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Journal articles on the topic 'Lawesson´s reagent'

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Published: 4 June 2021

Last updated: 13 February 2022

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1

Preuss, Fritz, and Harald Noichl. "Oxo-und Thiovanadium(V)-Thiolate/Oxo and Thiovanadium(V) Thiolates." Zeitschrift für Naturforschung B 42, no. 2 (1987): 121–29. http://dx.doi.org/10.1515/znb-1987-0201.

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Abstract Syntheses of oxovanadium(V) thiolates such as O = V(SR)3 (R = tC4H9 , SiPh3 ) and O=V(OtC4H9 )n(StC4H9)3-n(n = 1, 2) are described. The thiovanadium(V) compounds S=V(OtC4H9 )3 , S = V(StC4H9)(OtC4H9) 2 and S=V(SSiPh3)3 have been prepared by various methods :substition using Lawesson reagent, oxidation of V(OtC4H9)4 by sulfur, or disproportionation reaction of VCl4 with LiSSiPh3 ; O = V (OSiR3)3 (R = Me , Ph) undergoes a reaction with Lawesson reagent to yield dithiophosphonate complexes. All compounds obtained are characterized by 1H and 51V NMR spectroscopy; the stability of thiovana

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2

Nizamov, Il'yas S., Alexey V. Matseevskii, Elvira S. Batyeva, Irina I. Vandyukova, Boris E. Abalonin, and Roald R. Shagidullin. "REACTIONS OF LAWESSON′S REAGENT WITH ARSENIC (III) ALKOXIDES." Phosphorus, Sulfur, and Silicon and the Related Elements 126, no. 1 (1997): 137–43. http://dx.doi.org/10.1080/10426509708043553.

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3

Aragoni, M. Carla, Massimiliano Arca, Alexander J. Blake, Vito Lippolis, Martin Schroeder, and Claire Wilson. "ChemInform Abstract: 4-Methoxyphenylphosphonic Acid: Reactivity of Lawesson′s Reagent." ChemInform 33, no. 38 (2010): no. http://dx.doi.org/10.1002/chin.200238170.

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4

Osyanin, V. A., E. A. Ivleva, and Yu N. Klimochkin. "ChemInform Abstract: Reactions of 2-Hydroxymethylphenols with Lawesson′s Reagent." ChemInform 43, no. 17 (2012): no. http://dx.doi.org/10.1002/chin.201217186.

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5

Bringmann, Gerhard, Andreas Wuzik, Olaf Schupp, Karl Peters, and Eva-Maria Peters. "1,3-Di-terf-butyl-6H-benzo[b]naphtho[1,2-d]pyran-6-thione, a Severely Helically Distorted Thionolactone-Bridged Biaryl." Zeitschrift für Naturforschung B 52, no. 3 (1997): 355–58. http://dx.doi.org/10.1515/znb-1997-0310.

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Abstract The title compound 2c, a potentially useful synthetic intermediate in stereoselective biaryl synthesis, has been prepared from the oxolactone 1c, by treatment with Lawesson′s reagent. An X-ray structure analysis reveals its strongly helically distorted structure, the overall molecular distortion even slightly exceeding that of the corresponding oxo compound 1c.

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6

He, Liang-Nian, Tian-Bao Huang, Fei Cai, and Ru-W. Chen. "STUDIES ON REACTIONS OF LAWESSON′S REAGENT WITH PHENYLTHIOUREA AND OXAMIDE." Phosphorus, Sulfur, and Silicon and the Related Elements 132, no. 1 (1998): 147–53. http://dx.doi.org/10.1080/10426509808036982.

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7

He, Liangnian, Yanping Luo, Kai Li, et al. "ChemInform Abstract: A Novel Route to Spiro Phosphorus-Heterocycle via Lawesson′s Reagent." ChemInform 33, no. 39 (2010): no. http://dx.doi.org/10.1002/chin.200239174.

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8

Red'kin, V. M., T. A. Stroganova, V. K. Vasilin, and G. D. Krapivin. "ChemInform Abstract: Reaction of Vicinal Thieno[2,3-b]pyridine Aminoamides with Lawesson′s Reagent." ChemInform 44, no. 34 (2013): no. http://dx.doi.org/10.1002/chin.201334181.

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9

Nishio, Takehiko, Norikazu Okuda, Yo-ichi Mori, and Choji Kashima. "Reaction of 3-Hydroxyisoindolin-1-ones with Lawesson Reagent. Synthesis of Isoindoline-1-thiones." Synthesis 1989, no. 05 (1989): 396–97. http://dx.doi.org/10.1055/s-1989-27264.

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10

Shabana, R., L. S. Boulos, and Y. M. Shaker. "ChemInform Abstract: Organophosphorus Compounds. Part 18. The Reaction of Lawesson′s Reagent with Trihydroxy Compounds." ChemInform 30, no. 19 (2010): no. http://dx.doi.org/10.1002/chin.199919187.

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11

Ju, Jingyue, and McKenna Charles E. McKenna Charles E. "ChemInform Abstract: Synthesis of Oligodeoxyribonucleoside Phosphorothioates Using Lawesson′s Reagent for the Sulfur Transfer Step." ChemInform 33, no. 36 (2010): no. http://dx.doi.org/10.1002/chin.200236217.

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12

Slimani, Hosni, та Soufiane Touil. "ChemInform Abstract: Facile Synthesis of β,β′-Diketophosphine Sulfides from Imines and Lawesson′s Reagent." ChemInform 43, № 13 (2012): no. http://dx.doi.org/10.1002/chin.201213203.

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13

He, Liang-Nian, Ren-Xi Zhuo, Ru-Yu Chen, Kai Li, and You-Jie Zhang. "ChemInform Abstract: Synthesis of Biologically Active Phosphorus Heterocycles via Cyclization Reactions of Lawesson′s Reagent." ChemInform 30, no. 27 (2010): no. http://dx.doi.org/10.1002/chin.199927188.

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14

NISHIO, T. "ChemInform Abstract: Sulfur-Containing Heterocycles Derived by the Reaction of Hydroxy- Amides and Lawesson′s Reagent." ChemInform 26, no. 50 (2010): no. http://dx.doi.org/10.1002/chin.199550040.

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15

NISHIO, T. "ChemInform Abstract: Sulfur-Containing Heterocycles Derived by Reaction of ω-Keto Amides with Lawesson′s Reagent." ChemInform 29, № 41 (2010): no. http://dx.doi.org/10.1002/chin.199841041.

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16

Touil, Soufiane, та Aymen Wahbi. "ChemInform Abstract: Reaction of Lawesson′s Reagent with γ-Phosphonyloximes: Synthesis of Novel 1,2,5-Oxazaphospholine Derivatives." ChemInform 46, № 35 (2015): no. http://dx.doi.org/10.1002/chin.201535221.

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17

Shimada, Kazuaki, Keiichi Kodaki, Shigenobu Aoyagi, Yuji Takikawa, and Chizuko Kabuto. "ChemInform Abstract: Formation of Kinetically Stabilized Dithiiranes by Treating Thione S-Oxides Bearing a Bulky Substituent with Lawesson′s Reagent." ChemInform 30, no. 46 (2010): no. http://dx.doi.org/10.1002/chin.199946115.

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18

Kaneko, Kimiyoshi, Hajime Katayama, Toshio Wakabayashi, and Tadahiro Kumonaka. "Pyrimidine Derivatives; 1. The Highly Regioselective 4-Thionation of Pyrimidine-2,4(1H,3H)-dione Derivatives with Lawesson Reagent." Synthesis 1988, no. 02 (1988): 152–54. http://dx.doi.org/10.1055/s-1988-27499.

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19

Polozov, Alexandre M., Sheldon E. Cremer, and Phillip E. Fanwick. "ChemInform Abstract: Stereospecific Thionation of 2-Ethoxy-1,2-oxaphosphorinane 2-Oxide and Its Derivatives with Lawesson′s Reagent." ChemInform 31, no. 2 (2010): no. http://dx.doi.org/10.1002/chin.200002190.

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20

NISHIO, T. "ChemInform Abstract: Reaction of (1,ω)-N-Acylamino Alcohols with Lawesson′s Reagent: Synthesis of Sulfur-Containing Heterocycles." ChemInform 28, № 26 (2010): no. http://dx.doi.org/10.1002/chin.199726161.

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21

Nishio Takehiko, Nishio Takehiko, та Hiroshi Sekiguchi. "ChemInform Abstract: Thionation of ω-Hydroxy Amides with Lawesson′s Reagent: Synthesis of Thioenamides and Sulfur-Containing Heterocycles." ChemInform 30, № 35 (2010): no. http://dx.doi.org/10.1002/chin.199935066.

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22

Gholinejad, Mohammad. "ChemInform Abstract: One-Pot Copper-Catalyzed Thioetherification of Aryl Halides Using Alcohols and Lawesson′s Reagent in Diglyme." ChemInform 46, no. 45 (2015): no. http://dx.doi.org/10.1002/chin.201545099.

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23

Kumar, S. Vijay, G. Parameshwarappa, and H. Ila. "ChemInform Abstract: Synthesis of 2,4,5-Trisubstituted Thiazoles via Lawesson′s Reagent-Mediated Chemoselective Thionation-Cyclization of Functionalized Enamides." ChemInform 44, no. 47 (2013): no. http://dx.doi.org/10.1002/chin.201347126.

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24

OZTURK, T. "ChemInform Abstract: An Unusual Reaction of Lawesson′s Reagent with 1,8-Diketones: A Synthesis of Fused 1,4-Dithiins and Thiophenes." ChemInform 27, no. 32 (2010): no. http://dx.doi.org/10.1002/chin.199632192.

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25

Mohamed, Nadia R., Nahed Y. Khaireldin, Amin F. Fahmy, and Ahmed A. El-Sayed. "ChemInform Abstract: The Utility of Carbon Disulfide and Lawesson′s Reagent for Synthesis of Different Fused Heterocycles for Antimicrobial Evaluation." ChemInform 45, no. 18 (2014): no. http://dx.doi.org/10.1002/chin.201418179.

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26

Nishio, Takehiko, та Mayuko Ori. "ChemInform Abstract: Thionation of ω-Acylamino Ketones with Lawesson′s Reagent: Convenient Synthesis of 1,3-Thiazoles and 4H-1,3-Thiazines." ChemInform 33, № 4 (2010): no. http://dx.doi.org/10.1002/chin.200204069.

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27

MUKAIYAMA, T., K. SAITO, H. KITAGAWA, and N. SHIMOMURA. "ChemInform Abstract: Combined Use of Diphenyltin Sulfide or Lawesson′s Reagent and Silver Perchlorate as Effective Catalyst Systems in Aldol Reaction." ChemInform 25, no. 36 (2010): no. http://dx.doi.org/10.1002/chin.199436051.

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28

YANBORISOV, T. N., N. N. KASIMOVA, O. A. YANBORISOVA, et al. "ChemInform Abstract: Reaction of 3-Aroylmethylene-1,2,3,4-tetrahydroquinoxalin-2-ones with Lawesson′s Reagent and Biological Activity of the Reaction Products." ChemInform 27, no. 30 (2010): no. http://dx.doi.org/10.1002/chin.199630085.

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29

MUKAIYAMA, T., K. WATANABE, and I. SHIINA. "ChemInform Abstract: The Catalytic Diels-Alder Reaction Using Combined Catalyst System of Diphenyltin Sulfide or Lawesson′s Reagent and Silver Perchlorate." ChemInform 26, no. 27 (2010): no. http://dx.doi.org/10.1002/chin.199527065.

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30

Ding, Qiuping, Xianjin Liu, Hongming Wang, Min Chen, and Yiyuan Peng. "ChemInform Abstract: Synthesis of 1,3-Dihydrobenzo[c]thiophene-imines via Tandem Reactions of o-(1-Alkynyl)benzamides and Lawesson′s Reagent." ChemInform 43, no. 27 (2012): no. http://dx.doi.org/10.1002/chin.201227104.

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31

SHABANA, R., E. M. YAKOUT, and S. S. ATREES. "ChemInform Abstract: Studies on Organo-Phosphorus Compounds. Part 14. The Reaction of Visnaginone, Khillinone, and o-Hydroxy-acetophenone with Lawesson′s Reagent." ChemInform 25, no. 10 (2010): no. http://dx.doi.org/10.1002/chin.199410226.

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32

TESTA, M. G., G. PERRINI, U. CHIACCHIO, and A. CORSARO. "ChemInform Abstract: 1,2-Dihydro-2-(4-methoxyphenyl)-2-sulfide-1,3,2-diazaphosphorin-4(3H)- thiones from 3-Aminopropenenitrile Derivatives and Lawesson′s Reagent." ChemInform 25, no. 42 (2010): no. http://dx.doi.org/10.1002/chin.199442194.

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33

Nishio, Takehiko, Yukako Konno, Mayuko Ori, and Masami Sakamoto. "ChemInform Abstract: Stereoselective Synthesis of 4H-5,6-Dihydro-1,3-thiazines by the Reaction of 3-N-Acylamino Alcohols with Lawesson′s Reagent." ChemInform 33, no. 17 (2010): no. http://dx.doi.org/10.1002/chin.200217156.

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34

Ori, Mayuko, and Takehiko Nishio. "ChemInform Abstract: Thionation of N-Acylthreonine and Its Methyl Ester with Lawesson′s Reagent: Synthesis of 5-Oxazolones, 5-Thiazolones and Thiazolines." ChemInform 32, no. 23 (2010): no. http://dx.doi.org/10.1002/chin.200123036.

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35

SHIMOMURA, N., T. MATSUTANI та T. MUKAIYAMA. "ChemInform Abstract: Stereoselective Syntheses of β-D-Ribonucleosides Catalyzed by the Combined Use of Silver Salts and Diphenyltin Sulfide or Lawesson′s Reagent." ChemInform 26, № 17 (2010): no. http://dx.doi.org/10.1002/chin.199517221.

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36

Qiu, Guanyinsheng, Yi Hu, Qiuping Ding, Yiyuan Peng, Xiangzheng Hu, and Jie Wu. "ChemInform Abstract: Synthesis of 4-Methylene-4H-benzo[d][1,3]thiazines via a Tandem Reaction of 1-(2-Alkynylphenyl)ketoximes with Lawesson′s Reagent." ChemInform 42, no. 52 (2011): no. http://dx.doi.org/10.1002/chin.201152173.

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37

Boulos, Leila S., and Hoda A. Abd-El-Malek. "ChemInform Abstract: Action of Lawesson′s Reagent on Substituted 2-Amino-1,4-naphthoquinones: Novel Synthesis of Benzodiphenoquinone-bis-1,3,2-thiazaphospholine-2-sulfide Derivatives (III)." ChemInform 30, no. 51 (2010): no. http://dx.doi.org/10.1002/chin.199951169.

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38

BUTLER, R. N., E. C. MCKENNA, and D. C. GROGAN. "ChemInform Abstract: [1,2,3]Triazolo[4,5-d][1,3,2]thiazaphospholes: A New Fused NPS Ring System from a Cycloaddition-Rearrangement Sequence with Lawesson′s Reagent, a Super Dipolarophile." ChemInform 29, no. 8 (2010): no. http://dx.doi.org/10.1002/chin.199808152.

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39

HE, L. N., R. X. ZHUO, R. Y. CHEN, and J. ZHOU. "ChemInform Abstract: Studies on Organophosphorus Heterocycles. Part 11. A New Route to Cyclic Phospholipid Analogues via Cyclization of Lawesson′s Reagent with Long-Chain 1-Glyceryl Ethers." ChemInform 28, no. 42 (2010): no. http://dx.doi.org/10.1002/chin.199742210.

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40

Kiryanov, Andre A., Paul Sampson, and Alexander J. Seed. "ChemInform Abstract: Synthesis of 2-Alkoxy-Substituted Thiophenes, 1,3-Thiazoles, and Related S-Heterocycles via Lawesson Reagent Mediated Cyclization under Microwave Irradiation: Applications for Liquid Crystal Synthesis." ChemInform 33, no. 17 (2010): no. http://dx.doi.org/10.1002/chin.200217047.

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41

Csomos, Peter, Lajos Fodor, Gabor Bernath, Antal Csampai, and Pal Sohar. "ChemInform Abstract: One-Step Ring-Closure Procedure for 4,5-Dihydro-1,3-thiazino[5,4-b]indole Derivatives with Lawesson′s Reagent. The Fifth Dihydro-1,3-thiazino[b]indole Isomer." ChemInform 43, no. 6 (2012): no. http://dx.doi.org/10.1002/chin.201206172.

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42

Bhowmik, Subhendu, Amita Mishra, and Sanjay Batra. "ChemInform Abstract: Microwave-Assisted One-Pot Synthesis of 2-Aryl-5,6-dihydro-4H-1,3-thiazines via Reaction Between Lawesson′s Reagent and Allyl Arylamides Derived from Morita-Baylis-Hillman Acetates." ChemInform 43, no. 13 (2012): no. http://dx.doi.org/10.1002/chin.201213191.

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43

SHABANA, R., F. H. OSMAN, and S. S. ATREES. "ChemInform Abstract: Organophosphorus Compounds. Part 15. Reaction of 2,4-Bis(4- methoxyphenyl)-1,3,2,4-dithiadiphosphetane-2,4-disulfide (Lawesson′s Reagent) with Aromatic Dihydroxy Compounds. Simple New Route to 1,3,2- Dioxaphospholane-2-sulfide." ChemInform 25, no. 42 (2010): no. http://dx.doi.org/10.1002/chin.199442192.

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44

Bergman, Jan. "Comparison of Two Reagents for Thionations." Synthesis 50, no. 12 (2018): 2323–28. http://dx.doi.org/10.1055/s-0036-1591989.

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Pyridine reacts readily with P4S10 to form a reagent with the composition C10H10N2P2S5 that is useful for thionations of amides. The thionating properties of this reagent are compared with those of Lawesson’s reagent.1 Introduction2 Development of C10H10N2P2S5 3 Use of Thionation for Modification of Biologically Active Compounds3.1 Thionations of Peptides3.2 Thionated Compounds of Interest as Potential Antivirals3.3 Thionations of Thalidomide and Related Molecules4 Comparison of Lawesson’s Reagent and C10H10N2P2S5

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45

Belikov, Mikhail Yu, Sergey V. Fedoseev, Mikhail Yu Ievlev, Oleg V. Ershov, and Victor A. Tafeenko. "ChemInform Abstract: Interaction of 4-Oxoalkane-1,1,2,2-tetracarbonitriles with Lawesson′s Reagent - A New Approach to the Synthesis of 2,2′-Disulfanediylbis(1H-pyrroles) (II). The Synthesis of Photochromic Diarylethene with a Disulfide Bridge (IIf)." ChemInform 46, no. 50 (2015): no. http://dx.doi.org/10.1002/chin.201550122.

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46

Scerba, Michael T., Maxime A. Siegler, and Nigel H. Greig. "Thionation of Aminophthalimide Hindered Carbonyl Groups and Application to the Synthesis of 3,6′-Dithionated Pomalidomides." Synlett 32, no. 09 (2021): 917–22. http://dx.doi.org/10.1055/s-0040-1720460.

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AbstractHerein, we present a new one-pot procedure for the 3,6′-dithionation of pomalidomide derivatives in which the key 3-position sulfur atom is preferentially installed at the desired (but sterically congested) carbonyl of the aminophthalimide system and with regiochemistry distinct from Lawesson’s Reagent thionation methods. When heated in 1,4-dioxane with P4S10–pyridine complex, pomalidomides are smoothly and reproducibly converted into their 3,6′-dithionated analogues in roughly 30% isolated yield and at various scales. While detrimental to the desired 3,6′-type outcome when employing L

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47

Krasavin, Mikhail, Sergey Chuprun, Dmitry Dar’in, Grigory Kantin та Petr Zhmurov. "α-Diazoacetamides in Sc(OTf)3-Catalyzed Tiffeneau–Demjanov Ring Expansion: Application towards the Synthesis of Rare Bicyclic Pyrazoles". Synlett 31, № 04 (2020): 373–77. http://dx.doi.org/10.1055/s-0039-1690047.

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A novel Sc(OTf)3-catalyzed Tiffeneau–Demjanov ring expansion of six-membered cyclic ketones has been developed. The resulting seven-membered cyclic β-keto carboxamides were found to be versatile precursors to rare bicyclic pyrazoles obtained in modest to good yields via condensation with aryl hydrazines in the presence of Lawesson’s reagent.

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48

Woollins, J., Guoxiong Hua, David Cordes, and Alexandra Slawin. "Application of One-Pot Three-Component Condensation Reaction for the Synthesis of New Organophosphorus–Sulfur Macrocycles." Synlett 29, no. 11 (2018): 1496–501. http://dx.doi.org/10.1055/s-0037-1609666.

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An efficient approach has been developed for the synthesis of new phosphorus–sulfur heterocycles by a one-pot three-component condensation reaction of a four-membered-ring thionation reagent [Lawesson’s reagent or its ferrocene analogue (2,4-diferrocenyl-1,3,2,4-diathiadiphosphetane 2,4-disulfide)], an alkane- or arenedithiol, and a dihaloalkane at room temperature in the presence of triethylamine. The simple synthesis method with mild conditions (room temperature and normal reactant concentrations) enhances further the application of the multicomponent reaction in the preparation of novel pho

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49

Soleimani, Ebrahim, Katherine N. Robertson, Cory C. Pye, and Jason A. C. Clyburne. "Homolytic cleavage of Lawesson's reagent: N-heterocyclic carbene complexes of ArPS2 (Ar = 4-CH3O-C6H4)." Dalton Transactions 47, no. 18 (2018): 6299–303. http://dx.doi.org/10.1039/c8dt00457a.

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Lawesson's reagent has been shown to react with the N-heterocyclic carbenes [1,3-bis(2,4,6-trimethylphenyl)imidazol-2-ylidene (IMes) and 1,3-bis(2,6-diisopropylphenyl)imidazolidin-2-ylidene (SIPr)] to give adducts of the general form NHC·P(S)<sub>2</sub>-C<sub>6</sub>H<sub>4</sub>OCH<sub>3</sub>.

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50

Wang, Xian-Liang, Jin-Xiang Chen, Xue-Shun Jia та Liang Yin. "Synthesis of α,β-Unsaturated Phosphine Sulfides". Synthesis 52, № 01 (2019): 141–49. http://dx.doi.org/10.1055/s-0039-1690685.

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α,β-Unsaturated phosphine sulfides may exhibit different reactivity from α,β-unsaturated phosphine oxides toward nucleophilic addition and thus may find new applications in copper(I)-catalyzed asymmetric reactions. Herein, various α,β-unsaturated phosphine sulfides were prepared in moderate to excellent yields from the parent α,β-unsaturated phosphine oxides with Lawesson’s reagent. The reaction enjoys a broad substrate scope and tolerates a variety of functional groups.

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