Relevant bibliographies by topics / Hydrogenolysis. Acetates

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Academic literature on the topic 'Hydrogenolysis. Acetates'

Author: Grafiati
Published: 4 June 2021
Last updated: 18 February 2022

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Journal articles on the topic "Hydrogenolysis. Acetates"

1

Belmont, James A., Jorge Soto, Roswell E. King, Andrew J. Donaldson, John D. Hewes, and M. Frederick Hawthorne. "Metallacarboranes in catalysis. 8. I: Catalytic hydrogenolysis of alkenyl acetates. II: Catalytic alkene isomerization and hydrogenation revisited." Journal of the American Chemical Society 111, no. 19 (1989): 7475–86. http://dx.doi.org/10.1021/ja00201a031.

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2

Robins, Morris J., Ruiming Zou, Fritz Hansske, and Stanislaw F. Wnuk. "Synthesis of sugar-modified 2,6-diaminopurine and guanine nucleosides from guanosine via transformations of 2-aminoadenosine and enzymatic deamination with adenosine deaminase." Canadian Journal of Chemistry 75, no. 6 (1997): 762–67. http://dx.doi.org/10.1139/v97-092.

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Treatment of 2,6-diaminopurine riboside (2-aminoadenosine) with α-acetoxyisobutyryl bromide in acetonitrile gave mixtures of the trans 2′,3′-bromohydrin acetates 2. Treatment of 2 with zinc–copper couple effected reductive elimination, and deprotection gave 2,6-diamino-9-(2,3-dideoxy-β-D-erythro-pent-2-enofuranosyl)purine (3a). Treatment of 2 with Dowex 1 × 2 (OH−) resin in methanol gave the 2′,3′-anhydro derivative 4. Stannyl radical-mediated hydrogenolysis of 2 and deprotection gave the 2′-deoxy 6a and 3′-deoxy 7a nucleosides. Treatment of the 3′,5′-O-(tetraisopropyldisiloxanyl) derivative (
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3

Tsuji, Jiro, Ichiro Minami, and Isao Shimizu. "Preparation of 1-Alkenes by the Palladium-Catalyzed Hydrogenolysis of Terminal Allylic Carbonates and Acetates with Formic Acid-Triethylamine." Synthesis 1986, no. 08 (1986): 623–27. http://dx.doi.org/10.1055/s-1986-31723.

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4

Agarwal, A. K., N. W. Cant, M. S. Wainwright, and D. L. Trimm. "Catalytic hydrogenolysis of esters: a comparative study of the reactions of simple formates and acetates over copper on silica." Journal of Molecular Catalysis 43, no. 1 (1987): 79–92. http://dx.doi.org/10.1016/0304-5102(87)87023-2.

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5

Gozlan, Charlotte, Elsa Deruer, Marie-Christine Duclos, et al. "Preparation of amphiphilic sorbitan monoethers through hydrogenolysis of sorbitan acetals and evaluation as bio-based surfactants." Green Chemistry 18, no. 7 (2016): 1994–2004. http://dx.doi.org/10.1039/c5gc02131f.

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6

Xu, Rui, Kunbo Lian, Zhikang Xu, et al. "Controllable synthesis of Ir(Rh)–Sn/SiO2 bimetallic catalysts via surface organometallic chemistry for the production of ethanol from hydrogenolysis of ethyl acetate." Catalysis Science & Technology 10, no. 4 (2020): 1086–95. http://dx.doi.org/10.1039/c9cy02071c.

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A series of highly active Ir–Sn/SiO<sub>2</sub> and Rh–Sn/SiO<sub>2</sub> catalysts for ethyl acetate hydrogenolysis to ethanol were prepared from the grafting synthesis based on the surface organometallic chemistry concept.
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7

Burns, CJ, M. Gill, and S. Saubern. "Pigments of Fungi. XXI. Synthesis of (±)-6-Demethoxyaustrocortirubin." Australian Journal of Chemistry 44, no. 10 (1991): 1427. http://dx.doi.org/10.1071/ch9911427.

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6-Demethoxyaustrocortirubin (6) is synthesized via the epoxide (21) which is available in 73% yield over four steps from naphthazarin (10). Hydrolysis of the epoxide (21) yields the diol (25) which on hydrogenolysis affords 6-demethoxy-1-deoxyaustrocortirubin (7). Stereoselective benzylic hydroxylation of (7) gives (6). Cleavage of the epoxide (21) with sodium acetate in acetic acid affords a mixture of the esters (22)-(24), while methanolysis yields the isomeric ethers (29) and (30). Hydrogenolysis of (22), (23) and (29) gives high yields of (7). Potentially more direct routes to the alcohol
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8

Perich, JW, RM Valerio, PF Alewood, and RB Johns. "Synthesis of Casein Related Peptides and Phosphopeptides. XIV. Solid Phase Synthesis of Glu-Ser(P)-Leu Through the Use of Protected Boc-Ser(PO3R2)-OH Derivatives." Australian Journal of Chemistry 44, no. 6 (1991): 771. http://dx.doi.org/10.1071/ch9910771.

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A solid phase method is described for the synthesis of O- phosphoseryl-containing peptides by the use of polystyrene resin (Merrifield) as the peptide support and protected Boc-Ser(PO3R2)-OH derivatives for the incorporation of the phosphorylated seryl residue. The viability of this solid phase approach was demonstrated by the synthesis of HBr.H-Glu-Ser (PO3Et2)-Leu-OH in high yield by the use of Bo -Ser(PO3Et2)-OH in peptide synthesis and subsequent use of HBr/CF3CO2H for cleavage of the Ser(PO3Et2)-containing tripeptide from the resin support. Similarly, the dipeptide, CF3CO2H.H-Ser(P)- Leu
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9

Kadyrov, Renat. "Hydrogenolysis of Amide Acetals and Iminium Esters." ChemCatChem 10, no. 1 (2017): 170–72. http://dx.doi.org/10.1002/cctc.201701287.

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10

Rajagopal, S., and A. F. Spatola. "Palladium-catalyzed transfer hydrogenolysis of benzyl acetate with ammonium formate." Applied Catalysis A: General 152, no. 1 (1997): 69–81. http://dx.doi.org/10.1016/s0926-860x(96)00342-0.

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