Academic literature on the topic 'Glutaryl Chloride'

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Journal articles on the topic "Glutaryl Chloride"

1

Nubbemeyer, Udo, Analuisa Nava, Lukas Trippe, Andrea Frank, Lars Andernach, and Till Opatz. "Synthesis of Optically Active Hydroxyalkyl Cycloheptatrienes: A Key Step in the Total Synthesis of 6,11-Methylene-LXB4." Synlett 32, no. 01 (2020): 45–50. http://dx.doi.org/10.1055/s-0040-1707282.

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AbstractStarting from methyl cycloheptatrienyl-1-carboxylate, 6-acylation was successfully achieved employing glutaryl chloride in the presence of AlCl3 under controlled reaction conditions to furnish keto carboxylic acid product. After protection of this keto carboxylic acid as tert-butyl ester, reagent-controlled enantioselective reductions delivered configuration-defined methyl-6-hydroxylalkyl cycloheptatriene-1-carboxylates with up to 80% ee. Whereas simple NaBH4 reduction of the keto carboxylic acid and subsequent lactonization afforded a methyl-6-tetrahydropyranonyl cycloheptatriene-1-ca
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2

Kiruba, B., and S. Chidambaravinayagam. "Photocrosslinking Property of Certain Synthesized Bis(arylidene)cycloalkanone based Random Copolyesters with Computational Support and their Anticancer Study." Journal of Scientific Research 14, no. 3 (2022): 901–15. http://dx.doi.org/10.3329/jsr.v14i3.57161.

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The synthesis of random copolyesters involves polycondensation of arylidene diol with curcumin and glutaryl chloride in 1:1:2 ratio. For this monomers, 2,6-bis-(4-hydroxy benzylidene) cyclohexanone, 2,6-bis-(4-hydroxy-3-methoxybenzylidene)cyclohexanone, 2,5-bis-(4-hydroxybenzylidene)cyclopentanone and 2,5-bis-(4-hydroxy-3-methoxy benzylidene)cyclopentanone were synthesized using acid catalyzed Claisen-Schmidt reaction. Qualitative solubility tests reveal that prepared copolyesters dissolve well in polar solvents. The successful formation of copolyesters was confirmed by Fourier transform-infra
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3

Jassim, Ibtisam, and Omar AbdulMohsin. "Synthesis, Characterization and Study of Biological Activity of Some New Schiff Bases." Academic Science Journal 3, no. 2 (2025): 166–83. https://doi.org/10.24237/asj.03.02.849b.

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In the present study, ( Schiff's bases 6a - 6e) and (new amids derivatives 6f - 6j) have been synthesized . The glutaroyl chloride(2) has been prepared by the reacting of glutaric acid and thionyl chloride in presence of (DMF) . The new compound bis(4-formylphenyl) glutarate (3) has been Synthesized from reaction of one mole of glutaroyl chloride and two moles of 4-hydroxybenzaldehyde . Compound 4,4'-(glutaroylbis(oxy))dibenzoic acid (4) was Synthesized from one mole of glutaroyl chloride and two moles of 4-hydroxybenzoic acid, while compound bis(4-(chlorocarbonyl)phenyl) glutarate (5) was pre
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4

Orlinkov, A. V., I. S. Akhrem, S. V. Vitt, L. V. Afanas'eva, and M. E. Vol'pin. "Transformation of glutaryl chloride to 4,5-dibromopentanoic acid in the presence of a saturated hydrocarbon as a reducing agent and AlBr3 as the brominating agent." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 38, no. 5 (1989): 1064–67. http://dx.doi.org/10.1007/bf00955451.

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5

Braginets, O. G., V. V. Ivasyk, B. O. Kondratskyi, D. L. Kachmaryk, and V. L. Novak. "The possibility of using silochrome sorbents for proteinase inhibitor aprotinin." Infusion & Chemotherapy, no. 3.1 (October 11, 2020): 13–14. http://dx.doi.org/10.32902/2663-0338-2020-3.1-09.

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Background. Aprotinin is a polypeptide, a proteinase inhibitor of natural origin. It inhibits kallikrein, kininogenase, plasmin, trypsin, chymotrypsin; blocks the activator of profibrinolysin, which helps to stop bleeding. Aprotinin is obtained from the lungs of cattle.
 Objective. To study the sorption of aprotinin on silochromic sorbents.
 Materials and methods. Affinity sorbents based on silochrome were used in the work: p-chlorobenzyl-silochrome, active bright blue K-silochrome, aminopropyl silochrome, phenyl-diol-silochrome, phenyl-glutaryl-silochrome. The optical density was me
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6

Smirnov, Alexander A., Alexandra D. Golikova, and Maria A. Toikka. "Efficiency of separation of alcohol — ester mixtures by deep eutectic solvents based on choline chloride." Transactions of the Kоla Science Centre of RAS. Series: Engineering Sciences 1, no. 1/2023 (2023): 218–22. http://dx.doi.org/10.37614/2949-1215.2023.14.1.039.

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The paper presents results of the study of liquid-liquid equilibrium in the systems ethanol — ethyl formate — DES and 1-propanol — 1-propyl formate — DES. DESs based on choline chloride with urea and glutaric acid were investigated. The distribution coefficients of alcohol and ester in the systems, as well as the selectivity values of the separation of the alcohol — ether systems by these DESs, were calculated using LLE data. DES based on choline chloride and urea more effectively separates the alcohol-ether systems than DES with glutaric acid. Systems with heavier alcohols and esters have hig
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7

Pearce, Kyle G., Vladimir Simenok, and Ian R. Crossley. "Phosphacycloalkyldiones: synthesis and coordinative behaviour of 6- and 7-member cyclic diketophosphanyls." Dalton Transactions 49, no. 17 (2020): 5482–92. http://dx.doi.org/10.1039/d0dt00864h.

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Condensation of glutaryl and adipoyl chlorides with bis(silyl)phosphanes RP(SiMe<sub>3</sub>)<sub>2</sub> (R = Me, <sup>n</sup>Bu, <sup>t</sup>Bu, Ph, Mes) affords the conformationally fluxional phosphacycloalkyldiones (CH<sub>2</sub>)<sub>n</sub>(CO)<sub>2</sub>PR (n = 3, 4); their coordination behaviour is explored.
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8

Park, Hey-Jung, Jeong-Su Moon, Hong-Gyum Kim та ін. "Characterization of a second gene encoding γ-glutamyl transpeptidase from Schizosaccharomyces pombe". Canadian Journal of Microbiology 51, № 3 (2005): 269–75. http://dx.doi.org/10.1139/w04-137.

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The first gene encoding γ-glutamyl transpeptidase (GGTI) of the fission yeast has previously been characterized, and its expression was found to be regulated by various oxidative stress-inducing agents. In this work, a second gene, encoding GGTII, was cloned and characterized from the fission yeast Schizosaccharomyces pombe. The structural gene encoding GGTII was amplified from the genomic DNA of the fission yeast and ligated into the shuttle vector pRS316 to generate the recombinant plasmid pPHJ02. The determined sequence contains 3040 bp and is able to encode the putative 611 amino acid sequ
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9

Pant, Atul, Abel Fok, Matthew T. Parsons, Jackson Mak, and Allan K. Bertram. "Deliquescence and crystallization of ammonium sulfate-glutaric acid and sodium chloride-glutaric acid particles." Geophysical Research Letters 31, no. 12 (2004): n/a. http://dx.doi.org/10.1029/2004gl020025.

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10

Nam, Irina, Dong Seon Uh, Chang Il Oh, Jin Kuk Lee, Jae Min Oh, and Jong Seob Kim. "Synthesis and Solubility Study of the Polyamides Containing 4,4'-(9- fluorenylidene)dianiline in the Backbone as an Antireflecting Spin-on Hardmask Materials." Eurasian Chemico-Technological Journal 9, no. 1 (2007): 39–46. https://doi.org/10.18321/ectj253.

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Due to the continuous demand for smaller microelectronic devices, there exists a need to reduce the size of structural shapes in microelectronics and other related industries. Toward this end, effective lithographic techniques are essential to achieve a reduction in the size of microelectronic structures. Typical lithographic processes involve etch resistant photoresist underlying materials having antireflecting properties at a certain wavelength exposure. In this work, such materials were synthesized by the step-polymerization of diamines 2,2'-bis(3-amino- 4-hydroxyphenyl)hexafluoropropane (6
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