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Journal articles on the topic 'Kristallzüchtung'

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Published: 4 June 2021

Last updated: 27 January 2023

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1

Müller, G. "Kristallzüchtung." Zeitschrift für Kristallographie 189, no. 1-2 (January 1989): 155–56. http://dx.doi.org/10.1524/zkri.1989.189.1-2.155a.

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2

Hulliger, Jürg. "Chemie und Kristallzüchtung." Angewandte Chemie 106, no. 2 (January 19, 1994): 151–71. http://dx.doi.org/10.1002/ange.19941060204.

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3

Bertram, Rainer. "Zur Bedeutung der chemischen Analyse in der Kristallzüchtung." Zeitschrift für anorganische und allgemeine Chemie 638, no. 10 (August 2012): 1616. http://dx.doi.org/10.1002/zaac.201204100.

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4

Aleksic, Jelena, and Janusz A. Szymczyk. "Experimentelle Oszillatonsanalyse der Grenzflächenströmung bei einer simulierten Czochralski-Kristallzüchtung." PAMM 3, no. 1 (December 2003): 322–23. http://dx.doi.org/10.1002/pamm.200310433.

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5

Bock, Hans, and Sven Holl. "Kristallzüchtung und Strukturbestimmung eines metallorganischen Donator/Akzeptor-Komplexes von I2C=CI2." Zeitschrift für anorganische und allgemeine Chemie 627, no. 8 (August 2001): 1870–76. http://dx.doi.org/10.1002/1521-3749(200108)627:8<1870::aid-zaac1870>3.0.co;2-1.

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6

Kraft, Thorsten, and Martin Jansen. "Zur Existenz des Hexahydroxoperiodonium-Ions — Kristallzüchtung und Strukturanalyse von α- und β-H6IO6HSO4." Chemische Berichte 126, no. 11 (November 1993): 2415–19. http://dx.doi.org/10.1002/cber.19931261112.

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7

Haussühl, S. "K.-Th. Wilke, J. Bohm: Kristallzüchtung, VEB Verlag der deutschen Wissenschaften, Berlin 1988. Preis: DM 198,-." Berichte der Bunsengesellschaft für physikalische Chemie 94, no. 2 (February 1990): 209. http://dx.doi.org/10.1002/bbpc.19900940230.

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8

Bock, Hans, Andreas Rauschenbach, Christian Näther, Markus Kleine, and Zdenek Havlas. "Wechselwirkungen in Molekülkristallen, 111. Kristallzüchtung und Strukturbestimmung von Donator/Akzeptor-Komplexen aus 1,2,4,5-Tetrakis(alkylthio)benzolen und Brom oder Iod." Liebigs Annalen 1996, no. 12 (December 1996): 2185–94. http://dx.doi.org/10.1002/jlac.199619961232.

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9

Glaum, R., H. Thauern, A. Schmidt, and M. Gerk. "Beiträge zum Koordinationsverhalten von Oxidionen in anorganischen Feststoffen. III [1] Mn2P2O7, Mn2P4O12 und Mn2Si(P2O7)2 — Kristallzüchtung, Strukturverfeinerungen und Elektronenspektren von Mangan(II)-Phosphaten." Zeitschrift für anorganische und allgemeine Chemie 628, no. 12 (December 2002): 2800–2808. http://dx.doi.org/10.1002/1521-3749(200212)628:12<2800::aid-zaac2800>3.0.co;2-#.

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10

Kötitz, G. "K.-Th. Wilke, J. Bohm. Kristallzüchtung. VEB Deutscher Verlag der Wissenschaften, Berlin 1988, 641 Abb., 117 Tab., 1088 S., Preis 146,—M, ISBN 3-326-00092-8." Crystal Research and Technology 25, no. 6 (June 1990): 682. http://dx.doi.org/10.1002/crat.2170250613.

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11

Bock, Hans, Andreas Seibe, Mark Sievert, and Zdenek Havlas. "Wechselwirkungen in Molekülkristallen, 155 [1, 2]. Kristallzüchtung und Strukturbestimmung des Radikalkation-Salzes [Tetrahydrotetrathiafulvalenium●⊕] [AlCl4⊖]/Interaction in Molecular Crystals, 155 [1,2]. Crystallization and Structure Determination of the Radicalcation Salt [Tetrahydrotetrathiafulvalenium●⊕][AlCl4⊖]." Zeitschrift für Naturforschung B 55, no. 7 (July 1, 2000): 597–602. http://dx.doi.org/10.1515/znb-2000-0707.

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The dark red tetrahydrotetrathiafulvalenium radical cation has been generated 20 years ago by iodine oxidation of hexathia-dispiro[4.0.4.4]decane and characterized in solution by its temperature-dependent ESR spectrum. Here we report the single crystal growth of its tetrachloroaluminate salt as well as its low temperature structure determination, which proves the C=C double bond to be elongated to 140 pm length and one molecular half to be twisted by 7°. The assumed slight cyanine type distortion is supported by structural comparison with tetrakis(dimethylamino)ethene dication salts and with the 1:3 complex of tetrahydrotetrathiafulvalene mercury dichloride. Unrestricted Density Functional Theory calculations predict both the spin as well as the positive charge to be distributed predominantly within the π molecular center {S2C=CS2}.

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12

Bock, Hans, and Erik Heigel. "Wechselwirkungen in Molekülkristallen, 174 [1, 2]. Kristallzüchtung und Strukturbestimmung verschiedenartig Methyl-substituierter Imidodiphosphorsäuretetraphenylester / Interaction in Molecular Crystals, 174 [1, 2]. Crystal Growth and Structure Determination of Differently Methyl-Substituted Tetraphenyl Imidodiphosphates." Zeitschrift für Naturforschung B 56, no. 6 (June 1, 2001): 469–82. http://dx.doi.org/10.1515/znb-2001-0604.

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Abstract Four differently methyl-substituted tetraphenyl imidodiphosphates [(H3C)nC6H5-n]2PO-NH-PO[C6H5-n(C3)n] (n = 1, 2), i. e. the 4-, 3,4-, 3,5-and 2,3-derivatives, have been crystallized and their structures determined to gain information on the spatial requirements as ligands in the corresponding cesium salts. According to the packing coefficients calculated from the structural data, they increase in the sequence 4<3,5<3,4<2,3. The most perturbed structural motif is the hydrogen bonded, eight-membered of each the dimer subunits.

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13

Meyer, Klaus. "Kristallzüchtung: Von K.-Th. Wilke unter Mitarbeit von J. Bohm; VEB Deutscher Verlag der Wissenschaften, Berlin 1973; 923 Seiten mit 438 Bildern und 145 Tabellen; Format 16,5 × 23 cm, Preis 146, - M, außerhalb der DDR 160, - M." Zeitschrift für Chemie 14, no. 11 (September 1, 2010): 457. http://dx.doi.org/10.1002/zfch.19740141128.

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14

Bock, Hans, Erik Heigel, and Norbert Nagel. "Wechselwirkungen in Molekülkristallen, 156 [1, 2]. Kristallzüchtung und Strukturbestimmung von (Imidodiphosphat)-Alkalisalzen mit Kationen niedriger und hoher Koordinationszahlen / Interaction in Molecular Crystals, 156 [1, 2]. Crystal Growth and Structure Determination of Alkali(imidodiphosphate) Salts with Cations of Low and High Coordination Numbers." Zeitschrift für Naturforschung B 55, no. 9 (September 1, 2000): 773–84. http://dx.doi.org/10.1515/znb-2000-0901.

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Imidodiphosphates ⊖N[PO(OR)2]2 and Imidodiphosphonates ⊖N[POR2]2 are effective chelating ligands for a variety of metal cations including even Na⊕, for which a lipophilically wrapped hexameric polyion cluster has been structurally characterized. The corresponding hexameric lithium and polyrubidium ion complexes reported here exhibit considerable structural differences: The rather small Li⊕ cations of coordination number five and tetraphenylimidodiphosphate form an isolated hexameric aggregate analogous to the Na⊕ one, whereas the larger Rb⊕ with coordination number seven and (3,4-dimethylphenyl)substituents crystallizes as a chain polymer. Based on the crystal structures, the dominant Coulomb attractions between cations and anions, the spatial requirement of the ligands and the essential phenyl/phenyl interactions in their lipophilic skin are discussed

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15

Bock, Hans, Sven Holl, and Volker Krenzel. "Wechselwirkungen in Molekülkristallen, 166 [1, 2]. Polyiod-Moleküle I2C=CI2, (IC)4S, (IC)4NH, (IC)4N-CH3 und HCI3: Strukturbestimmung nach Kristallzüchtung oder durch Dichtefunktionaltheorie-Berechnung / Interaction in Molecular Crystals, 166 [1, 2], Polyiodo Molecules I2C=CI2, (IC)4S, (IC)4 NH, (IC)4N-CH and HCI3: Structure Determination Following Crystallization or by Density Functional Theory Calculation." Zeitschrift für Naturforschung B 56, no. 1 (January 1, 2001): 13–24. http://dx.doi.org/10.1515/znb-2001-0104.

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Abstract The structures of tri-and tetraiodo-substituted carbon compounds are determined either experimentally by X-Ray Structure Analysis or, because crystallization of tetraiodothiophene could not be achieved, approximated by Density Functional Theory optimization of structural data from a donor/acceptor complex. The structures show noteworthy details such as a second polymorph of tetraiodoethene crystallized by sublimation or herringbone crystal packing patterns of tetraiodopyrrole derivatives. All molecular geometries are discussed and compared based on relativistic density functional theory calculations with 6 -31G* basis sets including iodine pseudopotentials. They reproduce even finer structural details due to van der Waals repulsion of the bulky iodo substituents. Natural Bond Orbital (NBO) charge distributions suggest positive partial charges at all iodine centers with the strongest polarization Cδ㊀ → Iδ㊉ in HCI3, which contains well over 97% iodine.

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16

Bock, Hans, and Sven Holl. "Wechselwirkungen in Molekülkristallen, 167 [1, 2]. Kristallzüchtung und Strukturbestimmung von σ-Donator/Akzeptor- Komplexen zwischen 1,4-Dioxan und den Polyiod-Molekülen I2,I2C=CI2, (IC)4S sowie (IC)4NR (R = H, CH3) / Interaction in Molecular Crystals, 167 [1, 2]. C rystallization and Structure Determination of σ -Donor/Acceptor Complexes between 1,4-Dioxane and the Polyiodine Molecules I2,I2C=CI2, (IC)4S and (IC)4NR (R = H, CH3)." Zeitschrift für Naturforschung B 56, no. 2 (February 1, 2001): 111–21. http://dx.doi.org/10.1515/znb-2001-0201.

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Abstract With 1,4-dioxane as the constant donor, five new donor/acceptor complexes with the polyiodine compounds I-I, I2C=CI2, tetraiodothiophene and two tetraiodopyrrole derivatives could be crystallized and their structures determined despite their decomposition in air. They provide interesting facets for selforganisation on crystallization: The 1,4-dioxane addition causes at best small structural changes of the polyiodine compounds. All adducts crystallize in chains of alternating donors and acceptors, which also staple separatedly. The direction of the contacts O···I depends on the incorporation of the 1,4-dioxane molecules into the iodine acceptor layers. The structural results correlate with those obtained for donor/acceptor complexes with organosulfur donors and, therefore, add to the rationalization of intermolecular interactions.

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17

Bock, Hans, Erik Heigel, and Zdenek Havlas. "Wechselwirkungen in Molekülkristallen, 175 [1, 2]. Kristallzüchtung und Strukturbestimmung von {Cäsium-tetraphenylimido- diphosphat}-Aggregaten mit unterschiedlicher lipophiler Umhüllung durch verschiedenartig Methyl-substituierte Phenylringe sowie relativistische DFT-Modellberechnungen zu Cäsium/Cäsium-Wechselwirkungen / Interaction in M olecular Crystals, 175 [1,2]. Crystal Growth and Structure Determination of {Cesium-tetraphenylimidodiphosphate} Aggregates with Differing Lipophilic Wrapping Due to Differently Methyl-Substituted Phenyl Rings, and Relativistic DFT-Model Calculations of Cesium/Cesium Interactions." Zeitschrift für Naturforschung B 56, no. 6 (June 1, 2001): 483–511. http://dx.doi.org/10.1515/znb-2001-0605.

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AbstractIn alkali-tetraphenylimidodiphosphate ion aggregates, the size of the cation determines the curvature of the ligand and, therefore, whether hexameric ellipsoidal clusters or polymeric chains are formed. To further characterize the ligand spatial requirements, the phenyl rings have been methylsubstituted in 4-, 3/5-, 3/4- or 2,3-positions, their conformations structurally analyzed and correlated with the van der Waals substituent profiles. In addition, relativistic density functional theory potential curves have been calculated for the Cs⊕ ··· Cs⊕interactions in simplified model systems.

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18

Bock, Hans, K. Gharagozloo-Hubmann, and M. Sievert. "Wechselwirkungen in Molekülkristallen, 160 [1,2]. Kristallzüchtung und Strukturbestimmung der verschiedenartigen Polyphenyl-Kontaktionenmultipel [p-Quaterphenylee⊖⊖][Na⊕(DME)3]2, [p-Quaterphenyl⊖⊖(Na⊕(THF)3)2] und [p-Terphenyl⊖⊖Na⊕(DME)2Na⊕(DME)]2 / Interaction in Molecular Crystals, 160 [1, 2]. Crystallization and Structure Determination of the Different Polyphenyl Contact Ion Multiples [p-Quaterphenylee⊖⊖][Na⊕(DME)3]2, [p-Quaterphenyl⊖⊖(Na⊕(THF)3)2] und [p-Terphenyl⊖⊖Na⊕(DME)2Na⊕(DME)]2." Zeitschrift für Naturforschung B 55, no. 12 (December 1, 2000): 1103–13. http://dx.doi.org/10.1515/znb-2000-1201.

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The π-hydrocarbons p-terphenyl and p-quaterphenyl are reduced to their dianions in aprotic solutions of different ethers at sodium metal mirrors. Single crystal structure determinations of the solvent-separated or solvens-shared contact ion multiples, [p-terphenyl⊖⊖ Na⊕(DME)2Na⊕DME]2, p-quaterphenyl⊖⊖ ][Na⊕(DME)3]2 and [p-quaterpheny⊖⊖( Na⊕(THF)3)2], prove the essential cation solvation by the chelating dimethoxyethane (DME) versus the bulky tetrahydrofuran (THF) ligands: The solution network of equilibria between solvent separated and solvent shared ion aggregates can be considerably and transparently modified by the ether solvent selected. In addition, the structures of the monomeric sodium salts reveal partly novel details of metal cation coordination by contacts Na⊕ ··· O as well as Na⊕ ··· Cπ such as in the dimeric sodium salt of p-terphenyl dianion, [(DME)2Na⊕ (terphenyl⊖⊖)(Na⊕ DME)(terphenyl⊖⊖)Na⊕ (DME)2].

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19

Rittner, P., and R. Glaum. "Kristallzüchtung und Einkristallstrukturverfeinerungen der Rhodium(III)-phosphate RhPO4 und RhP3O9." Zeitschrift für Kristallographie - Crystalline Materials 209, no. 2 (January 1, 1994). http://dx.doi.org/10.1524/zkri.1994.209.2.162.

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20

Abdelhameed, A. H., G. Angloher, P. Bauer, A. Bento, E. Bertoldo, R. Breier, C. Bucci, et al. "Cryogenic characterization of a $$\hbox {LiAlO}_{2}$$ crystal and new results on spin-dependent dark matter interactions with ordinary matter." European Physical Journal C 80, no. 9 (September 2020). http://dx.doi.org/10.1140/epjc/s10052-020-8329-4.

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AbstractIn this work, a first cryogenic characterization of a scintillating $$\hbox {LiAlO}_{2}$$ LiAlO 2 single crystal is presented. The results achieved show that this material holds great potential as a target for direct dark matter search experiments. Three different detector modules obtained from one crystal grown at the Leibniz-Institut für Kristallzüchtung (IKZ) have been tested to study different properties at cryogenic temperatures. Firstly, two 2.8 g twin crystals were used to build different detector modules which were operated in an above-ground laboratory at the Max Planck Institute for Physics (MPP) in Munich, Germany. The first detector module was used to study the scintillation properties of $$\hbox {LiAlO}_{2}$$ LiAlO 2 at cryogenic temperatures. The second achieved an energy threshold of ($$213.02\pm 1.48$$ 213.02 ± 1.48 ) eV which allows setting a competitive limit on the spin-dependent dark matter particle-proton scattering cross section for dark matter particle masses between $$350\,\hbox {MeV/c}^{2}$$ 350 MeV/c 2 and $$1.50\,\hbox {GeV/c}^{2}$$ 1.50 GeV/c 2 . Secondly, a detector module with a 373 g $$\hbox {LiAlO}_{2}$$ LiAlO 2 crystal as the main absorber was tested in an underground facility at the Laboratori Nazionali del Gran Sasso (LNGS): from this measurement it was possible to determine the radiopurity of the crystal and study the feasibility of using this material as a neutron flux monitor for low-background experiments.

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21

"Referate des Symposiums „Oxidkristalle“ und der Jahrestagung der Deutschen Gesellschaft für Kristallwachstum und Kristallzüchtung vom 17. bis 20. März 1987 in Osnabrück." Zeitschrift für Kristallographie 180, no. 1-4 (January 1987): 1–36. http://dx.doi.org/10.1524/zkri.1987.180.1-4.1.

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22

"Referate der 24. Diskussionstagung der Arbeitsgemeinschaft Kristallographie der Deutschen Mineralogischen Gesellschaft, der Deutschen Physikalischen Gesellschaft, der Gesellschaft Deutscher Chemiker und der 16. Jahrestagung der Deutschen Gesellschaft für Kristallwachstum und Kristallzüchtung (DGKK) zusammen mit der Kontaktgroep Kristalgroei Nederland (KKN), 19. bis 22. März 1985 in Köln." Zeitschrift für Kristallographie - Crystalline Materials 170, no. 1-4 (January 1985): 1–202. http://dx.doi.org/10.1524/zkri.1985.170.14.1.

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