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Journal articles on the topic 'HR FESEM.Photocatalysis'

Author: Grafiati

Published: 3 June 2025

Last updated: 20 July 2025

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1

Brijesh, Pare, Joshi Vaishali, and Piplode Satish. "EFFECT OF OPERATIONAL PARAMETERS ON PHOTOCATALYTIC DEGRADATION OF TOLUIDINE BLUE UTILIZING BiOCl NANOPLATES IN SOLAR LIGHT." International Journal of Engineering Technologies and Management Research 4, no. 12 : SE (2017): 43–54. https://doi.org/10.5281/zenodo.1162996.

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<strong><em>This work is devoted to the study of the effects of various operational parameters such as H<sub>2</sub>O<sub>2</sub>, K<sub>2</sub>S<sub>2</sub>O<sub>8, </sub>NaCl,<sub> </sub>Na<sub>2</sub>CO<sub>3</sub>, FeCl<sub>3</sub>, Fenton’s reagent, O<sub>2</sub>, N<sub>2</sub> purging, effect of other photocatalysts on the photocatalytic degradation of toluidine blue dye by as synthesized nano BiOCl under solar light in following conditions pH= 11, catalyst loading= 30 mg/100ml and initial dye concentration= 4 × 10<sup>-5 </sup>mol L<sup>-1</sup>. Nano BiOCl was prepared by a

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2

Pare, Brijesh, Vaishali Joshi, and Satish Piplode. "EFFECT OF OPERATIONAL PARAMETERS ON PHOTOCATALYTIC DEGRADATION OF TOLUIDINE BLUE UTILIZING BiOCl NANOPLATES IN SOLAR LIGHT." International Journal of Engineering Technologies and Management Research 4, no. 12 (2020): 43–54. http://dx.doi.org/10.29121/ijetmr.v4.i12.2017.590.

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This work is devoted to the study of the effects of various operational parameters such asH2O2, K2S2O8, NaCl, Na2CO3, FeCl3, Fenton’s reagent, O2, N2 purging, effect of otherphotocatalysts on the photocatalytic degradation of toluidine blue dye by as synthesized nanoBiOCl under solar light in following conditions pH= 11, catalyst loading= 30 mg/100ml andinitial dye concentration= 4 × 10-5 mol L-1. Nano BiOCl was prepared by a simple hydrolysismethod at room temperature and characterized by X-ray diffraction (XRD) and HighResolution Field Emission Scanning Microscope (HR FESEM). XRD pattern sug

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3

Brijesh, Pare, Piplode Satish, and Joshi Vaishali. "EFFECT OF OPERATIONAL PARAMETER ON PHOTOCATALYTIC DEGRADATION OF OXAMYL PESTICIDE." International Journal of Engineering Technologies and Management Research 4, no. 12 : SE (2017): 74–84. https://doi.org/10.5281/zenodo.1163015.

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<strong><em>Flower like bismuth oxy chloride (BiOCl) was successfully synthesized by a simple hydrolytic method at room temperature. The precursor and as-prepared samples were characterized by X-ray diffraction (XRD), High Resolution Field Emission Scanning Electron Microscope (HR FESEM). The results indicated that the as-prepared BiOCl sample is self-assembled hierarchically with nano sheets. The photocatalytic activity of BiOCl was tested on the degradation of the Oxamyl (OM) under solar light irradiation. The results showed that pesticide molecules could be efficiently degraded over BiOCl u

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4

Hossen, Md Arif, Fatema Khatun, Riyadh Ramadhan Ikreedeegh, et al. "Enhanced Photocatalytic CO2 Reduction to CH4 Using Novel Ternary Photocatalyst RGO/Au-TNTAs." Energies 16, no. 14 (2023): 5404. http://dx.doi.org/10.3390/en16145404.

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Photocatalytic CO2 reduction into hydrocarbon fuels is one of the most efficient processes since it serves as a renewable energy source while also lowering atmospheric CO2 levels. The development of appropriate materials and technology to attain greater yield in CO2 photoreduction is one of the key issues facing the 21st century. This study successfully fabricated novel ternary reduced graphene oxide (RGO)/Au-TiO2 nanotube arrays (TNTAs) photocatalysts to promote CO2 photoreduction to CH4. Visible light-responsive RGO/Au-TNTAs composite was synthesized by facile electrochemical deposition of A

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Rokade, Vanita, Ramejabi Sayyad, and Sharda Gadale. "Synthesis and Structural, Optical and Photocatalytic Properties of Erbium doped Silica Nanocomposites." Research Journal of Chemistry and Environment 26, no. 6 (2022): 73–80. http://dx.doi.org/10.25303/2606rjce073080.

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Nowadays, increasing population and advanced industrialization have extended the use of synthetic dyes in day-to-day life which further results in dye pollution. Large numbers of photocatalysts are being used in industry to reduce pollution. In the present study, the Erbium doped silica nanocomposites were synthesised by sol gel method and used for photocatalytic applications. The characterization of catalysts was carried out by Powder X-ray diffraction analysis (XRD), Flame Emission scanning electron microscopy (FESEM), Energy-dispersed X-ray analysis (EDX), High Resolution transmission elect

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6

Kumar, A. Manisha Bhardwaj R. Yadav DD Anju and Jha R. "One Pot Synthesized 2H - MoS2 as Efficient Photocatalyst for Degradation of Titan Yellow Dye under Solar Light Illumination." Environmental Science Archives 3, no. 2 (2024): 103–15. https://doi.org/10.5281/zenodo.13879984.

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Molybdenum disulfide (MoS2) was synthesized and employed as a promising catalyst under sunlight illumination for the photocatalytic degradation of Titan yellow (TY) dye. The structural and physiochemical features of the hydrothermally synthesized MoS2 nanoparticles were examined by X-ray Diffraction (XRD), X-ray Photoelectron Spectroscopy (XPS), Field Emission Scanning Electron Microscopy (FESEM), High-Resolution Transmission Electron Microscopy (HR-TEM) and UV-Vis spectrophotometer. XRD affirmed the formation of 2H-MoS2, which is the most stable phase of the MoS2. Additionally, morphological

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Husein, Saddam, Ryan Rafi Rustamadji, Reno Pratiwi, Eniya Listiani Dewi, and Slamet. "Simultaneous tartrazine-tetracycline removal and hydrogen production in the hybrid electrocoagulation-photocatalytic process using g-C3N4/TiNTAs." Communications in Science and Technology 9, no. 1 (2024): 46–56. http://dx.doi.org/10.21924/cst.9.1.2024.1308.

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This study aimed to investigate the removal of tartrazine dye & tetracycline antibiotic and hydrogen (H2) production simultaneously through the hybrid electrocoagulation-photocatalytic process using g-C3N4/TiO2 nanotube arrays (TiNTAs) nanocomposite. The g-C3N4/TiNTAs was used as the photocatalyst. The melamine as the precursor of g-C3N4 was varied to obtain the optimal loading on the removal of tartrazine dye & tetracycline antibiotic and hydrogen (H2) production simultaneously. The integrated acrylic photoreactor was equipped with two 250-W mercury lamps. The nanotubular morphology o

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8

Chong, C. Y., T. H. W. Lee, J. C. Juan, et al. "Superparamagnetic Iron Oxide Decorated Indium Hydroxide Nanocomposite: Synthesis, Characterization and Its Photocatalytic Activity." Bulletin of Chemical Reaction Engineering & Catalysis 17, no. 1 (2021): 113–26. http://dx.doi.org/10.9767/bcrec.17.1.12352.113-126.

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A simple and scalable liquid-based method was developed to produce a nanocomposite photocatalyst which was comprised of Fe3O4 nanoparticles (4-5 nm) decorated indium hydroxide nanorods (mean width 33 nm and average aspect ratio 2-3). The nanocomposite was produced at 25 ℃ in water via a hydroxide-induced co-precipitation ensued by a cathodic reduction during which the non-magnetic Fe(OH)3 intermediate was reduced to magnetic Fe3O4 at 20 V within 1 h. The incorporation of Fe3O4 nanoparticles served to bestow magnetic recoverability to the photocatalyst and helped enhance visible light absorptio

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9

Chinnadhurai, S., M. Arockia Doss, and J. Kamalakkannan. "Effective, Reusable Applications of Nanostructured Silver-MnO2 for Dye Degradation under UV Light and Dye-Sensitized Solar Cells." Asian Journal of Chemistry 37, no. 3 (2025): 707–14. https://doi.org/10.14233/ajchem.2025.33255.

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Silver-MnO2, a metal-doped semiconductor oxide, was synthesized using a simple precipitation technique and characterized with XRD, FESEM, HR-SEM, TEM, EDS, UV-Vis DRS and PL spectroscopy. The XRD and EDS results confirmed that MnO2 and metallic silver (Ag) are present in the catalyst, whereas FESEM images revealed a blend of nanoparticles with many cavities and hexagonal nanosheets. The HR-SEM and TEM analyses indicated that MnO2 particles have a pentagonal or hexagonal shape with silver clusters on their smooth surfaces. Interestingly, Ag-MnO2 absorbed more light in both the UV and visible ar

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10

El-Hadary, El-Hadary A., Hesham H. El-Feky, Amjad El-Qanni, Ibrahim M. Nassar, and Mostafa Y. Nassar. "CdO Nanostructures: Synthesis, Characterization, and Photocatalytic Degradation of Malachite Green Dye in Aqueous Media." Asian Journal of Chemical Sciences 13, no. 1 (2023): 24–36. http://dx.doi.org/10.9734/ajocs/2023/v13i1230.

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Cadmium oxide (CdO) nanoparticles were prepared by using co-precipitation method and applied on photodegradation of malachite green (MG) dye in an aqueous solution. The as-prepared CdO nanoparticles were characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), High-resolution transmission electron microscopy (HR-TEM) and (SAED), and Fourier transform infrared (FTIR) techniques. The XRD pattern confirmed the formation of crystalline CdO nanoparticles with cubic structure while the FESEM image validated the preparation of disc-like spherical irregular shape

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11

Pare, Brijesh, Satish Piplode, and Vaishali Joshi. "EFFECT OF OPERATIONAL PARAMETER ON PHOTOCATALYTIC DEGRADATION OF OXAMYL PESTICIDE." International Journal of Engineering Technologies and Management Research 4, no. 12 (2020): 74–84. http://dx.doi.org/10.29121/ijetmr.v4.i12.2017.595.

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Flower like bismuth oxy chloride (BiOCl) was successfully synthesized by a simple hydrolytic method at room temperature. The precursor and as-prepared samples were characterized by X-ray diffraction (XRD), High Resolution Field Emission Scanning Electron Microscope (HR FESEM). The results indicated that the as-prepared BiOCl sample is self-assembled hierarchically with nano sheets. The photocatalytic activity of BiOCl was tested on the degradation of the Oxamyl (OM) under solar light irradiation. The results showed that pesticide molecules could be efficiently degraded over BiOCl under solar l

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12

Yang, Chii Rong, Tun Ping Teng, and Yun Yu Yeh. "Characterizations and Process Parameters of Titanium Dioxide Thin Film by RF Sputtering." Journal of Nano Research 22 (May 2013): 9–21. http://dx.doi.org/10.4028/www.scientific.net/jnanor.22.9.

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In this study, we successfully combined RF magnetron sputtering of a pure Ti metal target and one-stage oxidation process with a wider oxygen ratio (10%-90%) and total sputtering flow rate (16-24 sccm) to produce TiO2thin films on a glass substrate. The crystallization, morphology, roughness, and thickness of the thin films were examined using XRD, HR-FESEM, AFM, and a profilometer. Subsequently, the photocatalytic performance was examined using a spectrometer and video tensiometer. The experimental results show that the TiO2thin films with a majority of anatase and higher roughness exhibit su

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13

Saharudin, Khairul Arifah, and Srimala Sreekantan. "Higher Photocatalytic Activity of P-Incorporated TiO₂ Nanotube Arrays." Advanced Materials Research 1087 (February 2015): 452–56. http://dx.doi.org/10.4028/www.scientific.net/amr.1087.452.

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TiO2 nanotubes arrays were prepared by anodization of Ti in EG containing H3PO4 and NH4F electrolyte. The samples were characterized by X-ray diffraction (XRD), Field emission scanning electron microscopy (FESEM), Energy dispersive X-ray spectroscopy (EDX) and photoluminescence spectra (PL). The as-anodized TiO2 nanotubes were annealed in inert (argon), reducing (nitrogen), or oxidizing (oxygen) atmosphere at 400 °C for 4 hr. XRD analysis revealed that the TiO2 nanotubes were anatase after annealing. In this study, the TiO2 nanotubes annealed in argon exhibited the highest degradation rate of

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14

Al-Hunaiti, Afnan, Qassem Mohaidat, Ibrahim Bsoul, Sami Mahmood, Deeb Taher, and Tareq Hussein. "Synthesis and Characterization of Novel Phyto-Mediated Catalyst, and Its Application for a Selective Oxidation of (VAL) into Vanillin under Visible Light." Catalysts 10, no. 8 (2020): 839. http://dx.doi.org/10.3390/catal10080839.

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Here, we report an efficient and highly selective oxidation of lignin model substrate using phyto-mediated ZnFe2O4 nanoparticle using Boswellia carterii extract. The nanocatalyst with an average size of 8 nm showed excellent photocatalytic activity of the synthesized carbonyl containing products under visible light irradiation. The catalytic activity and selectivity towards oxidation of vanillyl alcohol to vanillin with selectivity up to 99% at conversion over 98% and turn-over frequency values up to 1600 h−1 were obtained in the presence of H2O2 and base. The cubic spinel nano-ZnFe2O4 catalys

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15

Mohd Rozi, Nurshahira, Sheela Chandren, and Norazah Basar. "Garcinia mangostana Pericarp-Assisted Silver Nanoparticles as a Sustainable Solution for Tetracycline Contaminants Removal from Wastewater." Malaysian Journal of Fundamental and Applied Sciences 21, no. 3 (2025): 2032–44. https://doi.org/10.11113/mjfas.v21n3.3797.

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To date, research endeavours are progressively oriented toward uncovering sustainable approaches for synthesizing metal nanoparticles. Biosynthesis methods involving plants have emerged as a viable alternative to foster environmental sustainability. This study explores a one-pot and room-temperature method for synthesizing silver nanoparticles (AgNPs) using agricultural waste, Garcinia mangostana pericarp (GMP), to degrade tetracycline cost-effectively. High-performance liquid chromatography (HPLC) detected the presence of α-mangostin, suggesting a dual-functioning agent in reduction and stabi

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16

Muthukrishnaraj, Appusamy, Salma Ahmed Al-Zahrani, Ahmed Al Otaibi, et al. "Enhanced Photocatalytic Activity of Cu2O Cabbage/RGO Nanocomposites under Visible Light Irradiation." Polymers 13, no. 11 (2021): 1712. http://dx.doi.org/10.3390/polym13111712.

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Towards the utilization of Cu2O nanomaterial for the degradation of industrial dye pollutants such as methylene blue and methyl orange, the graphene-incorporated Cu2O nanocomposites (GCC) were developed via a precipitation method. Using Hummers method, the grapheme oxide (GO) was initially synthesized. The varying weight percentages (1–4 wt %) of GO was incorporated along with the precipitation of Cu2O catalyst. Various characterization techniques such as Fourier-transform infra-red (FT-IR), X-ray diffraction (XRD), UV–visible diffused reflectance (UV-DRS), Raman spectroscopy, thermo gravimetr

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17

Shemona, A. Mary George, S. Kanagaprabha, H. Johnson Jeyakumar, and S. Arul Vathana. "Green Synthesis of TiO<sub>2</sub> Nanoparticles Using Piper Longum Leaf Extract: Morphological, Optical and Antibacterial Characterization." Materials Science Forum 1143 (December 26, 2024): 73–88. https://doi.org/10.4028/p-8cplzy.

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In this study, Titanium dioxide nanoparticles (TiO2 NPs) were synthesized using Piper longum leaf extract as both a capping and reducing agent through a green synthesis approach. The synthesized TiO2 NPs were thoroughly characterized using multiple techniques: X-ray diffraction (XRD), Fourier transform infrared spectroscopy (FTIR), UV-Diffuse reflectance spectroscopy (UV-DRS), field emission scanning electron microscopy (FESEM), High-Resolution Transmission Electron Microscopy (HR-TEM), Brunauer-Emmett-Teller (BET) analysis, and X-ray photoelectron spectroscopy (XPS). XRD analysis confirmed th

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18

Horandghadim, Nazila, Mohammad Ghorbani, and Abolghasem Dolati. "Self-Cleaning TiO₂ Nanofilms on FTO Glass: Influence of Electrophoretic Deposition and UV Irradiation Conditions." Journal of Nano Research 30 (March 2015): 39–49. http://dx.doi.org/10.4028/www.scientific.net/jnanor.30.39.

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In this research, anatase TiO2nanoparticles were electrophoretically deposited on the FTO glass. This investigation was focused on the self-cleaning property of TiO2coatings and the effects of different parameters on this characteristic such as: applied voltages during electrophoretic depositions and durations of UV irradiation. Electrophoretic depositions of suspensions were performed in different voltages of 10, 30 and 60 V (for 10 s) at room temperature. TiO2coatings were sintered in 450°C for 1 hr. The phase transformation of TiO2films was considered using XRD. Morphology, average particle

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19

Singh, Karanpal, Nancy, Monika Bhattu, Gurjinder Singh, Nabisab Mujawar Mubarak, and Jagpreet Singh. "Light-absorption-driven photocatalysis and antimicrobial potential of PVP-capped zinc oxide nanoparticles." Scientific Reports 13, no. 1 (2023). http://dx.doi.org/10.1038/s41598-023-41103-7.

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AbstractToxic dyes in water bodies and bacterial pathogens pose serious global challenges to human health and the environment. Zinc oxide nanoparticles (ZnO NPs) demonstrate remarkable photocatalytic and antibacterial potency against reactive dyes and bacterial strains. In this work, PVP-ZnO NPs have been prepared via the co-precipitation method using polyvinylpyrrolidone (PVP) as a surfactant. The NPs’ microstructure and morphology were studied using X-ray diffraction (XRD), having a size of 22.13 nm. High-resolution transmission electron microscope (HR-TEM) and field emission scanning electr

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20

Gaur, Jyoti, Sanjeev Kumar, Harpreet Kaur, et al. "Eco-friendly innovation: Harnessing nature's blueprint for enhanced photocatalysis and antimicrobial potential in multi-structured PN/ZnO nanoparticles." Functional Composites and Structures, February 22, 2024. http://dx.doi.org/10.1088/2631-6331/ad2c10.

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Abstract This research unveils an innovative approach to green synthesis, detailed characterization, and multifunctional exploration of bio-functionalized zinc oxide nanoparticles (PN/ZnO NPs) adorned with phytochemicals from Piper nigrum (PN). Employing an extensive suite of spectroscopic techniques and physicochemical methods, including UV-vis spectroscopy, FE-SEM, HR-TEM, EDX spectroscopy, FTIR, XRD, and BET analysis, the study delves into the unique properties of PN/ZnO NPs. XRD confirms the development of the wurtzite phase with a crystallite diameter of 47.77 nm. FTIR reveals ZnO functio

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21

Oluwatobi David, Adekoya, Muhammad Tahir, and Nor Aishah Saidina Amin. "Copper modified TiO2 and g-C3N4 catalysts for photoreduction of CO2 to methanol using different reaction mediums." Malaysian Journal of Fundamental and Applied Sciences 11, no. 3 (2015). http://dx.doi.org/10.11113/mjfas.v11n3.376.

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In this study, Cu/TiO2 and Cu/g-C3N4 catalysts were tested for CO2 reduction to methanol. The catalysts were prepared by the wet impregnation method and, characterized by XRD and FESEM. The product identification and yield were determined using a GC with FID. The CO2 photoreduction process was performed in each of the following reaction mediums: H2O, NaOH, KOH, Na2CO3, K2CO3, NaHCO3 and KHCO3. The efficiency was studied by comparing the methanol yield for each. A slurry type photoreactor with a UV lamp of 365 nm wavelength was used. CO2 photoreduction to methanol using NaOH as the reaction med

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22

Moeinifard, Behzad, and Alireza Najafi Chermahini. "Fabrication of Au-doped mesoporous TiO2 supported on g-C3N4 as an efficient light-assisted catalyst for oxidative desulfurization of model fuels with different sulfur content." Journal of Materials Science: Materials in Engineering 20, no. 1 (2025). https://doi.org/10.1186/s40712-025-00225-8.

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Abstract In the present study, the mesoporous TiO2 that was supported on graphitic carbon nitride (g-C3N4) was decorated with Au. The nanocomposite (Au-m-TiO2/g-C3N4) has been successfully synthesized by combining sono-chemical and EISA methods and was subsequently used in photocatalytic oxidative desulfurization of dibenzothiophene (DBT) in n-octane as a model fuel and under visible illumination. The Au-m-TiO2/g-C3N4 photocatalyst was characterized by X-ray diffraction (XRD), field emission scanning electron microscopy (FESEM), UV–Vis diffusive reflectance spectra (UV–Vis DRS), high-resolutio

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23

Paul, Payal, Dewakar Sharma, Joydeep Biswas, Kamakhya Prakash Misra, Sanjib Kabi, and Saikat Chattopadhyay. "Effect of Growth Time on Structural and Optical Properties of Chemically Synthesized TiO2 Nanostructures." Current Nanoscience 20 (July 10, 2024). http://dx.doi.org/10.2174/0115734137306442240630051459.

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Introduction: Titanium Dioxide (TiO2) is popular in the scientific community due to its wide variety of applications in optoelectronic devices, solar cells, gas sensors, photocatalytic reagents, and the biomedical industry. It is a wide band gap semiconductor with a band gap of 3.2eV. Usually, it shows three different phases, like anatase, rutile, and brookite, based on the synthesis method and annealing temperature. Method: Here, we report a simple chemical process to synthesize TiO2 nanostructures (NSs) at low temperatures to study the impact of growth time on structural and morphological pr

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24

Sharif, Muhammad Shahid, Muhammad Aqeel, Ali Haider, et al. "Photocatalytic, Bactericidal and Molecular Docking Analysis of Annealed Tin Oxide Nanostructures." Nanoscale Research Letters 16, no. 1 (2021). http://dx.doi.org/10.1186/s11671-021-03495-1.

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AbstractNanosized tin oxide was fabricated with a simple and cost-effective precipitation technique and was analyzed by performing x-ray powder diffraction (XRD), Fourier-transform infrared (FT-IR) spectroscopy, high-resolution transmission electron (HR-TEM) microscopy, energy-dispersive x-ray (EDX) and UV–Vis spectroscopy. The XRD results revealed that tin oxide particles possessed typical orthorhombic structure and exhibited improved crystallinity with annealing. Calcination at 250 °C produced predominantly orthorhombic SnO which transformed to SnO2 at higher temperatures of 500 and 750 °C.

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