Academic literature on the topic 'HPLC-ESI-HR/MS/MS'

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Journal articles on the topic "HPLC-ESI-HR/MS/MS"

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Chuankid, Boontiya, Hedda Schrey, Benjarong Thongbai, et al. "Secondary metabolites of Phlebopus species from Northern Thailand." Mycological Progress 19, no. 12 (2020): 1525–36. http://dx.doi.org/10.1007/s11557-020-01643-y.

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AbstractSubmerged cultures of the edible mushrooms Phlebopus portentosus and Phlebopus spongiosus were screened for their secondary metabolites by HPLC-UV/Vis and HR-LC-ESI-MS. Two new compounds, 9′-hydroxyphenyl pulvinone (1), containing an unusual pulvinone structure, and phlebopyron (2), together with the seven known pigments, atromentic acid (3), xerocomic acid (4), variegatic acid (5), methyl atromentate (6), methyl isoxerocomate (7), methyl variegatate (8), and variegatorubin (9) were isolated from the cultures. Their structures were assigned on the basis of extensive 1D/2D NMR spectrosc
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Ramirez, Javier E., Ricardo Zambrano, Beatriz Sepúlveda, Edward J. Kennelly, and Mario J. Simirgiotis. "Anthocyanins and antioxidant capacities of six Chilean berries by HPLC–HR-ESI-ToF-MS." Food Chemistry 176 (June 2015): 106–14. http://dx.doi.org/10.1016/j.foodchem.2014.12.039.

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Singh, Awantika, Vikas Bajpai, Sunil Kumar, et al. "Distribution and Discrimination Study of Bioactive Compounds from Berberis species using HPLC-ESI-QTOF-MS/MS with Principle Component Analysis." Natural Product Communications 11, no. 12 (2016): 1934578X1601101. http://dx.doi.org/10.1177/1934578x1601101209.

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Berberis species have been used extensively as raw material in various herbal medicines. In this work, a fast and sensitive method based on reversed-phase high-performance liquid chromatography coupled with electrospray ionization quadrupole time-of-flight tandem mass spectrometry (HPLC-ESI-QTOF-MS/MS) was used to assist the distribution and discrimination study of bioactive compounds from Berberis species such as B. aristata, B. asiatica, B. chitria, B. jaeschkeana, B. koehneana, B. lyceum, B. petiolaris and B. pseudoumbellata. The HPLC separation was performed on a Thermo Betasil C8 column (
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Syed, Muzna, Muhammad Noman Khan, Adeeba Khadim, et al. "Chemical fingerprinting of three Anemone species and an adulteration study to detect cross mixing of medicinal plants by HPLC-HR-ESI-MS/MS method." Journal of King Saud University - Science 33, no. 5 (2021): 101461. http://dx.doi.org/10.1016/j.jksus.2021.101461.

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Bulduk, Ibrahim, and Fulya Taktak. "Isolation and Characterization of Antitumor Alkaloid from Poppy Capsules (Papaver somniferum)." Journal of Chemistry 2013 (2013): 1–4. http://dx.doi.org/10.1155/2013/493870.

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Noscapine, a phthalideisoquinoline alkaloid derived from opium, has been used in the treatment of various cancer types. Its low-toxicity profile has increased attention to this alkaloid. With regard to increasing demand for this compound, we developed a new method for isolation of noscapine from dried capsules ofPapaver somniferum. Noscapine was successfully isolated from poppy capsules for the first time and the purity of the isolated compound was determined to be over 99.59% by HPLC analysis. The structure of noscapine was confirmed by NMR, NMR, FT-IR, elemental analysis, and HR-ESI-MS metho
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Veselova, Marina V., Sergey A. Fedoreyev, Darya V. Tarbeeva, et al. "Cytotoxic Prenylated Polyphenolic Compounds from Maackia amurensis Root Bark." Natural Product Communications 12, no. 7 (2017): 1934578X1701200. http://dx.doi.org/10.1177/1934578x1701200709.

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Two new prenylated flavanones, isomaackiaflavanone A (1), isomaackiaflavanone B (2) and a new prenylated stilbene maackiastilbene (3), along with five known flavanones were isolated from the root bark of Maackia amurensis using repeated column chromatography on silica gel, Sephadex LH-20 and octadecyl silica (ODS-A) sorbents. The structures of the new compounds were elucidated by HPLC–PDA–MS, HR-ESI-MS, 1H, 13C, 1H–1H COSY, HSQC, ROESY and HMBC NMR analyses. The cytotoxicity of compounds 1–2, 4–8 against two human cancer cell lines HeLa and SK-MEL-5 was tested using the MTS method. Compounds 4
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Karady, Michal, Ondřej Novák, Aleš Horna, Miroslav Strnad, and Karel Doležal. "High Performance Liquid Chromatography/Electrochemistry/High Resolution Electrospray Ionization‐Mass Spectrometry (HPLC/EC/HR ESI‐MS) Characterization of Selected Cytokinins Oxidation Products." Electroanalysis 27, no. 2 (2015): 406–14. http://dx.doi.org/10.1002/elan.201400286.

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Mishchenko, Natalia P., Elena A. Vasileva, Andrey V. Gerasimenko, Valeriya P. Grigorchuk, Pavel S. Dmitrenok, and Sergey A. Fedoreyev. "Isolation and Structure Determination of Echinochrome A Oxidative Degradation Products." Molecules 25, no. 20 (2020): 4778. http://dx.doi.org/10.3390/molecules25204778.

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Echinochrome A (Ech A, 1) is one of the main pigments of several sea urchin species and is registered in the Russian pharmacopeia as an active drug substance (Histochrome®), used in the fields of cardiology and ophthalmology. In this study, Ech A degradation products formed during oxidation by O2 in air-equilibrated aqueous solutions were identified, isolated, and structurally characterized. An HPLC method coupled with diode-array detection (DAD) and mass spectrometry (MS) was developed and validated to monitor the Ech A degradation process and identify the appearing compounds. Five primary ox
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Mao, Ziling. "Chemical Composition of Essential Oil from Dalbergia odorifera Flowers and HPLC Analysis of Tectorigenin in Its Leaves and Branches." International Journal of Agriculture and Biology 25, no. 03 (2021): 723–29. http://dx.doi.org/10.17957/ijab/15.1721.

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Dalbergia odorifera T. Chen, as an important traditional Chinese medicinal plant, has been used in China over a long history. The chemical composition of volatile oil extracted from the D. odorifera flowers is described for the first time here. The volatile oil was extracted by hydro-distillation, and GC-MS was used for the chemical composition analysis. Tectorigenin, an isoflavonoid, was also isolated from the flowers. The structure of tectorigenin was established based on 1H and 13C NMR and HR-ESI-MS spectrometry. The main components of the volatile oil from the flowers were 4-hydroxy-4-meth
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Yu, Feng, Xiaomei Tian, Ying Sun, Yuhui Bi, Zhiguo Yu, and Li Qin. "Xenocyloin Derivatives from Liquid Cultures of Xenorhabdus bovienii SN52." Natural Product Communications 12, no. 12 (2017): 1934578X1701201. http://dx.doi.org/10.1177/1934578x1701201209.

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Members of genus Xenorhabdus are symbiotically associated with entomopathogenic nematodes of genus Steinernema. Herein, we describe the isolation and purification of four novel metabolites, xenocyloins G-J (1–4), from liquid cultures of Xenorhabdus bovienii SN52 by extensive column chromatography and semi-preparative HPLC. Chemical structures of the xenocyloin derivatives were determined based on comprehensive NMR spectra and HR-ESI-MS analyses. All compounds exhibited significant collagen-induced anti-platelet aggregation activities, among which xenocyloin H (2) exhibited the strongest activi
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Dissertations / Theses on the topic "HPLC-ESI-HR/MS/MS"

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Čáková, Veronika. "Contribution à l'étude phytochimique d'orchidées tropicales : identification des constituants d'Aerides rosea et d'Acampe rigida : techniques analytiques et préparatives appliquées à Vanda coerulea et Vanda teres." Phd thesis, Université de Strasbourg, 2013. http://tel.archives-ouvertes.fr/tel-00997451.

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L'analyse de la composition chimique de deux orchidées de la sous-tribu des Aeridinae, Aerides rosea Lodd. ex. Lindl. & Paxton et Acampe rigida (Buch.-Ham. ex Sm.) P. F. Hunt, a été menée en ayant recours à des techniques de couplages et grâce à une stratégie de déréplication. Dix dérivés phénanthréniques ont ainsi été identifiés dans les tiges d'A. rosea, dont deux nouvellement décrits. Quatre stilbénoïdes, trois dérivés d'acides phénoliques et quatre esters d'acide cinnamique ont été identifiés dans les tiges d'A. rigida. Nous avons également effectué des dosages de traceurs dans différents
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