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Dissertations / Theses on the topic 'Ligands Metal complexes Electrochemistry'

Author: Grafiati

Published: 4 June 2021

Last updated: 5 February 2022

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1

Foster, Keith A. "Preparative, structural, and electrochemical investigation of metal complexes of tetraazamacrocyclic ligands containing tertiary amine donors." Diss., Georgia Institute of Technology, 1986. http://hdl.handle.net/1853/30370.

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2

Smith, Mark Edward. "Molecular wires : syntheses, electrochemistry and properties of metal complexes containing carbon chains /." Title page, contents and abstract only, 2002. http://web4.library.adelaide.edu.au/theses/09PH/09phs654.pdf.

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Thesis (Ph.D.)--University of Adelaide, Dept. of Chemistry, 2002.<br>"September 2002" Includes as appendix: a list of publications by the author arising from this work; and, copies of some published journal articles. Includes bibliographical references.

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3

Mohamed, Nuralli. "Electrochemical studies of monosubstituted squarate ligands and its transition metal and lanthanide complexes." Thesis, University of the Western Cape, 2008. http://etd.uwc.ac.za/index.php?module=etd&action=viewtitle&id=gen8Srv25Nme4_9818_1263431045.

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<p>The study introduces and puts forward Sector Policing as a model to expand community Policing and to broaden the scope of crime prevention. It also demonstrates how Sector Policing can be utilised to decentralise policing and deepen community participation.</p>

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4

Yohannes, Desta Yonas. "Synthesis and electrochemistry of biodegradable ligands - iminodiglutaric acid and iminoglutaricsuccinic acid - and their complexes with selected metal ions (Zn²⁺, Cd²⁺, Cu²⁺)." Thesis, Stellenbosch : Stellenbosch University, 2004. http://hdl.handle.net/10019.1/50112.

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Thesis (MSc)--Stellenbosch University, 2004.<br>ENGLISH ABSTRACT: Two new potentially biodegradable aminopolycarboxylic acid ligands, iminodiglutaric acid tetra sodium salt (IDG-4Na) and iminoglutaricsuccinic acid tetra sodium salt (IGS- 4Na), were synthesized in reasonably good yield and purity. The commercially unavailable precursor for the two ligands, ethyl p-aminoglutarate, was synthesised in high yield and purity, and together with the two ligands were fully characterized by means of melting point measurements and various spectrometric techniques CH-NMR, 13C-NMR, MS and IR). For

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5

Brown, Douglas J. "Heteroleptic paddlewheel complexes and molecular assemblies of dimolybdenum and ditungsten a study of electronic and structural control /." Columbus, Ohio : Ohio State University, 2006. http://rave.ohiolink.edu/etdc/view?acc%5Fnum=osu1150289057.

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6

Lengkeek, Nigel Andrew. "Functional cage-amine complexes : polymerisable metallomonomers and multi-cage complexes." University of Western Australia. School of Biomedical, Biomolecular and Chemical Sciences, 2008. http://theses.library.uwa.edu.au/adt-WU2008.0138.

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[Truncated abstract] Chapter 1 provides an introduction to the 'sarcophagine' class of ligands and the field of metallopolymers. The synthesis, stereochemistry, physical properties and functionalisation of 'sarcophagines' and their metal complexes are discussed. A brief overview of the burgeoning field of metallopolymers is given with specific mention of the synthetic routes to pendant metallopolymers, and how these could be employed to prepared cage amine containing metallopolymers. Chapter 2 deals with the synthesis, characterisation and reactivity of cinnamylamino and styrylamido derivative

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7

Weiß, Daniel Traugott [Verfasser], Fritz E. [Akademischer Betreuer] Kühn, and Richard W. [Akademischer Betreuer] Fischer. "Influence of Open Chain, Tetradentate NHC and NHC/Pyridine Hybrid Ligands on the Coordination and Electrochemistry of Late Transition Metal Complexes / Daniel Traugott Weiß. Betreuer: Fritz E. Kühn. Gutachter: Fritz E. Kühn ; Richard W. Fischer." München : Universitätsbibliothek der TU München, 2015. http://d-nb.info/1079974563/34.

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8

Hicks, Owen Michael. "Complexes of redox-active cyanomanganese ligands." Thesis, University of Bristol, 1997. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.390377.

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9

Rajan, Siji. "Synthesis and complexes of bridging heterocyclic ligands." Thesis, University of Canterbury. Chemistry, 2014. http://hdl.handle.net/10092/9948.

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Ligand–mediated coupling between metal centres is of fundamental importance in inorganic and materials chemistry. Bridging ligands involving azo groups as coordinating π–acceptors can yield complexes with interesting properties. This thesis describes the synthesis of a series of N–heterocyclic compounds containing the azo functionality, designed for potential coordination to the metal through the azo nitrogen and a N–heterocyclic ring. The azo ligands are divided into four categories; ligands based on azobispyridines, ligands containing pyrimidine and fused aromatic azine groups and ligands

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10

Cheung, Wai Man. "Transition metal complexes with dichalcogenoimidodiphosphinate ligands /." View abstract or full-text, 2007. http://library.ust.hk/cgi/db/thesis.pl?CHEM%202007%20CHEUNG.

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11

McHugh, Paul. "Oligonuclear metal complexes of compartmental ligands." Thesis, University of Sheffield, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.408313.

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12

Onyiriuka, Emmanuel C. "Pyrazolyl ligands in mixed metal complexes." Thesis, University of British Columbia, 1986. http://hdl.handle.net/2429/27178.

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The anions LMo(CO)₃⁻ (L = MeGapz₃ or MeGa(3,5-Me₂pz)₃) have been isolated as the Na⁺, Et₄N⁺ or HAsPh₃⁺ salts and the solution structures of the Na⁺ salts in THF have been defined by analysis of the v[sub CO] ir spectra. Ion-pair interaction of the LMo(CO)₃⁻ anion with Na⁺cation in THF solution is apparent from the spectroscopic evidence obtained. The MeGapz₃Mo(CO)₃ ⁻anion reacted with HCl or EtBr to give the seven-coordinate [MeGapz₃]-Mo(CO)₃R (R = H or Et) complexes. However, with Mel or PhCOCl complexes of the type [MeGapz₃]Mo(CO)₂(n₂-COR) (R = Me or Ph) were obtained. The reactions of the

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13

Crofts, Rhona D. "Platinum metal complexes of macrocyclic ligands." Thesis, University of Edinburgh, 1995. http://hdl.handle.net/1842/13493.

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14

Humphrey, Elizabeth Rebecca. "Tris(pyrazolyl)borate metal complexes : new ligands and metal-metal interactions." Thesis, University of Bristol, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.340301.

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15

Nensala, Ngudiankama. "Photocatalytic reactions of metal diphthalocyanine complexes." Thesis, Rhodes University, 2000. http://hdl.handle.net/10962/d1004989.

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Photocatalytic reactions of tin diphthalocyanine, Sn ^IVPc₂ and anionic form of Nd^III, Dy^III, Eu^III, Tm^III and Lu^III diphthalocyanine complexes ( [Pc(-2)Nd^IIIpc(-2)]⁻ , [Pc(-2)Dy^IIIPc(-2)]⁻ , [Pc(-2)Eu^IIIPc(-2)⁻, [Pc(-2)Tm^IIlPc(-2)r and [Pc(-2)LuIIIpc(-2)]⁻ respectively) in the presence of CH₂CI₂, S0₂, pentachlorophenol (PCP), 4-chlorophenol (4-Cp) and thionyl chloride have been studied. Photoreactions involving lanthanide diphthalocyanines, filtered and unfiltered radiations were employed, whereas for photoreactions involving tin diphthalocyanine, only unfiltered radiation was employ

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16

Landman, Marile. "Synthesis of metal complexes with thiophene ligands." Thesis, Access to E-Thesis, 2000. http://upetd.up.ac.za/thesis/available/etd-12042006-143722/.

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17

Graham, Todd Warren. "Mixed-metal complexes incorporating polydentate bridging ligands." Thesis, National Library of Canada = Bibliothèque nationale du Canada, 1999. http://www.collectionscanada.ca/obj/s4/f2/dsk1/tape7/PQDD_0028/NQ39533.pdf.

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18

Skinner, Michael E. G. "Transition metal complexes of diamide-diamine ligands." Thesis, University of Oxford, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.365390.

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19

Niven, Stuart. "Chelating carbene ligands and their metal complexes." Thesis, Cardiff University, 2007. http://orca.cf.ac.uk/54628/.

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This thesis describes the synthesis of a number of functionalised imidazolium salts as precursors to N- heterocyclic carbenes and their subsequent coordination to Ag and Pd. Further a number of the Pd complexes were tested in the Heck reaction and their activities compared to complexes with similar structural features currently within the literature. A range of imidazolium salts have been synthesised which include quinoline and octahydroacridine moieties and have been characterised by a number of methods including X-ray crystallography. A bis imidazolium salt has also been prepared as a DIOP a

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20

O'Shaughnessy, Paul. "Alkali metal complexes of phosphorus donor ligands." Thesis, University of Newcastle Upon Tyne, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.323668.

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21

Okey, J. N. "Metal complexes of nitrogen-donor heteroaromatic ligands." Thesis, Imperial College London, 1987. http://hdl.handle.net/10044/1/47492.

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22

Seidel, Scott William 1971. "Transition metal complexes containing chelating amido ligands." Thesis, Massachusetts Institute of Technology, 1998. http://hdl.handle.net/1721.1/47411.

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23

Olson, Michael David. "Pyrazolyl based ligands in transition metal complexes." Thesis, University of British Columbia, 1989. http://hdl.handle.net/2429/27610.

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Several uninegative/ multidentate pyrazolyl based ligands were synthesized [eg. HBPZ₃₋, HBpz”₃₋, MeGapz₃₋/ MeGapz” ₃₋, H2BpZ₂₋/ Me2Bpz₂₋/ Me2GapZ₂₋/ Me2Gapz"₂₋/ Me₂Gapz(OCH₂CH₂NH₂)⁻Me₂Gapz(OCH₂CH₂CH=CH₂)⁻ ; pz pyrazolyl/ pz" = 3, 5 dimethylpyrazolyl]. These ligands were reacted with the sterically hindered metal complex, HBpz*₃MCl (M = Co, Ni; pz* = 3-iPr-4-Br-pyrazolyl) and the mixed-ligand transition metal complexes of general formulae, HBpz*₃ML, were isolated. The X-ray crystal structure of one such complex, HBpz*₃Nipz"₃BH was determined showing a near octahedral arrangement of ligands abo

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24

Turner, Steven Christopher. "Electrochemical release of oxygen from metal complexes." Thesis, Heriot-Watt University, 1991. http://hdl.handle.net/10399/867.

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25

Lam, Chong Ho. "Metal complexes containing oxygen tripod ligands : models of metal oxides /." View Abstract or Full-Text, 2003. http://library.ust.hk/cgi/db/thesis.pl?CHEM%202003%20LAMC.

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Thesis (Ph. D.)--Hong Kong University of Science and Technology, 2003.<br>Includes bibliographical references (leaves 275-290). Also available in electronic version. Access restricted to campus users.

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26

Dubberley, Stuart R. "New calix[4]arene metal complexes." Thesis, University of Oxford, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.365290.

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27

Burgess, Michael Graeme. "Metal Complexes of Acyclic and Macrocyclic Multifunctional Ligands." Thesis, University of Auckland, 2008. http://hdl.handle.net/2292/5171.

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This thesis describes the design, synthesis and study of metal derivatives of new acyclic and macrocyclic ligands containing pyridine and amide groups. Chapter 1 provides an overview of metal-carboxamide and pyridinamide chemistry including a number of important pincer compounds, macrocyclic involvement in formation of metal-templated rotaxanes and catenanes, oxidation catalysts, anion receptors and bimetallic complexes. Chapter 2 discusses new palladium(II) complexes of an acyclic ligand bearing pendant 2-pyridyl-6-methyl arms, N,N_-bis(6-methyl-2-pyridinyl)-2,6-pyridinedicarboxamide (H2LMe).

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28

Lawrence, Sally. "Early transition metal complexes of pyrazole-derived ligands." Thesis, University of Oxford, 2003. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.433560.

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29

Franks, Mark A. "Transition metal complexes containing phenylthiolate and phenolate ligands." Thesis, University of Nottingham, 2011. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.580393.

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Chapter 1 provides an introduction to metalloenzymes that either feature active sites containing Ni-thiolate ligation or utilise phenoxyl radicals to perform their catalytic function, with a particular emphasis on the enzymatic active sites of Ni-containing superoxide dismutase (Ni SOD), [NiFe] hydrogenase and galactose oxidase. Studies concerning low molecular weight complexes of each active site are reviewed and their relevance with respect to enzyme function discussed. Details of the project outline conclude the chapter. Chapter 2 details the syntheses and characterisation of the [Zn(tsalen

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30

Graham, A. "Binuclear and polynuclear metal complexes with bulky ligands." Thesis, University of Edinburgh, 2001. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.651687.

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This thesis presents routes to transition metal complexes of pyridonate and carboxylate ligands. Low nuclearity complexes with triphenyl acetate and 1<sup>st </sup>row transition metals of the formula [M<sub>4</sub>(OMe)<sub>4</sub>(O<sub>2</sub>CCPh<sub>3</sub>)<sub>4</sub>(MeOH)<sub>4</sub>] (M = Co, Ni or Zn) have been synthesised and mark a change from reactions with other carboxylates which produce linear trinuclear complexes. Molecular modelling studies investigate the close contacts that arise if triphenyl acetate is incorporated into a linear trinuclear compound to establish whether st

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31

Rivers, Christopher John. "Transition metal complexes incorporating trialkylsilyl substituted pentalene ligands." Thesis, University of Sussex, 2004. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.289228.

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32

Harriott, Patrick. "Pendant-arm macrocyclic ligands and their metal complexes." Thesis, Queen's University Belfast, 1989. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.336108.

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33

Herring, A. M. "New transition metal complexes containing functionalised phosphine ligands." Thesis, University of Leeds, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.383967.

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34

Khandelwal, B. "Metal complexes of electron-rich arsenic-sulphur ligands." Thesis, University of Exeter, 1987. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.378245.

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35

Rahoo, Haji. "Fluxional characteristics of metal complexes of sulphur ligands." Thesis, University of Exeter, 1991. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.280893.

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36

Wood, Andrew John. "Mixed-metal complexes incorporating redox-active cyanomanganese ligands." Thesis, University of Bristol, 2000. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.311404.

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37

Chiu, Winnie Wai Hang. "Metal complexes with sulfur and selenium donor ligands /." View abstract or full-text, 2009. http://library.ust.hk/cgi/db/thesis.pl?CHEM%202009%20CHIU.

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38

Greatorex, Sam. "Metal complexes of dioxolene and iminonitroxyl radical ligands." Thesis, University of Leeds, 2018. http://etheses.whiterose.ac.uk/21946/.

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This thesis focuses on the design, synthesis and analysis of multinuclear mixed-valent dioxolene complexes and Cu(II) nitroxyl complexes. Chapter 1 contains a review of the relevant literature for the field of mixed-valent dioxolene complexes and molecular magnetism in nitroxyl complexes. Chapter 2 reports the synthesis and crystallographic analysis of a series of novel highly porous solvent-supported supramolecular assemblies of triptycene derivatives. Chapter 3 reports the complexation and characterisation of triptycene derivatives and related multi-dioxolene ligands with Pt(II). Chapter 4 r

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39

Ivison, Peter. "Transition metal complexes of hard-soft donor ligands." Thesis, Kingston University, 1992. http://eprints.kingston.ac.uk/20562/.

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40

Graham, Alasdair. "Dinuclear and polynuclear metal complexes with bulky ligands." Thesis, University of Edinburgh, 2001. http://hdl.handle.net/1842/12051.

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41

Bell, Michael Niall. "Organometallic platinum group metal complexes incorporating macrocyclic ligands." Thesis, University of Edinburgh, 1987. http://hdl.handle.net/1842/13895.

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42

陳展榮 and Chin-wing Chan. "Transition metal complexes of quaterpyridines and photochemical studies of cyclometallated gold(III) and platinum(II) complexes." Thesis, The University of Hong Kong (Pokfulam, Hong Kong), 1993. http://hub.hku.hk/bib/B31233454.

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43

Chan, Chin-wing. "Transition metal complexes of quaterpyridines and photochemical studies of cyclometallated gold(III) and platinum(II) complexes /." [Hong Kong : University of Hong Kong], 1993. http://sunzi.lib.hku.hk/hkuto/record.jsp?B13671753.

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44

Greaves, Sarah Jennifer. "Transition metal O, O'-complexes : preparation, Raman spectra and electrochemistry." Thesis, Imperial College London, 1989. http://hdl.handle.net/10044/1/47454.

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45

Somasundrum, Mithran. "Electrochemistry of metal complexes and their use in amperometric sensors." Thesis, Cranfield University, 1994. http://dspace.lib.cranfield.ac.uk/handle/1826/3691.

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This thesis concerns the utilization of metal complexes in amperometric sensors. Chapter One provides a general introduction to the area. The electrochemical theories relating to the development and use of amperometric sensors, are described, and applications for such sensors are outlined. These include trace element analysis for environmental and clinical use and the determination of NADH for the detection of clinical analytes. In Chapter Two, the electrochemical changes occurring in a ligand upon complexation, are examined as a possible method of selective metal ion detection. Screen-printin

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46

Ho, Kin-ying. "Synthesis, characterization and spectroscopic properties of d6 and d10 metal complexes with pyridyl amine ligands /." Hong Kong : University of Hong Kong, 1999. http://sunzi.lib.hku.hk/hkuto/record.jsp?B20667905.

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47

Hao, Haijun. "Non-Cp Metal complexes Supported by Nitrogen Donor Ligands." Doctoral thesis, [S.l.] : [s.n.], 2001. http://hdl.handle.net/11858/00-1735-0000-0006-AE9A-C.

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48

Cade, Ian Alexander. "Antenna modified ethynyl benzene ligands and their metal complexes." Thesis, Imperial College London, 2005. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.417275.

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49

Ahmed, Aminu. "Mixed donor carbene pyridyl ligands and their metal complexes." Thesis, Cardiff University, 2008. http://orca.cf.ac.uk/54889/.

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This thesis describes the synthesis of a series of Ag(I), Pd(II), Rh(I) and Ir(I) complexes of quinoline functionalised nucleophilic heterocyclic carbene (NHC) ligands. The transmetallation properties of the Ag(I) complexes were utilised to prepare the corresponding Pd(II), Rh (I) and Ir(I) (NHC) complexes. A series of quinoline based imidazolium, pyrimidinium salts were prepared and characterised as NHC ligand precursors. Ag(I)(NHC) complexes were prepared by the reaction of the quinoline functionalised salts with Ag20 in DCM. All complexes were spectroscopically characterised and the results

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50

Hawkins, I. M. "New transition metal complexes containing phosphine and sulphur ligands." Thesis, University of East Anglia, 1988. http://ethos.bl.uk/OrderDetails.do?uin=uk.bl.ethos.235225.

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