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Journal articles on the topic 'Hydrothermal syntheses'

Author: Grafiati

Published: 4 June 2025

Last updated: 1 August 2025

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1

Benedek, Peter, Nils Wenzler, Maksym Yarema, and Vanessa C. Wood. "Low temperature hydrothermal synthesis of battery grade lithium iron phosphate." RSC Advances 7, no. 29 (2017): 17763–67. http://dx.doi.org/10.1039/c7ra00463j.

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Battery-grade LiFePO<sub>4</sub> is prepared via low-temperature hydrothermal synthesis. Optimizing the precursor concentration and the reaction time saves more than 30% energy compared to earlier hydrothermal syntheses of LiFePO<sub>4</sub> nanoparticles.

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2

Köferstein, Roberto. "Investigations on Bi25FeO40 powders synthesized by hydrothermal and combustion-like processes." Journal of Solid State Chemistry 217 (May 9, 2014): 50–56. https://doi.org/10.1016/j.jssc.2014.05.006.

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The syntheses of phase−pure and stoichiometric iron sillenite (Bi25FeO40) powders by a hydrothermal (at ambient pressure) and a combustion−like process are described. Phase−pure samples were obtained in the hydrothermal reaction at 100 °C (1), whereas the combustion−like process leads to pure Bi25FeO40 after calcination at 750 °C for 2 h (2a). The activation energy of the crystallite growth process of hydrothermally synthesized Bi25FeO40 was calculated as 48(9) kJ mol−1. The peritectic point was determined as 797(1) °C. The optical band gaps of the sam

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3

Kubo, Takashi, Masayuki Hogiri, Hiroshi Kagata, and Atsushi Nakahira. "Synthesis of Nano-Sized Barium Titanate Powder by Rotary-Hydrothermal Process." Key Engineering Materials 421-422 (December 2009): 269–72. http://dx.doi.org/10.4028/www.scientific.net/kem.421-422.269.

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Nano-sized BaTiO3 powders with narrow size distribution and the high tetragonality were attempted to synthesize by the rotary-hydrothermal process in water system, using two kinds of commercial anatase-type TiO2 (ST21/ST01) with different particle size and Ba(OH)2. The rotary-hydrothermal syntheses were done with the rotary-speed of 20 revolutions per minute at 523 K for 24 h. Highly- and mono-dispersed BaTiO3 powders were successfully synthesized by applying the rotary-hydrothermal process. For rotary-hydrothermal synthesis, it was found that the average size, tetragonality, and quality of th

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4

Christé, Esteves da Silva, and Pinto da Silva. "Evaluation of the Environmental Impact and Efficiency of N-Doping Strategies in the Synthesis of Carbon Dots." Materials 13, no. 3 (2020): 504. http://dx.doi.org/10.3390/ma13030504.

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The efficiency and associated environmental impacts of different N-doping strategies of carbon dots (CDs) were evaluated. More specifically, N-doped CDs were prepared from citric acid via two main synthesis routes: Microwave-assisted hydrothermal treatment with addition of N-containing small organic molecules (urea and ethylenediamine (EDA)); and microwave-assisted solvothermal treatment in N-containing organic solvents (n,n-dimethylformamide (DMF), acetonitrile and pyridine). These syntheses produced CDs with similar blue emission. However, XPS analysis revealed that CDs synthesized via both

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5

Regny, Sylvain, Yan Suffren, Olivier Leynaud, Isabelle Gautier-Luneau та Géraldine Dantelle. "Evidence of reaction intermediates in microwave-assisted synthesis of SHG active α-La(IO3)3 nanocrystals". CrystEngComm 22, № 14 (2020): 2517–25. http://dx.doi.org/10.1039/d0ce00156b.

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6

Mackinnon, Ian D. R., Graeme J. Millar, and Wanda Stolz. "Hydrothermal syntheses of zeolite N from kaolin." Applied Clay Science 58 (April 2012): 1–7. http://dx.doi.org/10.1016/j.clay.2012.02.008.

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7

Che, Guangbo, Wenlian Li, Zhiguo Kong, et al. "Hydrothermal Syntheses of Some Derivatives of Tetraazatriphenylene." Synthetic Communications 36, no. 17 (2006): 2519–24. http://dx.doi.org/10.1080/00397910600781323.

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8

Steunou, N., L. Bouhedja, S. Castro-Garcia, and J. Livage. "Chemically controlled hydrothermal syntheses of vanadium oxides." High Pressure Research 20, no. 1-6 (2001): 55–62. http://dx.doi.org/10.1080/08957950108206152.

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9

Auwal, Ismail Alhassan, Fitri Khoerunnisa, Florent Dubray, et al. "Effects of Synthesis Parameters on the Crystallization Profile and Morphological Properties of SAPO-5 Templated by 1-Benzyl-2,3-Dimethylimidazolium Hydroxide." Crystals 11, no. 3 (2021): 279. http://dx.doi.org/10.3390/cryst11030279.

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The formation of SAPO-5 molecular sieves is studied under hydrothermal conditions in the presence of a new templating agent, 1-benzyl-2,3-dimethylimidazolium hydroxide ([bzmIm]OH). The syntheses were carried out by varying the synthesis parameters, viz. crystallization temperature, heating time and reactants molar composition (SiO2, Al2O3, P2O5, [bzmIm]+, H2O) in order to investigate the role of each synthesis parameter on the formation of SAPO-5. The results showed that these synthesis parameters had significant influences on the entire crystallization process (induction, nucleation, crystal

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10

KILIÇ DOKAN, Fatma. "Investigation of the Effect of Different Synthesis Methods on the Photocatalytic Activity of TiO2: Comparison of Rutile and Anatase TiO2." Cumhuriyet Science Journal 43, no. 3 (2022): 409–15. http://dx.doi.org/10.17776/csj.1107688.

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In this study, the effect of the synthesis method (solid state, sol-gel and hydrothermal) on the photocatalytic activity of the anatase and rutile phases of TiO2 was evaluated. As a result of XRD, FESEM and BET analysis of pure phase TiO2 powders in anatase and rutile phases, the changes in particle structures, surface areas and morphologies were examined and the differences in both synthesis method and phase structures were evaluated with Photodegradation experiments. The results of the X-ray diffraction (XRD) analysis showed that the TiO2 compound synthesized in the anatase phase and by the

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11

Caramazana-González, P., P. W. Dunne, M. Gimeno-Fabra, et al. "Assessing the life cycle environmental impacts of titania nanoparticle production by continuous flow solvo/hydrothermal syntheses." Green Chemistry 19, no. 6 (2017): 1536–47. http://dx.doi.org/10.1039/c6gc03357a.

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12

Long, G., David Matatov, Acher Suissa, et al. "Hydrothermal Synthesis and Characterization of Mn-Doped VO2 Nanowires." MRS Advances 4, no. 14 (2019): 829–36. http://dx.doi.org/10.1557/adv.2019.60.

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AbstractMonoclinic VO2 is a known polymorph of vanadium dioxide that has received much attention due to its oxidative capabilities, geometric configuration, and promising applications in functional windows. VO2 can usually be obtained through a hydrothermal method under high pressure. In this work we report a synthesis of VO2 doped with Manganese using a rapid single-step hydrothermal process with V2O5, manganese (II) acetate and citric acid as precursors. Different syntheses were carried out in which the concentration of V2O5 and citric acid remained constant whereas the concentration of mang

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13

Komarneni, Sridhar, Young Dong Noh, Joo Young Kim, Seok Han Kim, and Hiroaki Katsuki. "Solvothermal/ Hydrothermal Synthesis of Metal Oxides and Metal Powders with and without Microwaves." Zeitschrift für Naturforschung B 65, no. 8 (2010): 1033–37. http://dx.doi.org/10.1515/znb-2010-0809.

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Anatase and Ca, Sr and Ca0.5Sr0.5 hydroxyapatites were synthesized by conventional-hydrothermal (C-H) as well asmicrowave-hydrothermal (M-H)methods.Microwave-assisted reactions led to accelerated syntheses of anatase but no such acceleration of reactions could be detected with the syntheses of hydroxyapatites because the crystallization of the latter materials occurred at very low temperature. Cu and Au metal powders were produced by using glucose, fructose or sucrose as reducing agents under C-H conditions at 160 ℃, where fructose and sucrose were found to be stronger reducing agents than glu

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14

Jagminas, Arūnas, Arnas Naujokaitis, Paulius Gaigalas, Simonas Ramanavičius, Marija Kurtinaitienė, and Romualdas Trusovas. "Substrate Impact on the Structure and Electrocatalyst Properties of Molybdenum Disulfide for HER from Water." Metals 10, no. 9 (2020): 1251. http://dx.doi.org/10.3390/met10091251.

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It is expected that utilization of molybdenum disulfide (MoS2)-based nanostructured electrocatalysts might replace the Pt-group electrodes most effectively applied for hydrogen evolution reaction from water. Therefore, in the past two decades, various approaches have been reported for fabrication of nanostructured MoS2-based catalysts, but their applications in practice are still missing due to lower activity and stability. We envisaged that the knowledge about the peculiarities of MoS2 nanoplatelets attachment to various conductive substrates by hydrothermal processing could be helpful for fa

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15

Shin, Yongsoon, Li-Qiong Wang, In-Tae Bae, Bruce W. Arey, and Gregory J. Exarhos. "Hydrothermal Syntheses of Colloidal Carbon Spheres from Cyclodextrins." Journal of Physical Chemistry C 112, no. 37 (2008): 14236–40. http://dx.doi.org/10.1021/jp801343y.

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16

Weng, Xiaole, Jingyi Zhang, Zhongbiao Wu, Yue Liu, Haiqiang Wang, and Jawwad A. Darr. "Continuous hydrothermal syntheses of highly active composite nanocatalysts." Green Chemistry 13, no. 4 (2011): 850. http://dx.doi.org/10.1039/c0gc00631a.

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17

Chang, Haibo, Mingyu Shang, Chenyang Zhang, Hongming Yuan, and Shouhua Feng. "Hydrothermal Syntheses and Structural Phase Transitions of AgNbO3." Journal of the American Ceramic Society 95, no. 11 (2012): 3673–77. http://dx.doi.org/10.1111/j.1551-2916.2012.05392.x.

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18

Yun, J., J. Lee, R. H. Song, and W. Tai. "Syntheses of La1-XSrxMnO3 Nanopowders by Hydrothermal Method." ECS Transactions 57, no. 1 (2013): 2313–19. http://dx.doi.org/10.1149/05701.2313ecst.

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19

Ling, Jie, Hongxia Zhang, Kunpeng Yuan, Dawanya Burgess, Jianjun Hu, and Ming Hu. "Hydrothermal syntheses and crystal structures of molybdenum tellurites." Journal of Solid State Chemistry 287 (July 2020): 121317. http://dx.doi.org/10.1016/j.jssc.2020.121317.

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20

Jun, Seong Yup, Kyeong Doo Ryou, Seong Soo Hong, et al. "Hydrothermal Syntheses of Nickel Nanosheets and Their Morphology." Materials Science Forum 510-511 (March 2006): 706–9. http://dx.doi.org/10.4028/www.scientific.net/msf.510-511.706.

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Nanocrystalline nickel powders were prepared by chemical reduction of nickel chloride hydrate with different surfactant at moderate temperature in a pressurized vessel. Nickel nanosheets were generated successfully through reducing the nickel ion complexes, formed by sodium tartrate, at alkaline condition by hydrazine hydrate. The nanosheets and nanowires were characterized by the means of an X-ray diffractomer (XRD), a field emission scanning electron microscopy (FESEM), an energy dispersive X-ray spectrometer (EDS) and a high sensitive magnetometer (HSM).

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21

Gao, Daojiang, Dingquan Xiao, Jian Bi, et al. "Hydrothermal Syntheses of Barium Strontium Titanate Thin Films." MATERIALS TRANSACTIONS 44, no. 7 (2003): 1320–23. http://dx.doi.org/10.2320/matertrans.44.1320.

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22

Singh, Manish Kumar, Prajwal Chettri, Ajay Tripathi, Archana Tiwari, Bratindranath Mukherjee, and R. K. Mandal. "Defect mediated magnetic transitions in Fe and Mn doped MoS2." Physical Chemistry Chemical Physics 20, no. 23 (2018): 15817–23. http://dx.doi.org/10.1039/c8cp02882f.

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23

Czarna-Juszkiewicz, Dorota, Piotr Kunecki, Rafał Panek, Jarosław Madej, and Magdalena Wdowin. "Impact of Fly Ash Fractionation on the Zeolitization Process." Materials 13, no. 5 (2020): 1035. http://dx.doi.org/10.3390/ma13051035.

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Coal combustion product in the form of fly ash has been sieved and successfully utilised as a main substrate and a carrier of silicon and aluminium in a set of hydrothermal syntheses of zeolites. The final product was abundant in zeolite X phase (Faujasite framework). Raw fly ash as well as its derivatives, after being sieved (fractions: ≤ 63, 63–125, 125–180 and ≥ 180 µm), and the obtained zeolite materials were subjected to mineralogical characterisation using powder X-ray diffraction, energy-dispersive X-ray fluorescence, laser diffraction-based particle size analysis and scanning electron

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24

Klenner, Mitchell A., Marina Cagnes, Kathleen Wood, Kazuki Mita, Mizuki Kishimoto, and Tamim Darwish. "Decagram scale production of deuterated mineral oil and polydecene as solvents for polymer studies in neutron scattering." Polymer Chemistry 11, no. 31 (2020): 4986–94. http://dx.doi.org/10.1039/d0py00690d.

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25

Drofenik, Miha, Darja Lisjak, and Darko Makovec. "The Synthesis and Properties of Magnetic Nanoparticles." Materials Science Forum 494 (September 2005): 129–36. http://dx.doi.org/10.4028/www.scientific.net/msf.494.129.

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Magnetic nanoparticles are materials of great interest because of the remarkable fundamental properties exhibited by these materials as well as their technological potential in the area of biomedicine and other areas. The technologically useful properties of magnetic nanomaterials are not limited to their structural, chemical or mechanical behaviour, but also involve the phenomena that arise from their finite size and the surface effects that dominate the magnetic behaviour of individual nanoparticles. New techniques that have been developed recently have permitted researchers to produce large

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26

Takezoe, S., Kazuyuki Hosoi, Masahiko Tajika, Yuki Yamasaki, and Atsushi Nakahira. "Syntheses of Bulky Y-Zeolite by Hydrothermal Hot-Pressing (HHP) Technique." Key Engineering Materials 317-318 (August 2006): 97–100. http://dx.doi.org/10.4028/www.scientific.net/kem.317-318.97.

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Synthesis of bulky Y-zeolite was attempted by a hydrothermal hot-pressing (HHP) method. These bulky products synthesized under hydrothermal conditions were identified as Y-zeolite single phase. Especially, bulky Y-zeolite having translucency, high density and large surface area was obtained by HHP treatment at 423K for 2h with 17wt% of 5M-NaOH solution. This solidified zeolite like single-crystal was considered to be made by dissolution and precipitation mechanism. High-density bulky zeolites can be expected as novel molecular sieves and catalysts with high activity.

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27

Zhang, Lichun, Liping Kang, Hao Lv, Zhikui Su, Kenta Ooi, and Zong-Huai Liu. "Controllable synthesis, characterization, and electrochemical properties of manganese oxide nanoarchitectures." Journal of Materials Research 23, no. 3 (2008): 780–89. http://dx.doi.org/10.1557/jmr.2008.0091.

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Flowerlike manganese oxide microspheres and cryptomelane-type manganese oxide nanobelts were selectively synthesized by a simple decomposition of KMnO4 under mild hydrothermal conditions without using template or cross-linking reagents. The effect of varying the hydrothermal times and temperatures on the nanostructure, morphology, compositional, and electrochemical properties of the obtained manganese oxides was investigated. X-ray diffraction (XRD), scanning electron microscopy (SEM), and transmission electron microscopy (TEM) studies showed that the flowerlike manganese oxide microspheres co

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28

Lebedev, V. A., A. I. Gavrilov, A. S. Shaporev, V. K. Ivanov, B. R. Churagulov, and Yu D. Tret’yakov. "Hydrothermal and hydrothermal-microwave syntheses of oriented nanorods of zinc oxide on an ITO substrate." Doklady Chemistry 444, no. 1 (2012): 117–19. http://dx.doi.org/10.1134/s0012500812050011.

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29

Yao, Wei Tang, and Shu Hong Yu. "Recent advances in hydrothermal syntheses of low dimensional nanoarchitectures." International Journal of Nanotechnology 4, no. 1/2 (2007): 129. http://dx.doi.org/10.1504/ijnt.2007.012320.

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30

WEITKAMP, J., R. SCHUMACHER, and U. WEISS. "ChemInform Abstract: Hydrothermal Syntheses and Characterization of EMT Zeolite." ChemInform 24, no. 21 (2010): no. http://dx.doi.org/10.1002/chin.199321259.

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31

Sousa, Paulla B. F., Lindiane Bieseki, and Sibele B. C. Pergher. "Seed-Assisted Crystallization in the Hydrothermal Synthesis of FAU Zeolite from Acid-Treated Residue Glass Powder." Materials 18, no. 7 (2025): 1393. https://doi.org/10.3390/ma18071393.

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A simple and low-cost synthesis assisted by seed crystals has been proposed to convert residual colorless glass powder into a Na-X zeolite. For this purpose, the optimal parameters for acid leaching of glass powder were studied to remove impurities that could interfere with the crystallization process. Then, the hydrothermal syntheses were supported by Na-X seed crystals (0% to 5%, wt.) to induce the growth of zeolite X, evaluating the crystallization time (12 h to 48 h) and the variation of the silicon source (acid-treated and untreated residues). The formation of the faujasite as the main ph

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32

Cockell, Charles S. "The origin and emergence of life under impact bombardment." Philosophical Transactions of the Royal Society B: Biological Sciences 361, no. 1474 (2006): 1845–56. http://dx.doi.org/10.1098/rstb.2006.1908.

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Craters formed by asteroids and comets offer a number of possibilities as sites for prebiotic chemistry, and they invite a literal application of Darwin's ‘warm little pond’. Some of these attributes, such as prolonged circulation of heated water, are found in deep-ocean hydrothermal vent systems, previously proposed as sites for prebiotic chemistry. However, impact craters host important characteristics in a single location, which include the formation of diverse metal sulphides, clays and zeolites as secondary hydrothermal minerals (which can act as templates or catalysts for prebiotic synth

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33

Rouchalová, Kamila, Dana Rouchalová, Vladimír Čablík, and Dalibor Matýsek. "Microwave-Assisted Hydrothermal Synthesis of Pure-Phase Sodalite (>99 wt.%) in Suspension: Methodology Design and Verification." Materials 17, no. 1 (2024): 269. http://dx.doi.org/10.3390/ma17010269.

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Despite numerous studies focused on the hydrothermal (HT) synthesis of fly ash zeolites (FAZs), this method still has many limitations, the main of which is the low yield of zeolites. Hydrothermally synthesized zeolites are typically multiphase and exhibit low purity, which limits their applicability. Pure-phase zeolites have been primarily prepared from filtrates after alkaline mineralization of fly ashes, not directly in suspension. In addition, the published methodologies have not been tested in a wider set of samples, and thus their reproducibility is not confirmed. The aim of the study is

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34

Bøjesen, Espen, Kirsten Jensen, Christoffer Tyrsted, Nina Lock, Mogens Christensen, and Bo Iversen. "In- and ex situ PXRD studies of ZnO nanoparticle growth in sub-critical water." Acta Crystallographica Section A Foundations and Advances 70, a1 (2014): C1413. http://dx.doi.org/10.1107/s2053273314085866.

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Zinc oxide (ZnO) is a material of great scientific and industrial relevance and is used widely in a variety of applications. Synthesis of ZnO nanoparticles can be performed by a wide range of methods resulting in a tremendous variety of sizes and shapes. Different in situ characterization methods have been used to investigate the ZnO formation under various synthesis conditions; these include numerous spectroscopic methods and small angle scattering. Common for these studies is that the primary focus has been to extract information on particle size and shape of ZnO, while a more rigorous micro

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35

Fernández-Sánchez, Lilia, and Mirella Gutiérrez-Arzaluz. "Synthesis of copper hydroxyphosphate under the principles of green chemistry." Applied Chemical Engineering 5, no. 2 (2022): 20. http://dx.doi.org/10.24294/ace.v5i2.1637.

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This work aims to present two syntheses according to the green chemistry principles of Cu2(OH)PO4. The first one is a mechanochemical synthesis which was carried out with Cu3(PO4)2 and NaOH at room temperature and without solvent (principles five and six), the second one employed an aqueous suspension of copper phosphate (principle six). The products were characterized by X-ray diffraction, scanning electron microscopy, infrared spectroscopy and elemental analysis. Using an analysis and evaluation scale based on green principles, the synthesis method reported in this study was compared with th

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36

Chakravarty, Disha, and Dattatray J. Late. "Microwave and hydrothermal syntheses of WSe2 micro/nanorods and their application in supercapacitors." RSC Advances 5, no. 28 (2015): 21700–21709. http://dx.doi.org/10.1039/c4ra12599a.

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37

Budrevičius, Darius, Eglė Buzaitytė, Kęstutis Mažeika, and Ramūnas Skaudžius. "Influence of Synthesis Conditions on the Monoclinic Structure Formation of Gd0.85−yLayPO4:15%Eu and Luminescent Properties." Crystals 15, no. 5 (2025): 441. https://doi.org/10.3390/cryst15050441.

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In this study, nanoparticles with a monoclinic crystal structure of Gd0.85−yLayPO4:15%Eu were synthesized through a hydrothermal method. Initial investigations focused on the influence of the precursor on the resulting structure of LaPO4:1%Eu, with variations in synthesis temperature. Various syntheses were conducted using ammonium dihydrogen phosphate (NH4H2PO4) and diammonium hydrogen phosphate ((NH4)2HPO4) as PO43− ion precursors, and the synthesis temperature ranged from room temperature to 200 °C. Based on the synthesis and analysis outcomes, diammonium hydrogen phosphate was selected as

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38

Chu, Suya, Weixia Zhou, Chenyang Zhang, Yi Zheng, Yang Liu, and Yongjun Liu. "Relationship between the structure and catalytic performance of MoS2 with different surfactant-assisted syntheses in the hydrodesulfurization reaction of 4,6-DMDBT." RSC Advances 10, no. 13 (2020): 7600–7608. http://dx.doi.org/10.1039/c9ra08407j.

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Liu, Fu-Chen, Yong-Fei Zeng, Jiong-Peng Zhao, et al. "Novel lanthanide–azido complexes: hydrothermal syntheses, structures and magnetic properties." Dalton Transactions, no. 12 (2009): 2074. http://dx.doi.org/10.1039/b819955h.

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40

Tränkle, Sebastian, Denis Jahn, Thomas Neumann, Luc Nicoleau, Nicola Hüsing, and Dirk Volkmer. "Conventional and microwave assisted hydrothermal syntheses of 11 Å tobermorite." Journal of Materials Chemistry A 1, no. 35 (2013): 10318. http://dx.doi.org/10.1039/c3ta11036b.

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41

Talley, Catherine E., Amanda C. Bean, and Thomas E. Albrecht-Schmitt. "Hydrothermal Syntheses of Layered Uranium Oxyfluorides: Illustrations of Dimensional Reduction." Inorganic Chemistry 39, no. 23 (2000): 5174–75. http://dx.doi.org/10.1021/ic000668e.

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42

Parker, T. Gannon, Justin N. Cross, Matthew J. Polinski, Jian Lin, and Thomas E. Albrecht-Schmitt. "Ionothermal and Hydrothermal Flux Syntheses of Five New Uranyl Phosphonates." Crystal Growth & Design 14, no. 1 (2013): 228–35. http://dx.doi.org/10.1021/cg401435w.

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43

Chen, Lijuan, Yanhua Fan, Junwei Zhao, et al. "Hydrothermal syntheses and structural characterization of two sandwich-type arsenotungstates." Journal of Coordination Chemistry 63, no. 12 (2010): 2042–55. http://dx.doi.org/10.1080/00958972.2010.496484.

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44

Lu, Jing, De-Qing Chu, Jie-Hui Yu, et al. "In situ ligands syntheses involving malic acid in hydrothermal condition." Inorganica Chimica Acta 359, no. 8 (2006): 2495–500. http://dx.doi.org/10.1016/j.ica.2006.02.043.

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45

Zhang, Zhibin, Jiuyu Guo, Jie Fu, et al. "Hydrothermal Syntheses and Crystal Structures of Two New Vanadium Phosphates." Journal of Cluster Science 23, no. 2 (2011): 177–87. http://dx.doi.org/10.1007/s10876-011-0385-3.

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46

Zhang, Chi, Jinming Liu, Min Ji, and Yonglin An. "Hydrothermal syntheses and characterization of two tetramethylammonium templated indium sulfides." Inorganic Chemistry Communications 44 (June 2014): 169–72. http://dx.doi.org/10.1016/j.inoche.2014.03.028.

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47

Liu, Yue, Yang Li, Ying Liu, et al. "Structure Information of Barium Hexaferrite and Strategies for its Syntheses." Applied Mechanics and Materials 69 (July 2011): 6–11. http://dx.doi.org/10.4028/www.scientific.net/amm.69.6.

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Structure information of barium hexaferrite is very important in designing higher efficient synthetic methods and in tailoring the magnetic properties of barium hexaferrite by doping. The structure information of M-type barium hexaferrite has helped to find new efficient routes of hydrothermal and co-precipitation methods in synthesizing barium hexaferrites and in altering their magnetic properties by doping.

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48

Klapiszewska, Izabela, Adam Kubiak, Anna Parus, Marcin Janczarek, and Agnieszka Ślosarczyk. "The In Situ Hydrothermal and Microwave Syntheses of Zinc Oxides for Functional Cement Composites." Materials 15, no. 3 (2022): 1069. http://dx.doi.org/10.3390/ma15031069.

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This study presents the results of research on cement mortars amended with two zinc oxides obtained by two different methods: hydrothermal ZnO-H and microwave ZnO-M. Our work indicates that, in contrast to spherical ZnO-H, ZnO-M was characterized by a columnar particle habit with a BET surface area of 8 m2/g, which was four times higher than that obtained for hydrothermally obtained zinc oxide. In addition, ZnO-M induced much better antimicrobial resistance, which was also reported in cement mortar with this oxide. Both zinc oxides showed very good photocatalytic properties, as demonstrated by

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Niu, Ben, Xin Wang, Kai Wu, Xianru He, and Rui Zhang. "Mesoporous Titanium Dioxide: Synthesis and Applications in Photocatalysis, Energy and Biology." Materials 11, no. 10 (2018): 1910. http://dx.doi.org/10.3390/ma11101910.

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Abstract:

Mesoporous materials are materials with high surface area and intrinsic porosity, and therefore have attracted great research interest due to these unique structures. Mesoporous titanium dioxide (TiO2) is one of the most widely studied mesoporous materials given its special characters and enormous applications. In this article, we highlight the significant work on mesoporous TiO2 including syntheses and applications, particularly in the field of photocatalysis, energy and biology. Different synthesis methods of mesoporous TiO2—including sol–gel, hydrothermal, solvothermal method, and other tem

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Ying, Yongling, Rongbo Zheng, Yongjun Zheng, Hongyan Wang, Junfeng Niu, and Housheng Xia. "Synthesis and Reduction Processes of Silver Nanowires in a Silver(I) Sulfamate–Poly (Vinylpyrrolidone) Hydrothermal System." Molecules 29, no. 7 (2024): 1558. http://dx.doi.org/10.3390/molecules29071558.

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Abstract:

Silver (Ag) nanowires, as an important one-dimensional (1D) nanomaterial, have garnered wide attention, owing to their applications in electronics, optoelectronics, sensors, and other fields. In this study, an alternative hydrothermal route was developed to synthesize Ag nanowires via modified reduction of Ag+. Silver sulfamate plays an important role in the formation of Ag nanowires via controlled release of free Ag+. Results of controlled experiments and characterizations such as UV–vis spectroscopy, FTIR, XPS, and 1H NMR revealed that sulfamic acid does not function as a reductant, supporti

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