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Relevant bibliographies by topics / Liquid and gas chromatography coupled with tandem mass spectrometry and high resolution mass spectrometry (UHPLC/GC - MS/MS and UHPLC-HRMS) / Journal articles

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Journal articles on the topic 'Liquid and gas chromatography coupled with tandem mass spectrometry and high resolution mass spectrometry (UHPLC/GC - MS/MS and UHPLC-HRMS)'

Author: Grafiati

Published: 25 May 2024

Last updated: 31 July 2025

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1

Syahfitr, Sari Anggraini, and Dan Ridho Asra. "Analysis of Medicinal Chemicals Contained on Jamu: A Review." Asian Journal of Pharmaceutical Research and Development 9, no. 2 (2021): 33–46. http://dx.doi.org/10.22270/ajprd.v9i2.931.

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Background: Jamu is commonly known as an Indonesian traditional herbal medicine that contains ingredients or ingredients derived from plants, animals, minerals, galenic, or mixtures of these ingredients that have been hereditary for medicinal use. Some studies reported the presence of medicinal chemicals that are deliberately added to Jamu. Jamuthat containing medicinal chemicals usually had a faster healing effect compared to Jamu that do not contain medicinal chemicals. Jamu added medicinal chemicals cause serious side effects if it is consumed regularly, overdose, and long period consumptio

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Szulc, Justyna, Małgorzata Okrasa, Katarzyna Majchrzycka, et al. "Microbiological and Toxicological Hazards in Sewage Treatment Plant Bioaerosol and Dust." Toxins 13, no. 10 (2021): 691. http://dx.doi.org/10.3390/toxins13100691.

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Despite the awareness that work in the sewage treatment plant is associated with biological hazards, they have not been fully recognised so far. The research aims to comprehensively evaluate microbiological and toxicological hazards in the air and settled dust in workstations in a sewage treatment plant. The number of microorganisms in the air and settled dust was determined using the culture method and the diversity was evaluated using high-throughput sequencing. Endotoxin concentration was assessed with GC-MS (gas chromatography-mass spectrometry) while secondary metabolites with LC-MS/MS (l

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Dahibhate, Nilesh Lakshman, and Kundan Kumar. "Metabolite profiling of Bruguiera cylindrica reveals presence of potential bioactive compounds." PeerJ Analytical Chemistry 4 (May 4, 2022): e16. http://dx.doi.org/10.7717/peerj-achem.16.

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Bruguiera cylindrica parts are commonly used in Chinese and Indian traditional medicine to treat diarrhea, fever, and many ailments. The present study aims non targeted analysis of key secondary metabolites of B. cylindrica by gas chromatography mass spectrometry (GC-MS) and ultra-high performance liquid chromatography hybrid quadrupole-Exactive-Orbitrap high resolution mass spectrometry (UHPLC-Q-Exactive Orbitrap HRMS). GC-MS and UHPLC-Q-Exactive Orbitrap HRMS were utilized for metabolic profiling of ethyl acetate extract of B. cylindrica leaves. Key metabolites in the extract were identified

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4

La Maida, Nunzia, Manuela Pellegrini, Esther Papaseit, et al. "Determination of the Synthetic Cannabinoids JWH-122, JWH-210, UR-144 in Oral Fluid of Consumers by GC-MS and Quantification of Parent Compounds and Metabolites by UHPLC-MS/MS." International Journal of Molecular Sciences 21, no. 24 (2020): 9414. http://dx.doi.org/10.3390/ijms21249414.

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The consumption of synthetic cannabinoids (SCs) has significantly increased in the last decade and the analysis of SCs and their metabolites in human specimens is gaining interest in clinical and forensic toxicology. A pilot study has been carried out using a combination of an initial last generation gas chromatography-mass spectrometry (GC-MS) screening method for the determination of JWH-122, JWH-210, UR-144) in oral fluid (OF) of consumers and an ultra-high performance liquid chromatography high resolution mass spectrometry (UHPLC-HRMS) confirmatory method for the quantification of the pare

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Rubić, Ivana, Richard Burchmore, Stefan Weidt, et al. "Multi Platforms Strategies and Metabolomics Approaches for the Investigation of Comprehensive Metabolite Profile in Dogs with Babesia canis Infection." International Journal of Molecular Sciences 23, no. 3 (2022): 1575. http://dx.doi.org/10.3390/ijms23031575.

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Canine babesiosis is an important tick-borne disease worldwide, caused by parasites of the Babesia genus. Although the disease process primarily affects erythrocytes, it may also have multisystemic consequences. The goal of this study was to explore and characterize the serum metabolome, by identifying potential metabolites and metabolic pathways in dogs naturally infected with Babesia canis using liquid and gas chromatography coupled to mass spectrometry. The study included 12 dogs naturally infected with B. canis and 12 healthy dogs. By combining three different analytical platforms using un

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Marchei, Emilia, Maria Alias Ferri, Marta Torrens, et al. "Ultra-High Performance Liquid Chromatography-High Resolution Mass Spectrometry and High-Sensitivity Gas Chromatography-Mass Spectrometry Screening of Classic Drugs and New Psychoactive Substances and Metabolites in Urine of Consumers." International Journal of Molecular Sciences 22, no. 8 (2021): 4000. http://dx.doi.org/10.3390/ijms22084000.

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The use of the new psychoactive substances is continuously growing and the implementation of accurate and sensible analysis in biological matrices of users is relevant and fundamental for clinical and forensic purposes. Two different analytical technologies, high-sensitivity gas chromatography-mass spectrometry (GC-MS) and ultra-high-performance liquid chromatography-high-resolution mass spectrometry (UHPLC-HRMS) were used for a screening analysis of classic drugs and new psychoactive substances and their metabolites in urine of formed heroin addicts under methadone maintenance therapy. Sample

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7

Scendoni, Roberto, Emanuele Bury, Erika Buratti, et al. "Detection of Morphine and Opioids in Fingernails: Immunohistochemical Analysis and Confirmation with Ultra-High-Performance Liquid Chromatography Coupled with High-Resolution Mass Spectrometry." Toxics 10, no. 8 (2022): 420. http://dx.doi.org/10.3390/toxics10080420.

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This study aimed to investigate the detection of morphine in fingernails from forensic autopsies using immunohistochemistry (IHC), with confirmation by ultra-high-performance liquid chromatography coupled with high-resolution mass spectrometry (UHPLC-HRMS). A primary antibody specific to morphine and a secondary antibody conjugated to horseradish peroxidase (HRP) was used. IHC on specimens of Subjects A and B (both drug addicts) resulted in the detection of morphine on a cell layer of the nail plate matrix. UHPLC-HRMS and GC-MS analysis showed that Subject A had a morphine concentration of 0.3

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Meirelles, João Victor, Débora Cristina Diniz Estevam, Vanessa Farelo dos Santos, et al. "Optimized Extraction Method for Neutral Cannabinoids Quantification Using UHPLC-HRMS/MS." Biomolecules 15, no. 2 (2025): 246. https://doi.org/10.3390/biom15020246.

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The Cannabis market is experiencing steady global growth. Cannabis herbal extracts (CHE) are interesting and sought-after products for many clinical conditions. The medical potential of these formulations is mainly attributed to neutral cannabinoids, such as cannabidiol (CBD), tetrahydrocannabinol (THC), and cannabinol (CBN), and their non-standardized content poses a significant fragility in these pharmaceutical inputs. High-resolution mass spectrometry portrays a powerful alternative to their accurate monitoring; however, further analytical steps need to be critically optimized to keep up wi

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Pellegrini, Manuela, Emilia Marchei, Esther Papaseit, Magí Farré, and Simona Zaami. "UHPLC-HRMS and GC-MS Screening of a Selection of Synthetic Cannabinoids and Metabolites in Urine of Consumers." Medicina 56, no. 8 (2020): 408. http://dx.doi.org/10.3390/medicina56080408.

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Background and Objectives: The use of synthetic cannabinoids has increased around the world. As a result, the implementation of accurate analysis in human biological matrices is relevant and fundamental. Two different analytical technologies, ultra-high-performance liquid chromatography-high-resolution mass spectrometry (UHPLC-HRMS) and high-sensitivity gas chromatography-mass spectrometry (GC-MS) were used for the determination of three synthetic cannabinoids JWH-122, JWH 210, UR-144 and their metabolites in urine of consumers. Materials and Methods: Sample preparation included an initial hyd

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Pezzatti, Julian, Víctor González-Ruiz, Julien Boccard, Davy Guillarme, and Serge Rudaz. "Evaluation of Different Tandem MS Acquisition Modes to Support Metabolite Annotation in Human Plasma Using Ultra High-Performance Liquid Chromatography High-Resolution Mass Spectrometry for Untargeted Metabolomics." Metabolites 10, no. 11 (2020): 464. http://dx.doi.org/10.3390/metabo10110464.

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Ultra-high performance liquid chromatography coupled to high-resolution mass spectrometry (UHPLC-HRMS) is a powerful and essential technique for metabolite annotation in untargeted metabolomic applications. The aim of this study was to evaluate the performance of diverse tandem MS (MS/MS) acquisition modes, i.e., all ion fragmentation (AIF) and data-dependent analysis (DDA), with and without ion mobility spectrometry (IM), to annotate metabolites in human plasma. The influence of the LC separation was also evaluated by comparing the performance of MS/MS acquisition in combination with three co

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Reinholds, I., G. Juodeikiene, E. Bartkiene, et al. "Evaluation of ozonation as a method for mycotoxins degradation in malting wheat grains." World Mycotoxin Journal 9, no. 3 (2016): 409–17. http://dx.doi.org/10.3920/wmj2015.2011.

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The influence of ozone (O3) gas on reducing the contamination with Fusarium mycotoxins in malting wheat grains was investigated. Ultra-high performance liquid chromatography coupled to triple quadrupole tandem mass spectrometry (UHPLC-QqQ-MS/MS) and Orbitrap high resolution mass spectrometry (UHPLC-Orbitrap-HRMS) were used to determine mycotoxins in wheat grains before and 40 to 130 min after the exposure to 20 mg/l O3. Pearson’s analysis (R2=0.96-0.98) showed a good correlation between the performance efficiency of both mass spectrometry quantification techniques. The concentrations of determ

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Theofel, Nadine, Marlene Wagner, Elke Vejmelka, Stefan Scholtis, and Michael Tsokos. "Herbal Medicine Must Be Treated with Care—A Case Report on Aconitine." Forensic Sciences 1, no. 1 (2021): 25–32. http://dx.doi.org/10.3390/forensicsci1010005.

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Pathologists usually only request a screening for natural toxic substances if plant material has been observed during autopsy or if there exists a hint in the police investigation file. This situation is aggravated by the fact that most toxins are not covered by typical immunoassays and gas chromatography–mass spectrometry (GC–MS) profiling systems. In addition, only a few forensic toxicological libraries based on liquid chromatography coupled to high-resolution tandem mass spectrometry (LC–HRMS/MS) exist. In the following case, femoral blood and urine were applied to systematic toxicological

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Mushtaq, Hamid, Simona Piccolella, Jose A. Mendiola, Lidia Montero, Elena Ibáñez, and Severina Pacifico. "Recovery of Bioactive Constituents from Olive Leaf Pruning Waste of Five Different Cultivars: A Comparison of Green Extraction Techniques to Maximize Health Benefits." Foods 14, no. 2 (2025): 297. https://doi.org/10.3390/foods14020297.

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Sustainable agro-waste revaluation is critical to enhance the profitability and environmental footprint of the olive oil industry. Herein, the valorization of olive leaf pruning waste from five cultivars (‘Caiazzana’, ‘Carolea’, ‘Itrana’, ‘Leccino’, and ‘Frantoio’) employed green extraction methods to recover compounds with potential health benefits. Sequential ultrasound-assisted maceration (UAM) in n-hexane and ethanol was compared with a compressed fluid extraction strategy consisting of supercritical fluid extraction (SFE) and pressurized liquid extraction (PLE) for their efficiency in rec

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14

Hoenigsberger, Michaela, Alexey Kopchinskiy, Christoph Bueschl, et al. "Volatiles from the Mandibular Gland Reservoir Content of Colobopsis explodens Laciny and Zettel, 2018, Worker Ants (Hymenoptera: Formicidae)." Molecules 24, no. 19 (2019): 3468. http://dx.doi.org/10.3390/molecules24193468.

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Forty-five volatile organic compounds (VOCs) were identified or annotated in the mandibular gland reservoir content (MGRC) of the Southeast Asian ant Colobopsis explodens Laciny and Zettel, 2018 (Hymenoptera: Formicidae), using headspace solid-phase microextraction (HS-SPME) coupled to gas chromatography mass spectrometry (GC-MS) and liquid extraction combined with GC-MS. In extension of previous reports on VOCs of C. explodens, members of different compound classes, such as alkanes, aliphatic and aromatic carboxylic acids, and phenolics, were detected. The ketone 2-heptanone and the biochemic

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Gheorghiu, Oana Ramona Cătălina, Anne Marie Ciobanu, Claudia Maria Guțu, et al. "Determination of Phosphodiesterase Type-5 Inhibitors (PDE-5) in Dietary Supplements." Molecules 28, no. 10 (2023): 4116. http://dx.doi.org/10.3390/molecules28104116.

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This study proposed a high-performance thin-layer chromatography (HPTLC) screening method to detect phosphodiesterase 5 (PDE-5) inhibitors as possible adulterant agents in various dietary supplements. Chromatographic analysis was performed on silica gel 60F254 plates using a mixture of ethyl acetate:toluene:methanol:ammonia in a volume ratio of 50:30:20:0.5 as a mobile phase. The system provided compact spots and symmetrical peaks of sildenafil and tadalafil with retardation factor values of 0.55 and 0.90, respectively. The analysis of products purchased from the internet or specialized stores

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Fiorentino, Marika, Simona Piccolella, Claudia Gravina, et al. "Encapsulating Calendula arvensis (Vaill.) L. Florets: UHPLC-HRMS Insights into Bioactive Compounds Preservation and Oral Bioaccessibility." Molecules 28, no. 1 (2022): 199. http://dx.doi.org/10.3390/molecules28010199.

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Wild edible plants, once consumed in times of famine or for health purposes, today represent an interesting dietary supplement, aimed at enriching local dishes and/or formulating healthy nutraceutical products. In fact, the broad content of different, and diversely bioactive, specialized metabolites therein suggests new scenarios of use which, in order to be as functional as possible, must maximize the bioactivity of these compounds while preserving their chemistry. In this context, based on a recent investigation on the metabolic profile of the organs of Calendula arvensis that highlighted th

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Zhu, Chenglin, Xin Pan, Guo Li, et al. "Lipidomics for Determining Giant Panda Responses in Serum and Feces Following Exposure to Different Amount of Bamboo Shoot Consumption: A First Step towards Lipidomic Atlas of Bamboo, Giant Panda Serum and Feces by Means of GC-MS and UHPLC-HRMS/MS." International Journal of Molecular Sciences 23, no. 19 (2022): 11544. http://dx.doi.org/10.3390/ijms231911544.

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Lipidic metabolites play essential roles in host physiological health and growth performance, serving as the major structural and signaling components of membranes, energy storage molecules, and steroid hormones. Bamboo, as wild giant pandas’ exclusive diet, is the main determinant of giant pandas’ lipidome, both as a direct source and through microbiota activity. Interestingly, the consumption of bamboo has attracted little attention from a lipidomic perspective. In the current study, we outline the lipidomic atlas of different parts of bamboo. By gas chromatography—mass spectrometry (GC-MS),

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Wang, Yuqi, Xiaodan Mei, Zihan Liu, et al. "Drug Metabolite Cluster-Based Data-Mining Method for Comprehensive Metabolism Study of 5-hydroxy-6,7,3′,4′-tetramethoxyflavone in Rats." Molecules 24, no. 18 (2019): 3278. http://dx.doi.org/10.3390/molecules24183278.

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The screening of drug metabolites in biological matrixes and structural characterization based on product ion spectra is among the most important, but also the most challenging due to the significant interferences from endogenous species. Traditionally, metabolite detection is accomplished primarily on the basis of predicted molecular masses or fragmentation patterns of prototype drug metabolites using ultra-high performance liquid chromatography coupled with high-resolution mass spectrometry (UHPLC-HRMS). Although classical techniques are well-suited for achieving the partial characterization

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Capperauld, Michael, Daniel Palberg, and R. J. Neil Emery. "Pulp or Potential? Magneto-Priming as a Seed Priming Technique Has Little Effect on Seedling Performance but Results in Significant Alteration of trans-Zeatin and cis-Zeatin in Soybean (Glycine max)." International Journal of Plant Biology 15, no. 4 (2024): 1288–303. https://doi.org/10.3390/ijpb15040089.

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Magneto-priming (MP) has been reported as a sustainable method to enhance crop yield and resistance to adverse environmental conditions; however, any physiochemical basis for these findings remains unavailable. In the present study, soybean (Glycine max) seeds (n = 232) were exposed to a static magnetic field (SMF) of 150–205 mT for 60 min. The effect of SMF exposure on seedling mass, hypocotyl length, radicleemergence rate, total seedling height, leaf area, chlorophyl content, and physiological attributes was evaluated. Differential analysis of the cytokinin (CK) profile of seedling tissues w

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Monga, Gaganpreet Kaur, Anima Ghosal, and Dil Ramanathan. "To Develop the Method for UHPLC-HRMS to Determine the Antibacterial Potential of a Central American Medicinal Plant." Separations 6, no. 3 (2019): 37. http://dx.doi.org/10.3390/separations6030037.

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The development of antibiotic resistance by microbials has long been acknowledged. The major challenge worldwide is to develop novel, natural, and potent antibiotics against the multidrug resistant bacteria. In this study, our aim was to develop the method for a highly sensitive instrument, ultra-high performance liquid chromatograph-high resolution mass spectrometer (UHPLC-HRMS), to evaluate the antibacterial property of a natural product. Aechmea magdalenae (Andre) Andre ex Baker, a plant belonging to the family Bromeliaceae, a native of Central America was used in this study. Based on the a

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Bechynska, Kamila, Jiri Sedlak, Leos Uttl, et al. "Metabolomics on Apple (Malus domestica) Cuticle—Search for Authenticity Markers." Foods 13, no. 9 (2024): 1308. http://dx.doi.org/10.3390/foods13091308.

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The profile of secondary metabolites present in the apple cuticular layer is not only characteristic of a particular apple cultivar; it also dynamically reflects various external factors in the growing environment. In this study, the possibility of authenticating apple samples by analyzing their cuticular layer extracts was investigated. Ultra-high-performance liquid chromatography coupled with high-resolution tandem mass spectrometry (UHPLC-HRMS/MS) was employed for obtaining metabolomic fingerprints. A total of 274 authentic apple samples from four cultivars harvested in the Czech Republic a

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Manaig, Yron Joseph Yabut, Silvia Sandrini, Sara Panseri, et al. "Low n-6/n-3 Gestation and Lactation Diets Influence Early Performance, Muscle and Adipose Polyunsaturated Fatty Acid Content and Deposition, and Relative Abundance of Proteins in Suckling Piglets." Molecules 27, no. 9 (2022): 2925. http://dx.doi.org/10.3390/molecules27092925.

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Elevated omega-6 (n-6) and omega-3 (n-3) polyunsaturated fatty acids (PUFAs) ratios in swine diets can potentially impose a higher risk of inflammatory and metabolic diseases in swine. A low ratio between the two omega PUFAs has beneficial effects on sows’ and piglets’ production performance and immunity status. At present, there are few studies on how sow nutrition directly affects the protein and fat deposition in suckling piglets. Two groups of sows were fed diets with high or low n-6/n-3 polyunsaturated ratios of 13:1 (SOY) and 4:1 (LIN), respectively, during gestation and lactation. Longi

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Alías-Ferri, Maria, Manuela Pellegrini, Emilia Marchei, et al. "New Psychoactive Substances Consumption in Opioid-Use Disorder Patients." Biology 11, no. 5 (2022): 645. http://dx.doi.org/10.3390/biology11050645.

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(1) Background: Since the beginning of the 21st century, the large number and wide chemical variety of new psychoactive substances (NPS) that enter the market every year has become a public health problem. Given the rapidity with which the drug market is changing, many NPS are not clinically investigated and their effects and health risks are unknown. Drug testing is a very useful tool for this purpose, but, unfortunately, it is not very widespread in individuals with opioid-use disorder under detoxification treatment. The aim of this study is to investigate the use of illicit drugs and NPS in

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Radman, Sanja, Martina Čagalj, Vida Šimat, and Igor Jerković. "Seasonal Monitoring of Volatiles and Antioxidant Activity of Brown Alga Cladostephus spongiosus." Marine Drugs 21, no. 7 (2023): 415. http://dx.doi.org/10.3390/md21070415.

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Cladostephus spongiosus was harvested once a month during its growing season (from May to August) from the Adriatic Sea. Algal volatile organic compounds (VOCs) were obtained by headspace solid-phase microextraction (HS-SPME) and hydrodistillation (HD) and analysed by gas chromatography and mass spectrometry (GC-MS). The effects of air drying and growing season on VOCs were determined. Two different extraction methods (ultrasound-assisted extraction (UAE) and microwave-assisted extraction (MAE)) were used to obtain ethanolic extracts of C. spongiosus. In addition, the seasonal antioxidant pote

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Jiménez-Ortega, Luis Alfonso, Jaime Villa-Bojórquez, Pedro de Jesús Bastidas-Bastidas, Rosalba Contreras-Martínez, José Armando Carrillo-Fasio та Manuel Alonzo Báez-Sañudo. "Dynamics of the Dissipation of Acetamiprid, Azoxystrobin, and β-Cyfluthrin in Jalapeño Pepper (Capsicum annuum L.) Produced Under Greenhouse and Open-Field Conditions". Foods 14, № 6 (2025): 1023. https://doi.org/10.3390/foods14061023.

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Pepper is one of the most widely consumed foods around the world. China is the leading producer, while Mexico is the primary exporter. To support these roles, the responsible use of agrochemicals is essential. Additionally, investigating the factors influencing pesticide dissipation is critical to ensure that residue levels do not exceed established Maximum Residue Limits (MRLs) and to achieve the required pre-harvest interval (PHI). This is essential to prevent trade-related issues and mitigate potential health risks to consumers. Consequently, this study aims to evaluate the dissipation dyna

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Fitzgerald, Christopher C. J., Rikard Hedman, Dimanthi R. Uduwela, et al. "Profiling Urinary Sulfate Metabolites With Mass Spectrometry." Frontiers in Molecular Biosciences 9 (February 23, 2022). http://dx.doi.org/10.3389/fmolb.2022.829511.

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The study of urinary phase II sulfate metabolites is central to understanding the role and fate of endogenous and exogenous compounds in biological systems. This study describes a new workflow for the untargeted metabolic profiling of sulfated metabolites in a urine matrix. Analysis was performed using ultra-high-performance liquid chromatography-high resolution tandem mass spectrometry (UHPLC-HRMS/MS) with data dependent acquisition (DDA) coupled to an automated script-based data processing pipeline and differential metabolite level analysis. Sulfates were identified through k-means clusterin

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Ding, Su, Nicole J. Bale, Ellen C. Hopmans, et al. "Lipidomics of Environmental Microbial Communities. II: Characterization Using Molecular Networking and Information Theory." Frontiers in Microbiology 12 (July 12, 2021). http://dx.doi.org/10.3389/fmicb.2021.659315.

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Structurally diverse, specialized lipids are crucial components of microbial membranes and other organelles and play essential roles in ecological functioning. The detection of such lipids in the environment can reveal not only the occurrence of specific microbes but also the physicochemical conditions to which they are adapted to. Traditionally, liquid chromatography coupled with mass spectrometry allowed for the detection of lipids based on chromatographic separation and individual peak identification, resulting in a limited data acquisition and targeting of certain lipid groups. Here, we ex

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Wagmann, Lea, Sascha K. Manier, and Markus R. Meyer. "Can the Intake of a Synthetic Tryptamine be Detected Only by Blood Plasma Analysis? A Clinical Toxicology Case Involving 4-HO-MET." Journal of Analytical Toxicology, June 17, 2021. http://dx.doi.org/10.1093/jat/bkab062.

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Abstract Tryptamines represent a group of hallucinogenic new psychoactive substances with increasing prevalence. Unfortunately, only limited data concerning their toxicology and bioanalysis are available as tryptamines are not included in routine screening procedures in many laboratories. In order to expand the current knowledge, we report a non-fatal clinical toxicology case involving the synthetic tryptamine 4-HO-MET (4-hydroxy-N-methyl-N-ethyl-tryptamine, 3-{2-[ethyl(methyl)amino]ethyl}-1H-indol-4-ol, metocin or methylcybin). As only blood of the intoxicated patient was available, our syste

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Guan, Huanyu, Junyan Ran, Qian Wang, et al. "Tissue Distribution and Biliary Excretion of a Classical Traditional Chinese Medicine Shengjiang Xiexin Decoction in Rats Analyzed by Ultra‐High Performance Liquid Chromatography Coupled to Mass Spectrometry." SEPARATION SCIENCE PLUS 8, no. 7 (2025). https://doi.org/10.1002/sscp.70090.

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ABSTRACTThe side effects caused by chemotherapeutic agent irinotecan (CPT‐11), such as diarrhea and steatosis, limit its clinical application. Shengjiang Xiexin decoction (SXD), a classical traditional Chinese medicine, is utilized to mitigate CPT‐11‐induced diarrhea. In our previous study, SXD was found to influence the hepato‐intestinal metabolism of CPT‐11. To better understand the potential active constituents, it is essential to explore the hepato‐intestinal distribution and excretion characteristics of SXD. In this study, an ultra‐high‐performance liquid chromatography coupled to quadrup

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Hegazi, Nesrine, Amira R. Khattab, Hamada H. Saad, Bishoy Abib, and Mohamed A. Farag. "A multiplex metabolomic approach for quality control of Spirulina supplement and its allied microalgae (Amphora & Chlorella) assisted by chemometrics and molecular networking." Scientific Reports 14, no. 1 (2024). http://dx.doi.org/10.1038/s41598-024-53219-5.

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AbstractMicroalgae species are of economic importance regarded as “green gold” being rich in bioactive compounds. Spirulina and Chlorella are the most popular microalgal species and are marketed as healthy food supplements. At the same time, Amphora holds potential as a source of healthy lipids and essential fatty acids. Yet, there are considerable variations in their reported chemical composition, and less is known about their compositional differences. A multiplexed metabolomic approach was adopted for the quality control (QC) of Spirulina supplements and to compare its constitutive metabolo

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Shaw, Julia, Pamela Brunswick, Tao Huan, and Dayue Shang. "Protecting endangered and CITES listed species: a review of wild American ginseng (P. quinquefolius) identification methods." Discover Plants 2, no. 1 (2025). https://doi.org/10.1007/s44372-025-00209-0.

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Abstract Ginseng, a popular herb in traditional medicine, is commonly believed to possess therapeutic benefits including anti-inflammatory, anticancer, neuroprotective, and antioxidant effects. The popularity of the herb encourages overharvesting of the species’ wild populations, consequentially reducing genetic diversity and threatening their long-term viability. The species has been listed under the Convention on International Trade in Endangered Species (CITES) Appendix II, indicating that it is vulnerable to extinction if its current level of trade and consumption continues uncontrolled. T

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Zhang, Yanjie, Qing Zhao, Youwei Feng, et al. "Integrated Transcriptomic and Metabolomic Analyses Reveal the Mechanisms Underlying Anthocyanin Coloration and Aroma Formation in Purple Fennel." Frontiers in Nutrition 9 (April 27, 2022). http://dx.doi.org/10.3389/fnut.2022.875360.

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The color and aroma are the significant traits of vegetables and fruits, but the metabolic and molecular mechanisms underlying anthocyanin accumulation and aroma formation remain almost unknown in fennel (Anethum foeniculum L.), which is a crucial vegetable crop and grown widely for aromatic leaves and bulbs. Here, ten major anthocyanins identified and quantified by ultra-high performance liquid chromatography coupled with quadrupole Orbitrap high-resolution mass spectrometry (UHPLC-Q-Orbitrap HRMS) were mainly responsible for the coloration of purple fennel leaf. With the application of GC-MS

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Alías-Ferri, María, Manuela Pellegrini, Emilia Marchei, et al. "Synthetic cannabinoids use in a sample of opioid-use disorder patients." Frontiers in Psychiatry 13 (August 3, 2022). http://dx.doi.org/10.3389/fpsyt.2022.956120.

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Cannabis is the most widely consumed illegal drug in the world and synthetic cannabinoids are increasingly gaining popularity and replacing traditional cannabis. These substances are a type of new psychoactive substance that mimics the cannabis effects but often are more severe. Since, people with opioids use disorder use widely cannabis, they are a population vulnerable to use synthetic cannabinoids. In addition, these substances are not detected by the standard test used in the clinical practice and drug-checking is more common in recreational settings. A cross-sectional study with samples o

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Jiang, Meng, Mengwen Peng, Yuxia Li, Guifang Li, Xiaobo Li, and Li Zhuang. "Quality evaluation of four Ferula plants and identification of their key volatiles based on non-targeted metabolomics." Frontiers in Plant Science 14 (January 4, 2024). http://dx.doi.org/10.3389/fpls.2023.1297449.

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IntroductionFerula is a traditional, edible, and important medicinal plant with high economic value. The distinction between edible and non-edible Ferula remains unclear.MethodsIn this study, headspace solid-phase microextraction coupled to gas chromatography-mass spectrometry (HS-SPME/GC-MS) and ultra-high performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS) non-targeted metabolomics techniques were used to systematically and comprehensively analyse secondary metabolites in the leaves and roots of four species of Ferula, considering their edibility.ResultsA total of 166 le

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Ryparova Kvirencova, Jana, Klara Navratilova, Vojtech Hrbek, and Jana Hajslova. "Detection of botanical adulterants in saffron powder." Analytical and Bioanalytical Chemistry, August 17, 2023. http://dx.doi.org/10.1007/s00216-023-04853-x.

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AbstractSaffron is a unique spice obtained by drying stigmas of saffron flowers (Crocus sativus L.). Due to its high price, economically motivated adulteration occurs relatively often. The presented study aimed to develop an effective strategy for the detection of the following potential botanical adulterants used for a saffron substitution or dilution: safflower (Carthamus tinctorius L.), calendula (Calendula officinalis L.), turmeric (Curcuma longa L.), achiote (Bixa orellana L.), red pepper (Capsicum spp.), mountain arnica (Arnica montana L.), beet (Beta vulgaris L.), and pomegranate (Punic

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Gunash, Jan, Juan J. Aristizabal Henao, and Ken D. Stark. "Palmitic and Stearic Free Fatty Acids Are Consistently Found in Materials used for Dried Blood Spot Collection." FASEB Journal 31, S1 (2017). http://dx.doi.org/10.1096/fasebj.31.1_supplement.955.13.

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BackgroundDried blood spotting has been used to collect samples for fatty acid analysis, particularly when access to analytical laboratories or ultra‐cold storage is limited. However, the materials used to collect dried blood spots are often contaminated with lipids and/or fatty acids.ObjectiveTo measure background/containment fatty acid and lipids on materials used to collect dried blood spots.MethodsThree materials used for dried blood spot collection that included 903 protein saver cards (Fischer Scientific, St. Louis, USA), chromatography paper cut into strips (Analtech Inc., Newark, DE),

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Hollender, Juliane, Emma L. Schymanski, Lutz Ahrens, et al. "NORMAN guidance on suspect and non-target screening in environmental monitoring." Environmental Sciences Europe 35, no. 1 (2023). http://dx.doi.org/10.1186/s12302-023-00779-4.

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AbstractIncreasing production and use of chemicals and awareness of their impact on ecosystems and humans has led to large interest for broadening the knowledge on the chemical status of the environment and human health by suspect and non-target screening (NTS). To facilitate effective implementation of NTS in scientific, commercial and governmental laboratories, as well as acceptance by managers, regulators and risk assessors, more harmonisation in NTS is required. To address this, NORMAN Association members involved in NTS activities have prepared this guidance document, based on the current

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