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Dissertations / Theses on the topic 'Ligand bis-pyridyl'

Author: Grafiati

Published: 4 June 2021

Last updated: 8 February 2022

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1

Sens, Llorca Cristina. "New mono- and dinuclear ruthenium complexes containing the 3,5-bis(2-pyridyl)pyrazole ligand. Synthesis, characterization and applications." Doctoral thesis, Universitat de Girona, 2005. http://hdl.handle.net/10803/8034.

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Se han sintetizado dos nuevos complejos mononucleares de Ru, con formula [RuCl2(Hbpp)(dmso)2], a partir de la reacción entre [RuCl2(dmso)4] y Hbpp (3,5-bis(2-piridil)pirazola). El hecho que sólo tres de los seis posibles estereoisómeros se obtengan a partir de esta reacción, se ha racionalizado en base a factores estructurales y electrónicos. Estos complejos se han caracterizado de forma estructural, espectroscópica y electroquímica. En acetonitrilo en medio básico, el isómero trans,cis-[RuCl2(Hbpp)(dmso)2] da lugar a procesos de isomerización de enlace de un ligando dmso cuando el Ru(II) se o

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2

Elie, Margaux. "Développement de nouveaux complexes organométalliques de métaux de transition polyvalents pour la scintillation et la chimie médicinale." Thesis, Normandie, 2017. http://www.theses.fr/2017NORMC227.

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Deux nouvelles familles de complexes de cuivre(I) cationiques, de formules [Cu(NHC)(N^N)][X] et [Cu(P^P)(N^N)][PF6], ont été synthétisées avec des ligands 2,2’ bis pyridyl pontés, chélates à six chaînons, facilement modulables. Ces complexes présentent des émissions à l’état solide centrées entre 455 et 520 nm (bleu à vert), avec de larges décalages de Stokes et des rendements quantiques pouvant atteindre 0,86. De plus, l’émission via un phénomène de fluorescence retardée activée thermiquement (TADF) a été prouvée pour les complexes [Cu(NHC)(N^N)][X]. Les premiers scintillateurs plastiques dop

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3

Batisai, Eustina. "Preparation and coordination chemistry of bis-pyridyl diamide ligands." Thesis, Stellenbosch : University of Stellenbosch, 2010. http://hdl.handle.net/10019.1/4128.

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Thesis (MSc (Chemistry and Polymer Science))--University of Stellenbosch, 2010.<br>ENGLISH ABSTRACT: The number of coordination complexes utilizing bis-pyridyl diamide ligands has increased significantly over the past decade. This is attributed to the relatively easy synthetic procedure of the ligands and interesting structural features such as helicity, water clusters and porosity that the coordination complexes possess. In the first part of this study, the following eight structurally related bis-pyridyl diamide ligands: • N,N'-bis(pyridin-4-ylmethyl)isophthalamide (ISO); • N,N'-bis(p

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4

Lee, Ting-wai. "Self-assembly and crystal structure analysis of some first-row transition metal coordination polymers of 1,3-bis(4-pyridyl)propane." Hong Kong : University of Hong Kong, 2001. http://sunzi.lib.hku.hk/hkuto/record.jsp?B23242322.

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5

李鼎威 and Ting-wai Lee. "Self-assembly and crystal structure analysis of some first-row transition metal coordination polymers of 1,3-bis(4-pyridyl)propane." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 2001. http://hub.hku.hk/bib/B31224660.

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6

Umuhire, Mahoro Gilbert. "Development of new cationic copper (l) complexes for white light-emitting electrochemical cells." Thesis, Normandie, 2021. http://www.theses.fr/2021NORMC202.

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De nouveaux complexes de cuivre(I) cationiques de formule générale [Cu(P^P)(N^N)][PF6] où P^P représente un ligand bis-phosphine chélatant, bis-[2- (diphenylphosphino)phenyl]ether (DPEPhos) et N^N, des ligands 2,2-bis-pyridyls ont été développés. Les complexes ont montré des émissions à l’état solide couvrant tout le spectre du visible et la présence de la fluorescence retardée activée thermiquement (TADF) a été démontrée. Ces complexes ont été évaluées dans des cellules électrochimiques luminescentes (LECs) et ont conduit aux LECs émettant dans de différentes couleurs, i.e., bleue, verte, jau

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7

Rahmouni, Noureddine. "Synthese et reactivite de complexes dinucleaires des metaux de transition." Université Louis Pasteur (Strasbourg) (1971-2008), 1986. http://www.theses.fr/1986STR13080.

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Synthese de complexes dinucleaires de cu(ii)-dppm, presentant des proprietes magnetiques interessantes et de cu(i)-dppm dont on etudie la structure. Etude particuliere de rh::(2)(dppm)(co)**(2+) et rh(dppm)::(2)(co)::(2)(mu -co)**(2+). Grande reactivite de ce dernier, notamment avec un alcyne terminal phcch dans lequel une activation c-h a lieu pour conduire a un complexe mu -eta -acetylene

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8

Chang, Miao-Ning, and 張妙寧. "Synthesis, Structures and Properties of Divalent Coordination Polymers Containing Bis-pyridyl-bis-amide and Polycarboxylate Ligands: Metal and Ligand Effect." Thesis, 2017. http://ndltd.ncl.edu.tw/handle/249x5s.

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碩士<br>中原大學<br>化學研究所<br>105<br>Ten divalent coordination polymers constructed from polycarboxylic acids and flexible bis-pyridyl-bis-amide ligands with different lengths and donor atom positions, {[Ni(L1)(3,5-PDA)(H2O)3]·2H2O}n (L1 = N,N’-di(3-pyridyl)suberoamide, 3,5-H2PDA = 3,5-pyridinedicarboxylic acid), 1, {[Ni2(L1)2(1,3,5-HBTC)2(H2O)4]·H2O}n (1,3,5-H3BTC = 1,3,5-benzenetricarboxylic acid), 2, {[Ni(L2)(5-tert-IPA)(H2O)2]·2H2O}n (L2 = N,N’-di(3-pyridyl)adipoamide, 5-tert-H2IPA = 5-tert-butylisophthalic acid), 3, [Ni(L3)1.5(5-tert-IPA)]n (L3 = N,N’-di(4-pyridyl)adipoamide), 4, [Co(L1)(1,3,5-H

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9

Yang, Fu-Ming, and 楊富明. "Synthesis of the 2,7-bis(2-pyridyl)-1,8-naphthyridine Ligand and its Palladium Complexes." Thesis, 2010. http://ndltd.ncl.edu.tw/handle/58670136280243761625.

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碩士<br>國立臺灣大學<br>化學研究所<br>99<br>2,7 –Bis(2-pyridyl)-1,8-naphthyridine (bpnp) is a multiple pyridinyl nitrogen donor, which is capable of binding with metal ions in a chelating manner. In case of coordination with two metal ions, these centers are in close distance to have metal-metal interactions, which raises a subject of considerable interest. In our work, we tried to synthesize the dipalladium complex with bpnp. Indeed, we have successfully obtained a palladium complex chelated with bpnp, but in a trimetallic form. The structure of the complex is revealed by X-ray single crystal analysis.

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10

Lan, Yung-Syuan, and 藍詠萱. "Synthesis and Catalytic Application of Dimetal complex with 2,7-bis(2-pyridyl)-1,8-naphthyridine ligand." Thesis, 2012. http://ndltd.ncl.edu.tw/handle/61127016587196660962.

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碩士<br>國立臺灣大學<br>化學研究所<br>100<br>This work involves the coordination study of a pyridinyl ligand 2,7-bis(2-pyridyl)-1,8-naphththyridine (bpnp) with various transition metal ions including Mn, Cu and Pd and catalytic activity of the resulting dicopper complex. Reaction of bpnp with [MnCl2] provided a mononuclear dimmer [{Mn(bpnp)(OMe)Cl2}(μ-Cl)2]. Such a manganese complex could undergo the metal exchange with Cu(II) ions to form a dinuclear species [Cu2(bpnp)(Cl)3(OH)]. Reaction of bpnp with Cu2O provided a dinuclear species [Cu2(bpnp)(HCOO)3(OH)]. These complexes were isolated and characterize

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11

Chang, Yu-An, and 張佑安. "Self-assembly, Structures, and Properties of Metal:Organic Coordination Polymers with Bis-pyridyl Substituted Triazole Ligand." Thesis, 2017. http://ndltd.ncl.edu.tw/handle/23729549750499956873.

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碩士<br>國立中央大學<br>化學學系<br>105<br>In this thesis, a series of supramolecular compounds and coordination polymers were synthesized via self-assembly processes and their structures and properties were examined. Compounds {[Cd(4-bdt)(atpa)(H2O)]·(DMF)(H2O)2}n (1), {[Cd(4-bdt)(htpa)(H2O)]·DMF}n (2), {[Cd(4-bdt)(ntpa)(H2O)]·DMF}n (3), respectively, were produced by the reaction of cadmium salts, 4-amino-3,5-bis(4-pyridyl)-1,2,4-triazole (4-bpt), and 2-aminoterephthalic acid (atpa), 2-hydroxyterephthalic acid (htpa) or 2-nitroterephthalic acid (ntpa) ligands in a mixture of DMF/H2O at 50 °C. The struct

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12

"New mono- and dinuclear ruthenium complexes containing the 3,5-bis(2-pyridyl)pyrazole ligand. Synthesis, characterization and applications." Universitat de Girona, 2005. http://www.tesisenxarxa.net/TDX-0505105-110753/.

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13

Lin, Cheng-Chen, and 林正城. "The Study of the Linear Trinuclear Metal Complexes of Bis(2- pyridyl)amido Ligand and the Bonding Type of the Electron Delocalized Metal Complexes." Thesis, 1996. http://ndltd.ncl.edu.tw/handle/13566150354182974382.

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14

Yang, Xiang-Kai, and 楊翔凱. "Study on Coordination Polymers supported by Formamidinate and Bis-Pyridyl-Bis-Amide Ligands." Thesis, 2016. http://ndltd.ncl.edu.tw/handle/30471741622873072834.

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碩士<br>中原大學<br>化學研究所<br>104<br>This thesis discusses the structures and properties of coordination polymers supported by formamidine and formamidinate ligands. Part I, Suzuki coupling was used to synthesize 4-(pyridin-4-yl)aniline, which was then reacted with triethyl orthoformate and copper(II) acetate in THF by one-pot solvothermal reaction to afford coordination polymer {Cu4(OAc)4(4-pyanf)2}n, 1. Part II, one-pot solvothermal reaction of 4-aminopyridine or 4-(aminomethyl)pyridine with triethyl orthoformate and cobalt chloride in THF afforded coordination polymers {[Co(4-pyf)Cl}·THF}n, 2 and

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15

Thapa, Kedar Bahadur, and 巴凱達. "Crystal Engineering of Coordination Polymers based on Flexible Bis-pyridyl-bis-amide and Tetracarboxylate Ligands." Thesis, 2016. http://ndltd.ncl.edu.tw/handle/74507455670869722843.

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博士<br>中原大學<br>化學研究所<br>105<br>In this dissertation, the syntheses, structures and properties of coordination polymers based on the flexible bis-pyridyl-bis-amide and/or tetracarboxylate ligands, have been extensively discussed and summarized basically in five parts. Part I: The contribution of flexible bis-pyridyl-bis-amide (bpba) ligands, which are also known as versatile ligands possessing various active coordination atoms (N and O) and different flexible –CH2– skeletons, is significant in the construction of coordination polymers. In this Highlight, structures of the different dimensi

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16

Cheng, Yung-Tang, and 鄭永塘. "Syntheses, Structures and Catalytic Properties of Coordination Polymers Based on Bis-pyridyl-bis-amide and Chiral Dicarboxylate Ligands." Thesis, 2019. http://ndltd.ncl.edu.tw/handle/2629uy.

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碩士<br>中原大學<br>化學研究所<br>107<br>A series of chiral coordination polymers constructed from N,N''-di(3-pyridyl)adipamide (L1), N,N''-di(3-pyridyl)sebacoamide (L2), N,N''-di(3-pyridyl)ethanediamide (L3) and N,N''-di-3-pyridinyl-[1,1''-Biphenyl]-4,4''-dicarboxamide (L4) and chiral and achiral dicarboxylic acid ligands, including {[Zn(4,4''-bipy)(L-DBTA)(H2O)2]∙H2O}n (L-H2DBTA = (−)-dibenzoyl-L-tartaric acid), 1, {[Zn(4,4''-bipy)(D-DBTA)(H2O)2]．H2O}n (D-H2DBTA = (+)-dibenzoyl-D-tartaric acid), 2, {[Zn(L1)(L-DBTA)]∙H2O}n,

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17

Lo, Hui-Ju, and 羅惠如. "Synthesis, Structures and properties of Cadmium(Ⅱ) Coordination Polymers Containing Flexible Bis-pyridyl-Bis-amide and Polycarboxylate Ligands." Thesis, 2018. http://ndltd.ncl.edu.tw/handle/b7zgd4.

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碩士<br>中原大學<br>化學研究所<br>106<br>Three Cd(II) coordination polymers constructed from flexible bis-pyridyl-bis-amide ligands and dicarboxylic acids with different flexibility, {[Cd(L1)(SA)]．5H2O．CH3OH}n, (L1 = N,N’-di(3-pyridyl)adipoamide ; H2SA = suberic acid), 1, {[Cd(L1)(AA)]．2H2O}n, (H2AA = adipic acid), 2, {[Cd(L2)(SA)]．5H2O．3H2O }n, (L2 = N,N’-di(3-pyridyl)suberoamide), 3, were synthesized by hydrothermal reactions. These complexes were structurally characterized by using single-crystal X-ray diffraction and churactized by using powder X-ray diffraction, Elemental Analyzer and IR spectra. Co

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18

YI, WEI-CHENG, and 易煒程. "Synthesis, Structures and Properties of Metal Coordination Polymers with Multi-carboxylate ligands and 1,3-bis(4-pyridyl)propane ligands." Thesis, 2019. http://ndltd.ncl.edu.tw/handle/67ramq.

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碩士<br>東吳大學<br>化學系<br>107<br>Research on the subject of this paper is synthesize metal coordination polymers by general traditional synthesis, there are two synthetic strategies, mixing different metal ions with the same ligand, and using different multi-carboxylic ligands for the synthesis of the same metal ion, and discuss its similarities and differences. Ten coordination polymers (CPs) with chemical formulas,{[Mn(bpp)(5-Nipa)(H2O)]‧H2O}n (1) ,{[Co(bpp)(5-Nipa)(H2O)]‧H2O}n (2) ,{[Cu(bpp)(5-Nipa)(H2O)]‧H2O}n (3) ,{[Cu(bpp)(5-Nipa)(H2O)]}n (4) ,{[Zn(bpp)(5-Nipa)(H2O)]}n (5) ,{[Zn2(bpp)2(BDC)2]

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19

Wang, Ying-Fung, and 王盈方. "Synthesis, Structural Characterization and Properties of Metal Coordination Polymers with 1,3-bis(4-pyridyl)propane and Oxygen-Containing Ligands." Thesis, 2014. http://ndltd.ncl.edu.tw/handle/74170644822462068086.

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碩士<br>東吳大學<br>化學系<br>102<br>Two coordination polymers with the formulas, {[Co(bpp)(2,6-ndc)(H2O)2 ]‧2(C2H5OH)}n (1) and {[Zn3(bpp)2(2,6-ndc)3(H2O)2]‧2(C2H5OH)}n (2), (bpp = 1,3-bis(4-pyridyl)propane, 2,6-ndc2- = 2,6-naphthalenedicarboxylate), have been synthesized and structurally characterized by single-crystal X-ray diffraction studies. In compound 1, the Co(II) ion is six-coordinate in a distorted octahedral environment bonded to two oxygen atoms of two bis-monodentate 2,6-ndc2- ligands, two nitrogen atoms of two bis-monodentate bpp ligands and two water molecules. A 2D layered metal-organi

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20

Hsu, Chih-Hsun, and 許智勛. "Syntheses, Structures and Properties of Cd(II), Co(II) and Ni(II) Coordination Polymers Containing Flexible Bis-pyridyl-bis-amide and Polycarboxylate Ligands: Structural Entanglement and Transformation." Thesis, 2017. http://ndltd.ncl.edu.tw/handle/2gw6wa.

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碩士<br>中原大學<br>化學研究所<br>105<br>A series of divalent coordination polymers constructed from N,N’-di(3-pyridyl)suberoamide (L1), N,N’-di(4-pyridyl)suberoamide (L2), N,N’-di(3-pyridyl)adipamide (L3) and angular polycarboxylaic ligands, including {[Cd(L1)(2,6-PDC)]·5H2O}n (2,6-H2PDC = 2,6-pyridinedicarboxylic acid), 1, {[Cd(L2)(2,6-PDC)]·2.5H2O}n, 2, {[Cd(L1)1.5(1,2,3-HBTC]·2H2O}n (1,2,3-H3BTC = 1,2,3-benzenetricarboxylic acid), 3, [Ni(L2)(1,3-PDA)(H2O)2]n (1,3-PDA = 1,3-phenylenediacetic acid), 4, [Co(L2)(1,3-PDA)(H2O)2]n, 5, [Co(L1)(5-NH2-IPA)]n (5-NH2-H2IPA = 5-aminoisophthalic acid), 6, {[Co(L2

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21

YAN, ONG VEI, and 王微欣. "Synthesis,Structural Characterization and Properties of Metal Coordination Polymers with 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene and carboxylate-based Ligands." Thesis, 2019. http://ndltd.ncl.edu.tw/handle/shx6fz.

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碩士<br>東吳大學<br>化學系<br>107<br>Assembly of 4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene (4-bpd) with first row transition metal salts [Zn(II), Co(II)] in combination with the various O-containing auxiliary ligands, such as (1,3-BDC-5(OH))、H4BT、H3BTC and Na2BDC, yielded six coordination polymers (CPs), using slow evaporation technique at room temperature. Coordonation polymers: {[Zn(4-bpd)0.5(1,3-BDC-5(OH))H2O]H2O} (1) {[Zn(4-bpd)(1,3-BDC-5(OH))]H2O} (2) {[Co(4-bpd)(HBTC)(H2O)3]·3H2O} (3) {[Co(4-bpd)(BDC)]2DMF} (4) {[Zn2(4-bpd)(BT)(H2O)2]5H2O}(5) {[Co2(4-bpd)2(BT)(H2O)3(EtOH)]EtOH3H2O} (6) The

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22

Wang, Hsin-Yu, and 王心瑀. "Synthesis, Structural Characterization and Properties of Metal Coordination Polymers with 1,4-bis(4-pyridyl)-2,3-diaza-1,3-butadiene and Carboxylate-based Ligands." Thesis, 2014. http://ndltd.ncl.edu.tw/handle/86599305825908922085.

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碩士<br>東吳大學<br>化學系<br>102<br>This thesis decribes the self-assembly of ten metal coordination polymers by different metal ions with 1,4-bis(4-pyridyl)-2,3-diaza-1,3- butadiene (4-bpd) and carboxylate-based ligands ( Na2BDC = Terephthalic acid , disodium salt, H3BTC = 1,3,5-Benzentricaboxylicacid ) are studied. All of them were prepared in solution and fully characterized by Infrared Spectroscopy, elemental analysis, single-crystal X-ray diffraction method, thermogravimetric, ad/desorption of solvent sorption, and in-situ powder X-ray diffraction. In first series, four metal-organic framework ha

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23

Wang, Tzu-Heng, and 王子衡. "Synthesis, Structural Characterization and Properties of Metal Coordination Polymers with 2,5-bis(4-pyridyl)-3,4-diaza-2,4-hexadiene (bpdh) and Oxygen-Containing Ligands." Thesis, 2019. http://ndltd.ncl.edu.tw/handle/yfq9dc.

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碩士<br>東吳大學<br>化學系<br>107<br>Abstract Assembly of 2,5-bis(4-pyridyl)-3,4-diaza-2,4-hexadiene (bpdh) with first row transition metal salts [Zn(II), Co(II), Mn(II)] in combination with the various O-containing auxiliary ligands, yielded eight coordination polymers (CPs), [Co(bpdh)(C4O4)(H2O)2] (1), [Zn(bpdh)(C4O4)(H2O)2] (2), [Zn(bpdh)2(C5O5)]∙C2H5OH (3), [Mn(bpdh)(5-Nipa)(H2O)2]∙H2O (4), [Co(bpdh)(5-Nipa)(H2O)2]∙H2O (5), [Zn(bpdh)(5-Nipa)] (6), [Co(bpdh)(1,3-BDC-5(OH))(H2O)]∙(bpdh)0.5 (7), [Zn(bpdh)(1,4-BDC-2,5(OH))]∙C2H5OH∙2H2O (8) using slow evaporation technique at room temperature. The c

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24

Cheng, Chia-Wen, and 鄭家雯. "Synthesis,structural characterization and properties of metal coordination polymers with 2,5-bis(4-pyridyl)-3,4-diaza-2,4-hexadiene (bphd) and oxygen-containing ligands." Thesis, 2016. http://ndltd.ncl.edu.tw/handle/22699065643083363761.

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碩士<br>東吳大學<br>化學系<br>104<br>Research on the subject of this paper is the use of general traditional synthesis, synthesis of supramolecular structure having a mixed fund genus complexes, using infrared spectroscopy (IR), elemental analyzer (EA), X ray single crystal diffraction instrument (X -Ray) to do the identification of measurement and structural properties of the compounds on. The paper denominated metal ions (Cd (II) and Zn (II)) with a nitrogen-containing oxygen-binding ligand and carboxylate group of the ligand, 2,5-bis (4-pyridyl) -3,4-diaza- 2,4-hexadiene (4-bpdh), 5-Nitroisophthalic

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