Relevant bibliographies by topics / High Resolution Ultrasonic Spectroscopy (HRUS)

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  1. Journal articles
  2. Dissertations / Theses
  3. Books
  4. Conference papers

Academic literature on the topic 'High Resolution Ultrasonic Spectroscopy (HRUS)'

Author: Grafiati
Published: 4 June 2021
Last updated: 11 February 2022

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Journal articles on the topic "High Resolution Ultrasonic Spectroscopy (HRUS)"

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Tian, Zhen, Nai Ci Bing, and Hong Yong Xie. "High-Resolution Ultrasonic Spectroscopy for Crystallization Process." Advanced Materials Research 508 (April 2012): 146–50. http://dx.doi.org/10.4028/www.scientific.net/amr.508.146.

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High-Resolution Ultrasonic Spectroscopy (HRUS) is a novel analytical technique for non-destructive material analysis for a wide range of samples and processes. This technique is based on precision measurements of velocity and attenuation of acoustical waves at high frequencies propagating through materials. It has considerable advantages over many alternative technologies because it can be applied to systems that are optically opaque and concentrated without the need of any sample preparation. It provides an unprecedented range of new analytical capabilities for research, product development, quality and process control. Applications of this technique include analysis of solution-phase crystallization, aggregation and gelation phenomena, particle sizing, stability of emulsions and suspensions, microstructural transitions and pharmaceutical manufacturing. Here, we review the theory of the HRUS and its applications on crystallization process.
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Buckin, Vitaly. "High-resolution ultrasonic spectroscopy." Journal of Sensors and Sensor Systems 7, no. 1 (March 29, 2018): 207–17. http://dx.doi.org/10.5194/jsss-7-207-2018.

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Abstract. High-resolution ultrasonic spectroscopy (HR-US) is an analytical technique for direct and non-destructive monitoring of molecular and micro-structural transformations in liquids and semi-solid materials. It is based on precision measurements of ultrasonic velocity and attenuation in analysed samples. The application areas of HR-US in research, product development, and quality and process control include analysis of conformational transitions of polymers, ligand binding, molecular self-assembly and aggregation, crystallisation, gelation, characterisation of phase transitions and phase diagrams, and monitoring of chemical and biochemical reactions. The technique does not require optical markers or optical transparency. The HR-US measurements can be performed in small sample volumes (down to droplet size), over broad temperature range, at ambient and elevated pressures, and in various measuring regimes such as automatic temperature ramps, titrations and measurements in flow.
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Buckin, Vitaly, and Evegny Kudryashov. "Super sonic: High-resolution ultrasonic spectroscopy." Biochemist 24, no. 4 (August 1, 2002): 25–27. http://dx.doi.org/10.1042/bio02404025.

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High-resolution ultrasonic spectrometry is a novel analytical technique with enormous potential for the investigation of a wide range of samples and dynamic processes. The non-destructive technique is based on measuring the changes that take place to ultrasonic waves as they pass through materials.
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Ajeena, Ihsan M., Raed H. Al-Saad, Ahmed Al-Mudhafar, Najah R. Hadi, and Sawsan H. Al-Aridhy. "Ultrasonic Assessment of Females with Carpal Tunnel Syndrome Proved by Nerve Conduction Study." Neural Plasticity 2013 (2013): 1–6. http://dx.doi.org/10.1155/2013/754564.

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Introduction. Carpal tunnel syndrome (CTS) is the most commonly diagnosed entrapment neuropathy of the upper extremity. The objective of this study was to diagnose CTS and to assess its severity using high resolution ultrasound (HRUS) depending on the results of nerve conduction study (NCS).Methods. A prospective cross-sectional study, in which HRUS was performed at 63 wrists of 35 female patients with different severity of CTS (as proved by NCS). Furthermore, 40 healthy volunteers (80 wrists) underwent the same tests as the patients and have been chosen to match the patients in gender, age, and body mass index (BMI). The cross section area (CSA) of the median nerve (MN) was obtained using HRUS at the carpal tunnel inlet by direct tracing method.Results.There was a significant difference in the CSA of the MN at the tunnel inlet in CTS patients when compared with the control group. In fact, the CSA of the control group showed a significant difference from each of patients subgroups. Furthermore, a significant difference in the CSA was seen in between these subgroups. In conclusion, the US examination of the MN seems to be a promising method in diagnosing and grading of carpal tunnel syndrome.
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Kučerík, J., H. Čechlovská, P. Bursáková, and M. Pekař. "Lignite humic acids aggregates studied by high resolution ultrasonic spectroscopy." Journal of Thermal Analysis and Calorimetry 96, no. 2 (November 11, 2008): 637–43. http://dx.doi.org/10.1007/s10973-008-9391-6.

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SMYTH, C. "High-resolution ultrasonic spectroscopy for analysis of industrial emulsions and suspensions." Journal of the Association for Laboratory Automation 9, no. 2 (April 2004): 87–90. http://dx.doi.org/10.1016/j.jala.2004.01.008.

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Resa, P., E. Kudryashov, and V. Buckin. "Direct real time monitoring of cellulose saccharification using high-resolution ultrasonic spectroscopy." New Biotechnology 25 (September 2009): S264—S265. http://dx.doi.org/10.1016/j.nbt.2009.06.591.

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Kargerová, Andrea, and Miloslav Pekař. "High-Resolution Ultrasonic Spectroscopy Study of Interactions between Hyaluronan and Cationic Surfactants." Langmuir 30, no. 40 (October 3, 2014): 11866–72. http://dx.doi.org/10.1021/la501852a.

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Cespi, Marco, Giulia Bonacucina, Giovanna Mencarelli, Stefania Pucciarelli, Gianfabio Giorgioni, and Giovanni F. Palmieri. "Monitoring the aggregation behaviour of self-assembling polymers through high-resolution ultrasonic spectroscopy." International Journal of Pharmaceutics 388, no. 1-2 (March 2010): 274–79. http://dx.doi.org/10.1016/j.ijpharm.2009.12.053.

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Buckin, V., P. Resa, and E. Kudryashov. "Ultrasonic enzyme assays. Real time monitoring of enzyme reactions in solutions and complex media using high-resolution ultrasonic spectroscopy." New Biotechnology 25 (September 2009): S130. http://dx.doi.org/10.1016/j.nbt.2009.06.439.

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Dissertations / Theses on the topic "High Resolution Ultrasonic Spectroscopy (HRUS)"

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Drastík, Martin. "Využití vysocerozlišovací ultrazvukové spektroskopie při charakterizaci huminových látek." Doctoral thesis, Vysoké učení technické v Brně. Fakulta chemická, 2010. http://www.nusl.cz/ntk/nusl-233314.

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Předkládaná dizertační práce se zabývá využitím techniky vysoce rozlišovací ultrazvukové spektroskopie (HRUS) při analýze huminových látek, za účelem získání hlubšího vhledu do problematiky vztahu mezi jejich primárními charakteristikami (elementární složení a rozložení uhlíku ve funkčních skupinách) a agregačními vlastnostmi. V literární rešerši jsou shrnuty nejnovější poznatky z oblasti studia huminových látek a představeny základní principy HRUS. Dále jsou uvedeny základní informace z oblasti fraktální analýzy a její aplikace na data získaná pomocí různých metod při studiu huminových látek. První úkol experimentální části je zaměřen na výhodné využití HRUS pro výzkum huminových látek, zde reprezentovaných standardy Mezinárodní společnosti pro huminové látky (IHSS) a to sodnými solemi huminových a fulvinových kyselin. Fulvinové kyseliny v jejich protonované formě byly taktéž zkoumány a to z důvodu objasnění vlivu sodného kationu. Pro popis chování vzorků byla použita mocninná funkce, jejíž empirické parametry byly korelovány s primárními charakteristikami. Byla vytvořena metoda fraktální analýzy a následně byla aplikována na data získána ultrazvukovou spektroskopií. Data získaná pomocí ultrazvukové spektroskopie byla zpracována i alternativní metodou. Ta spočívala v globálním pohledu na závislost ultrazvukové rychlosti na koncentraci a využití lineární regrese. Druhým z cílů práce je získání informací o vlivu teploty na stabilitu agregátů HS (IHSS standardy). Byl zkoumán vliv teplotních gradientů na chování agregátů při čtyřech různých koncentracích. V třetí části práce pak byly zkoumány koncentrační závislosti u vzorků pocházejících především z lokalit příliš nezasažených lidskou činností. HRUS data byla proložena mocninnou funkcí a zkoumána pomocí fraktální analýzy. Takto získané parametry byly korelovány s primárními vlastnostmi. Ze znalosti hustoty při dané koncentraci mohly být stanoveny velikosti hydratačních obálek. Jak se v současné době ukazuje, informace o agregačním chování huminových biomolekul mohou být v budoucnu velmi důležité pro navrhování průmyslových aplikací huminových látek, zejména v zemědělství a v ochraně životního prostředí, ale také například v medicíně.
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Poledňáková, Halina. "Teplotní závislost karagenanu a hyaluronanu." Master's thesis, Vysoké učení technické v Brně. Fakulta chemická, 2017. http://www.nusl.cz/ntk/nusl-316690.

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This diploma thesis focuses on the study of temperature dependence of -carrageen, hyaluronan of low molecular weight (250–450 kDa) and hyaluronan of high molecular weight (1 500–1 750 kDa) in aqueous solutions. The description of temperature depending changes in properties of these substance is based on rheological method. This work concentrates on the characterization of viscoelasticity through measurement of the storage (elastic) and loss (viscous) modulus using -carrageen and hyaluronan solutions of different molecular weights and different concentrations depending on temperature (20–50 °C, alternatively, in carrageen, 20–80 °C). The temperature dependence was further measured using an uncommon technique called high resolution ultrasonic spectroscopy (HR-US) which measured relative velocity of selected concentrations of -carrageen and hyaluronan of high molecular weight depending on the temperature of heating and cooling (20–80 °C). The measurements of temperature dependence were carried out for varied oscillation frequencies of rheometer sensor/frequency of ultrasonic waves. Knowledge of temperature dependence of the investigated substances may be applied in drug chemistry, primarily with respect to degradation due to high temperatures. The measured data gives information about sol-gel temperature and gel-sol temperature of carrageen.
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Trtek, Jan. "Interakce hyaluronanu s tenzidem CAE." Master's thesis, Vysoké učení technické v Brně. Fakulta chemická, 2018. http://www.nusl.cz/ntk/nusl-376801.

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The diploma thesis is focused on the study of interactions between hyaluronan of various molecular weights with CAE surfactant. This surfactant does not have the exact composition and there is not known their molecular weight. One of the main parameters needed to describe the interactions between surfactant and hyaluronan, there is the determination of critical micellar concentration. The value of critical micellar concentration of CAE is not known yet. All measurements were made for solutions in aqueous solution and 0.15 M NaCl. The determination of the molecular weight of this surfactant was performed by the technique SEC-MALS-dRI. High resolution ultrasonic spectroscopy was chosen to determine the critical micellar concentration and tensiometry was chosen as a complementary method. The interactions of CAE surfactant with polysaccharide of hyaluronan were showed by high resolution ultrasonic spectroscopy and densitometry. Compressibility was calculated from ultrasonic velocity and density.
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Čechlovská, Hana. "Studium hydrofobních domén v huminových kyselinách." Doctoral thesis, Vysoké učení technické v Brně. Fakulta chemická, 2008. http://www.nusl.cz/ntk/nusl-233282.

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Fyzikálně-chemická povaha hydrofobních domén huminových kyselin byla studována z několika hledisek. K objasnění významu fluorescenčních spekter byly vzorky podrobeny sekvenční frakcionaci, která pomohla k částečnému objasnění vlivu vodorozpustných složek, volných a vázaných lipidů na optické vlastnosti huminových kyselin. Výsledky naznačily, že fluorescenční píky tradičně přiřazované superpozici jednotlivých struktur jsou spíše důsledkem agregačních vlastností huminových molekul tvořících vlivem hydrofobního efektu zdánlivě vysoce aromatické struktury. Dále pak bylo zjištěno, že na optických vlastnostech huminových kyselin mají podíl i molekuly, které nemají primárně fluoroforní nebo chromoforní vlastnosti. Tento pohled je v souladu s teorií supramolekulárního uspořádání huminových kyselin. Dále byly studovány agregace, konformační chování a termodynamická stabilita huminových kyselin pomocí metody vysoce rozlišovací ultrazvukové spektroskopie. Bylo prokázáno, že huminové kyseliny mají schopnost agregovat už od velmi nízkých koncentrací (
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Jugl, Adam. "Studium interakcí hyaluronan-aminokyseliny." Master's thesis, Vysoké učení technické v Brně. Fakulta chemická, 2016. http://www.nusl.cz/ntk/nusl-240595.

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The master´s thesis deals with the study of the interaction between the polysaccharide hyaluronan of diffrerent molecular weights with the amino acids arginine, lysine, arginine hydrochloride and 6-aminocaproic acid. They are expected interaction between carboxyl groups of hyaluronan and amino groups of amino acids. These interactions were investigated by using ultrasonic spectroscopy, DLS, measuring pH and conductivity. Obtained results were compared with sodium polystyrene sulfonate. With ultrasonic spectroscopy was observed a change of concentration inkrement for titration of amino acid to water or polymers solutions especially for high molecular weight hyaluronan and for NaPSS in combination with 6AKK in concentration range of added amino acid 0–30 mM. The size of this change could mean a degree of interaction between polymers and amino acids. This theory has not been confirmed by other methods. By pH and conductivity measurements interations between arginine and low molecular weight hyaluronan and NaPSS were only confirmed. There was no possibility to make unequivocal conclusions from determination of particle size and zeta potential by DLS. Overall, the issue of the interaction of amino acids with polyanions was proved above expectations complex and will be appropriate to further expand the observations made in this thesis.
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Sovová, Šárka. "Vliv "zaplňovacích" činidel na interakce DNA-tenzid." Master's thesis, Vysoké učení technické v Brně. Fakulta chemická, 2017. http://www.nusl.cz/ntk/nusl-316190.

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Tato diplomová práce se zabývá vlivem zaplňovacích činidel na interakce v systému DNA-tenzid. DNA o velikosti 4017 párů bází byla připravena polymerázovou řetězovou reakcí, jako templát byl použit plasmid pSB-E1g. Polyetylen glykol (PEG) byl použit jako zaplňovací činidlo a jeho vliv na DNA-tenzid interakce byl zkoumán experimenty založenými na fluorescenci a gelové elektroforéze. Také byl studován vliv iontové síly za použití NaBr na interakce DNA-tenzid za použití zaplňovacího činidla. Data byla vyhodnocena a evaluována v této práci. V úvahu byl brán i možný vliv polyetylen glykolu na kritickou micelarní koncentraci (CMC) tenzidu, bylo provedeno měření CMC pomocí ultrazvuku s vysokým rozlišením, avšak nebyl zjištěn žádný značný vliv zaplňovacího činidla na CMC tenzidu. Část této práce bude zahrnuta v publikaci s anglickým názvem Combined role of macromolecular crowding and cationic surfactant in efficient DNA condensation.
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Hurčíková, Andrea. "Charakterizace hyaluronanu a jeho interakcí s tenzidy ultrazvukovou spektroskopií a densitometrií." Doctoral thesis, Vysoké učení technické v Brně. Fakulta chemická, 2014. http://www.nusl.cz/ntk/nusl-233394.

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This disertation thesis is focused on the study of physico-chemical interactions of hyaluronan (with molecular weights from 10 to 1750 kDa) with cationic surfactants measured using uncommon technique named high resolution ultrasonic spectroscopy. Densitometer was also used for the study of these interactions, in measuring of density and ultrasonic velocity of hyaluronan with different molecular weight in dependence on elevated temperature (25 50 °C). The aim is the determination of critical micelle concentration (CMC) and critical aggregation concentration (CAC) of the suractants in the absence and in the presence of hyaluronan with various molecular weights. Interactions in this system are important for the design of the systems for the targeted delivery, especially for the drugs. The experiments were made in water and sodium chloride solution. The significant breakpoint in the ultrasonic velocity showed changes in the system hyaluronan-surfactant.
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Books on the topic "High Resolution Ultrasonic Spectroscopy (HRUS)"

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Buckin, V. High-Resolution Ultrasonic Spectroscopy Cloth. Wiley & Sons, Limited, John, 2021.

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Conference papers on the topic "High Resolution Ultrasonic Spectroscopy (HRUS)"

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Buckin, V., and M. Caras Altas. "C1.1 - High-resolution ultrasonic spectroscopy." In AMA Conferences 2017. AMA Service GmbH, Von-Münchhausen-Str. 49, 31515 Wunstorf, Germany, 2017. http://dx.doi.org/10.5162/sensor2017/c1.1.

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Sharahi, Hossein J., Gajendra Shekhawat, Vinayak Dravid, Philip Egberts, and Seonghwan Kim. "Towards non-invasive high-resolution 3D nano-tomography by ultrasonic scanning probe microscopy." In International Conference on Nano-Bio Sensing, Imaging, and Spectroscopy 2017, edited by Jaebum Choo and Seung-Han Park. SPIE, 2017. http://dx.doi.org/10.1117/12.2269817.

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Lan, Jie, and Xiaochun Li. "Magnesium Matrix Nano-Composite Fabricated by Ultrasonic Dispersion of Nano-Sized SiC Particles in Molten Magnesium Alloy." In ASME 2004 International Mechanical Engineering Congress and Exposition. ASMEDC, 2004. http://dx.doi.org/10.1115/imece2004-61408.

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The use of ultrasonic nonlinear effects to disperse nano-sized ceramic particles in molten metal has been studied and nanosized SiC particle reinforced AZ91D magnesium composites were fabricated. The microstructure of the composites was investigated by high resolution scanning electron microscopy (SEM), X-ray photo spectroscopy (XPS) and high resolution X-Ray Diffractometer(XRD) techniques. Experimental results show a nearly uniform distribution and good dispersion of the SiC nanoparticles within the magnesium matrix, although some of small agglomerates (less than 300nm) were found in matrix. The microhardness of composites have been improved significantly compared to that of pure AZ91D. The ultrasonic fabrication methodology is striking to rapidly produce a wide range of nano-sized particles reinforced metal matrix composites.
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Sheng, Xiong, Dongsheng Hou, and Jinyang Zheng. "Investigation on Acoustic Propagation of Ultrasound in Polyethylene Pipe Used in Nuclear Power Plant." In ASME 2017 Pressure Vessels and Piping Conference. American Society of Mechanical Engineers, 2017. http://dx.doi.org/10.1115/pvp2017-65578.

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Polyethylene (PE) pipe, particularly high-density polyethylene (HDPE) pipe, has been successfully utilized to transport cooling water for both non-safety-related applications and safety-related applications in nuclear power plant (NPP). However, concerns of a lack of non-destructive examination (NDE) procedures and qualifications specialized for HDPE pipe impede its broader application. Traditional approximation without considering effects of acoustic dispersion could work for PE pipe with a small inspection depth. But for PE pipe of large size used in nuclear power plant, effects of acoustic attenuation and dispersion accumulate with depth, and have influence on waveforms of target pules, which brings great challenges to the energy concentration when performing ultrasonic phased-array inspection for PE pipe in NPP. In this paper, a theoretical method applying Szabo’s causal convolutional propagation operator based on causality theory was presented to obtain wave equations of ultrasound in PE considering both attenuation and dispersion, in which attenuation coefficient and phase velocity were used to separately characterize acoustic attenuation and dispersion. Then, an experimental method using ultrasonic spectroscopy technology was proposed to confirm the proposed model, and a good agreement was obtained. The results indicated that attenuation coefficient of PE had an approximately linear relation with frequency and that phase velocity rose logarithmically with frequency. Finally, effects of attenuation and dispersion on amplitude spectrum and waveform in time domain of the target signal were investigated. Frequency downshift and time delay shift had an influence on image resolution and focus capability, and were believed to be a restriction of current inspection technology. This work also theoretically proved that lower testing frequencies (less than 2.5MHz) could improve the inspection effectiveness of the applied inspecting systems for HDPE pipes in NPP applications.
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Datir, Harish, Knut Arne Birkedal, Sachin Kriplani, Hege Porten, and Niles Andre Aarseth. "ENHANCING THE RESERVOIR PERFORMANCE BY ACCESSING THE RESERVOIR SWEET SPOTS GUIDED BY FAR-FIELD SONIC IMAGING: AN INTEGRATED CASE STUDY FROM THE NORWEGIAN NORTH SEA." In 2021 SPWLA 62nd Annual Logging Symposium Online. Society of Petrophysicists and Well Log Analysts, 2021. http://dx.doi.org/10.30632/spwla-2021-0057.

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The gas present in the Valhall overburden crest area interferes with the seismic data and obscures the fault detection (minor faults). Spatially resolving fractures and fracture network is essential for subsurface understanding and future well placement in this field, and it is a critical input to the dynamic reservoir model. Additionally, mapping the fracture network in poor permeable reservoir formation beyond the wellbore is crucial to identify completion intervals to maximize productivity/injectivity, and hence field value. The well 2/8-F-18 A was drilled on the crest of the Valhall field as a pilot water injector in Lower Hod formation, where core and data analysis formed the foundation for a future potential 11 well development. The well is placed in the southern section of the Valhall crest, and no major faults or strong amplitude features were mapped out in the overburden via surface seismic before drilling. In this case study, an integrated workflow is proposed and tested within the reservoir formation to identify “sweet” (permeable and fractured) zones beyond the wellbore. This is achieved using borehole acoustic data combined with image and ultrasonic imaging to characterize fracture networks beyond the borehole wall. The sonic imaging workflow identifies reflection events from fractures and faults and provides the true dip, azimuth, and location in 3-dimensions. This data is complemented by nuclear magnetic resonance (NMR), dielectric and spectroscopy data to understand reservoir petrophysics. NMR-derived permeability has also been evaluated for identifying high permeable zone in this formation, which primarily focuses on intergranular permeability of the formation a few inches away from the borehole wall. Reservoir textural heterogeneity and fractures beyond the wellbore wall make this method difficult to estimate or enhance the effective permeability estimate. The baseline assumption for the NMR permeability estimation is also not valid in Hod formation; the Timur and SDR equation needs significant change to match core permeability. Hence, the primary aim is to identify a fracture network that will help support water injection and maximize hydrocarbons production through them. The goal is to establish a workflow from the learnings of this study, performed on the pilot well, validate its findings with the near-field data (core, imaging, and ultrasonic), and optimize it if needed (described in the methodology section). The developed workflow is then intended to be used to optimize the placement of future wells. The results achieved from the integrated workflow identified a key fault and mapped it approximately 23 meters away on each side of the borehole. It also captures acoustic anomalies (high amplitudes), validated based on near-field data, resulting from a fracture network potentially filled with hydrocarbons. The final results show the sub-seismic resolution of the fracture and fault network not visible on surface seismic due to the gas cloud above the reservoir and frequency effect on the surface seismic when compared to borehole sonic data. Evidently enhancing the blurred surface image, which helps enhance the structural and dynamic model of the reservoir.
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