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Journal articles on the topic 'Liquid Chromatography Mass Spectrometry Analysis'

Author: Grafiati

Published: 3 June 2025

Last updated: 31 July 2025

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1

Kataev, S. S., O. N. Dvorskaya, M. A. Gofenberg, A. V. Labutin, and A. B. Melentyev. "ANALYTICAL FEATURES OF SYNTHETIC MDMB(N)-073F CANNABIMIMETICS AND ITS MARKERS IN BIOLOGICAL MATERIAL." Pharmacy & Pharmacology 7, no. 4 (2019): 184–97. http://dx.doi.org/10.19163/2307-9266-2019-7-4-184-197.

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The aim of the research is to study both analytical features of synthetic MDMB(N)-073F cannabimimetics of indazole carboxamides group by gas chromatography methods combined with tandem mass spectrometry (GC-MS) and high performance liquid chromatography with high-resolution mass spectrometry (HPLC-HRMS) as well as characteristics of the major MDMB(N)-073F metabolite, its glucuronide and derivatives, using gas chromatography with mass-spectrometric (GC-MS) detection and high-performance liquid chromatography (HPLC) with MS/MS mass spectrometry (HPLC-MS/MS) in urine samples to be applied in expe

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2

Archita, Tiwari, Dubey Vishwanath, Mishra Shilpi, et al. "General Instrumentation of LC-MS Technique and their Recent Applications." International Journal of Innovative Science and Research Technology 7, no. 5 (2022): 1469–73. https://doi.org/10.5281/zenodo.6760060.

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This review summarizes the advancement in liquid chromatography-mass spectrometry (LC-MS). Liquid Chromatography and Mass Spectrometer is a hyphenated technique of separation of compounds. over the past years, the combination 0f high-performance liquid chromatography and mass spectrometry (LC-MS) has been used which has a remarkable effect on drug research and development. LC-MS played a vital role in the assessment and interpretation of bioavailability and bioequivalence. This article reviews the principle of LCMS analysis using liquid chromatography and mass spectrometry. Mass spectrometry c

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3

Ndjoko, K., J. L. Wolfender, and K. Hostettmann. "Analysis of cannabinoids by liquid chromatography— Thermospray mass spectrometry and liquid chromatography— Tandem mass spectrometry." Chromatographia 47, no. 1-2 (1998): 72–76. http://dx.doi.org/10.1007/bf02466788.

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4

Radović, Radmila, Bojana Radić, Sanja Đekić, Sanja Belić, and Jovana Kos. "State-of-the-art mycotoxin analysis: Insights from LC/MS-MS method." Food and Feed Research, no. 00 (2025): 73. https://doi.org/10.5937/ffr0-55401.

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Mycotoxins are secondary metabolites produced by fungi, known for their chemical and thermal stability, which makes them resistant to common food and feed processing methods. These toxins can contaminate food and feed, and cause a range of toxic effects upon ingestion, including mutagenic, teratogenic, carcinogenic, immunotoxic, neurotoxic, hepatotoxic, and dermatotoxic effects. In recent years, the application of liquid chromatography combined with tandem mass spectrometry has grown significantly for mycotoxin analysis, owing to its remarkable sensitivity and specificity. Recent literature hi

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5

Miroshnichenko, I. I., and Y. E. Shilov. "Analysis of Biological Samples in a Contemporary Laboratory Practice (Review)." Drug development & registration 8, no. 2 (2019): 115–20. http://dx.doi.org/10.33380/2305-2066-2019-8-2-115-120.

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Introduction. In the present publication highlights the key points of the main stages of development of methods for determining trace amounts of drugs and metabolites in biological samples using chromatographic and chromatography-mass spectrometry methods. The main sources of errors are specified. The main attention is paid to chromatography-mass spectrometry, which is the basic method of analysis of small molecules in biological samples. Examples from literary sources and authors' own practice are given.Text. The review highlights some of the practical issues of preparation of calibration sam

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6

Synbulatov, IV V., A. V. Voronin, and T. V. Voronina. "ANALYsis oF RYRRoLIDiNopHENoNE DERivATivEs iN BioLoGiOAL FLuiDs." Aspirantskiy Vestnik Povolzhiya 19, no. 1-2 (2019): 33–40. http://dx.doi.org/10.17816/2072-2354.2019.19.1.33-40.

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Pyrrolidinophenone derivatives are the group of narcotic drugs controlled in the Russian Federation. The review presents the trends of biotransformation of а-pyrrolidinovalerophenone and 3,4-methylenedioxypyrovalerone, the data about their primary metabolites is provided. Various techniques of the sample preparation of biological fluids for analytical toxicology studies for substances of the pyrrolidinophenone derivative group are discussed. The use of enzymatic hydrolysis followed by solid-phase extraction (sorption) provides low detection limits for native sub- PHARMACY ФАРМАЦИЯ stances of t

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7

Midorikawa, Kiyoshi, Arjun H. Banskota, Yasuhiro Tezuka, et al. "Liquid chromatography-mass spectrometry analysis of propolis." Phytochemical Analysis 12, no. 6 (2001): 366–73. http://dx.doi.org/10.1002/pca.605.

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8

Meyer, Martin, Lidia Montero, Sven W. Meckelmann, and Oliver J. Schmitz. "Comparative study for analysis of carbohydrates in biological samples." Analytical and Bioanalytical Chemistry 414, no. 6 (2021): 2117–30. http://dx.doi.org/10.1007/s00216-021-03845-z.

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AbstractThis work presents a comparative study for the analysis of carbohydrates for four common chromatographic methods, each coupled to mass spectrometry. Supercritical fluid chromatography (SFC), hydrophilic interaction liquid chromatography (HILIC), reversed-phase liquid chromatography (RP-LC) and gas chromatography (GC) with detection by triple quadrupole mass spectrometer (QqQ-MS) are compared. It is shown that gas chromatography and reversed-phase liquid chromatography, each after derivatisation, are superior to the other two methods in terms of separation performance. Furthermore, comp

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Gómez-Almenar, M. C., and J. A. García-Mesa. "Determination of pesticide residues in olives by liquid extraction surface analysis followed by liquid chromatography/tandem mass spectrometry." Grasas y Aceites 66, no. 2 (2015): e078. http://dx.doi.org/10.3989/gya.0828142.

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10

Itoh, Satsuki, Nana Kawasaki, Miyako Ohta, and Takao Hayakawa. "Structural analysis of a glycoprotein by liquid chromatography–mass spectrometry and liquid chromatography with tandem mass spectrometry." Journal of Chromatography A 978, no. 1-2 (2002): 141–52. http://dx.doi.org/10.1016/s0021-9673(02)01423-1.

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11

Omelchun, Y., and A. Kobish. "Modern methods for the determination of pesticide residues in beekeeping products and for the diagnostics of bee poisoning." Naukovij vìsnik veterinarnoï medicini, no. 2(176) (December 27, 2022): 101–10. http://dx.doi.org/10.33245/2310-4902-2022-176-2-101-110.

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Intensification of agricultural production is associated with the use of a significant amount of pesticides, which negatively affects the environment and human health, and food products, including beekeeping products, accordingly require mandatory control of residual amounts of pesticides. This article provides a comparative analysis of the available chromatographic methods for pesticide residue research. The necessity of using modern chromatographic methods to determine residual amounts of pesticides in samples of dead bees and beekeeping products is well-founded. Chromatographic methods of s

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12

Loos, Glenn, Ann Van Schepdael, and Deirdre Cabooter. "Quantitative mass spectrometry methods for pharmaceutical analysis." Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences 374, no. 2079 (2016): 20150366. http://dx.doi.org/10.1098/rsta.2015.0366.

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Quantitative pharmaceutical analysis is nowadays frequently executed using mass spectrometry. Electrospray ionization coupled to a (hybrid) triple quadrupole mass spectrometer is generally used in combination with solid-phase extraction and liquid chromatography. Furthermore, isotopically labelled standards are often used to correct for ion suppression. The challenges in producing sensitive but reliable quantitative data depend on the instrumentation, sample preparation and hyphenated techniques. In this contribution, different approaches to enhance the ionization efficiencies using modified s

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13

Betowski, L. Donnelly, and Tammy L. Jones. "The analysis of organophosphorus pesticide samples by high-performance liquid chromatography/mass spectrometry and high-performance liquid chromatography/mass spectrometry/mass spectrometry." Environmental Science & Technology 22, no. 12 (1988): 1430–34. http://dx.doi.org/10.1021/es00177a007.

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14

Mladenovic, Aleksandar, Milka Jadranin, Aleksandar Pavlovic, et al. "Liquid chromatography and liquid chromatography-mass spectrometry analysis of donepezil degradation products." Chemical Industry and Chemical Engineering Quarterly 21, no. 3 (2015): 447–55. http://dx.doi.org/10.2298/ciceq141023047m.

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This study describes the investigation of degradation products of donepezil (DP) using stability indicating RP-HPLC method for determination of donepezil, which is a centrally acting reversible acetylcholinesterase inhibitor. In order to investigate the stability of drug and formed degradation products, a forced degradation study of drug sample and finished product under different forced degradation conditions has been conducted. Donepezil hydrochloride and donepezil tablets were subjected to stress degradation conditions recommended by International Conference on Harmonization (ICH). Donepezi

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15

Dabhi, Ranjitsinh C., Unnati P. Patel, Vaibhavi B. Rathod, Siddharth N. Shah, and Jayesh J. Maru. "Process optimization for acid-amine coupling: a catalytic approach." Current Chemistry Letters 12, no. 1 (2023): 133–40. http://dx.doi.org/10.5267/j.ccl.2022.8.010.

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Proficient routes were devised for coupling different aromatic/aliphatic acids with amines to form amide linkage using various catalysts. Under the optimized reaction conditions, highest conversion was possible without formation of any by-products. All synthesized compounds were purified using column chromatography and characterized by mass spectrometry, nuclear magnetic resonance spectrometry and liquid chromatography-mass spectrometric analysis.

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16

Ahonen, Linda, Pekka Keski-Rahkonen, Taija Saarelainen, et al. "Comparison of liquid chromatography-microchip/mass spectrometry to conventional liquid chromatography–mass spectrometry for the analysis of steroids." Analytica Chimica Acta 721 (April 2012): 115–21. http://dx.doi.org/10.1016/j.aca.2012.01.039.

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17

GAMOH, Keiji, M. C. PRESCOTT, L. J. GOAD, and Suguru TAKATSUTO. "Analysis of brassinosteroids by liquid chromatography/mass spectrometry." Bunseki kagaku 45, no. 6 (1996): 523–27. http://dx.doi.org/10.2116/bunsekikagaku.45.523.

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18

Thakur, Rohan A., and J. Scott Smith. "Liquid Chromatography/Thermospray/Mass Spectrometry Analysis of Beauvericin†." Journal of Agricultural and Food Chemistry 45, no. 4 (1997): 1234–39. http://dx.doi.org/10.1021/jf960506u.

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19

Niessen, W. M. A. "Analysis of antibiotics by liquid chromatography–mass spectrometry." Journal of Chromatography A 812, no. 1-2 (1998): 53–75. http://dx.doi.org/10.1016/s0021-9673(98)00281-7.

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20

WUHRER, M., A. DEELDER, and C. HOKKE. "Protein glycosylation analysis by liquid chromatography–mass spectrometry." Journal of Chromatography B 825, no. 2 (2005): 124–33. http://dx.doi.org/10.1016/j.jchromb.2005.01.030.

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21

Wolfender, Jean-Luc, Marc Maillard, and Kurt Hostettmann. "Thermospray liquid chromatography-mass spectrometry in phytochemical analysis." Phytochemical Analysis 5, no. 4 (1994): 153–82. http://dx.doi.org/10.1002/pca.2800050402.

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22

Syahfitr, Sari Anggraini, and Dan Ridho Asra. "Analysis of Medicinal Chemicals Contained on Jamu: A Review." Asian Journal of Pharmaceutical Research and Development 9, no. 2 (2021): 33–46. http://dx.doi.org/10.22270/ajprd.v9i2.931.

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Background: Jamu is commonly known as an Indonesian traditional herbal medicine that contains ingredients or ingredients derived from plants, animals, minerals, galenic, or mixtures of these ingredients that have been hereditary for medicinal use. Some studies reported the presence of medicinal chemicals that are deliberately added to Jamu. Jamuthat containing medicinal chemicals usually had a faster healing effect compared to Jamu that do not contain medicinal chemicals. Jamu added medicinal chemicals cause serious side effects if it is consumed regularly, overdose, and long period consumptio

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23

Song, Ki-Cheol, Ka-Jeong Lee, Ji-Hoe Kim, Ho-Dong Yoon, Hong-Sik Yu, and Jong-Soo Mok. "Tetramine Analysis using Liquid Chromatography-Tandem Mass Spectrometry and Ion Chromatography." Korean Journal of Fisheries and Aquatic Sciences 44, no. 1 (2011): 45–49. http://dx.doi.org/10.5657/kfas.2011.44.1.045.

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24

Helleur, R. J., and P. Jackman. "Thermal fragmentation analysis of neutral polysaccharides and the presence of 1,6-anhydrooligosaccharides." Canadian Journal of Chemistry 68, no. 7 (1990): 1038–43. http://dx.doi.org/10.1139/v90-162.

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Small quantities of pyrolysates were obtained from micro-scale off-line pyrolysis of the neutral polysaccharides: cellulose, amylose, laminaran, nigeran, and a mannan from ivory nut. The pyrolytic fragments were analyzed by desorption chemical ionization – mass spectrometry, trimethylsilyl derivatization – capillary gas chromatography (– ammonia chemical ionization mass spectrometry) and benzoyl derivatization – high pressure liquid chromatography. Intact 1,6-anhydrohexosemonosaccharide, and -disaccharide fragments were identified as major products. By using off-line analytical pyrolysis infor

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25

Agriopoulou, Sofia, Eygenia Stamatelopoulou, and Theodoros Varzakas. "Advances in Analysis and Detection of Major Mycotoxins in Foods." Foods 9, no. 4 (2020): 518. http://dx.doi.org/10.3390/foods9040518.

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Mycotoxins are the most widely studied biological toxins, which contaminate foods at very low concentrations. This review describes the emerging extraction techniques and the current and alternatives analytical techniques and methods that have been used to successfully detect and identify important mycotoxins. Some of them have proven to be particularly effective in not only the detection of mycotoxins, but also in detecting mycotoxin-producing fungi. Chromatographic techniques such as high-performance liquid chromatography coupled with various detectors like fluorescence, diode array, UV, liq

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26

Kawasaki, Nana, Miyako Ohta, Sumiko Hyuga, Osamu Hashimoto, and Takao Hayakawa. "Analysis of Carbohydrate Heterogeneity in a Glycoprotein Using Liquid Chromatography/Mass Spectrometry and Liquid Chromatography with Tandem Mass Spectrometry." Analytical Biochemistry 269, no. 2 (1999): 297–303. http://dx.doi.org/10.1006/abio.1999.4026.

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27

Chinaka, Satoshi, Yoshiaki Iwamuro, Reiko Iio, et al. "Simultaneous Analysis of Pyrethroid Pesticides by Thin Layer Chromatography, Gas Chromatography/Mass Spectrometry and Liquid Chromatography/Mass Spectrometry." Japanese Journal of Forensic Science and Technology 13, no. 2 (2008): 177–86. http://dx.doi.org/10.3408/jafst.13.177.

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28

Zhang, Jing, and Hongye Zhang. "Research progress on the detection of water-soluble vitamins in food using liquid chromatography." Theoretical and Natural Science 37, no. 1 (2024): 158–69. http://dx.doi.org/10.54254/2753-8818/37/20240183.

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Currently, liquid chromatography is widely used for the analysis and determination of water-soluble vitamins (WSVs) in functional foods. However, due to the diversity of sample characteristics and the requirement for purification accuracy, the chromatographic conditions and specific methods used vary. This paper reviews the chromatographic conditions of liquid chromatography techniques for detecting WSVs in food, as well as the selection of liquid chromatography methods in different application fields. The chromatographic conditions include chromatographic columns, column temperature, mobile p

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29

Sauvage, François-Ludovic, Franck Saint-marcoux, Bénédicte Duretz, Didier Deporte, Gérard Lachatre, and Pierre Marquet. "Screening of Drugs and Toxic Compounds with Liquid Chromatography-Linear Ion Trap Tandem Mass Spectrometry." Clinical Chemistry 52, no. 9 (2006): 1735–42. http://dx.doi.org/10.1373/clinchem.2006.067116.

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Abstract Background: In clinical and forensic toxicology, general unknown screening is used to detect and identify exogenous compounds. In this study, we aimed to develop a comprehensive general unknown screening method based on liquid chromatography coupled with a hybrid triple-quadrupole linear ion trap mass spectrometer. Methods: After solid-phase extraction, separation was performed using gradient reversed-phase chromatography. The mass spectrometer was operated in the information-dependent acquisition mode, switching between a survey scan acquired in the Enhanced Mass Spectrometry mode wi

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30

Kosicka, Katarzyna, Anna Siemiątkowska, Agata Szpera-Goździewicz, Mariola Krzyścin, Grzegorz Bręborowicz, and Franciszek Główka. "High-performance liquid chromatography methods for the analysis of endogenous cortisol and cortisone in human urine: comparison of mass spectrometry and fluorescence detection." Annals of Clinical Biochemistry: International Journal of Laboratory Medicine 56, no. 1 (2018): 82–89. http://dx.doi.org/10.1177/0004563218783789.

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Background The analysis of steroids in biological matrices is challenging. One can apply immunoassay as well as gas and liquid chromatography with various types of detection, depending on the available equipment and the experience of the analyst. The question is how the methods are interchangeable between themselves. Doubts were reported having compared immunoassays and chromatography-mass spectrometry, but there are scarce data on chromatographic methods with detection types other than mass spectrometry. Methods Here, we present the detailed comparison of two liquid chromatographic methods fo

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31

Vanitha Madhuri T, Santhosh Kumar Sorapalli, Kishore Babu Kagitha, et al. "A Review of Liquid Chromatography-Mass Spectrometry and its Applications in Chemical Analysis." Journal of Pharma Insights and Research 2, no. 6 (2024): 025–32. https://doi.org/10.69613/gre1zt18.

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Liquid Chromatography-Mass Spectrometry (LC-MS) has emerged as a powerful analytical technique combining the separation capabilities of liquid chromatography with the high sensitivity and selectivity of mass spectrometry. This sophisticated instrumentation enables precise identification and quantification of complex chemical mixtures across diverse fields including pharmaceuticals, environmental monitoring, food safety, and biological research. Modern LC-MS systems offer enhanced resolution, improved ionization methods, and sophisticated mass analyzers that facilitate accurate molecular weight

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32

Moon, Myeong Hee. "Phospholipid Analysis by Nanoflow Liquid Chromatography-Tandem Mass Spectrometry." Mass Spectrometry Letters 5, no. 1 (2014): 1–11. http://dx.doi.org/10.5478/msl.2014.5.1.1.

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33

WATSON, DAVID, STEPHEN MURRAY, and GRAHAM W. TAYLOR. "Steroid conjugates: analysis by thermospray liquid chromatography–mass spectrometry." Biochemical Society Transactions 13, no. 6 (1985): 1224. http://dx.doi.org/10.1042/bst0131224.

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34

Berberich, David W., Richard A. Yost, and Dean D. Fetterolf. "Analysis of Explosives by Liquid Chromatography/Thermospray/Mass Spectrometry." Journal of Forensic Sciences 33, no. 4 (1988): 12517J. http://dx.doi.org/10.1520/jfs12517j.

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35

Medzihradszky, Katalin F. "Noncovalent Dimer Formation in Liquid Chromatography–Mass Spectrometry Analysis." Analytical Chemistry 86, no. 18 (2014): 8906–9. http://dx.doi.org/10.1021/ac502790j.

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36

Ruhaak, L. Renee, André M. Deelder, and Manfred Wuhrer. "Oligosaccharide analysis by graphitized carbon liquid chromatography–mass spectrometry." Analytical and Bioanalytical Chemistry 394, no. 1 (2009): 163–74. http://dx.doi.org/10.1007/s00216-009-2664-5.

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37

Dreyfuss, Jonathan M., Christopher Jacobs, Yevgeniy Gindin, Gary Benson, Gregory O. Staples, and Joseph Zaia. "Targeted analysis of glycomics liquid chromatography/mass spectrometry data." Analytical and Bioanalytical Chemistry 399, no. 2 (2010): 727–35. http://dx.doi.org/10.1007/s00216-010-4235-1.

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38

Gelpí, Emilio. "Analysis of neuropeptides by liquid chromatography and mass spectrometry." TrAC Trends in Analytical Chemistry 4, no. 6 (1985): XXIII—XXIV. http://dx.doi.org/10.1016/0165-9936(85)88015-8.

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39

Di Stefano, Vita, Giuseppe Avellone, David Bongiorno, et al. "Applications of liquid chromatography–mass spectrometry for food analysis." Journal of Chromatography A 1259 (October 2012): 74–85. http://dx.doi.org/10.1016/j.chroma.2012.04.023.

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40

Min, Jeuk, Chan Seo, Hyung‐Jin Park, et al. "Flavonoid Profiling Analysis by Liquid Chromatography–Tandem Mass Spectrometry." Bulletin of the Korean Chemical Society 40, no. 12 (2019): 1162–66. http://dx.doi.org/10.1002/bkcs.11885.

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41

Niessen, W. M. A., R. A. M. Van Der Hoeven, and J. Van Der Greef. "Analysis of intact oligosaccharides by liquid chromatography/mass spectrometry." Organic Mass Spectrometry 27, no. 3 (1992): 341–42. http://dx.doi.org/10.1002/oms.1210270329.

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42

Shounak, Mande*. "A Review Article on Hyphenated Techniques Used in Analytical Method and Development." International Journal of Pharmaceutical Sciences 3, no. 1 (2025): 2407–17. https://doi.org/10.5281/zenodo.14762916.

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The hyphenated techniques refers to the combination or synthesis of distinct analytical methodologies. Spectroscopic techniques are mostly paired with chromatographic techniques. After that, an interphase will allow the mixture's separated components from the chromatographic approach to enter the spectroscopic technique. In GC-MS After separation from gas chromatography, ionization and mass spectrometry are added to MS. analysis and measurement of the mass-to-charge ratios of the ions that the mass spectrometer generates from each analysis. GC and MS can be connected by a membrane separator, j

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43

Iram, Rashid Gore* Swati Wakchoure¹ Dhanashree Kathole Dev Gaikwad Nishita Hole. "Documentation of Liquid Chromatography-Mass Spectrometry (LC-MS) Technique for Quantitative Analysis of Naproxen in Human Plasma." International Journal of Pharmaceutical Sciences 2, no. 12 (2024): 3064–72. https://doi.org/10.5281/zenodo.14551254.

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Naproxen is a commonly used non steroidal anti-inflammatory drug (NSAID) employed in treatment of pain, fever and inflammation. It has the ability to bind and inhibit synthesis of prostaglandins and produces anti inflammatory effect. Accurate quantification of naproxen in human plasma is essential for bioavailability, pharmacokinetic and clinical studies. Liquid chromatography -Mass Spectrometry has emerged as a gold standard analytical approach for such purpose due to its good sensitivity, specificity and rapid analysis. A quick and selective LC-MS approach for quantification of naproxen in h

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Chen, Su, Qing Li, Paul M. Carvey, and Kawan Li. "Analysis of 9-fluorenylmethyloxycarbonyl derivatives of catecholamines by high performance liquid chromatography, liquid chromatography/mass spectrometry and tandem mass spectrometry." Rapid Communications in Mass Spectrometry 13, no. 18 (1999): 1869–77. http://dx.doi.org/10.1002/(sici)1097-0231(19990930)13:18<1869::aid-rcm731>3.0.co;2-h.

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45

Rhourrhi-Frih, B., C. West, L. Pasquier, P. André, P. Chaimbault, and M. Lafosse. "Classification of natural resins by liquid chromatography–mass spectrometry and gas chromatography–mass spectrometry using chemometric analysis." Journal of Chromatography A 1256 (September 2012): 177–90. http://dx.doi.org/10.1016/j.chroma.2012.07.050.

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46

Watson, D. G., and A. R. Pitt. "Analysis of flavonoids in tablets and urine by gas chromatography/mass spectrometry and liquid chromatography/mass spectrometry." Rapid Communications in Mass Spectrometry 12, no. 4 (1998): 153–56. http://dx.doi.org/10.1002/(sici)1097-0231(19980227)12:4<153::aid-rcm122>3.0.co;2-4.

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47

Garcia, Xavier, Maria Sabaté, Jorge Aubets, Josep Jansat, and Sonia Sentellas. "Ion Mobility–Mass Spectrometry for Bioanalysis." Separations 8, no. 3 (2021): 33. http://dx.doi.org/10.3390/separations8030033.

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This paper aims to cover the main strategies based on ion mobility spectrometry (IMS) for the analysis of biological samples. The determination of endogenous and exogenous compounds in such samples is important for the understanding of the health status of individuals. For this reason, the development of new approaches that can be complementary to the ones already established (mainly based on liquid chromatography coupled to mass spectrometry) is welcomed. In this regard, ion mobility spectrometry has appeared in the analytical scenario as a powerful technique for the separation and characteri

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48

Volmer, Dietrich, and Karsten Levsen. "Mass spectrometric analysis of nitrogen- and phosphorus-containing pesticides by liquid chromatography-Mass Spectrometry." Journal of the American Society for Mass Spectrometry 5, no. 7 (1994): 655–75. http://dx.doi.org/10.1016/1044-0305(94)85007-0.

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49

Onghena, Matthias, Y. Moliner-Martinez, Yolanda Picó, P. Campíns-Falcó, and Damià Barceló. "Analysis of 18 perfluorinated compounds in river waters: Comparison of high performance liquid chromatography–tandem mass spectrometry, ultra-high-performance liquid chromatography–tandem mass spectrometry and capillary liquid chromatography–mass spectrometry." Journal of Chromatography A 1244 (June 2012): 88–97. http://dx.doi.org/10.1016/j.chroma.2012.04.056.

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50

Clemente, M., M. P. Hermo, D. Barrón, and J. Barbosa. "Confirmatory and quantitative analysis using experimental design for the extraction and liquid chromatography–UV, liquid chromatography–mass spectrometry and liquid chromatography–mass spectrometry/mass spectrometry determination of quinolones in turkey muscle." Journal of Chromatography A 1135, no. 2 (2006): 170–78. http://dx.doi.org/10.1016/j.chroma.2006.09.041.

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