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Journal articles on the topic 'Kristallstrukturbestimmung'

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Published: 4 June 2021

Last updated: 5 February 2022

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1

Burger, Harald, Karl Hensen, and Peter Pickel. "Kristallstrukturbestimmung von N-Trimethylsily-N?-methylimidazoliumbromid." Zeitschrift f�r anorganische und allgemeine Chemie 617, no. 11 (November 1992): 93–95. http://dx.doi.org/10.1002/zaac.19926170115.

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2

Henseler, Ulrich, and Martin Jansen. "Modifizierte Darstellung und Kristallstrukturbestimmung von ?-Na2CS3." Zeitschrift f�r anorganische und allgemeine Chemie 619, no. 7 (July 1993): 1203–8. http://dx.doi.org/10.1002/zaac.19936190709.

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3

Johrendt, D., and A. Mewis. "Er3Pd7P4 ? Kristallstrukturbestimmung und Extended H�ckel Rechnungen." Zeitschrift f�r anorganische und allgemeine Chemie 620, no. 3 (March 1994): 561–65. http://dx.doi.org/10.1002/zaac.19946200329.

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4

Kraft, Thorsten, and Martin Jansen. "Reindarstellung, Kristallz�chtung und Kristallstrukturbestimmung von Iodtrioxid." Zeitschrift f�r anorganische und allgemeine Chemie 622, no. 1 (January 1996): 167–72. http://dx.doi.org/10.1002/zaac.19966220124.

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5

Burger, Harald, Karl Hensen, and Peter Pickel. "Synthese und Kristallstrukturbestimmung von Dimethyldi-(N-Methylimidazolium)siliciumbromid." Zeitschrift f�r anorganische und allgemeine Chemie 621, no. 1 (January 1995): 101–4. http://dx.doi.org/10.1002/zaac.19956210118.

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6

Irran, Elisabeth, and Lars von Chrzanowski. "Synthese und Kristallstrukturbestimmung der Trithionate Rb2S3O6 und Cs2S3O6." Zeitschrift für anorganische und allgemeine Chemie 630, no. 11 (September 2004): 1731. http://dx.doi.org/10.1002/zaac.200470077.

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7

Pertlik, Franz, and Reza Zahiri. "Rhodonit mit geringem Kalziumgehalt: Kristallstrukturbestimmung und kristallchemische Berechnungen." Monatshefte fuer Chemie/Chemical Monthly 130, no. 2 (1999): 257. http://dx.doi.org/10.1007/s007060050185.

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8

Tobias, K. M., and M. Jansen. "Untersuchungen an festem Dichlorhexoxid: Erste Kristallstrukturbestimmung an einem Chloroxid." Zeitschrift f�r anorganische und allgemeine Chemie 550, no. 7 (July 1987): 16–26. http://dx.doi.org/10.1002/zaac.19875500703.

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9

Frank, Walter. "Kristallstrukturbestimmung praxisorientiert: Kristallstrukturbestimmung (Reihe: Teubner Studienbücher Chemie). Von W. Massa. Teubner, Stuttgart, 1994. 262 S., Broschur, 32,80 DM. ISBN 3-519-03527-8." Nachrichten aus Chemie, Technik und Laboratorium 43, no. 6 (June 1995): 705–6. http://dx.doi.org/10.1002/nadc.19950430623.

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10

Würthwein, Ernst-Ulrich, Rainer Kupfer, Stefan Meier, Magda Krestel, and Rudolf Allmann. "Zur Struktur vonN-Methylencarbamidsäureestern: Kristallstrukturbestimmung, spektroskopische Untersuchung und quantenmechanische Berechnungen." Chemische Berichte 121, no. 4 (April 1988): 591–96. http://dx.doi.org/10.1002/cber.19881210403.

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11

Müller, Ulrich, Sergei Ivlev, Stephan Schulz, and Christoph Wölper. "Die Fallen der automatisierten Kristallstrukturbestimmung: Korrektur der Kristallstrukturen von Iodazid." Angewandte Chemie 133, no. 32 (June 29, 2021): 17592–94. http://dx.doi.org/10.1002/ange.202105666.

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12

Würthwein, Ernst-Ulrich, Rainer Kupfer, Stefan Meier, Magda Krestel, and Rudolf Allmann. "Zur Struktur vonN-(Dialkoxymethylen)carbonsäureamiden: Kristallstrukturbestimmung, quantenmechanische Berechnungen und spektroskopische Untersuchungen." Chemische Berichte 121, no. 5 (May 1988): 991–98. http://dx.doi.org/10.1002/cber.19881210525.

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13

Schultz-Coulon, Verena, Elisabeth Irran, Bernd Putz, and Wolfgang Schnick. "β-SrNH und β-SrND - Synthese und Kristallstrukturbestimmung mittels Röntgen- und Neutronenbeugung an Pulvern." Zeitschrift für anorganische und allgemeine Chemie 625, no. 7 (July 1999): 1086–92. http://dx.doi.org/10.1002/(sici)1521-3749(199907)625:7<1086::aid-zaac1086>3.0.co;2-b.

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14

Röhr, Caroline. "Werner Massa: Kristallstrukturbestimmung. Teubner-Verlag, Stuttgart, ISBN: 3-5 19-13527-2, DM 32,80." Berichte der Bunsengesellschaft für physikalische Chemie 101, no. 3 (March 1997): 640–41. http://dx.doi.org/10.1002/bbpc.19971010344.

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15

Fritsch, Gerrit, Gerwalt Zinner, Dietrich Mootz, Marianne Scherf, and Hartmut Wunderlich. "Neue Untersuchungen auf dem Gebiet des 1,5-Diazabicyclo[3.3.0]octan-2,4,6,8-tetrons einschließlich Kristallstrukturbestimmung der unsubstituierten Stammverbindung." Archiv der Pharmazie 319, no. 7 (1986): 646–54. http://dx.doi.org/10.1002/ardp.19863190714.

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16

Karau, Friedrich, and Wolfgang Schnick. "Synthese von Cadmiumnitrid Cd3N2 durch thermischen Abbau von Cadmiumazid Cd(N3)2 und Kristallstrukturbestimmung aus Röntgen-Pulverbeugungsdaten." Zeitschrift für anorganische und allgemeine Chemie 633, no. 2 (February 2007): 223–26. http://dx.doi.org/10.1002/zaac.200600253.

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17

Schmidt, R. E., and D. Babel. "Strukturen caesiumhaltiger Fluoride. VIII. Cs7Ni4F15 und Cs7Co4F15: Die Kristallstrukturbestimmung an den bisher caesiumreichsten Verbindungen in den zugeh�rigen Systemen CsF/MF2." Zeitschrift f�r anorganische und allgemeine Chemie 529, no. 10 (October 1985): 118–28. http://dx.doi.org/10.1002/zaac.19855291016.

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18

Nuss, Hanne, and Martin Jansen. "Synthese und Kristallstrukturbestimmung von Cs([18]Krone-6)Au · 8NH3/ Synthesis and Crystal Structure Determination of Cs([18]crown-6)Au· 8NH3." Zeitschrift für Naturforschung B 61, no. 10 (October 1, 2006): 1205–8. http://dx.doi.org/10.1515/znb-2006-1003.

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Cs([18]crown-6)Au ・ 8NH3 was synthesized from CsAu and [18]crown-6 in liquid ammonia. The extremely air- and temperature-sensitive colorless, block-shaped crystals were analyzed by single crystal X-ray diffractometry. The compound forms triclinic crystals of space group P1 (no. 1) with a = 8.765(2), b = 11.186(2), c = 13.997(3) Å , α = 86.180(6), β = 89.669(6), γ = 83.774(6)°, V = 1361.2(4) Å3. The crystal structure consists of ammonia nets extending perpendicular to [110] in which the Cs([18]crown-6) fragments and the auride anions are embedded

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19

Hensena, Karl, Markus Kettner, Thorsten Stumpf, and Michael Bolte. "Synthese und Kristallstrukturbestimmung von Silicium-Komplexen der Koordinationszahl sechs mit Dimethylpyridinen/ Syntheses and Crystal Structure Determination of Hexacoordinated Silicon-Complexes with Dimethylpyridines." Zeitschrift für Naturforschung B 55, no. 10 (October 1, 2000): 901–6. http://dx.doi.org/10.1515/znb-2000-1003.

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Abstract Trichlorosilane, HSiCl3, forms with 3,4-dimethylpyridine in aprotic solvents a crystalline l:2-compound which is stable at room temperature and readily soluble in CHCl3. Colourless crystals of the dicationic complex, [H2Si(3,4-dimethylpyridine)4]2+ 2Cl- · 6 CHCl3 (verified by X-ray structure analysis) are obtained by dismutation of HSiCl3(3,4-dimethylpyridine)2 in CHCl3 within one week at room temperature.29Si NM R indicates that SiCl4 is generated as a second product. H2SiCl2 with 2,4-dimethylpyridine as well as MeHSiBr2 with 3,5-dimethylpyridine in aprotic solvents form 1:2-compounds stable at room temperature. X-ray structure analyses in both cases establish neutral-complexes with a hexa-coordinated silicon atom

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20

Angermund, Klaus. "Gutes Studienbuch: Kristallstrukturbestimmung. 2., überarb. Aufl. Von W. Massa. Teubner, Stuttgart, 1996. 262 S., brosch., 34,- DM. ISBN 3-519-13527-2." Nachrichten aus Chemie, Technik und Laboratorium 45, no. 11 (November 1997): 1109–14. http://dx.doi.org/10.1002/nadc.199700037.

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21

Hensen, Karl, Frank Gebhardta, and Michael Bolteb. "Synthese und Kristallstrukturbestimmung von Additionsverbindungen aus Alkyldimethylbromsilanen und N-Trimethylsilylimidazol/Syntheses and Crystal Structure Determination of Addition Compounds of Alkyldimethylbromosilanes and N-Trimethylsilylimidazole." Zeitschrift für Naturforschung B 52, no. 12 (December 1, 1997): 1491–96. http://dx.doi.org/10.1515/znb-1997-1209.

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Abstract The bromosilanes RMe2SiBr (R = Me, Et, n-Pr and i-Pr) form ionic 1:1-compounds with N-trimethylsilylimidazole (NTMSI), stable at room temperature. Crystals of the compounds with R = Et, n-Pr and i-Pr are obtained by sublimation. From the product of the reaction of 1,1-dibromosilacyclopentane with NTMSI single crystals of N,N′-bis(trimethylsilyl)imidazolium-bromide (R = Me) were obtained. In the new adducts both silicon atoms are tetracoordinated.

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22

Sichla, Th, F. Altorfer, D. Hohlwein, K. Reimann, M. Steube, J. Wrzesinski, and H. Jacobs. "Kristallstrukturbestimmung an einer Strontium-hydrid-imid-nitrid-Phase - Sr2(H)N/SrNH bzw. Sr2(D)N/SrND - mit R�ntgen-, Neutronen- und Synchrotron-Strahlung." Zeitschrift f�r anorganische und allgemeine Chemie 623, no. 1-6 (1997): 414–22. http://dx.doi.org/10.1002/zaac.19976230166.

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23

Burger, Harald, Karl Hensen, and Peter Pickel. "Aluminiumbromid-Pyridiniumbromid-Verbindung: Kristallstruktur Kristallstrukturbestimmung von [Tris(pyridinium)bromid]bis(tetrabromoaluminat(III))/ Aluminiumbromide-Pyridiniumbromide Compounds: Crystal Structure Crystal Structure Determination of [Tris(pyridinium)bromide]bis(tetrabromoaluminate(III))." Zeitschrift für Naturforschung B 43, no. 8 (August 1, 1988): 963–65. http://dx.doi.org/10.1515/znb-1988-0809.

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AbstractThe compound [(PyH)3Br][AlBr4]2 is formed by melting stoichiometric amounts of AlBr/PyHBr in a ratio of 2:3. It crystallizes in the orthorhombic space group Pbca with lattice constants a = 1365.5(2), b = 1616.0(2), c = 2783.7(3) pm, Z = 8, Dc = 2.21 g/cm3. The structure was solved from 2810 diffractometer measured intensities (Cu -Kα radiation) and refined to Rw (F) = 0.071. The cation shows three pyridinium ions attached via N - H - Br hydrogen bonds to a central bromide ion. The N - Br distances are 321(1), 321(2) and 332(2) pm.

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24

Peschel, B., M. Molinier, and D. Babel. "Kristallstrukturbestimmungen an vier monoklinen Weberiten Na2MIIMIIIF7 (MII = Fe, Co; MIII = V, Cr)." Zeitschrift f�r anorganische und allgemeine Chemie 621, no. 9 (September 1995): 1573–81. http://dx.doi.org/10.1002/zaac.19956210923.

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25

Megges, Klaus, Evgeni V. Avtomonov, and Jörg Lorberth. "Darstellung und Kristallstrukturbestimmung von 1,2-Di-t-butyl-1,2-diiodo- diarsan (t-C4H9AsI)2 und Synthese von 1,2,3,4-Tetrakis(t-butyl)tetraarsetan (t-C4H9As)4 über selektive Reduktion von t-Butylarsendiiodid t-C4H9AsI2 Synthesis and Crystal Structure of 1,2-Di-t-butyl-1,2-diiododiarsane (t-C4H9AsI)2 and Synthesis of 1,2,3,4-Tetrakis(t-butyl)tetraarsetane (t-C4H9As)4 via Selective Reduction of t-Butylarsenic Diiodide t-C4H9AsI2." Zeitschrift für Naturforschung B 52, no. 7 (July 1, 1997): 790–94. http://dx.doi.org/10.1515/znb-1997-0704.

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Abstract 1,2,3,4-Tetrakis(t-butyl)tetraarsetane (t-C4H9As)4(4) has been synthesized by reduction of t-butylarsenic (III) diiodide (1) with equivalent quantities of either Mg, Ca, Zn, Li, or CoCp2 in THF at low temperatures in high yields. Treatment of 1 with CoCp2 in a molar ratio 1:1 in n-pentane at -78 °C leads to the formation of 1,2-di-t-butyl-1,2-diiododiarsine (2) (t-C4H9AsI)2 in 69 % yield. The products have been characterized by spectroscopic methods (H, 13C-NMR, EI-MS) and elemental analyses. The crystal structure of 2 has been determined by X-ray diffraction methods.

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26

Peschel, S., B. Ziegler, M. Schwarten, and D. Babel. "Kristallstrukturbestimmungen an Cs2NaCr(CN)6 und weiteren Verbindungen A2BM(CN)6 (A = Rb, Cs; B = Na, K, Rb, NH4; M = Cr, Mn, Fe, Co): Oktaederkippung und Toleranzfaktor von Cyanokryolithen." Zeitschrift für anorganische und allgemeine Chemie 626, no. 7 (July 2000): 1561–66. http://dx.doi.org/10.1002/1521-3749(200007)626:7<1561::aid-zaac1561>3.0.co;2-j.

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