0026-265x(92)90080-m.

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5

Haken, J. K. "Gas-liquid-solid chromatography (Chromatographic Science Series, Vol. 56)." Journal of Chromatography A 657, no. 1 (December 1993): 227. http://dx.doi.org/10.1016/0021-9673(93)83058-z.

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6

Wickramanayake, Palitha P., and Walter A. Aue. "A bonded polyoxyethylene phase for gas and liquid chromatography." Canadian Journal of Chemistry 64, no. 3 (March 1, 1986): 470–76. http://dx.doi.org/10.1139/v86-073.

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Bonded phases were produced by reacting 2,4,7,9-tetramethyl-5-decyne-4,7-bis(polyethyleneoxide 30 mol) ether (Surf[Formula: see text]nol® 485) with silicic supports of high and low surface area. There is circumstantial evidence (a) that the nonextractable layer is held by multiple hydrogen bonding and (b) that the synthesis of these packings involves a reaction at the crosslinking site of the surfactant. The bonded phases, with layer thicknesses between 10 and 30 Å, were tested with three chromatographic techniques. In gas–solid chromatography, the phase proved well deactivated and yielded a reduced plate height of 2.5 (using a silica gel support). In gel permeation chromatography, polyethyleneglycols eluted within the mobile-phase volume. In liquid–solid (normal-phase adsorption) chromatography, the elution pattern differed significantly from that of unmodified silica gel. In each case, high-efficiency separations were obtained. The chromatographic experiments thus demonstrated the potential usefulness of the new phase for both gas and liquid chromatography. However, it was not tested in direct comparison with conventional phases nor was its utility established by subjecting it to routine analytical use.
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7

Janák, Jaroslav. "Gazozhidko-tverdofaznaya khromatografiya (Gas-liquid-solid chromatography)." Journal of Chromatography A 396 (January 1987): 445. http://dx.doi.org/10.1016/s0021-9673(01)94092-0.

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8

Gutiérrez, M. C., S. Osuna, and I. Baráibar. "Solid surface mapping by inverse gas chromatography." Journal of Chromatography A 1087, no. 1-2 (September 2005): 142–49. http://dx.doi.org/10.1016/j.chroma.2005.03.047.

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9

Roubani–Kalantzopoulou, Fani. "Determination of isotherms by gas–solid chromatography." Journal of Chromatography A 1037, no. 1-2 (May 2004): 191–221. http://dx.doi.org/10.1016/j.chroma.2003.12.005.

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10

Moskvin, L. N., and O. V. Rodinkov. "Analytical Application of Liquid-Gas and Liquid-Gas-Solid Chromatography." Critical Reviews in Analytical Chemistry 24, no. 5-6 (January 1994): 317–25. http://dx.doi.org/10.1080/10408349408048822.

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11

Parcher, Jon F., and Lang B. Hung. "Cooperative adsorption effects in gas—liquid—solid chromatography." Journal of Chromatography A 399 (January 1987): 75–86. http://dx.doi.org/10.1016/s0021-9673(00)96112-0.

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12

Bhairi, A., D. Rothstein, R. Madey, Huang Jan-Chan, and K. B. Lee. "Gas—solid chromatography of an argon—helium mixture." Journal of Chromatography A 361 (January 1986): 3–11. http://dx.doi.org/10.1016/s0021-9673(01)86888-6.

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13

Mills, T. A., and C. S. G. Phillips. "Study of salt hydrates by gas-solid chromatography." Journal of Chromatography A 557 (September 1991): 495–99. http://dx.doi.org/10.1016/s0021-9673(01)87157-0.

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14

Ogihara, Hirokazu, Yasumi Horimoto, Zhi Hai Wang, Brenton J. Skura, and Shuryo Nakai. "Solid Phase Microextraction/Gas Chromatography ofSalmonella-Infected Beef." Journal of Agricultural and Food Chemistry 48, no. 6 (June 2000): 2253–59. http://dx.doi.org/10.1021/jf991201t.

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15

Ren, Yuli, and Peifen Zhu. "Application of inverse gas chromatography to solid propellants." Journal of Chromatography A 457 (January 1988): 354–61. http://dx.doi.org/10.1016/s0021-9673(01)82083-5.

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16

Panzer, U. "Characterization of solid surfaces by inverse gas chromatography." Colloids and Surfaces 57, no. 2 (January 1991): 369–74. http://dx.doi.org/10.1016/0166-6622(91)80169-o.

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17

Sidelnikov, Vladimir N., Yuri V. Patrushev, and Yuri P. Belov. "Sol–gel multicapillary columns for gas–solid chromatography." Journal of Chromatography A 1101, no. 1-2 (January 2006): 315–18. http://dx.doi.org/10.1016/j.chroma.2005.11.021.

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18

Kleinová, J., and B. Klejdus. "Determination of volatiles in beer using solid-phase microextraction in combination with gas chromatography/mass spektrometry ." Czech Journal of Food Sciences 32, No. 3 (June 11, 2014): 241–47. http://dx.doi.org/10.17221/567/2012-cjfs.

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Headspace solid phase microextraction and purge and trap analysis were used for the determination of volatiles in beer. These methods were compared with the analysis of unconcentrated gas phase and liquid extraction. Solid phase microextraction proved to be the most useful and was investigated more closely. Volatiles were isolated by the means of different combinations of sorbents, sorption was performed at various temperatures and times. The addition of salt to the sample and stirring of the sample were examined to enhance the analyte concentration in the gas phase. Ultrasonic bath and filtration were tested to remove carbon dioxide. Not all methods improved the sorption of volatiles. Stirring was characterised by low repeatability and ultrasonic bath causes to the loss of volatile analytes. Distribution constants of volatiles depend on their boiling points and thus different sorption temperatures are suitable for different substances.
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19

Mehler, C., F. Thielmann, and W. Peukert. "Combination of a Dielectric Continuum Model with Inverse Gas Chromatography for the Characterization of Solid Surfaces." Adsorption Science & Technology 20, no. 9 (November 2002): 835–48. http://dx.doi.org/10.1260/02636170260555769.

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The use of a dielectric continuum model for the characterization of solid surfaces was combined for the first time with inverse gas chromatography. Extension of dielectric continuum models to adsorption from the gaseous phase allowed the distributed surface properties of solid surfaces to be determined. An inverse gas chromatograph was used for the measurement of adsorption equilibria as a quick alternative to time-consuming measurements by gravimetric or volumetric set-ups. Combination of the two techniques allowed the rapid determination of the distributed properties of solid surfaces to be effected and the results were interpreted in a fundamental physical sense. This led to a novel and promising way for the rapid and exact characterization of solid surfaces.
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20

Peña-Alvarez, Araceli, Laura Dı́az, Alejandra Medina, Carmen Labastida, Santiago Capella, and Luz Elena Vera. "Characterization of three Agave species by gas chromatography and solid-phase microextraction–gas chromatography–mass spectrometry." Journal of Chromatography A 1027, no. 1-2 (February 2004): 131–36. http://dx.doi.org/10.1016/j.chroma.2003.10.082.

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21

Onjia, A. E., S. K. Milonjic, and Lj V. Rajakovic. "Inverse gas chromatography of chromia. Part I. Zero surface coverage." Journal of the Serbian Chemical Society 66, no. 4 (2001): 259–71. http://dx.doi.org/10.2298/jsc0104259o.

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The surface properties of the solid obtained from colloidal chromiawere investigated by inverse gas chromatography (IGC), at zero surface coverage conditions. The solid samples I dried at 423 K and II heated at 1073 K in the amorphous and crystalline form, respectively, were studied in the temperature range 383-423 K. The dispersive components of the surface free energies, enthalpies, entropies, and the acid/base constants for the solidswere calculated from the IGCmeasurements and compared with the data for a commercially available chromia (III). Significantly lower enthalpies and entropies were obtained for cyclohexane on solid II and chloroform, highly polar organic, on solid I. The dispersive contributions to the surface energy of solid II and III were similar, but much greater in the case of solid I. All the sorbents had a basic character, with the KD/KA ratio decreasing in the order I > II > III. The retention and resolution in the separation of a vapour mixture of C5-C8 n-alkanes on the three substrates were different.Arapid separationwas observed on solid II and an enhanced retention on solid I. Generally, the heated chromia (II) exhibited diminished adsorption capacity, and enhanced homogeneity of the surface.
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22

Denis, Elizabeth H., Carlos G. Fraga, Nicholas L. Huggett, William C. Weaver, Lydia A. Rush, Brian P. Dockendorff, Angel S. Breton-Vega, and April J. Carman. "Physicochemical Gas–Solid Sorption Properties of Geologic Materials Using Inverse Gas Chromatography." Langmuir 37, no. 23 (June 3, 2021): 6887–97. http://dx.doi.org/10.1021/acs.langmuir.0c03676.

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23

Jaroniec, M., X. Lu, and R. Madey. "Theory of gas-solid adsorption chromatography for heterogeneous adsorbents." Journal of Physical Chemistry 94, no. 15 (July 1990): 5917–21. http://dx.doi.org/10.1021/j100378a057.

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24

Teske, Klaus, Peter Popp, and Jörg Baumbach. "Solid-state coulometric cell as detector for gas chromatography." Journal of Chromatography A 360 (January 1986): 417–20. http://dx.doi.org/10.1016/s0021-9673(00)91690-x.

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25

Julák, Jaroslav, Eva Procházková-Francisci, Eva Stránská, and Vlasta Rosová. "Evaluation of exudates by solid phase microextraction–gas chromatography." Journal of Microbiological Methods 52, no. 1 (January 2003): 115–22. http://dx.doi.org/10.1016/s0167-7012(02)00148-3.

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26

Boudreau, Scott P., and William T. Cooper. "Determination of surface polarity by heterogeneous gas-solid chromatography." Analytical Chemistry 59, no. 2 (January 15, 1987): 353–58. http://dx.doi.org/10.1021/ac00129a028.

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27

Judge, Michael D. "Solid Propellant Degradation Kinetics via headspace sampling gas chromatography." Propellants, Explosives, Pyrotechnics 22, no. 1 (February 1997): 11–14. http://dx.doi.org/10.1002/prep.19970220105.

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28

Xinquan, X., and Dai Anbang. "Solid state reactions of coordination compounds by gas chromatography." Pure and Applied Chemistry 60, no. 8 (January 1, 1988): 1217–24. http://dx.doi.org/10.1351/pac198860081217.

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29

Bruner, F., G. Crescentini, and F. Mangani. "Gas-liquid-solid chromatography with coated graphitized carbon black." Pure and Applied Chemistry 61, no. 11 (January 1, 1989): 1997–2000. http://dx.doi.org/10.1351/pac198961111997.

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30

El-Ghorab, Ahmed H., Kazutoshi Fujioka, and Takayuki Shibamoto. "Determination of Acrylamide Formed in Asparagine/d-Glucose Maillard Model Systems by Using Gas Chromatography with Headspace Solid-Phase Microextraction." Journal of AOAC INTERNATIONAL 89, no. 1 (January 1, 2006): 149–53. http://dx.doi.org/10.1093/jaoac/89.1.149.

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Abstract A gas chromatographic method, along with a headspace solid-phase microextraction (HS-SPME), was developed for the determination of acrylamide formed in Maillard reaction model systems. The developed method was validated by liquid chromatography/mass spectrometry. A headspace sample was collected from an aqueous acrylamide solution (100 μg/mL) by SPME and directly injected into a gas chromatograph equipped with a nitrogen-phosphorus detector. The recovery of acrylamide from an aqueous solution was satisfactory, i.e, &gt;93% under the conditions used. Acrylamide formed in an asparagine/d-glucose (molar ratio, 1/2) Maillard reaction model system heated at 150 and 170C for 20 min was collected and analyzed by the newly developed method using gas chromatography with nitrogen-phosphorus detection and HS-SPME. The amounts of acrylamide were 318 33 μg/g asparagine from a sample heated at 150C and 3329 176 g/g asparagine from a sample heated at 170C. Addition of cysteamine or glutathione to the above model system reduced acrylamide formation. Acrylamide formation was not observed when cysteamine or glutathione was added to asparagine in the above model systems to obtain equimolar concentrations of both compounds. This newly developed method is simple and sensitive, and requires no solvent extraction.
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31

BorFuh, C., Y. C. Yang, H. Y. Tsai, and L. S. Ho. "Solid-phase microextraction coupled with gas chromatography and gas chromatography—Mass spectrometry for public health pesticides analysis." Chromatographia 57, no. 7-8 (April 2003): 525–28. http://dx.doi.org/10.1007/bf02492552.

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32

Uematsu, Yoko, Keiko Hirata, Kumi Suzuki, Kenji Iida, Teruo Kan, and Kazuo Saito. "Determination of Sucrose Esters of Fatty Acids in Food Additive Premixes by Gas Chromatography and Confirmation of Identity by Gas Chromatography/Mass Spectrometry." Journal of AOAC INTERNATIONAL 84, no. 2 (March 1, 2001): 498–506. http://dx.doi.org/10.1093/jaoac/84.2.498.

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Abstract A gas chromatographic (GC) method was developed for the determination of sucrose monoesters of fatty acids (mono-SuE) and sucrose acetate isobutyrate (SAIB) in food additive premixes. Mono-SuE and SAIB fractions were prepared by column chromatography with either a C8 or a silica gel solid-phase extraction column. The mono-SuE fraction was acetylated and applied to a wide-bore GC column (0.53 mm × 15 m) by splitless injection for determination. The SAIB fraction was applied to the GC column without derivatization. Gas chromatography/mass spectrometry was used to confirm the identity of GC peaks. The detection limits for mono-SuE and SAIB were 0.005 and 0.01%, respectively. Mono-SuE (C12, C14, C16, C18, and C18:1) and SAIB were found in commercial food additive premixes and some foods.
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33

Jordáková, I., J. Dobiáš, M. Voldich, and J. Poustka. "Determination of vinyl chloride monomer in food contact materials by solid phase microextraction coupled with gas chromatography/mass spectrometry." Czech Journal of Food Sciences 21, No. 1 (November 18, 2011): 13–17. http://dx.doi.org/10.17221/3472-cjfs.

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The present study concerns the optimisation of the headspace solid phase microextraction (HS/SPME) combined with gas chromatography/mass spectrometry (GC/MS) for the vinyl chloride monomer determination. Samples of PVC materials were analysed using the Carboxen/Polydimethylsiloxane (CX/PDMS) 75 &micro;m fibre. For this fibre, the achieved limit of detection was 0.05 &micro;g/kg, and that of quantification 0.17 &micro;g/kg, respectively, with RSD 5%. The levels of VCM found ranged from 0.29 to 0.44 mg/kg, in the case of foil, the VCM content determined was 3.65 mg/kg which means that the maximal limit allowed was exceeded. &nbsp;
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34

Asres, Daniel Derbie, and Hélène Perreault. "A gas-to-solid phase methanolysis method for the analysis of small amounts of oligosaccharides." Canadian Journal of Chemistry 74, no. 8 (August 1, 1996): 1512–23. http://dx.doi.org/10.1139/v96-168.

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A gas-to-solid phase methanolysis method for the analysis of oligosaccharides is presented. The advantages of using this new gas-to-solid phase method, as opposed to conventional bulk phase techniques, are described, along with comparisons of results obtained from both techniques. The reliable bulk phase methanolysis methods are used as benchmarks for assessing the extent of completion of the gas-to-solid reactions. Gas chromatographic – mass spectrometric (GC–MS) data show that, in general, higher temperatures and longer reaction times are required for completion of the gas-to-solid methanolysis process than for completion of the bulk phase reaction. On the other hand, the gas-to-solid procedure requires only minimal amounts of substrate that would be difficult to characterize using bulk phase methanolysis due to losses during clean-up procedures. Gas-to-solid methanolysis reactions of permethylated di- and trisaccharides were investigated (GC–FID and GC–MS), following initial experiments performed in order to characterize the GC retention times and mass spectra of permethylated standard monosaccharides. Conversion of neutral disaccharides, as well as neutral and acidic trisaccharides, to their respective monosaccharides was successful using the gas-to-solid method. The GC–FID and GC–MS traces show that the gas-to-solid method gives a cleaner reaction than the bulk phase method. Key words: oligosaccharides, methanolysis, permethylation, gas chromatography – mass spectrometry, mass spectrometry.
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35

Voelkel, A., K. Adamska, B. Strzemiecka, and K. Batko. "Determination of Hansen solubility parameters of solid materials by inverse gas-solid chromatography." Acta Chromatographica 20, no. 1 (March 2008): 1–14. http://dx.doi.org/10.1556/achrom.20.2008.1.1.

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36

Carlsen, Lars, Anders Feldthus, and Peter Bo. "Solid state pyrolyses Part 2: Solid state kinetics studied by pyrolysis—gas chromatography." Journal of Analytical and Applied Pyrolysis 19 (July 1991): 15–27. http://dx.doi.org/10.1016/0165-2370(91)80032-4.

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37

Shrotri, Pravin Y., Asmitha Mokashi, and Doble Mukesh. "Prediction of retention times in temperature-programmed gas-solid and gas-liquid chromatography." Journal of Chromatography A 387 (January 1987): 399–403. http://dx.doi.org/10.1016/s0021-9673(01)94543-1.

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38

Voelkel, Adam, Kalina Batko, Katarzyna Adamska, and Beata Strzemiecka. "Determination of Hansen Solubility Parameters by Means of Gas-Solid Inverse Gas Chromatography." Adsorption Science & Technology 26, no. 1-2 (February 2008): 93–102. http://dx.doi.org/10.1260/026361708786035378.

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39

Berezkin, V. G., I. V. Malyukova, and V. R. Alishoev. "Investigation of the role of the carrier gas in capillary gas-solid chromatography." Russian Chemical Bulletin 45, no. 3 (March 1996): 587–93. http://dx.doi.org/10.1007/bf01435787.

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40

Berezkin, Viktor G., Irina V. Malyukova, Victor R. Alishoev, and Jaap de Zeeuw. "The influence of the carrier gas on retention in capillary gas-solid chromatography." Journal of High Resolution Chromatography 19, no. 5 (May 1996): 272–76. http://dx.doi.org/10.1002/jhrc.1240190507.

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41

Afanassiev, A. M., V. N. Demeshev, E. P. Kalyazin, and G. V. Kovalev. "Chromatography of diols. Regularities in the retention of linear diprimary diols in gas-solid and gas-liquid chromatography." Chromatographia 20, no. 2 (February 1985): 102–8. http://dx.doi.org/10.1007/bf02280606.

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42

Ziembowicz, Sabina, Małgorzata Kida, and Piotr Koszelnik. "Development of an analytical method for dibutyl phthalate (DBP) determination in water samples using gas chromatography." E3S Web of Conferences 44 (2018): 00200. http://dx.doi.org/10.1051/e3sconf/20184400200.

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The aim of the work described here was to develop and validate a method by which dibutyl phthalate may be subject to determinations using solid phase extraction and gas chromatography. Optimization of the chromatographic method was based on the selection of working conditions for both the chromatograph and the detector. Following the optimization of extraction and separation parameters, the method was validated by evaluating specificity, the analytical curve, linearity, limits of detection and quantification and recovery. The proposed method has been evaluated in terms of linearity, over a range of concentrations from 0 to 7.5 mg·L-1.The analytical curves show values for correlation coefficients higher than 0.99. Mean recoveries from samples ranged from 97 to 127%, with relative standard deviation lower than 11%. Limit of detection LOD and limit of quantification LOQ values were 0.02 and 0.053 mg·L-1 respectively.
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43

Levchyk, Valentyna, and M. Zui. "Solid-phase microextraction of benzophenones coupled with gas chromatography analysis." French-Ukrainian Journal of Chemistry 4, no. 2 (2016): 55–62. http://dx.doi.org/10.17721/fujcv4i2p55-62.

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In this study, solid-phase microextraction method combines with gas chromatography-flame ionization detector. The proposed method is used for the preconcentration of some benzophenones. Influence of different factors on the efficiency of extraction is described in detail. The analytical procedure was optimized for fiber coating selection, extraction time, temperature, sample pH, ionic strength. For all benzophenones, the highest enrichment factors were achieved using carboxen/polydimethylsiloxane/divinylbenzene fibre immersed directly into the water samples, containing 100 mg/mL of sodium chloride, at room temperature. The optimum pH range is 5.0 – 7.0. The relative standard deviations (RSDs) were from 1.3 to 10.0 % (n = 3). The method was applied to the determination of benzophenone, benzophenone-3, 2-hydroxybenzophenone in the lake water and urine.
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44

Dugheri, Stefano, Nicola Mucci, Alessandro Bonari, Giorgio Marrubini, Giovanni Cappelli, Daniela Ubiali, Marcello Campagna, Manfredi Montalti, and Giulio Arcangeli. "Solid phase microextraction techniques used for gas chromatography: a review." Acta Chromatographica 32, no. 1 (March 2020): 1–9. http://dx.doi.org/10.1556/1326.2018.00579.

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In the last decade, the development and adoption of greener and sustainable microextraction techniques have been proved to be an effective alternative to classical sample preparation procedures. In this review, 10 commercially available solid-phase microextraction systems are presented, with special attention to the appraisal of their analytical, bioanalytical, and environmental engineering. This review provides an overview of the challenges and achievements in the application of fully automated miniaturized sample preparation methods in analytical laboratories. Both theoretical and practical aspects of these environment-friendly preparation approaches are discussed. The application of chemometrics in method development is also discussed. We are convinced that green analytical chemistry will be really useful in the years ahead. The application of cheap, fast, automated, “clever”, and environmentally safe procedures to environmental, clinical, and food analysis will improve significantly the quality of the analytical data.
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45

Mohnke, Manfred, and Jürgen Heybey. "Gas-solid chromatography on open-tubular columns: an isotope effect." Journal of Chromatography A 471 (June 1989): 37–53. http://dx.doi.org/10.1016/s0021-9673(00)94153-0.

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46

Enoch, Petra, Aggi Putzler, Dieter Rinne, and Jörg Schlüter. "Automated solid-phase extraction on-line coupled to gas chromatography." Journal of Chromatography A 822, no. 1 (September 1998): 75–82. http://dx.doi.org/10.1016/s0021-9673(98)00576-7.

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47

Szabó, Z. G. "Classification of active centres on solid catalysts by gas chromatography." Chromatographia 30, no. 9-10 (November 1990): 597–99. http://dx.doi.org/10.1007/bf02269811.

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48

Loeper, Joseph M., and Robert L. Grob. "Determination of water in solid samples using headspace gas chromatography." Journal of Chromatography A 463 (January 1989): 365–74. http://dx.doi.org/10.1016/s0021-9673(01)84490-3.

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49

Hamieh, T., S. Abdessater, and J. Toufaily. "Physicochemical characterization of some solid materials by inverse gas chromatography." Journal de Physique IV (Proceedings) 124 (May 2005): 37–40. http://dx.doi.org/10.1051/jp4:2005124006.

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50

Deibler, Kathryn D., Terry E. Acree, and Edward H. Lavin. "Solid Phase Microextraction Application in Gas Chromatography/Olfactometry Dilution Analysis." Journal of Agricultural and Food Chemistry 47, no. 4 (April 1999): 1616–18. http://dx.doi.org/10.1021/jf981012v.

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