Relevant bibliographies by topics / IR-NMR spectroscopy

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  1. Journal articles

Academic literature on the topic 'IR-NMR spectroscopy'

Author: Grafiati
Published: 4 June 2021
Last updated: 6 February 2022

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Journal articles on the topic "IR-NMR spectroscopy"

1

Bashta, Bogdana, Volodymyr Donchak, Marta Plonska-Brzezinskа, Olena Astakhova, and Michael Bratychak. "Investigation of Functional Carboxy-Containing Oligomers by IR and NMR Spectroscopy." Chemistry & Chemical Technology 10, no. 2 (2016): 125–34. http://dx.doi.org/10.23939/chcht10.02.125.

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New functional oligomers have been synthesized via intereaction of epoxy oligomers with carboxylic ones or with dibasic carboxy acids. In some cases synthesis was accompanied by ROP-polymerization of DGEBA, initiated by carboxylic oligomer. The structure of obtained products was investigated by IR, 1Н and 13C NMR spectroscopy.
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2

Zubyk, Halyna, Marta Plonska-Brzezinska, Olena Shyshchak, Olena Astakhova, and Michael Bratychak. "Study of Phenol-Formaldehyde Oligomers Derivatives Structure by IR- and NMR-Spectroscopy." Chemistry & Chemical Technology 9, no. 4 (2015): 435–43. http://dx.doi.org/10.23939/chcht09.04.435.

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3

Pelzer, Stefanie, Beate Neumann, Hans-Georg Stammler, Nikolai Ignat’ev, Reint Eujen, and Berthold Hoge. "Synthesis and Characterization of Tetrakis(pentafluoroethyl)germane." Synthesis 49, no. 11 (2017): 2389–93. http://dx.doi.org/10.1055/s-0036-1589005.

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This paper describes the synthesis and comprehensive characterization of tetrakis(pentafluoroethyl)germane. In addition to a complete NMR spectroscopic characterization, including the rarely used 73Ge NMR spectroscopy, Ge(C2F5)4 was studied by IR spectroscopy, mass spectrometry as well as X-ray diffraction analysis. A 73Ge NMR investigation as well as an X-ray diffraction study of the related germane Ge(CF3)4 are also included.
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4

Bakhmutov, Vladimir I., Ekaterina V. Bakhmutova, Natalia V. Belkova, et al. "In-depth NMR and IR study of the proton transfer equilibrium between [{(MeC(CH2PPh2)3}Ru(CO)H2] and hexafluoroisopropanol." Canadian Journal of Chemistry 79, no. 5-6 (2001): 479–89. http://dx.doi.org/10.1139/v00-196.

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The (carbonyl)dihydride complex [(triphos)Ru(CO)H2] (2) has been synthesized by reaction of the ruthenate [(triphos)RuH3]K (triphos = MeC(CH2PPh2)3) with ethanol saturated with CO. A single crystal X-ray analysis and IR and NMR experiments have shown that 2 adopts in both the solid state and solution an octahedral coordination geometry with a facial triphos ligand, two cis terminal hydrides, and a terminal carbonyl. The reaction of hexafluoro-2-propanol (HFIP) with 2 has been studied in CH2Cl2 solution by IR and NMR spectroscopy. The proton donor interacts with a terminal hydride of 2 forming
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5

Shah, A. M., and A. J. Rojivadiya. "Synthesis and Characterization of Imidazo[1,2-a]Pyrimidine." International Letters of Chemistry, Physics and Astronomy 52 (June 2015): 1–4. http://dx.doi.org/10.18052/www.scipress.com/ilcpa.52.1.

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An efficient protocol for the synthesis of imidazo [1,2-a] pyrimidine was developed by using three component one-pot Biginelli synthesis. The synthesized compounds were characterized by spectroscopic techniques like FT-IR, 1H NMR, 13C NMR, and mass spectroscopy.
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6

Bonjour, Jessica L., Alisa L. Hass, David W. Pollock, Aaron Huebner, and John A. Frost. "Bringing NMR and IR Spectroscopy to High Schools." Journal of Chemical Education 94, no. 1 (2016): 38–43. http://dx.doi.org/10.1021/acs.jchemed.6b00406.

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7

Shah, A. M., and A. J. Rojivadiya. "An Expeditious Synthesis of 1,2,4-Triazolo[1,5-a]Pyrimidine." International Letters of Chemistry, Physics and Astronomy 51 (May 2015): 1–4. http://dx.doi.org/10.18052/www.scipress.com/ilcpa.51.1.

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A simple, efficient, and diversity oriented synthesis of library of 1,2,4-triazolo [1,5-a] pyrimidine was undertaken using 5-amino,1,2,4-triazole as a building block. The synthesized analogues were fully characterized by known spectroscopic techniques like FT-IR, 1H NMR, 13C NMR, and mass spectroscopy.
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8

Lin, Whei Oh, Maria C. B. V. de Souza, and Helmut G. Alt. "Synthesis, Characterization and Complexation Studies with K + and Ca2+ Cations of trans-1.2-Cyclohexanedioxydiacetamides." Zeitschrift für Naturforschung B 43, no. 2 (1988): 165–70. http://dx.doi.org/10.1515/znb-1988-0206.

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The synthesis of trans-1.2-cyclohexanedioxydiacetamides starting with trans-1.2-cyclohexane-diol is described. Eleven of these compounds are characterized by IR, 1H NMR, 13C NMR and mass spectroscopy as well as elemental analyses. Most of these compounds are suitable ionophors for the cations K+ and Ca2+. The coordination sites of these ligands in the 1:2 complexes were determined by IR and NMR spectroscopy
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9

Nyquist, R. A., and G. L. Jewett. "IR and NMR Correlations for Alkyl Isocyanates." Applied Spectroscopy 46, no. 5 (1992): 841–42. http://dx.doi.org/10.1366/0003702924124790.

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Correlations are presented for υasym.NCO vs. δ(13C) for NCO, δ13C for NCO vs. the number of protons on the alkyl α-carbon atom, and υasym.NCO vs. the number of protons on the alkyl α-carbon atom for alkyl isocyanates. Correlations such as these are useful in the elucidation of unknown molecular structures containing the isocyanate group.
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10

Rana, Fazale R., Alan J. Mautone, and Richard A. Dluhy. "Combined Infrared and 31P NMR Spectroscopic Method for Determining the Fractional Composition in Langmuir-Blodgett Films of Binary Phospholipid Mixtures." Applied Spectroscopy 47, no. 7 (1993): 1015–23. http://dx.doi.org/10.1366/0003702934415318.

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A method has been developed to determine the exact fractional composition of binary mixtures of phospholipids at the air/water (A/W) interface by infrared spectroscopy in combination with 31P NMR spectroscopy and Langmuir-Blodgett surface chemistry. This procedure utilizes the wavenumber shift observed upon the synthetic replacement of hydrogen with deuterium in the lipid acyl chains to separate the vibrational bands due to each component in mixtures of deuterated and normally proteated lipids. Classical Langmuir-Blodgett monolayer transfer techniques are used to transfer the binary lipid mixt
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