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Academic literature on the topic 'Inorganik'

Author: Grafiati

Published: 4 June 2021

Last updated: 1 February 2022

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Journal articles on the topic "Inorganik"

Utomo, N. B. P., Winarti, and A. Erlina. "Growth of Spirulina platensis Cultured with Inorganic Fertilizer (Urea, TSP and ZA) and Chicken Manure." Jurnal Akuakultur Indonesia 4, no. 1 (January 1, 2007): 41. http://dx.doi.org/10.19027/jai.4.41-48.

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This experiment was conducted to compare the effectiveness of inorganic fertilizer and chicken manure on population growth and nutrient content of Spirulina platensis. It was found that Spirulina platensis cultured in inorganic medium reached a maximum population on day-9 with a density of 614.77x103 Sin/ml, containing 56.39% of crude protein and 17.92% of lipid. On the other hand, Spirulina platensis cultured in 250 ppm of chicken manure reached a maximum population on day-4 with a density of 434.32x103 Sin/ml, containing 45.39% of crude protein and 12.50% of lipid. Keywords: spirulina, Spirulina platensis, culture, inorganic fertilizer, chicken manure, population maximum ABSTRAK Penelitian ini dilakukan untuk membandingkan efektivitas pupuk inorganik (urea, TSP dan ZA) dan kotoran ayam terhadap pertumbuhan dan kandungan nutrien Spirulina platensis. Hasil penelitian menunjukkan bahwa Spirulina platensis dikultur menggunakan pupuk inorganik mencapai puncak populasi pada hari ke-9 dengan kepadatan 614,77x103 Sin/ml, mengandungkan protein kasar 56,39% dan lemak 17,92%. Sementara itu, Spirulina platensis dikultur menggunakan kotoran ayam 250 ppm mencapai puncak populasi pada hari ke-4 dengan kepadatan 434,32x103 Sin/ml, kandungan protein kasar 45,39% dan lemak 12,50%. Kata kunci: spirulina, Spirulina platensis, kultur, pupuk inorganik, kotoran ayam, populasi maksimal

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Sipan SOYSAL and Murat ERMAN. "Siirt Ekolojik Koşullarında Mikrobiyolojik ve İnorganik Gübrelemenin Nohut (Cicer arietinum l.)’un Kalite Özellikleri Üzerine Etkileri." ISPEC Journal of Agricultural Sciences 4, no. 4 (December 4, 2020): 923–39. http://dx.doi.org/10.46291/ispecjasvol4iss4pp921-937.

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Siirt ekolojik koşullarında mikrobiyolojik ve inorganik gübrelemenin nohut (Cicer arietinum L.)’ un verim, verim öğeleri ve nodülasyonu üzerine etkilerini belirlemek amacıyla yapılan bu çalışma tesadüf bloklarında faktöriyel deneme deseninde 3 tekerrürlü olarak 2016-2017 ve 2017-2018 yılları arasında yürütülmüştür. Çalışmada simbiyotik bakteri olarak Mesorhizobium ciceri, asimbiyotik bakteri olarak azot bağlayıcı Basillus atrophaeus, fosfat çözücü olarak Basillus GC-group ve inorganik gübre olarak DAP gübresi kullanılmıştır. Araştırmada; tane protein oranı, protein verimi, tane fosfor içeriği, tane potasyum içeriği, tane nem oranı ve tanede toplam kuru madde oranı özellikleri incelenmiştir. Çalışmadan elde edilen bulgulara göre, tane protein oranı %22.3-25.6, protein verimi 21.2-40.4 kg/da, tane fosfor içeriği %0.43-0.71, tane potasyum içeriği %0.96-1.58, tane nem oranı %4.02-6.01 ve tanede toplam kuru madde oranı %93.98-95.97 arasında değişim göstermiştir. Çalışmada en yüksek protein içeriği, Mesorhizobium ciceri + %50 DAP ve Bacillus atrophaeus (N) + %50 DAP uygulamaları ile elde edilmiştir. Sonuç olarak, mikrobiyolojik gübre kullanımının inorganik gübrelere tamamen bir alternatif olmamasına rağmen kullanım miktarının azalmasına olanak sağladığı tespit edilmiştir.

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Ramadhan, Laode Muhamad Asdiq Hamsin, Budi Nugroho, Arief Hartono, and Untung Sudadi. "DINAMIKA FRAKSI FOSFOR DAN SIFAT KIMIA TANAH SAWAH TERKAIT INDEKS PERTANAMAN PADI SAWAH DAN KONDISI PENGGENANGAN." Jurnal Ilmu Tanah dan Lingkungan 19, no. 1 (March 13, 2019): 19. http://dx.doi.org/10.29244/jitl.19.1.19-24.

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Dinamika fraksi-fraksi P dan sifat kimia lainnya pada tanah sawah terkait dengan indeks pertanaman (IP) dan kadar air tanah pada kondisi lapang (KAL) akibat kondisi penggenangan. Penelitian ini bertujuan mengevaluasi pengaruh KAL setelah 7, 9, 11 dan 13 minggu penggenangan serta aplikasi jerami dan pupuk P pada tanah sawah dengan IP 100%, 200% dan 300% terhadap dinamika fraksi P, sifat kimia tanah lainnya dan produksi padi sawah. Contoh tanah komposit diambil pada lahan sawah petani dengan IP 100%, 200% dan 300% pada keempat periode penggenangan. Fraksionasi P dilakukan dengan metode Tiessen dan Moir (2008) yang dimodifikasi untuk memperoleh fraksi PH2O, PNaHCO3-inorganik (Pi), PNaHCO3-organik (Po), PNaOH-Pi, PNaOH-Po dan PHCl. Pada keempat masa penggenangan, KAL pada IP 100% < IP 200% ≈ IP 300%. Sifat-sifat kimia dan fraksi-fraksi P-organik pada IP 100% cenderung menurun, sedangkan fraksi-fraksi P-inorganik cenderung meningkat dengan peningkatan KAL. Dinamika fraksi-fraksi P pada ketiga IP terutama ditentukan oleh Corg. Peningkatan Corg menurunkan kadar P-inorganik pada IP 100% dan P-organik pada IP 200% tetapi meningkatkan P-inorganik pada IP 300%. Penurunan dosis P2O5 dan peningkatan dosis jerami menurunkan Eh. Faktor yang paling berpengaruh terhadap produksi padi sawah adalah dosis jerami. Kata kunci : Pupuk P, jerami padi, kadar air lapang tanah, Fraksi P tanah

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Handayani, Noer Abyor, Herry Santosa, Bunga Profegama, and Aditya Yuna. "FORTIFIKASI INORGANIK ZINK PADA TEPUNG UBI JALAR UNGU SEBAGAI BAHAN BAKU BUBUR BAYI INSTAN." Reaktor 15, no. 2 (February 27, 2014): 111. http://dx.doi.org/10.14710/reaktor.15.2.111-116.

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Fortifikasi zink pada bubur instan bayi berbahan dasar tepung ubi jalar ungu diharapkan mampu memberikan inovasi produk yang dapat mengatasi permasalahan defisiensi zink pada balita. Penelitian ini bertujuan untuk mengkaji pengaruh konsentrasi fortifikan inorganic (ZnO) terhadap sifat fisik (penampilan fisik, densitas kamba, dan daya rehidrasi) dari produk instan. Bubur bayi instan yang dihasilkan melalui tahap pembuatan tepung, fortifikasi zink, dan tahap pembuatan bubur bayi instan. Bubur bayi instan tanpa fortifikan digunakan sebagai variabel kontrol. Hasil penelitian menunjukkan bahwa konsentrasi zink pada bubur bayi instan berhasil meningkat, namun tingkat efektifitas dari fortifikasi sangat rendah. Fortifikasi inorganik zink dapat menurunkan 27,6% nilai densitas kamba dan mampu menaikkan 15% daya rehidrasi dibandingkan dengan bubur bayi instan tanpa fortifikan. Terdapat perubahan warna dari bubur bayi instan setelah mengalami proses fortifikasi zink.

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Bentli, İsmail. "Kömür Lavvar Tesisi Atıkların Flokülasyonunda İnorganik Elektrolitlerin Etkisi." Ekoloji 19, no. 76 (August 5, 2010): 71–77. http://dx.doi.org/10.5053/ekoloji.2010.768.

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TEKKARIŞMAZ, Nihan, Dilek TORUN, and Rüya ÖZELSANCAK. "What is the Level of Awareness About the Foods Containing Inorganic Phosphorus in Patients with Chronic Renal Failure?" Journal of Traditional Medical Complementary Therapies 2, no. 3 (2019): 130–37. http://dx.doi.org/10.5336/jtracom.2019-72202.

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Marwoto, Jarot, Oceana Windyartanti, and Muslim Muslim. "Pengaruh Padatan Tersuspensi terhadap Konsentrasi Klorofil-a dan Fosfat Inorganik Terlarut di Muara Banjir Kanal Barat, Semarang." Jurnal Kelautan Tropis 24, no. 2 (May 30, 2021): 223–31. http://dx.doi.org/10.14710/jkt.v24i2.10703.

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The large number of activities along the West Banjir Kanal river has triggered a change in the condition of its sea waters. The condition most affected is turbidity which caused high concentration of Total Suspended Solid (TSS) in estuary waters and interfere with the entry of sunlight into the waters. The purpose of the study is to determine the effect of the of concentration TSS on the concentration chlorophyll a and dissolved inorganic phosphate (DIP) in the waters of West Banjir Kanal estuary. Water sampling was conducted on October 3, 2019. Water quality parameters such as brightness, pH, temperature, DO and salinity were measured in situ. Meanwhile, chlorophyll a, TSS and DIP measurements were analyzed in the laboratory. The results showed that the highest concentration of TSS, chlorophyll a and DIP were in the estuary area and decreased with further distance from the river mouth with concentration were 70.17-151.50 mg/L, 0.03–2.67 µg/L and 0.71–0.98 µM respectively. Based on the results of the Principal Component Analysis (PCA) showed that TSS affected chlorophyll a by 8.7% (r=0.392; p<0.05) and DIP by 54.46% (r=0.931; p<0.01). The low regression between TSS and chlorophyll a was due to the presence of large amounts of inorganic particles in the West Banjir Kanal river, which makes the river waters become turbid. So, the turbidity of the waters caused the release of phosphate in the sediment to water column which was used by phytoplankton for photosynthesis, so the TSS not only contain sediment particles, but also phytoplankton. Banyaknya aktivitas di sepanjang sungai Banjir Kanal Barat Semarang, memicu kondisi perairan lautnya menjadi berubah. Kondisi yang paling terpengaruh adalah kekeruhan yang menyebabkan tingginya konsentrasi Material Padatan Tersuspensi (MPT) di perairan muara dan mengganggu masuknya cahaya matahari ke perairan. Penelitian ini bertujuan untuk mengetahui pengaruh MPT terhadap konsentrasi klorofil-a dan fosfat inorganik terlarut (DIP=Dissolved Inorganic Phosphate) di perairan Muara Banjir Kanal Barat Semarang. Pengambilan sampel air dilakukan pada tanggal 3 Oktober 2019. Parameter kualitas perairan seperti kecerahan, pH, suhu, DO dan salinitas diukur secara in situ. Sedangkan pengukuran klorofil-a, MPT dan DIP dianalisis di laboratorium. Hasil penelitian menunjukkan bahwa konsentrasi MPT, klorofil-a dan DIP tertinggi di daerah muara sungai dan menurun dengan makin jauhnya muara sungai dengan konsentrasi secara berturut-turut sebesar 70,17-151,50 mg/L, 0,03-2,67 µg/L dan 0,71-0,98 µM. Berdasarkan hasil Analisis Komponen Utama (AKU) menunjukkan bahwa MPT mempengaruhi klorofil-a sebesar 8,7% (r = 0,392; P < 0,05) dan fosfat inorganik terlarut sebesar 54,46% (r = 0,931; P < 0,01). Rendahnya hubungan antara MPT dengan klorofil-a ini disebabkan oleh adanya masukan partikel anorganik dalam jumlah besar di badan Sungai Banjir Kanal Barat yang membuat perairan sungai menjadi keruh. Jadi kekeruhan perairan menyebabkan terlepasnya fosfat di sedimen yang dimanfaatkan oleh fitoplankton untuk proses fotosintesa, sehingga yang terkandung dalam MPT selain partikel sedimen juga fitoplankton.

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Sipan SOYSAL and Murat ERMAN. "Siirt Ekolojik Koşullarında Mikrobiyolojik Ve İnorganik Gübrelemenin Nohut (Cicer arietinum l.)’un Verim, Verim Öğeleri Ve Nodülasyonu Üzerine Etkilerinin Araştırılması." ISPEC Journal of Agricultural Sciences 4, no. 3 (September 16, 2020): 649–70. http://dx.doi.org/10.46291/ispecjasvol4iss3pp649-670.

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Siirt ekolojik koşullarında mikrobiyolojik ve inorganik gübrelemenin nohut (Cicer arietinum L.)’ un verim, verim öğeleri ve nodülasyonu üzerine etkilerini belirlemek amacıyla yapılan bu çalışma tesadüf bloklarında faktöriyel deneme deseninde 3 tekerrürlü olarak 2016-2017 ve 2017-2018 yılları arasında yürütülmüştür. Çalışmada simbiyotik bakteri olarak Mesorhizobium ciceri, asimbiyotik bakteri olarak azot bağlayıcı Basillus atrophaeus, fosfat çözücü olarak Basillus GC-group ve inorganik gübre olarak DAP gübresi kullanılmıştır. Araştırmada; bitki boyu, ilk bakla yüksekliği, ana dal sayısı, yan dal sayısı, bitkide bakla sayısı, bitkide tane sayısı, 100 tane ağırlığı, tane verimi, biyolojik verim, hasat indeksi, bitkide nodül sayısı, nodül yaş ağırlığı ve nodül kuru ağırlığı incelenmiştir. Çalışma sonuçlarına göre, bitki boyu 52.1-59.3 cm, ilk bakla yüksekliği 32.0-38.0 cm, ana dal sayısı 2.46-3.36 adet/bitki, yan dal sayısı 4.03-5.90 adet/bitki, bitkide bakla sayısı 16.0-35.3 adet/bitki, bitkide tane sayısı 14.7-33.1 adet/bitki, 100 tane ağırlığı 30.3-34.2 g, tane verimi 86.0-174.0 kg/da, biyolojik verim 247.7-613.7 kg/da, hasat indeksi %26.3-34.8, bitkide nodül sayısı 28.3-44.6 adet/bitki, nodül yaş ağırlığı 1.504-2.507 g ve nodül kuru ağırlığı 0.235-0.443 g arasında değişim göstermiştir. Araştırma sonucunda en yüksek tane verimi Bacillus atrophaeus (N)+ DAP %50 uygulamasında 174.0 kg/da olarak elde edilmiştir.

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Pratikno, Bungkus, and Nurfadhlini Nurfadhlini. "Studi Komposisi Rasio Isotop 13C Air Hujan di Wilayah Lebak Bulus, Jakarta Selatan." Jurnal Ilmiah Aplikasi Isotop dan Radiasi 13, no. 2 (December 20, 2017): 123. http://dx.doi.org/10.17146/jair.2017.13.2.3548.

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Telah dilakukan pengukuran komposisi isotop 13C/12C (d 13C) dari contoh air hujan wilayah Lebak Bulus, Jakarta Selatan. Studi ini bertujuan untuk mengetahui dampak emisi gas buang antrofogenik terhadap kualitas udara di atmosfir Jakarta. Pengamatan dilakukan berdasarkan sampel air hujan yang jatuh khususnya di wilayah PAIR-BATAN, Lebak Bulus, Jakarta Selatan pada September 2009 sampai dengan Juni 2010. Penelitian menggunakan metode pengukuran komposisi rasio isotop 13C dari karbon inorganik terlarut (Dissolverd Inorganic Carbon, DIC) dalam air hujan. Pengukuran komposisi rasio isotop 13C (d13C) menggunakan spektrometer massa rasio isotop SIRA-9 VG ISOGAS. Dari hasil sepuluh bulan pengukuran d13C air hujan didapat d13C bulan Februari 2010 sebesar -10,710/00 dan merupakan nilai yang paling rendah (depleted) dibanding dengan pengukuran sembilan bulan lainnya, sedangkan hasil pengukuran yang tinggi (enrich) didapat pada bulan Desember 2009 sebesar -8,52 0/00. Dari hasil penelitian menunjukkan bahwa komposisi rasio isotop d13C dari gas CO2 atmosfir Lebak Bulus, Jakarta Selatan lebih depleted dibandingkan dengan atmosfir daerah udara bersih yang hanya sebesar -8,1 0/00. Perbedaan ini mengindikasikan bahwa ada penambahan gas buang CO2 hasil kegiatan antropogenik.

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Demirbağ, Sena, and Sennur Alay Aksoy. "Production and Characterization of Heat Storing Microcapsules with Enhanced." Tekstil ve Mühendis 20, no. 92 (December 31, 2013): 27–35. http://dx.doi.org/10.7216/130075992013209203.

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Dissertations / Theses on the topic "Inorganik"

Vervacke, Céline. "Sensing and Transport Properties of Hybrid Organic/Inorganic Devices." Doctoral thesis, Universitätsbibliothek Chemnitz, 2014. http://nbn-resolving.de/urn:nbn:de:bsz:ch1-qucosa-152484.

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Over the past two decades, organic semiconductors played a growing part as active layers in several electronic systems such as sensors, field‑effect transistors or light emitting diodes to cite a few. In fact, organic materials offer a high versatility and flexibility. However, pure organic systems often lack stability and robustness, which can be overcome by combining them with inorganic scaffolds. In this work, a conducting polymer, polypyrrole (PPy) is employed to create new sensor elements based on the combination of both inorganic and organic layers. Electrical measurements, infrared spectroscopy and current sensing atomic force microscopy provides a better understanding of the polymer behavior upon immersion in aqueous solutions. The observed discharge in water leads to a straightforward application of the device as an in‑flow sensor for several acids like HCl, H2SO4 and H3PO4. The wide range of sensing concentrations as well as the low detection limit place the present detector among the best reported so far in the literature. In a further step to turn towards lab‑in‑a‑tube devices, tubular‑shaped‑integrated microelectrodes are developed by using the rolled‑up technology. As a proof of concept, the successful integration of PPy as an active layer and its use as a gas sensor for volatile organic compounds (VOCs) is demonstrated. Finally, by adapting the rolled‑up top electrodes, as developed by Bof Bufon et al. for self‑assembled monolayers (SAMs), thin PPy films (<50 nm) are vertically contacted and their electrical characteristics measured as a function of temperature and electric field. From the transport investigations, it is observed that an insulating‑to‑metallic transition occurs in the polymeric film by increasing the bias voltage. Other molecular layers like CuPc can be incorporated in these platforms, opening the way towards emerging organic devices.

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Araujo, Márcio Peres de [UNESP]. "Complexos cofaciais de dirutênio contendo haletos em ponte e fosfinas como ligantes: estudos espectrais, eletroquímicos e de reatividade." Universidade Estadual Paulista (UNESP), 2001. http://hdl.handle.net/11449/105810.

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Made available in DSpace on 2014-06-11T19:35:08Z (GMT). No. of bitstreams: 0 Previous issue date: 2001Bitstream added on 2014-06-13T20:46:06Z : No. of bitstreams: 1 araujo_mp_dr_araiq.pdf: 1100502 bytes, checksum: 61f93c05d5083f37f2c488086757122a (MD5)
O complexo mer-[RuCl3(dppb)H2O] foi utilizado como precursor para a síntese de uma série de complexos binucleares de valência mista, estes apresentam fórmula geral [Ru2Cl5(dppb)(P)2] e [Ru2Cl5(dppb)(P-P)] e forma estudados por técnicas eletroquímicas e espectroscópicas. A maior característica destas espécies é que apresentam acoplamento metal-metal, ou seja transferência de elétrons entre seus centros metálicos em função dessa caracterísitica apresentam absorção na região do infravermelho-próximo do espectro eletrônico, além de dois processos eletroquímicos com separação (ΔE1/2) ~0,60 V, indicativo de forte interação entre os centros metálicos. Complexos com fórmula [Ru2Cl4CO(dppb)(P)2] e [Ru2Cl4(N-het.)(dppb)2] foram sintetizados e caracterizados. Alguns dos complexos obtidos foram testados em reações de hidrogenação de iminas, sendo que alguns mostraram grande atividade. Complexos do tipo [RuCl2(dppb)(N-N)] e [RuCl2(dppb)(N)2] foram utilizados para a redução da acetofenona usando transferência de hidrogênio, as conversões alcançadas foram satisfatórias em função das condições não terem sido optimizadas. Além disso o aqua complexo mer-[RuCl3(dppb)H2O] também foi eficiente para gerar in situ espécies catalíticamente ativas. A reatividade do complexo [Ru2Cl4(dppb)3] com CuCl2.2H2O e [NBu4][AuCl4] foi testada e o produto destas reações foi identificado como [Ru2Cl5(dppb)2]. Estas reações ocorrem via oxidação do complexo de rutênio e posterior fomação do complexo de valência mista contendo três cloretos em ponte. O complexo [RuCl2(PPh3)3] também foi oxidado com excesso de CuCl2.2H2O levando a formação de [CuCl(PPh3)3] (caracterizado por RMN 31P{1H}) e do complexo solvato [RuCl3(PPh3)2MeOH]MeOH (caracterizado por RPE), além destas espécies uma solução amarela é obtida e com a adição de dppm a esta solução o complexo...
The compound mer-[RuCl3(dppb)H2O] was used as precursor for the synthesis of a wide range of mixed valence complexes and present the general formula [Ru2Cl5(dppb)(P)2] and [Ru2Cl5(dppb)(PP)]. These complexes were studied by electrochemical and spectroscopic techniques. The main characteristic of these species is that they present metal-metal coupling or metal-metal electron transfer due to this electron transfer absorptions in the near infrared region can be observed. Cyclic voltammetry studies reveals that these complexes show two reversible electrochemical processes with separation (ΔE1/2) ~0,60 V, which is indicative of strong interaction between metallic centers. Complex with formula [Ru2Cl4(CO)(dppb)(P)2] and [Ru2Cl4(N-het.)(dppb)2] were synthesized and characterized. Some of the compounds synthesized were tested in reactions of imines hydrogenation, and some showed great activity. Complexes of the type [RuCl2(dppb)(N-N)] and [RuCl2(dppb)(N)2] were used for the acetophenone reduction using hydrogen-transfer reactions, conversions were satisfactory due to the conditions has not been optimized. Besides the aqua complex mer-[RuCl3(dppb)H2O] was also efficient to in situ generates active species. The reactivity of the compound [Ru2Cl4(dppb)3] with CuCl2.2H2O and [NBu4][AuCl4] was tested and the product of these reactions was identified as [Ru2Cl5(dppb)2]. These reactions occurs through oxidation and dimerization of the ruthenium complexes to form the mixed valence complex. The compound [RuCl2(PPh3)3] was reacted with excess of CuCl2.2H2O leading to the formation of [CuCl(PPh3)3] (characterized by RMN 31P{1H}) and the compound [RuCl3(PPh3)2MeOH]MeOH (characterized by RPE), besides these species a yellow solution was obtained and with addition of dppm to this solution the compound [Ru2Cl5(dppm)2] is obtained. X-ray structures for the compounds [Ru2Cl5(dppb)2], [Ru2Cl5(dppm)2],...(Complete abstract click electronic access below)

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Araujo, Márcio Peres de. "Complexos cofaciais de dirutênio contendo haletos em ponte e fosfinas como ligantes : estudos espectrais, eletroquímicos e de reatividade /." Araraquara : [s.n.], 2001. http://hdl.handle.net/11449/105810.

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Orientador: Alzir Azevedo Batista
Banca: Benedito dos Santos Lima Neto
Banca: Edward Ralph Dockal
Banca: Luiz Antonio Andrade de Oliveira
Banca: Wagner Ferraresi de Giovani
Resumo: O complexo mer-[RuCl3(dppb)H2O] foi utilizado como precursor para a síntese de uma série de complexos binucleares de valência mista, estes apresentam fórmula geral [Ru2Cl5(dppb)(P)2] e [Ru2Cl5(dppb)(P-P)] e forma estudados por técnicas eletroquímicas e espectroscópicas. A maior característica destas espécies é que apresentam acoplamento metal-metal, ou seja transferência de elétrons entre seus centros metálicos em função dessa caracterísitica apresentam absorção na região do infravermelho-próximo do espectro eletrônico, além de dois processos eletroquímicos com separação (ΔE1/2) ~0,60 V, indicativo de forte interação entre os centros metálicos. Complexos com fórmula [Ru2Cl4CO(dppb)(P)2] e [Ru2Cl4(N-het.)(dppb)2] foram sintetizados e caracterizados. Alguns dos complexos obtidos foram testados em reações de hidrogenação de iminas, sendo que alguns mostraram grande atividade. Complexos do tipo [RuCl2(dppb)(N-N)] e [RuCl2(dppb)(N)2] foram utilizados para a redução da acetofenona usando transferência de hidrogênio, as conversões alcançadas foram satisfatórias em função das condições não terem sido optimizadas. Além disso o aqua complexo mer-[RuCl3(dppb)H2O] também foi eficiente para gerar in situ espécies catalíticamente ativas. A reatividade do complexo [Ru2Cl4(dppb)3] com CuCl2.2H2O e [NBu4][AuCl4] foi testada e o produto destas reações foi identificado como [Ru2Cl5(dppb)2]. Estas reações ocorrem via oxidação do complexo de rutênio e posterior fomação do complexo de valência mista contendo três cloretos em ponte. O complexo [RuCl2(PPh3)3] também foi oxidado com excesso de CuCl2.2H2O levando a formação de [CuCl(PPh3)3] (caracterizado por RMN 31P{1H}) e do complexo solvato [RuCl3(PPh3)2MeOH]MeOH (caracterizado por RPE), além destas espécies uma solução amarela é obtida e com a adição de dppm a esta solução o complexo...(Resumo completo, clicar acesso eletrônico abaixo)
Abstract: The compound mer-[RuCl3(dppb)H2O] was used as precursor for the synthesis of a wide range of mixed valence complexes and present the general formula [Ru2Cl5(dppb)(P)2] and [Ru2Cl5(dppb)(PP)]. These complexes were studied by electrochemical and spectroscopic techniques. The main characteristic of these species is that they present metal-metal coupling or metal-metal electron transfer due to this electron transfer absorptions in the near infrared region can be observed. Cyclic voltammetry studies reveals that these complexes show two reversible electrochemical processes with separation (ΔE1/2) ~0,60 V, which is indicative of strong interaction between metallic centers. Complex with formula [Ru2Cl4(CO)(dppb)(P)2] and [Ru2Cl4(N-het.)(dppb)2] were synthesized and characterized. Some of the compounds synthesized were tested in reactions of imines hydrogenation, and some showed great activity. Complexes of the type [RuCl2(dppb)(N-N)] and [RuCl2(dppb)(N)2] were used for the acetophenone reduction using hydrogen-transfer reactions, conversions were satisfactory due to the conditions has not been optimized. Besides the aqua complex mer-[RuCl3(dppb)H2O] was also efficient to in situ generates active species. The reactivity of the compound [Ru2Cl4(dppb)3] with CuCl2.2H2O and [NBu4][AuCl4] was tested and the product of these reactions was identified as [Ru2Cl5(dppb)2]. These reactions occurs through oxidation and dimerization of the ruthenium complexes to form the mixed valence complex. The compound [RuCl2(PPh3)3] was reacted with excess of CuCl2.2H2O leading to the formation of [CuCl(PPh3)3] (characterized by RMN 31P{1H}) and the compound [RuCl3(PPh3)2MeOH]MeOH (characterized by RPE), besides these species a yellow solution was obtained and with addition of dppm to this solution the compound [Ru2Cl5(dppm)2] is obtained. X-ray structures for the compounds [Ru2Cl5(dppb)2], [Ru2Cl5(dppm)2],...(Complete abstract click electronic access below)
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Patarroyo, Rengifo Javier Ivan. "Exploring synthetic strategies for the production of complex inorganic nanoparticles." Doctoral thesis, Universitat Autònoma de Barcelona, 2018. http://hdl.handle.net/10803/666652.

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Los nanomateriales han sido un área intrigante de investigación científica en las últimas décadas, dada sus particulares propiedades físico-químicas que los hacen adecuados para aplicaciones en campos como fotonica, catálisis, biomedicina, remediación ambiental, conversión y almacenamiento de energía, sensores, etc. Los avances en nanociencia han estado acompañados por mejoras en las capacidades de suministrar control composicional y morfológico de los materiales. La síntesis de nanoparticulas (NPs), donde la ciencia de materiales se dirige con técnicas de química orgánica, son especialmente desafiantes y a veces difíciles de entender y por lo tanto controlar. Esta dificultad surge por el incremento en la complejidad de los mecanismos de mineralización en los cuales los precursores moleculares son transformados en NPs, junto con su fuerte susceptibilidad a la cinética de reacción. Por lo tanto, la pregunta es cómo correlacionar las transformaciones morfológicas que tienen lugar en las NPs durante su formación con el número de procesos fundamentales solapados y reacciones competitivas que están involucradas. Esta tesis, presenta el desarrollo de metodologías reproducibles para la producción de nanoparticulas sólidas y huecas de metales nobles y de nanoparticulas hibridas de metales nobles-oxidos metálicos (heterodimeros y nanoparticulas tipo core@shell); y además, examinar su comportamiento óptico, quimico y catalítico.
Nanomaterials have been an intriguing area of scientific research over the previous few decades because of their unique physical and chemical properties that make them suitable for applications in fields like photonics, catalysis, biomedicine, environmental remediation, energy conversion and storage, sensors, etc. Advances in nanoscience have been accompanied by improvements in the capabilities to deliver compositional and morphological control of materials. Syntheses of nanoparticles (NPs), where material science elements are addressed with organic chemistry precision techniques, are specially challenging and often difficult to understand, hence to control. This difficulty arises from the increased complexity of the mineralization mechanisms in which molecular precursors are transformed into NPs, along with their strong susceptibility to the reaction kinetics. Therefore, the persisting question is how to correlate the morphological transformations that take place in NPs during their formation with the number of overlapped fundamental processes and competing reactions that are involved. This thesis dissertation present the development of reproducible methodologies for the production of high quality solid and hollow noble metal NPs and hybrid noble metal–metal oxide NPs (heterodimer and core@shell NPs); and, in addition, examine their optical, chemical and catalytic behaviour.

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Clancy, Gerald Patrick. "Synthetic inorganic chemistry : novel metallocenes and inorganic fullerenes." Thesis, University of Oxford, 2000. http://ora.ox.ac.uk/objects/uuid:9c7f7c35-bb8f-4117-8e2e-e56a9fbcbeab.

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This thesis is divided into two parts. The first part concerns the synthesis and characterisation of substituted metallocene complexes of the transition and main group metals. The second part describes the preparation and characterisation of inorganic fullerene (IF)-related materials. Chapter 1 reviews the chemistry of dialkyl- and diaryl-phosphino substituted cyclopentadienyl complexes of the transition metals. Chapter 2 describes the synthesis and characterisation of the new ligands [M(C₅Me₄)CH₂PMe₂] (M = H, Li, Na and K) via the precursors [HC₅Me₄)CH₂PHMe₂][X] (X = Cl and PF₆). The synthesis, characterisation and chemical reactivity of the compounds [Zr{{η-C₅Me₄)CH₂PMe₂}₂Cl₂ and [Mn{η-C₅Me₄)CH₂PMe₂}₂] is reported together with supporting evidence for the synthesis of the bimetallic complex [Zr{U+03B7-C₅Me₄)CH₂PMe₂}₂Cl₂PtI₂] and the complex [Mn{η-C₅Me₄)CH₂PMe₂B(C₆F₅)₃}₂]. Chapter 3 provides a brief introduction into the field of main group metallocenes and describes the synthesis and characterisation of the new main group metallocenes [M{η- C₅H₄)CMe₂PMe₂}₂] (M = Pb and Sn). The B(C₆F₅)_{3 adduct [Pb{η-C₅H₄)CMe₂PMe₂(B(C₆F₅)₃}₂] has also been synthesised. The main group - transition metal bimetallic complex [Pb{η-C₅H₄)CMe₂PMe₂}₂PtI_{2_{in which the substitutedplumbocene acts as a bidentate ligand, has been characterised by mass spectrometry and ³¹P{¹H}NMR spectroscopy. Chapter 4 provides an introduction into the field of IF-related materials and an overview of the analytical techniques used in their characterisation. Chapter 5 describes the preparation and characterisation of IF-MoS₂ and IF-(Nb,W)S₂ materials from MoC and the binary oxides Nb₈ W₉O₄₇ and Nb₄W₁₃O₄₇ respectively. A powder X-ray diffraction study of the conversion of WC to WO_3-X and the subsequent sulfidisation by H₂S to form novel IF-WS₂ morphologies is also described. Chapter 6 describes the preparation of amorphous Group 5 metal (V, Nb and Ta) oxides using the metal vapour synthesis technique. These amorphous precursors have been annealed in a reducing atmosphere to form the oxide phases U+03B1-V₂O₃, NbO₂ and TT-Ta₂O₅ which have been identified by powder X-ray diffraction. Upon reaction with H₂S, the crystalline oxides afford layered sulfides of the form MS₂ (M = V, Nb and Ta), some of which exhibit behaviour typical of IF-like materials and have been characterised by HRTEM, powder X-ray diffraction and EDX analysis. Chapter 7 outlines the experimental details for the synthesis, characterisation, reactions and compounds described in the preceding chapters. Chapter 8 presents the characterising data for the new compounds described in chapters 2 and 3. Appendix A contains details of the crystallographic data for the structurally characterised compound [Mn{η-C₅Me₄)CH_PMe₂}₂].}}}

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Otsuka, Takeshi. "Functionalization of Organic-Inorganic Nano-Hybrids Utilizing Inorganic Nanoparticles." 京都大学 (Kyoto University), 2010. http://hdl.handle.net/2433/126813.

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Vincent, Paul Robert. "Investigation of inorganic materials for the application of inorganic pigments." Thesis, University of Southampton, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.415239.

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Brinza, Daniel L. "Novel inorganic membranes." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 2000. http://www.collectionscanada.ca/obj/s4/f2/dsk1/tape3/PQDD_0019/MQ58444.pdf.

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Ridley, Brent (Brent Alan) 1974. "Printed inorganic transistors." Thesis, Massachusetts Institute of Technology, 2003. http://hdl.handle.net/1721.1/62382.

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Thesis (Ph. D.)--Massachusetts Institute of Technology, School of Architecture and Planning, Program in Media Arts and Sciences, 2003.
Includes bibliographical references (leaves 146-175).
Forty years of exponential growth of semiconductor technology have been predicated on the miniaturization of the transistors that comprise integrated circuits. While complexity has greatly increased within a given area of processed silicon, the cost per area has not decreased. Current fabrication methods are further hindered by high facility costs and environmentally unfriendly processing. Moving to a new means of semiconductor fabrication may drastically reduce both financial and environmental costs. One such approach is based on the extension of printing techniques to the fabrication of electronic devices. Such printed electronics are envisioned to enable applications in flexible displays and electronic paper, personal fabrication, wearable computing, and disposable medical diagnostics. This dissertation focuses on the development of printable materials, specifically inorganic semiconductor inks. At the outset of this research, organic semiconductors were the only materials known and pursued as printable semiconductors. The ability to process organic semiconductors in common organic solvents makes them amenable to a wide range of printing technologies, but their electrical performance is fundamentally limited and their utility is confined to applications in which only low speeds are required. The goal of this thesis was to demonstrate the feasibility of printing inorganic materials, the same materials that are used to fabricate high quality semiconductor devices. Cadmium selenide was studied as a model inorganic semiconductor and silicon was studied because of its commercial dominance. The insolubility and high processing temperatures of inorganic semiconductors, both of which can prevent
(cont.) their use in printed electronics, were overcome through the use of nanoparticle inks. At very small sizes, nanoparticles can be highly soluble in organic solvents and can have a pronounced melting point depression. Leveraging these size-dependent properties, the first semiconductor nanoparticle inks were developed using cadmium selenide and the first all-printed inorganic thin film transistors were demonstrated. Printed active layers in thin film transistors attained a semiconductor mobility of 1 cm²V⁻¹s⁻¹and an ON/OFF ratio in excess of 10⁴. Further development of inorganic nanoparticle inks and efforts to extend this approach to silicon are described, addressing silicon nanoparticle synthesis, purification, and ink formulation.
Brent Ridley.
Ph.D.

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Price, Adam Jacob. "New inorganic catalysts." Thesis, University of Cambridge, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.621059.

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Books on the topic "Inorganik"

Sanderson, R. T. Simple inorganic substances. Malabar, Fla: Krieger Pub. Co., 1989.

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Bertini, Ivano. Inorganic and bio-inorganic chemistry. Oxford: Eolss Publishers, 2009.

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Eldik, Rudi van, and Grazyna Stochel. Advances in inorganic chemistry: Inorganic photochemistry. Amsterdam: Academic Press, 2011.

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1932-, Tarr Donald A., ed. Inorganic chemistry. 3rd ed. Upper Saddle River, N.J: Pearson Education, 2004.

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House, J. E. Inorganic chemistry. Boston: Academic Press, 2008.

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Kaesz, Herbert D. Inorganic syntheses. Edited by Wiley online library. New York: Wiley, 1989.

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Inorganic chemistry. 2nd ed. London: Bios Scientific Publishers, 2004.

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R, Allcock H., and West Robert 1928-, eds. Inorganic polymers. Englewood Cliffs, N.J: Prentice Hall, 1992.

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1932-, Tarr Donald A., ed. Inorganic chemistry. Englewood Cliffs, N.J: Prentice Hall, 1991.

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Inorganic chemistry. Springhouse, Pa: Springhouse Corp., 1993.

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Book chapters on the topic "Inorganik"

Gooch, Jan W. "Inorganic." In Encyclopedic Dictionary of Polymers, 390. New York, NY: Springer New York, 2011. http://dx.doi.org/10.1007/978-1-4419-6247-8_6345.

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Heppner, John B., D. G. Boucias, J. C. Pendland, Andrei Sourakov, Timothy Ebert, Roger Downer, Kun Yan Zhu, et al. "Inorganic." In Encyclopedia of Entomology, 1955. Dordrecht: Springer Netherlands, 2008. http://dx.doi.org/10.1007/978-1-4020-6359-6_1532.

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Peresypkina, Eugenia, Claudia Heindl, Alexander Virovets, and Manfred Scheer. "Inorganic Superspheres." In Clusters – Contemporary Insight in Structure and Bonding, 321–73. Cham: Springer International Publishing, 2016. http://dx.doi.org/10.1007/430_2016_2.

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Willey, Neil. "Inorganic Toxins." In Environmental Plant Physiology, 279–304. New York, NY : Garland Science, 2016.: Garland Science, 2018. http://dx.doi.org/10.1201/9781317206231-12.

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Fresenius, Wilhelm, Karl Ernst Quentin, and Wilhelm Schneider. "Inorganic Parameters." In Water Analysis, 195–476. Berlin, Heidelberg: Springer Berlin Heidelberg, 1988. http://dx.doi.org/10.1007/978-3-642-72610-1_3.

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Gooch, Jan W. "Inorganic Coatings." In Encyclopedic Dictionary of Polymers, 390. New York, NY: Springer New York, 2011. http://dx.doi.org/10.1007/978-1-4419-6247-8_6346.

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Gooch, Jan W. "Inorganic Fibers." In Encyclopedic Dictionary of Polymers, 390. New York, NY: Springer New York, 2011. http://dx.doi.org/10.1007/978-1-4419-6247-8_6347.

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Gooch, Jan W. "Inorganic Pigments." In Encyclopedic Dictionary of Polymers, 390. New York, NY: Springer New York, 2011. http://dx.doi.org/10.1007/978-1-4419-6247-8_6348.

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Gooch, Jan W. "Inorganic Polymer." In Encyclopedic Dictionary of Polymers, 390. New York, NY: Springer New York, 2011. http://dx.doi.org/10.1007/978-1-4419-6247-8_6349.

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van der Put, Paul J. "Inorganic Molecules." In The Inorganic Chemistry of Materials, 87–110. Boston, MA: Springer US, 1998. http://dx.doi.org/10.1007/978-1-4899-0095-1_3.

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Conference papers on the topic "Inorganik"

Green, Martin A. "Inorganic nanophotovoltaics." In NOBEL SYMPOSIUM 153: NANOSCALE ENERGY CONVERTERS. AIP, 2013. http://dx.doi.org/10.1063/1.4794699.

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Yee, Shannon K., Nelson Coates, Jeffrey J. Urban, Arun Majumdar, and Rachel A. Segalman. "A High-Performance Solution-Processable Hybrid Thermoelectric Material." In ASME 2012 Third International Conference on Micro/Nanoscale Heat and Mass Transfer. American Society of Mechanical Engineers, 2012. http://dx.doi.org/10.1115/mnhmt2012-75002.

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Thermoelectrics have the potential to become an alternative power source for distributed electrical generation as they could provide co-generation anywhere thermal gradients exist. More recent material and manufacturing advances have further suggested that thermoelectrics could independently generate primary power [1]. However, due to cost, manufacturability, abundance, and material performance, the full potential of thermoelectrics has yet to be realized. In the last decade, thermoelectric material improvements have largely been realized by diminishing thermal conductivities via nanostructuring without sacrificing performance in electrical transport [2]. An alternative approach is to decouple and optimize the electrical conductivity and thermopower using the unique properties of organic-inorganic interfaces [3]. One method to do this could leverage the electrical properties of a conducting polymer in combination with the thermoelectric proprieties of an inorganic semiconductor in such a way that the interaction between these materials breaks mixture theory. Furthermore, it is expected that the thermal conductivity of this hybrid material would be low due to the inherent vibration mode mismatch between polymers and inorganics. Previously, we have developed a method for producing a solution-processable thermoelectric material suitable for thin film applications using a hybrid polymer-inorganic systems consisting of crystalline tellurium nanowires coated in a thin layer of a conducting polymer (i.e., PEDOT:PSS) [4]. The interfacial properties could be realized in bulk and films demonstrate enhanced transport properties beyond those of either component. More recently, we have been able to significantly improve the thermoelectric properties of these materials by morphological and chemical modifications. Here, we present our methodology and experimental transport properties of this new material where the thermal conductivity, electrical conductivity, and thermopower predictably vary as a function of composition, size, and the structural conformation caused by the solvent. The mechanism for these improvements is currently under investigation, but experimental results suggest that transport is dominated by interfacial phenomena. Furthermore, experiments suggest that both the electrical conductivity and thermopower can be independently increased without appreciably increasing the thermal conductivity. These improvements, in concert with the solution processable nature of this material, make it ideal for new thermoelectric applications.

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Truong, Vo-Van. "Inorganic ion conductors." In Institutes for Advanced Optical Technologies, edited by Carl M. Lampert and Claes-Göran Granqvist. SPIE, 1990. http://dx.doi.org/10.1117/12.2283628.

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Neuroth, Norbert. "Inorganic optical glasses." In Critical Review Collection. SPIE, 1996. http://dx.doi.org/10.1117/12.245186.

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Araujo, Roger. "Inorganic photosensitive materials." In Critical Review Collection. SPIE, 1996. http://dx.doi.org/10.1117/12.245194.

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Kutal, Charles, Bentley J. Palmer, and Zhikai Wang. "Novel inorganic photoinitiators." In SPIE's 1995 Symposium on Microlithography, edited by Robert D. Allen. SPIE, 1995. http://dx.doi.org/10.1117/12.210372.

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Goncalves, Rogeria R., Giovanni Carturan, Sergio Scarpari, D. C. Oliveira, Luciano A. Bueno, Sidney J. L. Ribeiro, Younes Messaddeq, et al. "Inorganic nanoparticles in organic-inorganic hybrid hosts for planar waveguides." In International Symposium on Optical Science and Technology, edited by Robert A. Norwood. SPIE, 2002. http://dx.doi.org/10.1117/12.456538.

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Kasikov, Aarne. "LaF3 as a high-index material in VUV." In Optical Organic and Inorganic Materials. SPIE, 2001. http://dx.doi.org/10.1117/12.496649.

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Scurtul, K. D. "Thin films of EuO-CeO2 semiconductor system." In Optical Organic and Inorganic Materials. SPIE, 2001. http://dx.doi.org/10.1117/12.425480.

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Juska, Gytas. "Transport features of photogenerated and equilibrium charge carriers in thin PPV polymer layers." In Optical Organic and Inorganic Materials. SPIE, 2001. http://dx.doi.org/10.1117/12.425484.

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Reports on the topic "Inorganik"

Benson, S., P. Sweeny, H. Abrahamson, L. Radonovich, C. Zygarlicke, W. Puffe, and M. Maldonado. Combustion inorganic transformations. Office of Scientific and Technical Information (OSTI), April 1988. http://dx.doi.org/10.2172/6959295.

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Phillips, M. L. F., P. I. Pohl, and C. J. Brinker. Selective inorganic thin films. Office of Scientific and Technical Information (OSTI), April 1997. http://dx.doi.org/10.2172/494134.

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Collord, Andrew, David J. Kissel, C. Jeffrey Brinker, Christopher Alan Apblett, and Eric D. Branson. Polymer/inorganic superhydrophobic surfaces. Office of Scientific and Technical Information (OSTI), September 2009. http://dx.doi.org/10.2172/1001016.

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Fain, D. E. (Advances in inorganic membranes). Office of Scientific and Technical Information (OSTI), January 1989. http://dx.doi.org/10.2172/5118694.

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Phillips, M. L. F., L. A. Weisenbach, and M. T. Anderson. Selective inorganic thin films. Office of Scientific and Technical Information (OSTI), May 1995. http://dx.doi.org/10.2172/105137.

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Neilson, Robert H. New Inorganic Polymer Systems. Fort Belvoir, VA: Defense Technical Information Center, February 1991. http://dx.doi.org/10.21236/ada232447.

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Stone, M. L. Inorganic polymer engineering materials. Office of Scientific and Technical Information (OSTI), June 1993. http://dx.doi.org/10.2172/10134395.

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Egan, B. Z., S. P. N. Singh, D. E. Fain, G. E. Roettger, and D. E. White. Gas separations using inorganic membranes. Office of Scientific and Technical Information (OSTI), April 1992. http://dx.doi.org/10.2172/10150064.

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Thomas, George Harrison. Alkoxide routes to Inorganic Materials. Office of Scientific and Technical Information (OSTI), December 2007. http://dx.doi.org/10.2172/971209.

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Reports on the topic "Inorganik"