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Journal articles on the topic 'Ligand non-innocent'

Author: Grafiati

Published: 4 June 2021

Last updated: 22 February 2025

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1

Hazari, Arijit Singha, Alexa Paretzki, Jan Fiedler, Stanislav Zalis, Wolfgang Kaim та Goutam Kumar Lahiri. "Different manifestations of enhanced π-acceptor ligation at every redox level of [Os(9-OP)L2]n, n = 2+, +, 0, − (9-OP− = 9-oxidophenalenone and L = bpy or pap)". Dalton Transactions 45, № 45 (2016): 18241–51. http://dx.doi.org/10.1039/c6dt03764j.

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2

Kumar, M., S. Ahmad, K. Khatoon, et al. "Copper(II)-Mediated Transformation of a Hexadentate Non-Innocent Ligand into a Pentadentate Non-Innocent Ligand." Russian Journal of Inorganic Chemistry 68, no. 14 (2023): 1941–55. http://dx.doi.org/10.1134/s0036023623602970.

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3

Lehtonen, Ari. "Metal Complexes of Redox Non-Innocent Ligand N,N′-Bis(3,5-di-tertbutyl-2-hydroxy-phenyl)-1,2-phenylenediamine." Molecules 29, no. 5 (2024): 1088. http://dx.doi.org/10.3390/molecules29051088.

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Redox non-innocent ligands react with metal precursors to form complexes where the oxidation states of the ligand and thus the metal atom cannot be easily defined. A well-known example of such ligands is bis(o-aminophenol) N,N′-bis(3,5-di-tertbutyl-2-hydroxy-phenyl)-1,2-phenylenediamine, previously developed by the Wieghardt group, which has a potentially tetradentate coordination mode and four distinct protonation states, whereas its electrochemical behavior allows for five distinct oxidation states. This rich redox chemistry, as well as the ability to coordinate to various transition metals,

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4

Braun, Jason D., Paul A. Gray, Baldeep K. Sidhu, Dion B. Nemez, and David E. Herbert. "Zn-Templated synthesis of substituted (2,6-diimine)pyridine proligands and evaluation of their iron complexes as anolytes for flow battery applications." Dalton Transactions 49, no. 45 (2020): 16175–83. http://dx.doi.org/10.1039/d0dt00543f.

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Zn<sup>2+</sup> templating enables synthesis of redox ‘non-innocent’ diimine pyridine ligands with strong electron-withdrawing groups, allowing construction of iron complexes with multiple ligand-based reductions for application in redox flow batteries.

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5

Dutta, Debarpan, Suvendu Maity, Suman Kundu, and Prasanta Ghosh. "Mixed-valence di-ruthenium(ii,iii) complexes of redox non-innocent N-aryl-o-phenylenediamine derivatives." Dalton Transactions 50, no. 22 (2021): 7791–803. http://dx.doi.org/10.1039/d1dt00779c.

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6

Ghorai, Samir, and Chandan Mukherjee. "Copper(II)-Mediated Transformation of a Tridentate Non-Innocent Ligand into a Tetradentate Salen-Type Innocent Ligand." Chemistry - An Asian Journal 9, no. 12 (2014): 3518–24. http://dx.doi.org/10.1002/asia.201402868.

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7

Wan, Ho Chuen, Jing-Xuan Zhang, Chung Sum Leung, Fu Kit Sheong, and Zhenyang Lin. "Inter-ligand delocalisations in transition metal complexes containing multiple non-innocent ligands." Dalton Transactions 48, no. 39 (2019): 14801–7. http://dx.doi.org/10.1039/c9dt02806d.

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8

Simler, Thomas, Andreas A. Danopoulos, and Pierre Braunstein. "Non-symmetrical, potentially redox non-innocent imino NHC pyridine ‘pincers’ via a zinc ion template-assisted synthesis." Dalton Transactions 46, no. 18 (2017): 5955–64. http://dx.doi.org/10.1039/c7dt01014a.

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A Zn<sup>II</sup>-promoted modular synthesis allows access to new non-symmetrical, redox-active imino NHC pyridine pincer ligands. Radical anionic and dianionic redox states of the ligand are involved in its Fe<sup>II</sup> complexes obtained from FeBr<sub>2</sub>/KC<sub>8</sub>.

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9

Mondal, Manas Kumar, Abul Kalam Biswas, Bishwajit Ganguly, and Chandan Mukherjee. "Unprecedented iminobenzosemiquinone and iminobenzoquinone coordinated mononuclear Cu(ii) complex formation under air." Dalton Transactions 44, no. 20 (2015): 9375–81. http://dx.doi.org/10.1039/c4dt03263b.

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Ligand H4LS(AP/AP) comprised of two orthogonally placed non-innocent unit that were bridged by a common -ortho S atom. It reacted with CuCl<sub>2</sub>·2H<sub>2</sub>O and provided a mononuclear diamagnetic Cu(ii) complex where two non-innocent units were in two different oxidation states.

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10

Buncic, Gojko, Zhiguang Xiao, Simon C. Drew, Jonathan M. White, Anthony G. Wedd, and Paul S. Donnelly. "Copper complexes of a novel non-innocent quadridentate ligand." Chemical Communications 48, no. 20 (2012): 2570. http://dx.doi.org/10.1039/c2cc16658e.

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11

Balatskiy, Denis, Ivan Tkachenko, Irina Malakhova, Natalia Polyakova, and Svetlana Bratskaya. "Polyethylenimine as a Non-Innocent Ligand for Hexacyanoferrates Immobilization." Molecules 27, no. 23 (2022): 8489. http://dx.doi.org/10.3390/molecules27238489.

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To understand how polyethyleneimine (PEI), as a ligand, affects structure and properties of the transition metals hexacyanoferrates (HCFs) immobilized in cross-linked PEI matrix, we have synthesized Cu(II), Zn(II), and Fe(III) HCFs via successive ion-exchange reactions with metal salts and K4[FeII(CN)6] or K3[FeIII(CN)6]. The structure and properties of the obtained materials in comparison with the crystalline HCF analogs were investigated with FT-IR, Mössbauer, and UV–Vis spectroscopy. Complete reduction of Fe(III) to Fe(II) by PEI in HCF(III) was confirmed. When synthesis was performed at pH

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12

Piehl, Patrick, Miguel Peña-López, Anna Frey, Helfried Neumann, and Matthias Beller. "Hydrogen autotransfer and related dehydrogenative coupling reactions using a rhenium(i) pincer catalyst." Chemical Communications 53, no. 22 (2017): 3265–68. http://dx.doi.org/10.1039/c6cc09977g.

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13

McQuarters, Ashley B., and Nicolai Lehnert. "{RuNO}6vs. co-ligand oxidation: two non-innocent groups in one ruthenium nitrosyl complex." Dalton Trans. 43, no. 37 (2014): 13835–38. http://dx.doi.org/10.1039/c4dt01388c.

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The one-electron oxidation of the {RuNO}<sup>6</sup> complex [Ru(L)(PPh<sub>3</sub>)(NO)(Cl)]<sup>2+</sup> (where L = 1-phenyl-1-(pyridin-2-yl)-2-(pyridin-2-ylmethylene)hydrazine) leads to the generation of a co-ligand radical. This complex therefore represents a rare example of a ruthenium complex with two different non-innocent ligands bound.

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14

Chuang, Yu-Chun, Chou-Fu Sheu, Gene-Hsiang Lee, Yu-Sheng Chen, and Yu Wang. "Charge density studies of 3dmetal (Ni/Cu) complexes with a non-innocent ligand." Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials 73, no. 4 (2017): 634–42. http://dx.doi.org/10.1107/s2052520617007119.

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High-resolution X-ray diffraction experiments and atom-specific X-ray absorption experiments are applied to investigate a series of square planar complexes with the non-innocent ligand of maleonitriledithiolate (mnt), [S2C2(CN)2]z−, containingM—S bonds. Four complexes of (PyH)z[M(mnt)2]z−, whereM= Ni or Cu,z= 2 or 1 and PyH+= C5NH6+, were studied in order to clarify whether such one-electron oxidation–reduction, [M(mnt)2]2−/[M(mnt)2]1−, is taking place at the metal or the ligand site. Combining the techniques of metalK-,L-edge and SK-edge X-ray absorption spectroscopy with high-resolution X-ra

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15

Lever, A. BP. "A computational study of a cyano-bridged dinuclear ruthenium complex containing the non-innocent methylpyrazinium ligand." Canadian Journal of Chemistry 82, no. 6 (2004): 1102–11. http://dx.doi.org/10.1139/v04-068.

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The properties of a series of complexes trans-[LRu(NH3)4-NC-Ru(NH3)4(methylpyrazinium)]n+ where L is an anion (Cl, F, CN, OH) or neutral ligand (CO, H2O, pyridine, CH3NO2) were analyzed using density functional theory. The objective was to probe the change in electronic coupling between the two ruthenium atoms and between ruthenium and the non-innocent methylpyrazinium ligand as L is varied. Molecular orbital coefficients and optical spectra were derived. The electronic interactions involved are seen to be quite sensitive to the charge on the ruthenium to which the ligand L is attached as

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16

Wang, Yichen, Jing Li, Li Zhang, et al. "Magnetic on–off switching in redox non-innocent ligand bridged binuclear cobalt complexes." Dalton Transactions 47, no. 48 (2018): 17211–15. http://dx.doi.org/10.1039/c8dt04157a.

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17

Vijaykumar, Gonela, Anand Pariyar, Jasimuddin Ahmed, Bikash Kumar Shaw, Debashis Adhikari, and Swadhin K. Mandal. "Tuning the redox non-innocence of a phenalenyl ligand toward efficient nickel-assisted catalytic hydrosilylation." Chemical Science 9, no. 10 (2018): 2817–25. http://dx.doi.org/10.1039/c7sc04687a.

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18

Chakraborty, Soumi, Arpan Das, Jasimuddin Ahmed, Sayani Barman, and Swadhin K. Mandal. "Designing a Cr-catalyst bearing redox non-innocent phenalenyl-based ligand towards hydrosilylative CO2 functionalization." Chemical Communications 56, no. 89 (2020): 13788–91. http://dx.doi.org/10.1039/d0cc05348a.

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19

Lee, Nicholas A., Ken T. Ngo, Gerald E. Gilligan, Massimilliano Lamberto, and Jonathan Rochford. "Non-innocent ligand flavone and curcumin inspired ruthenium photosensitizers for solar energy conversion." Physical Chemistry Chemical Physics 23, no. 31 (2021): 16516–24. http://dx.doi.org/10.1039/d1cp01853a.

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20

Lima, Lidiane M. A., Heide Murakami, D. Jackson Gaebler, et al. "Acute Toxicity Evaluation of Non-Innocent Oxidovanadium(V) Schiff Base Complex." Inorganics 9, no. 6 (2021): 42. http://dx.doi.org/10.3390/inorganics9060042.

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The vanadium(V) complexes have been investigated as potential anticancer agents which makes it essential to evaluate their toxicity for safe use in the clinic. The large-scale synthesis and the acute oral toxicity in mice of the oxidovanadium(V) Schiff base catecholate complex, abbreviated as [VO(HSHED)dtb] containing a redox-active ligand with tridentate Schiff base (HSHED = N-(salicylideneaminato)-N’-(2-hydroxyethyl)-1,2-ethylenediamine) and dtb = 3,5-di-(t-butyl)catechol ligands were carried out. The body weight, food consumption, water intake as well biomarkers of liver and kidney toxicity

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21

Salojärvi, Esko, Anssi Peuronen, Jani Moilanen, et al. "A diamagnetic iron complex and its twisted sister – structural evidence on partial spin state change in a crystalline iron complex." Dalton Transactions 50, no. 43 (2021): 15831–40. http://dx.doi.org/10.1039/d1dt01607e.

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Diamagnetic Fe complex was made of a redox non-innocent ligand precursor N,N′-bis(3,5-di-tert-butyl-2-hydroxy-phenyl)-1,2-phenylene-diamine and FeCl3. Its phenoxazine derivative was obtained via intra-ligand cyclisation of the parent complex.

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22

Ringenberg, Mark R., Swarna Latha Kokatam, Zachariah M. Heiden, and Thomas B. Rauchfuss. "Redox-Switched Oxidation of Dihydrogen Using a Non-Innocent Ligand." Journal of the American Chemical Society 130, no. 3 (2008): 788–89. http://dx.doi.org/10.1021/ja076801k.

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23

Chen, Kun-Hao, Yi-Hung Liu, and Ching-Wen Chiu. "A Non-innocent Ligand Supported Germylene and Its Diverse Reactions." Organometallics 39, no. 24 (2020): 4645–50. http://dx.doi.org/10.1021/acs.organomet.0c00671.

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24

Zhang, Yangyang, Qianxiong Zhou, Yue Zheng, et al. "DNA Photocleavage by Non-innocent Ligand-Based Ru(II) Complexes." Inorganic Chemistry 55, no. 9 (2016): 4296–300. http://dx.doi.org/10.1021/acs.inorgchem.6b00028.

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25

DAS, AMIT, DIPANWITA DAS, TANAYA KUNDU, and GOUTAM KUMAR LAHIRI. "Electronic structures of ruthenium complexes encircling non-innocent ligand assembly." Journal of Chemical Sciences 124, no. 6 (2012): 1181–89. http://dx.doi.org/10.1007/s12039-012-0316-3.

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26

Allan, Christopher J., Benjamin F. T. Cooper, Hugh J. Cowley, Jeremy M. Rawson, and Charles L. B. Macdonald. "Non-Innocent Ligand Effects on Low-Oxidation-State Indium Complexes." Chemistry - A European Journal 19, no. 43 (2013): 14470–83. http://dx.doi.org/10.1002/chem.201301881.

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27

Mathew, J., Y. Nakajima, Y. K. Choe, et al. "Olefin hydrosilylation catalyzed by cationic nickel(ii) allyl complexes: a non-innocent allyl ligand-assisted mechanism." Chemical Communications 52, no. 40 (2016): 6723–26. http://dx.doi.org/10.1039/c6cc01665k.

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28

Nasibipour, Mina, Elham Safaei, Marziyeh Sadat Masoumpour, and Andrzej Wojtczak. "Ancillary ligand electro-activity effects towards phenyl acetylene homocoupling reaction by a nickel(ii) complex of a non-innocent O-amino phenol ligand: a mechanistic insight." RSC Advances 10, no. 41 (2020): 24176–89. http://dx.doi.org/10.1039/d0ra04362a.

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29

Wang, Yingxia, Andreas Eichhöfer, Florian Weigend, Dieter Fenske, and Olaf Fuhr. "The coordination behavior of 2,3-bis(diphenylphosphino)maleic-N-phenylimide towards copper, silver, gold and palladium." Dalton Transactions 48, no. 20 (2019): 6863–71. http://dx.doi.org/10.1039/c8dt05003a.

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30

Pakpour, Fatemeh, Elham Safaei, S. Mohammad Azami, Andrzej Wojtczak, and Karolina Kaldunska. "The role of a redox-active non-innocent ligand in additive-free C–C Glaser–Hay and Suzuki coupling reactions by an o-aminophenol palladium(ii) complex." RSC Advances 13, no. 5 (2023): 3278–89. http://dx.doi.org/10.1039/d2ra07252a.

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31

Benson, Christopher R., Alice K. Hui, Kumar Parimal, et al. "Multiplying the electron storage capacity of a bis-tetrazine pincer ligand." Dalton Trans. 43, no. 17 (2014): 6513–24. http://dx.doi.org/10.1039/c4dt00341a.

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32

Kim, Jee Eon, Patrick J. Carroll, and Eric J. Schelter. "Bidentate nitroxide ligands stable toward oxidative redox cycling and their complexes with cerium and lanthanum." Chemical Communications 51, no. 81 (2015): 15047–50. http://dx.doi.org/10.1039/c5cc06052d.

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33

Horak, Kyle T., Alexandra Velian, Michael W. Day, and Theodor Agapie. "Arene non-innocence in dinuclear complexes of Fe, Co, and Ni supported by a para-terphenyl diphosphine." Chem. Commun. 50, no. 34 (2014): 4427–29. http://dx.doi.org/10.1039/c4cc00838c.

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34

Li, Ying-Ying, Xiao-Yan Wang, Hui-Ji Li, et al. "Theoretical study on the mechanism of water oxidation catalyzed by a mononuclear copper complex: important roles of a redox non-innocent ligand and HPO₄²⁻ anion." RSC Advances 13, no. 12 (2023): 8352–59. http://dx.doi.org/10.1039/d3ra00648d.

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35

Ghosh, Ashta Chandra, Jakob Klaus Reinhardt, Markus Karl Kindermann, and Carola Schulzke. "The ring opening reaction of 1,3-dithiol-2-one systems is fully reversible." Chem. Commun. 50, no. 70 (2014): 10102–4. http://dx.doi.org/10.1039/c4cc04414b.

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The deprotection of a common precursor moiety in dithiolene chemistry was discovered to be fully reversible, which, besides being relevant for researchers working in very different fields with these non-innocent ligand systems, may even have an impact on CO<sub>2</sub> housekeeping, as the deprotected ligand acts as an efficient trap.

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36

Zell, Thomas, Petr Milko, Kathlyn L. Fillman, et al. "Iron Dicarbonyl Complexes Featuring Bipyridine-Based PNN Pincer Ligands with Short Interpyridine CC Bond Lengths: Innocent or Non-Innocent Ligand?" Chemistry - A European Journal 20, no. 15 (2014): 4403–13. http://dx.doi.org/10.1002/chem.201304631.

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37

Herich, Peter, Marek Fronc, and Jozef Kožíšek. "New isostructural transition metal complexes with a non-innocent dithiolate ligand." Acta Crystallographica Section C Structural Chemistry 71, no. 2 (2015): 159–64. http://dx.doi.org/10.1107/s2053229615001436.

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Three new complexes with 3,6-dichlorobenzene-1,2-dithiol (bdtCl2), namely methyltriphenylphosphonium bis(3,6-dichlorobenzene-1,2-dithiolato-κ2S,S′)cobaltate(1−), (C19H18P)[Co(C6H2Cl2S2)2], (I), bis(methyltriphenylphosphonium) bis(3,6-dichlorobenzene-1,2-dithiolato-κ2S,S′)cuprate(2−) dimethyl sulfoxide disolvate, (C19H18P)2[Cu(C6H2Cl2S2)2]·2C2H6OS, (II), and methyltriphenylphosphonium bis(3,6-dichlorobenzene-1,2-dithiolato-κ2S,S′)cuprate(1−), (C19H18P)[Cu(C6H2Cl2S2)2], (III), have been synthesized and characterized by single-crystal X-ray diffraction. The X-ray structure analyses of all three c

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38

Khairul, Wan M., Mark A. Fox, Phil A. Schauer, et al. "Ligand redox non-innocent behaviour in ruthenium complexes of ethynyl tolans." Inorganica Chimica Acta 374, no. 1 (2011): 461–71. http://dx.doi.org/10.1016/j.ica.2011.02.043.

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39

Orchanian, Nicholas M., Lorena E. Hong, David A. Velazquez, and Smaranda C. Marinescu. "Electrocatalytic syngas generation with a redox non-innocent cobalt 2-phosphinobenzenethiolate complex." Dalton Transactions 50, no. 31 (2021): 10779–88. http://dx.doi.org/10.1039/d0dt03270k.

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40

Duarte, Gabriel M., Jason D. Braun, Patrick K. Giesbrecht, and David E. Herbert. "Redox non-innocent bis(2,6-diimine-pyridine) ligand–iron complexes as anolytes for flow battery applications." Dalton Transactions 46, no. 47 (2017): 16439–45. http://dx.doi.org/10.1039/c7dt03915h.

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41

Nasibipour, Mina, Elham Safaei, Andrzej Wojtczak, Zvonko Jagličić, Agustín Galindo, and Marzieh Sadat Masoumpour. "A biradical oxo-molybdenum complex containing semiquinone and o-aminophenol benzoxazole-based ligands." RSC Advances 10, no. 67 (2020): 40853–66. http://dx.doi.org/10.1039/d0ra06351g.

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Biradical molybdenum(iv) complex, MoOLBISLSQ, has been prepared from the reaction of the o-iminosemibenzoquinone form of a tridentate non-innocent benzoxazole ligand, LBIS, and MoO<sub>2</sub>(acac)<sub>2</sub> and used as catalyst in oxidation reaction..

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42

Zhang, Bo, Yu’ai Duan, Xin Zhang, and Shuai Guo. "Uncommon carbene-to-azole ligand rearrangement of N-heterocyclic carbenes in a ruthenium system." Chemical Communications 57, no. 56 (2021): 6879–82. http://dx.doi.org/10.1039/d1cc01871j.

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43

Schorpp, Marcel, Stephan Rein, Stefan Weber, Harald Scherer, and Ingo Krossing. "Guilty and charged: a stable solution of the hexamethylbenzene radical cation as a ligand forming oxidising agent." Chemical Communications 54, no. 72 (2018): 10036–39. http://dx.doi.org/10.1039/c8cc04690e.

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44

Takaichi, June, Kei Ohkubo, Hideki Sugimoto та ін. "Copper complexes of the non-innocent β-diketiminate ligand containing phenol groups". Dalton Trans. 42, № 7 (2013): 2438–44. http://dx.doi.org/10.1039/c2dt32413j.

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45

Fourmigue, Marc, and Benoit Domercq. "ChemInform Abstract: A Non-Innocent Ligand in Coordination Chemistry: The Dithiolene Complexes." ChemInform 30, no. 24 (2010): no. http://dx.doi.org/10.1002/chin.199924292.

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46

Khatua, Manas, Bappaditya Goswami, and Subhas Samanta. "Dehydrogenation of amines in aryl-amine functionalized pincer-like nitrogen-donor redox non-innocent ligands via ligand reduction on a Ni(ii) template." Dalton Transactions 49, no. 20 (2020): 6816–31. http://dx.doi.org/10.1039/d0dt00466a.

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47

Liu, Jiale, Rong-Zhen Liao, Frank W. Heinemann, et al. "Electrocatalytic Hydrogen Evolution by Cobalt Complexes with a Redox Non-Innocent Polypyridine Ligand." Inorganic Chemistry 60, no. 23 (2021): 17976–85. http://dx.doi.org/10.1021/acs.inorgchem.1c02539.

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48

Marks, Sebastian, Tarun K. Panda, and Peter W. Roesky. "Bis(phosphinimino)methanides as non-innocent ligand in zinc chemistry: synthesis and structures." Dalton Transactions 39, no. 31 (2010): 7230. http://dx.doi.org/10.1039/c0dt00186d.

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49

Khoo, Sabrina, Yu-Liang Shan, Ming-Chung Yang, Yongxin Li, Ming-Der Su, and Cheuk-Wai So. "B–H Bond Activation by an Amidinate-Stabilized Amidosilylene: Non-Innocent Amidinate Ligand." Inorganic Chemistry 57, no. 10 (2018): 5879–87. http://dx.doi.org/10.1021/acs.inorgchem.8b00321.

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50

Dunn, Tim J., Linus Chiang, Caterina F. Ramogida, et al. "Non-innocent ligand behaviour of a bimetallic Cu complex employing a bridging catecholate." Dalton Transactions 41, no. 26 (2012): 7905. http://dx.doi.org/10.1039/c2dt30444a.

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