Relevant bibliographies by topics / II.> 5

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  2. Dissertations / Theses
  3. Books
  4. Book chapters
  5. Conference papers
  6. Reports

Academic literature on the topic 'II.> 5'

Author: Grafiati
Published: 4 June 2021
Last updated: 7 February 2022

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Journal articles on the topic "II.> 5"

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NAKAMURA, YOHEI. "II-5. Coral reefs." NIPPON SUISAN GAKKAISHI 76, no. 6 (2010): 1095. http://dx.doi.org/10.2331/suisan.76.1095.

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Poirier, Paul-Hubert. "Traité 25 (II,5)." Studies in Religion/Sciences Religieuses 29, no. 1 (March 2000): 122. http://dx.doi.org/10.1177/000842980002900127.

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Burnyeat, M. F. "DE ANIMA II 5." Phronesis 47, no. 1 (2002): 28–90. http://dx.doi.org/10.1163/156852802760075693.

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AbstractThis is a close scrutiny of De Anima II 5, led by two questions. First, what can be learned from so long and intricate a discussion about the neglected problem of how to read an Aristotelian chapter? Second, what can the chapter, properly read, teach us about some widely debated issues in Aristotle's theory of perception? I argue that it refutes two claims defended by Martha Nussbaum, Hilary Putnam, and Richard Sorabji: (i) that when Aristotle speaks of the perceiver becoming like the object perceived, the assimilation he has in mind is ordinary alteration of the type exemplified when fire heats the surrounding air, (ii) that this alteration stands to perceptual awareness as matter to form. Claim (i) is wrong because the assimilation that perceiving is is not ordinary alteration. Claim (ii) is wrong because the special type of alteration that perceiving is is not its underlying material realisation. Indeed, there is no mention in the text of any underlying material realisation for perceiving. The positive aim of II 5 is to introduce the distinction between first and second potentiality, each with their own type of actuality. In both cases the actuality is an alteration different from ordinary alteration. Perception exemplifies one of these new types of alteration, another is found in the acquisition of knowledge and in an embryo's first acquisition of the power of perception. The introduction of suitably refined meanings of 'alteration' allows Aristotle to explain perception and learning within the framework of his physics, which by definition is the study of things that change. He adapts his standard notion of alteration, familiar from Physics III 1-3 and De Generatione et Corruptione I, to the task of accounting for the cognitive accuracy of (proper object) perception and second potentiality knowledge: both are achievements of a natural, inborn receptivity to objective truth. Throughout the paper I pay special attention to issues of text and translation, and to Aristotle's cross-referencing, and I emphasise what the chapter does not say as well as what it does. In particular, the last section argues that the textual absence of any underlying material realisation for perceiving supports a view I have defended elsewhere, that Aristotelian perception involves no material processes, only standing material conditions. This absence is as telling as others noted earlier. Our reading must respect the spirit of the text as Aristotle wrote it.
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Corallo, J. "II.5 L’Hélicobacter Pylori." Acta Endoscopica 21, S1 (January 1991): 112–17. http://dx.doi.org/10.1007/bf02970833.

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Yang, Jun, and Hong-Ji Chen. "Poly[(μ3-5-bromonicotinato)(5-bromonicotinato)copper(II)]." Acta Crystallographica Section E Structure Reports Online 65, no. 10 (September 30, 2009): m1262—m1263. http://dx.doi.org/10.1107/s1600536809038331.

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HAGA, MIZUE. "II-5. Cookery and nutrition." NIPPON SUISAN GAKKAISHI 79, no. 1 (2013): 71. http://dx.doi.org/10.2331/suisan.79.71.

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Casellato, U., R. Ettorre, and R. Graziani. "Bis(5-bromocytosinium) tetrachloropalladate(II)." Acta Crystallographica Section C Crystal Structure Communications 49, no. 5 (May 15, 1993): 956–57. http://dx.doi.org/10.1107/s0108270192011429.

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Viossat, B., P. Khodadad, and N. Rodier. "Diamminechloro(5-oxoprolinato)platine(II)." Acta Crystallographica Section C Crystal Structure Communications 49, no. 7 (July 15, 1993): 1370–72. http://dx.doi.org/10.1107/s0108270193000046.

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Miao, Zhi-Xin, Min Shao, and Ming-Xing Li. "Bis(5-aminoisoquinoline)diazidozinc(II)." Acta Crystallographica Section E Structure Reports Online 63, no. 7 (June 6, 2007): m1808. http://dx.doi.org/10.1107/s1600536807026700.

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Rinaldi, F., G. Schneider, K. Kaljurand, S. Clematide, T. Vachon, and M. Romacker. "OntoGene in BioCreative II.5." IEEE/ACM Transactions on Computational Biology and Bioinformatics 7, no. 3 (July 2010): 472–80. http://dx.doi.org/10.1109/tcbb.2010.50.

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Dissertations / Theses on the topic "II.> 5"

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Chadghan, Arafa. "Síntesis y caracterización estructural de complejos de Co(II), Ni(II), Cu(II) y Pd(II) con ligandos pirazólicos 3, 5-disustituidos." Doctoral thesis, Universitat Autònoma de Barcelona, 1998. http://hdl.handle.net/10803/3125.

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Se han sintetizado y caracterizado mediante AE, IR, 1H, 13C-RMN y EM cuatro nuevos ligandos derivados del pirazol (3-fenil-5-(2-piridil)pirazol (HL0), 3-fenil-5-(6-metil-(2-piridil))pirazol (HL1), bis(3-fenil)-5-(2,6-piridil)dipirazol (H2L2), 3-(2,6-piridil)-bis(5-(2-piridil))dipirazol (H2L3)) y se ha estudiado la química de coordinación del sistema M:HL (M=Co(II), Ni(II), Cu(II) y Pd(II); HL=HL0, HL1) en presencia de haluros, nitratos y acetatos como ligandos adicionales.
Los complejos aislados se han caracterizado mediante AE, IR de la zona media y lejana, conductividad molar en solución, UV-Visible y siempre que ha sido posible mediante difracción de Rayos-X de monocristal.
- Se han determinado 7 estructuras cristalinas demostrando la existencia de un gran diversidad estructural. Esta diversidad se manifiesta a diferentes niveles:
Mononucleares:
- [Co(HL0)2(H2O)Cl]Cl. H2O, especie iónica con entorno de coordinación del Co(II) [CoN4OCl], octaédrico distorsionado. El ligando actúa como quelato (bidentado) y neutro.
- [Ni(HL1)2(H2O)2]Br2, especie iónica con entorno de coordinación del Ni(II) [NiN4O2], octaédrico distorsionado. El ligando actúa como quelato (bidentado) y neutro.
- [Cu(HL0)(H2O)2(NO3)] (NO3), especie iónica con entorno de coordinación del Cu(II) [CuN2O3], pirámide de base cuadrada distorsionada. El ligando actúa como quelato (bidentado) y neutro.
- [Cu(L0)2], especie neutra con entorno de coordinación del Cu(II) [CuN4] es plano cuadrado. El ligando actαa como quelato (bidentado) y aniónico.
Sal doble:
-[Ni(HL0)2(H2O)Cl][Ni(HL0)2(H2O)2]Cl3.CH3OH. H2O, en esta especie coexisten dos tipos de entornos de Ni(II): [NiN4O2] i [NiN4OCl] formando geormetrias octaédricas distorsionadas. El ligando actúa como quelato (bidentado) y neutro.
Dinucleares:
- [Cu(ClL1)(DMF)Cl]2 (ClL1 = 4-cloro-3-fenil-5-(6-metil-2-piridil)pirazol), cada Cu(II) coordina a dos ligandos, un Cl y una molécula de DMF, con entorno pentacoordinado [CuN3OCl], y geometría de pirámide de base cuadrada distorsionada. Los ligandos actúan como tridentados vía 3N (dos N pirazólico y un N piridínico) y aniónicos.
- [Pd2(L1)4], cada paladio coordina a tres ligandos: dos de ellos vía un N pirazólico y el tercero por un N pirazólico y un N piridínico. Todos los ligandos son aniónicos. Los dos Pd(II) tienen un entorno [PdN4] y geometría plano cuadrada distorsionada.
- El estudio de la conductividad molar demuestra que los haluros y nitratos pueden estar tanto dentro como fuera de la esfera de coordinación de los metales, obteniéndose una fórmula general [M(HL)nXx]Xy (n = 1, 2; X = Cl-, Br-, NO3-, OH-; x = 0, 1, 2; y = 0, 1, 2). Mientras que los acetatos se encuentran siempre coordinados al metal.
- El estudio de los espectros IR de la zona 4000 - 400 cm-1 permiten:
Saber el tipo de coordinación de los nitratos y acetatos en los diferentes complejos. Para los primeros se consigue estudiando la zona entre 2500-1600 cm-1 y para los segundos llevando a cabo el estudio entre 1615-1500 cm-1 y 1415-1380 cm-1 que es donde aparecen las vibraciones n(COO)as y n(COO)s respectivamente.
El estudio del IR en zona baja (450-100 cm-1) permite ver las bandas correspondientes a las vibraciones n(M-N), n(M-O) y n(M-X) (X=Cl-, Br-).
- El estudio de los espectros UV-Visible -NIR realizado en diferentes medios, ha permitido conocer el número de coordinación del metal en la mayoría de los complejos:
-Co(II): el Co(II) tiene coordinación 6 y geometría octaédrica en metanol y presentan un equilibrio entre la coordinación 4 y 6 en acetonitrilo.
-Todos los complejos de Ni(II) tienen coordinación 6 y geometría octaédrica distorsionada.
-Los complejos de Cu(II) son los que presentan una mayor variedad de coordinaciones 4, 5 o 6 y posibles geometrias Td, BPT, PBC o Oh.
- El estudio preliminar de voltametría cíclica con los compuestos de Cu(II) y acetatos en DMF ha puesto en evidencia una transferencia eléctrica lenta (a=0,35) de Cu(II) / Cu(I) y la alta adsorción de los compuestos de Cu(I) a la superficie del electrodo.
Four new pyrazole-derived ligands 3-phenyl-5-(2-pyridyl) pyrazole (HL0), 3-phenyl-5-(6-methyl-(2-pyridyl)) pyrazole (HL1), bis (3-phenyl)-5-(2,6-pyridyl) dipyrazole (H2L2) and 3-(2,6-pyridyl)-bis (5-(2-pyridyl)) dipyrazole (H2L3)) have been synthesized and characterized by means of elemental analyses (EA), infrared espectra (IR), 1H and 13C-NMR spectroscopies and mass spectra (ME). The coordination chemistry of the system metal salt with the corresponding pyrazole ligands M:HL (M=Co(II), Ni(II), Cu(II) and Pd(II); HL=HL0, HL1) in presence of halides, nitrates and acetates like additional ligands has been also studied.
The isolated complexes have been characterized by means of EA, IR, conductivity measurements, UV-Vis electronic spectroscopy and with monocrystal X-Ray diffraction when it has been posible.
- Seven crystalline structures have determinated, which demonstrat the existence of a great structural diversity. Such diversity is manifested at different levels:
Mononuclear:
- [Co(HL0)2(H2O)Cl]Cl.H2O, ionique structure with the environment coordination of Co(II) [CoN4OCl], distorted octaedral geometry. The ligands acts as chelate (bidentate) and neutral.
-[Ni(HL1)2(H2O)2]Br2, ionique structure with the environment coordination of Ni(II) [NiN4O2], distorted octaedral geometry. The ligands acts as chelate (bidentate) and neutral.
- [Cu(HL0)(H2O)2(NO3)](NO3), ionique structure with the environment coordination of Cu(II) [CuN2O3], distorted tetragonal piramid geometry. The ligand acts as chelate (bidentate) and neutral.
- [Cu(L0)2], neutral structure with the environment coordination of Cu(II) [CuN4] is a square planar. The ligand acts as chelate (bidentate) and anionic.

Double salt:
- [Ni(HL0)2(H2O)Cl][Ni(HL0)2(H2O)2]Cl3.CH3OH.H2O, in this structure coexist two different forms of mononuclear Ni(II): [NiN4O2] and [NiN4OCl]: forming distorted octahedral geometries. The ligands acts as chelate (bidentate) and neutral.
Dinuclear:
- [Cu(ClL1)(DMF)Cl]2 (ClL1 = 4-chloro-3-phenyl-5-(6-methyl-2-pyridyl)pyrazole), every Cu(II) coordinates two ligands, a Cl and a DMFÕs molecule, forming pentacoordinated spheres [CuN3OCl] with distorted square pyramid geometry. The ligands are tridented via 3N (two pyrazole nitrogen and one pyridine nitrogen) and anionics.
- [Pd2(L1)4], every palladium coordinates three ligands: two of them via pyrazolic N and the third ligand via pyrazolic N and pyridinic N. All ligands are anionics. The two Pd(II) have an environmental [PdN4] and a distorted square-planar geometry.
- The study of conductivity measurements demonstrate that the halides and nitrates can be so much inside like out of the coordination sphere of the metals, being obtained a general complexes formula [M(HL)nXx]Xy (n=1, 2; X=Cl-, Br-, NO3-, OH-; x=0, 1, 2; y=0, 1, 2). Whereas the acetates are coordinated always to the metal.
- The study of IR spectroscopies of the zone among 4000 and 400 cm-1 allows:
To differentiate the type of coordination of the nitrates and acetates in the different complexes. For the first ones it is obtained studying the zone among 2500-1600 cm-1 and for the second ones carrying out the study among 1615-1500 cm-1 and 1415-1380 cm-1 where n(COO)as y n(COO)s vibrations appear respectively.
The study of IR in lower zone 450-100 cm-1 allows to see the bands corresponding to the vibrations n(M-N), n(M-O) y n(M-X) (X=Cl-, Br-).
- The study of UV-Vis-NIR spectroscopies fulfilled by different media allowed to know the number of metal coordination in the majority of the complexes:
-In Co(II): the Co(II) has coordination 6 and octahedral geometry in methanol, and present a balance between the coordination 4 and 6 in acetonitril.
- All the Ni(II) complexes have coordination 6 and distorted octahedral geometry.
- Cu(II) complexes are those which present a major variety of coordinations 4, 5 or 6 and possible Td, BPT, PBC or Oh geometries.
- The prilimenar study of cyclic voltametry with Cu(II) compounds and acetates in DMF has reveled a slow electrical transference (a=0,35) of Cu(II) / Cu(I) and the discharge adsortion of Cu(I)'s compounds to the electrode surface.
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Osuagwu, Tochukwu. "An ideological-critical interpretation of justice and righteousness in Amos 5." Diss., University of Pretoria, 2016. http://hdl.handle.net/2263/63000.

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This dissertation attempts to critically analyse the effect of ideology on the text of Amos 5 and how this impacts on hermeneutics. It begins with a look at the historical-political-sociological situations of Amos’ time. It also looks at ideology and the text and the effect of ideology both on the writer and the interpreter. Chapter 3 and 4 are exegetical and rhetorical readings of the texts of Amos 5. Chapter 4 focuses on the concept of justice and righteousness in Amos 5 and also in the entire book of Amos. Lastly, Chapter 5 looks at the concept of justice and righteousness and its contemporary relevance. In course of the study, it was discovered that time and experience play an important role in the Bible experience. Further, it was discovered that both the writer and the interpreter are considerably under the influence of ideology. None is exempt from it. This study therefore is about the struggles that a modern interpreter encounter in course of doing biblical interpretation and application. Since the texts is an ancient and was written at a time different from now. It implies therefore that contemporary interpreter has to interpret the text honestly in other for biblical message to be relevant to the present.
Dissertation (MA)--University of Pretoria, 2016.
Old Testament Studies
MA
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Marvin, Brock C. "QUANTUM MIXING IN 5-COORDINATE HS COBALT (II) EPR SPECTRA." Miami University / OhioLINK, 2014. http://rave.ohiolink.edu/etdc/view?acc_num=miami1417431017.

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Marasinghe, Gishanthi P. K. "OVER-EXPRESSION AND CHARACTERIZATION OF A MITOCHONDRIAL GLYOXALASE II FROM ARABIDOPSIS THALIANA." Miami University / OhioLINK, 2004. http://rave.ohiolink.edu/etdc/view?acc_num=miami1096574528.

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Ishizuka, Marise Akemi. "Tradução para o português e validação do teste POMA II \"Performance-Oriented Mobility Assessment II." Universidade de São Paulo, 2008. http://www.teses.usp.br/teses/disponiveis/5/5144/tde-12012009-142854/.

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As quedas em idosos são eventos multifatoriais que representam grande importância para os gerontólogos, já que aparecem com grande morbidade e mortalidade nesta faixa etária. Esta pesquisa tem como objetivo principal realizar a tradução, adaptação transcultural para o português brasileiro e a validação do POMA II (Performance-Oriented Mobility Assessment II). Têm como objetivos secundários avaliar sua confiabilidade; seu grau de associação entre o POMA II e outros testes funcionais similares, bem como sua sensibilidade, especificidade e sua validade preditiva. Num primeiro momento o teste POMA II foi traduzido para o português e então novamente traduzido para o inglês. Uma nova versão em português foi então avaliada por uma comissão de profissionais da área e por um professor de lingüística para a adaptação cultural. Essa versão foi aplicada por 15 profissionais para a verificação de aplicabilidade e compreensão do teste. O mesmo foi usado em grupo de 20 idosos para a verificação do grau de compreensão de cada item. A versão final foi avaliada em relação a sua validade e fidedignidade através da aplicação do mesmo em idosos residentes de uma Instituição de Longa Permanência para Idosos (ILPI) e idosos do Grupo de Atendimento Multifatorial ao Idoso Ambulatorial (GAMIA). O POMA II apresentou uma boa correlação intra e inter-observador (ICC entre 0,702 a 0,972 com exceção do domínio marcha do grupo GAMIA= 0,510) assim como uma boa correlação com testes funcionais similares (r entre 0,500 e 0,920 todos com p<0,001), além de consistência interna expressiva ( de Cronbach de 0,890 e 0,832). O teste apresentou uma correlação fraca (r= -0,282) com as quedas sofridas durante o ano, mas esta correlação é significativa (p= 0,033). O teste mostrou uma boa validade divergente (p< 0,001), onde descriminou os dois grupos que são significamente distintos. A sua sensibilidade foi de 61% e sua especificidade de 66%. Concluímos que o POMA II é um teste confiável com boas correlações intra e inter-observadores, consistente em termos de medir o mesmo fenômeno e com boa validade concorrente. Porém a validade preditiva, a especificidade e a sensibilidade do teste mostraram dados menos significativos, apresentando correlações moderadas
Falls in elderly people are multi factorial events that represent great importance for gerontologists, since they appear with high morbidity and death rates in this age range.This research has the main purpose of performing the trans-cultural translation, validation and adaptation of POMA II (Performance-Oriented Mobility Assessment II) to Brazilian Portuguese and, as secondary purposes, to assess its reproducibility and association between this and other similar functional tests; to calculate its sensitivity and specificity and its predicitive validity.At first, the POMA II test was brought to Portuguese and translated again into English. After the adequacies between the translators, a new Portuguese version was elaborated. The new version was assessed by an experts Committee comprised of doctors with knowledge in the area and by a linguistics professor for cultural adaptations. This version was applied by 15 professionals from the healthcare industry to verify the test applicability and comprehension and in a group of 20 elderly people to verify the level of comprehension of each item. The ultimate version, after the inclusion of a few suggestions, was assessed regarding its validity and its fidelity through its application in elderly individuals residing in a long permanence elderly residence and community elderly individuals (GAMIA- Grupo de Atendimento Multidisciplinar ao Idoso Ambulatorial). POMA II has presented a good intra and inter-rater correlation (r between 0.702 to 0.972, except for gait domain of the GAMIA= 0.510 group) as well as a good correlation with similar functional tests (between 0.500 and 0.920 all with p<0.001), in addition to significant internal consistency (Cronbach of 0.890 and 0.832). The test presented a significant correlation with the related years falls (p= 0.033) but this correlation was poor (r= -0.282). The test showed a good divergent validity (p< 0.001), which showed that the two groups were different. The sensivity was 61% and the specificity was 66%. We have concluded that POMA II is a reliable test with good intra and inter rater correlations, consistent to measure the same phenomenon and with good concurrent validity. However, the predictive validity, specificity and sensitivity of the test showed moderate correlations
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Vincent, Sabrina, and Fredric Olsson. "Solvens II : En konkurrensfördel för de svenska försäkringsbolagen?" Thesis, Södertörns högskola, Institutionen för ekonomi och företagande, 2011. http://urn.kb.se/resolve?urn=urn:nbn:se:sh:diva-9107.

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The purpose of this essay is to investigate whether the implementation of the Solvency II directive will create a competitive advantage for the Swedish insurance companies compared with other insurance companies in Europe. Therefore the theoretical perspective illustrates the specific requirements and risk culture of the insurance industry and defines the critical success factors for a successful implementation of the directive. The empirical foundation is built on the QIS 5 reports for Sweden and Europe, interviews with the financial services and If insurance company as well as information from a seminar organized by KPMG. The analysis shows that the Swedish insurance companies meets the capital requirements of Solvency II by a large margin and that they are accustomed to risk management and reporting requirements from the traffic light model. This implies that the three critical success factors for a successful implementation of Solvency II are met, although with some limitations, and that Swedish insurance companies could possibly have a competitive advantage.
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Захарченко, Борис Володимирович. "Координаційні сполуки паладію (II) з 5-заміщеними-3-(2-піридил)-1,2,4-триазолами." Diss. of Candidate of Chemical Sciences, Київ. нац. ун-т ім. Тараса Шевченка, М-во освіти і науки України, 2019.

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Fowler, Leslie Ann. "PCB Effects on Brain Type II 5'Deiodinase Activity in Developing Brids." Thesis, Virginia Tech, 2000. http://hdl.handle.net/10919/9768.

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PCBs are known to cause thyroid disruption in laboratory rats and are thought to be the causal agent in thyroid gland alterations in herring gulls in the Great Lakes. This study examined the regulation of thyroid hormone supply during development in (1) domestic chicken embryos (Gallus domesticus) exposed to a specific dioxin-like PCB congener (PCB-126) and (2) herring gull (Larus argentatus) embryos and pre-fledglings from Great Lakes sites with different chemical pollutant exposures. Specifically, PCB effects on thyroid status were evaluated by measuring plasma thyroid hormone concentrations and brain type II 5'D activity (to determine if PCB exposure was associated with alteration in brain 5'D type II activity that could maintain local T3 supply to the brain). If PCB-126 and PCB mixtures altered thyroid function, we expected to see decreased plasma thyroid hormone concentrations and subsequent increases in 5'D-II activity. Chicken eggs were injected (into the air cell) before incubation with five dose levels (0.0512, 0.128, 0.32, 0.64, 0.8 ng/g) of PCB-126 (3,3, 4,4',5-pentachlorobiphenyl), or vehicle (sunflower oil); sampling was on day 20 of the 21-day incubation period. Studies on PCB-treated embryos included a preliminary study and a larger study encompassing a serious of smaller studies. Herring gull embryos (at pipping, on day 25 of the 26 day incubation), and 28-day pre-fledgling chicks were sampled (for two field seasons) at several Great Lakes sites with different contaminant exposures (with Kent Island being the reference site). In PCB-treated chicken embryos, there were no statistically significant decreases in plasma T4 or T3 concentrations and no significant increases in brain 5'D-II activity in either the preliminary or the larger study. We found no clear pattern of altered thyroid function in herring gulls from polluted Great Lakes' sites. Plasma TH concentrations were not significantly decreased and 5'D-II activity did not significantly increase in birds from more contaminated sites in comparison to birds from Kent Island or sites with less contamination. Although pipped embryos from Strachnan Island had a significant increase in 5'D-II activity when compared to Kent Island, there were no differences in plasma TH concentrations, and brain 5'D-II activity was not significantly increased in birds from sites with greater PCB loads than Strachnan Island. Plasma T4 and T3 concentrations were significantly decreased in prefledglings from West Sister Island and Detroit Edison in comparison to Kent Island, but there was no subsequent increase in brain 5'D-II activity. The present study is the first to evaluate the potential effects of PCBs, alone and in a mixed environmental exposure, on circulating THs and brain 5'D-II activity in developing birds. Although thyroid function was not altered by the specific PCB congener used in my study or by exposure to environmental pollutants, more complete evaluations are needed before determining whether PCBs alter thyroid function in birds.
Master of Science
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Ivassechen, Janaíne do Rocio [UNESP]. "Sílica mesoporosa como suporte sólido para o ancoramento da molécula 4-amino-3-hidrazino-5-mercapto-1,2,4-triazole e aplicação na adsorção de Cu(II), Cd(II), Ni(II), Pb(II) e Co(II) em amostras aquosas." Universidade Estadual Paulista (UNESP), 2016. http://hdl.handle.net/11449/134329.

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A determinação direta de metais presentes em baixas concentrações em amostras de águas naturais é geralmente dificultada devido à presença de espécies interferentes. Os metais que foram estudados, Cu (II), Pb(II), Co (II), Ni (II) e Cd (II) são de interesse ambiental em razão de seu uso intensivo, distribuição e por serem absolutamente não-degradáveis podem acumular-se em matrizes ambientais manifestando toxicidade. Neste projeto desenvolveu-se a sílica como suporte sólido para o ancoramento da molécula 4-amino-3-hidrazino-5-mercapto-1,2,4-triazole e sua aplicação na adsorção/remoção de íons em solução aquosa. O material foi caracterizado por espectroscopia na região do infravermelho (FTIR), o qual apresentou bandas em 1690- 1649 e 790 cm-1 , característica de ligações N-H de aminas primárias do ligante. A ressonância magnética nuclear de 13C e 29Si (RMN) comprovam o ancoramento do ligante. As medidas de área de superfície específica pelo método de BET e diâmetro de poro resultaram em uma área de 795,51 ± 1,14 m2 g-1 e poros numa gama de 1,1 a 7,1 nm. A Microscopia Eletrônica de Varredura (MEV) mostrou que o material tem formato esférico com tamanhos aproximadamente de 10 μm e a Análise por Energia Dispersiva de Raios X (EDX) mostrou uma distribuição homogênea do sililante por toda a superfície do material. Com isso, confirmou-se a ocorrência da reação de modificação. O material foi aplicado em estudos de adsorção para determinação da sua capacidade máxima, bem como estudos da influência do pH e estudos cinéticos no processo de equilíbrio Os experimentos foram realizados pelo método de batelada. O primeiro teste foi o pHPZC, que indica a melhor faixa de pH (5-9) para a adsorção. Os estudos de adsorção dos metais em solução apresentaram o melhor resultado quando o pH era igual a 6, o equilíbrio de adsorção foi atingido depois de 50 minutos de agitação. Para todas as espécies investigadas o processo de adsorção é melhor descrito pelo modelo de pseudo- segunda ordem. Com esses parâmetros estabelecidos os valores de capacidade máxima de adsorção foram encontrados, sendo 0,129; 0,102; 0,105; 0,113; e 0,076 mmol g-1 para o Cu, Ni, Pb, Co e Cd, respectivamente. A sílica modificada foi aplicada na pré-concentração de Cu (II) em amostras aquosas. Com um fator de enriquecimento de 20 vezes, a coluna provou ser estável ao longo de 24 ciclos de adsorção/dessorção.
The direct determination of metals present at trace levels in natural water samples is generally difficult due to the presence of interfering species. Metals that were studied, Cu(II), Pb(II), Co(II), Ni(II) and Cd(II) are of environmental interest because of its intensive use, distribution, and as a consequence of its non-degradability can be accumulated in environmental matrices manifesting toxicity. In this project was developed a mesoporous silica as solid support for the anchoring of 4-amino-3-hydrazino-5-mercapto-1,2,4-triazole molecule to be applied in the adsorption/removal of metals from aqueous solution. The material was characterized by infrared spectroscopy (FTIR), which showed bands at 1649 and 1690- 790 cm-1, characteristic of NH bonds of primary amines, existing in molecule ligand. The nuclear magnetic resonance 13C and 29Si (NMR) confirm the anchoring of the ligand. Measurements of specific surface area by the BET method and pore diameter resulted in an area of 795.51 ± 1.14 m2 g-1 and pores in a range from 1.1 to 7.1 nm. Scanning Electron Microscopy (SEM) showed that the material has spherical shape with sizes of approximately 10 μm and the analysis by Energy Dispersive X-ray (EDX) showed a homogeneous distribution of silylant over material surface. Thus, it was confirmed the occurrence of the modification reaction. The material was applied in adsorption studies to determine its maximum adsorption capacity, as well as studies of the influence of pH and kinetic studies on the balance process. The experiments were performed by the batch method. The first test was the pHPZC which indicates the best pH range (5-9) for the adsorption. Adsorption studies showed the best results when pH was near 6 and the adsorption equilibrium was attained after 50 minutes of stirring time. For all species investigated the adsorption process is better described by the pseudo- second order kinetic model. With these parameters established the maximum adsorption capacity values found were 0.129, 0.102, 0.105, 0.113 and 0.076 mmol g-1 for Cu(II), Ni(II), Pb(II), Co(II) and Cd(II), respectively. Modified silica was also applied in the preconcentration of Cu(II) from aqueous samples with 20 fold enrichment factor and the packed column proved to be stable over 24 cycles of adsorption/desorption.
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Berta, Holló. "Sinteza i karakterizacija nekih derivata pirazola i njihove reakcije sa prelaznim metalima." Phd thesis, Univerzitet u Novom Sadu, Prirodno-matematički fakultet u Novom Sadu, 2011. http://dx.doi.org/10.2298/NS20110922HOLLO.

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Abstract:
Reactions of 3,5-dimethylpyrazole-1-carboxamidinium nitrate (dpca∙HNO3) and 4-acetyl-3-amino-5-methylpyrazole (aamp) with transition metals under different reaction conditions are presented. The template reaction of aamp with triethyl orthoformate (teof) in the presence of metal ion is described. Besides, condensation of aamp with thiosemicarbazide (tsc) and the coordination of its product to copper(II) ion is also described. Twelve new complex compounds are synthesized and fully characterized. The characterization of two other, already known complexes is significantly enriched. The influence of HSAB interactions between the metal ions and ligators on the structures of obtained compounds is studied. The influence of the reaction conditions on the composition, structure and quality of crystals obtained in the reactions is investigated. Compounds are characterized by structural analysis, elemental analysis, molar conductivity data, infrared spectrometry and thermal analysis. Some selected complexes are characterized by UV-Vis spectra, magnetic measurements and biological activity tests, too.
Reactions of 3,5-dimethylpyrazole-1-carboxamidinium nitrate (dpca∙HNO3) and 4-acetyl-3-amino-5-methylpyrazole (aamp) with transition metals under different reaction conditions are presented. The template reaction of aamp with triethyl orthoformate (teof) in the presence of metal ion is described. Besides, condensation of aamp with thiosemicarbazide (tsc) and the coordination of its product to copper(II) ion is also described. Twelve new complex compounds are synthesized and fully characterized. The characterization of two other, already known complexes is significantly enriched. The influence of HSAB interactions between the metal ions and ligators on the structures of obtained compounds is studied. The influence of the reaction conditions on the composition, structure and quality of crystals obtained in the reactions is investigated. Compounds are characterized by structural analysis, elemental analysis, molar conductivity data, infrared spectrometry and thermal analysis. Some selected complexes are characterized by UV-Vis spectra, magnetic measurements and biological activity tests, too
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Books on the topic "II.> 5"

1

Boudník, Vladimír. Loď 5.II.1952. [Prague?]: Inverze, 1990.

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Plotinus. Traité 25 (II, 5). Paris: Cerf, 1998.

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Aomori-ken Maizō Bunkazai Chōsa Sentā. Ienomae iseki II, Takahoko iseki II: Heisei 5-nendo. Aomori-shi: Aomori-ken Kyōiku Iinkai, 1994.

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Scott, Ruth. The Canadian spelling program II, 5. Toronto: Gage Educational Pub., 1988.

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Russell, Edward C. Building simulation models with SIMSCRIPT II.5. La Jolla, Calif: CACI Products Co., 1990.

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Pescasio, Luigi. Federico II Gonzaga: 5. marchese, 1. duca. Suzzara: Bottazzi, 1997.

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Guidon, Jacques, ed. Ouvras II. Schlarigna, CH: Uniun dals Grischs, 1992.

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Opus Dei: Archeologia dell'ufficio : Homo sacer, II, 5. Torino: Bollati Boringhieri, 2012.

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Paul, John. Giovanni Paolo II all'Assemblea dell'ONU: 5 ottobre 1995. Città del Vaticano: L'Osservatore romano, 1995.

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Seminar Nasional Wanita (2nd 1992 Bogor, Indonesia). Seminar Nasional Wanita II, Bogor, 5-6 Agustus 1992. [Jakarta: Pusat Antar Universitas Untuk Peningkatan dan Pengembangan Aktivitas Instruksional di Universitas Terbuka, Direktorat Jenderal Pendidikan Tinggi, Departemen Pendidikan dan Kebudayaan, 1992.

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Book chapters on the topic "II.> 5"

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Kovacec, Alexander. "Contributions to Inequalities II." In General Inequalities 5, 65–72. Basel: Birkhäuser Basel, 1987. http://dx.doi.org/10.1007/978-3-0348-7192-1_4.

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Symonds, Michael. "Adorno II." In The Appeal of Art in Modernity, 111–38. New York: Routledge, 2020.: Routledge, 2019. http://dx.doi.org/10.4324/9781351233941-5.

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Doak, Jonathan, Claire McGourlay, and Mark Thomas. "Witnesses II." In Evidence: Law and Context, 94–132. [Fifth edition]. | Abingdon, Oxon [UK]; New York, NY:: Routledge, 2018. http://dx.doi.org/10.4324/9781315166285-5.

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Hanusch, Frederic. "Analysis II." In Democracy and Climate Change, 84–114. Abingdon, Oxon ; New York, NY, USA : Routledge is an imprint of the Taylor & Francis Group, an informa business, [2017]: Routledge, 2017. http://dx.doi.org/10.4324/9781315228983-5.

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Grunwald, Armin. "Theory II." In Technology Assessment in Practice and Theory, 151–80. Abingdon, Oxon ; New York, NY : Routledge, 2019.: Routledge, 2018. http://dx.doi.org/10.4324/9780429442643-5.

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"5 II." In Handbook of Polymer Degradation, 555. CRC Press, 2000. http://dx.doi.org/10.1201/9781482270181-101.

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Manssen, Gerrit. "§ 5. Grundrechtsverpflichtete." In Staatsrecht II, 33–46. Verlag C.H.BECK oHG, 2020. http://dx.doi.org/10.17104/9783406759598-33.

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Manssen, Gerrit. "§ 5. Grundrechtsverpflichtete." In Staatsrecht II, 34–49. Verlag C.H.BECK oHG, 2021. http://dx.doi.org/10.17104/9783406778292-34.

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Tibullus], Tibullus [Albius. "5." In Tibullus: Elegies II, edited by Paul Murgatroyd, 10–235. Oxford University Press, 1994. http://dx.doi.org/10.1093/oseo/instance.00088124.

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Rader, Olaf B. "5 Der Gesetzgeber." In Friedrich II., 153–96. Verlag C.H.BECK oHG, 2010. http://dx.doi.org/10.17104/9783406616761-153.

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Conference papers on the topic "II.> 5"

1

Garrison, William J. "NETWORK II.5 tutorial NETWORK II.5 without programming." In the 20th conference. New York, New York, USA: ACM Press, 1988. http://dx.doi.org/10.1145/318123.318180.

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Garrison, William J. "NETWORK II.5 tutorial." In the 18th conference. New York, New York, USA: ACM Press, 1986. http://dx.doi.org/10.1145/318242.318298.

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Garrison, William J. "Network II.5 tutorial." In the 19th conference. New York, New York, USA: ACM Press, 1987. http://dx.doi.org/10.1145/318371.318426.

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Russell, Edward C. "SIMSCRIPT II.5 tutorial." In the 18th conference. New York, New York, USA: ACM Press, 1986. http://dx.doi.org/10.1145/318242.318266.

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Russell, Edward C. "SIMSCRIPT II.5 tutorial." In the 17th conference. New York, New York, USA: ACM Press, 1985. http://dx.doi.org/10.1145/21850.253073.

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Garrison, William J. "NETWORK II.5 tutorial." In the 17th conference. New York, New York, USA: ACM Press, 1985. http://dx.doi.org/10.1145/21850.253080.

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Russell, Edward C. "SIMSCRIPT II.5 and SIMGRAPHICS." In the 20th conference. New York, New York, USA: ACM Press, 1988. http://dx.doi.org/10.1145/318123.318174.

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"Switching II [Session 5 A]." In 2004 Workshop on High Performance Switching and Routing, 2004. HPSR. IEEE, 2004. http://dx.doi.org/10.1109/hpsr.2004.1303451.

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"SESSION 5: Mobile Computing II." In 2021 International Mobile, Intelligent, and Ubiquitous Computing Conference (MIUCC). IEEE, 2021. http://dx.doi.org/10.1109/miucc52538.2021.9447591.

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"Part II: Putting theory into practice." In MDG+5 Workshop. Wien: Verlag der Österreichischen Akademie der Wissenschaften, 2007. http://dx.doi.org/10.1553/mdgresearch2005s34.

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Reports on the topic "II.> 5"

1

Ruther, W. E., J. D. Staffon, B. G. Carlson, and T. R. Allen. The EBR-II materials-surveillance program. 5: Results of SURV-5. Office of Scientific and Technical Information (OSTI), January 1998. http://dx.doi.org/10.2172/658149.

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Krushnisky, A., P. Mercier-Langevin, P. S. Ross, J. Goutier, C. Pilote, C. Bernier, and L. Moore. (Day 3 - part II) The Horne 5 deposit. Natural Resources Canada/ESS/Scientific and Technical Publishing Services, 2017. http://dx.doi.org/10.4095/306257.

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Benedict, Terry. Trident II (D-5) Sea Launched Ballistic Missile UGM 133A (Trident II Missile). Fort Belvoir, VA: Defense Technical Information Center, November 2015. http://dx.doi.org/10.21236/ad1019554.

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AIR FORCE TEST PILOT SCHOOL EDWARDS AFB CA. Volume II. Flying Qualities Phase. Chapter 5: Longitudinal Static Stability. Fort Belvoir, VA: Defense Technical Information Center, October 1990. http://dx.doi.org/10.21236/ada319976.

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Laughery, R., R. Archer, and G. Fontenelle. Design Specification for (MPT)2 Product 5. Manpower Determination Aid. Volume II. Fort Belvoir, VA: Defense Technical Information Center, January 1988. http://dx.doi.org/10.21236/ada396537.

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Zinkle, S. J., L. L. Snead, J. P. Robertson, and A. F. Rowcliffe. Strain rate dependence of the tensile properties of V-(4--5%)Cr-(4--5%)Ti irradiated in EBR-II and HFBR. Office of Scientific and Technical Information (OSTI), March 1998. http://dx.doi.org/10.2172/335367.

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Doty, F. D., A. Boman, S. Arnold, J. B. Spitzmesser, D. Jones, D. McCree, and L. J. Hacker. Development of 0.5-5 W, 10K Reverse Brayton Cycle Cryocoolers - Phase II Final Report. Office of Scientific and Technical Information (OSTI), October 2001. http://dx.doi.org/10.2172/899973.

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Sandstrom, Mary M., Geoffrey W. Brown, Daniel N. Preston, Colin J. Pollard, Kirstin F. Warner, Daniel N. Sorenson, Daniel L. Remmers, et al. Integrated Data Collection Analysis (IDCA) Program - RDX Type II Class 5 Standard, Data Set 1. Office of Scientific and Technical Information (OSTI), April 2011. http://dx.doi.org/10.2172/1305880.

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Toutin, T. Comparison of stereo-extracted DTM from different high-resolution sensors: SPOT-5, EROS-A, IKONOS-II, and QuickBird. Natural Resources Canada/ESS/Scientific and Technical Publishing Services, 2004. http://dx.doi.org/10.4095/220073.

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Guay, F., P. Pilote, R. Daigneault, and V. McNicoll. (Day 5 - part II) The "Malartic Lake Shore" gold showing and the Rivière-Héva Fault Zone, Abitibi, Québec, Canada. Natural Resources Canada/ESS/Scientific and Technical Publishing Services, 2017. http://dx.doi.org/10.4095/306260.

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