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Journal articles on the topic 'Liquid crystals – Synthesis'

Author: Grafiati

Published: 4 June 2021

Last updated: 10 February 2022

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1

Nagaraj, Mamatha. "Liquid Crystals Templating." Crystals 10, no. 8 (2020): 648. http://dx.doi.org/10.3390/cryst10080648.

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Liquid crystal templating is a versatile technique to create novel organic and inorganic materials with nanoscale features. It exploits the self-assembled architectures of liquid crystal phases as scaffolds. This article focuses on some of the key developments in lyotropic and thermotropic liquid crystals templating. The procedures that were employed to create templated structures and the applications of these novel materials in various fields including mesoporous membranes, organic electronics, the synthesis of nanostructured materials and photonics, are described.

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2

Fang, Zeguo, Nawaf Al-Maharik, Peer Kirsch, Matthias Bremer, Alexandra M. Z. Slawin, and David O’Hagan. "Synthesis of organic liquid crystals containing selectively fluorinated cyclopropanes." Beilstein Journal of Organic Chemistry 16 (April 14, 2020): 674–80. http://dx.doi.org/10.3762/bjoc.16.65.

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This paper describes the synthesis of a series of organic liquid crystals (LCs) containing selectively fluorinated cyclopropanes at their termini. The syntheses used difluorocarbene additions to olefin precursors, an approach which proved straightforward such that these liquid crystal candidates could be efficiently prepared. Their physical and thermodynamic properties were evaluated and depending on individual structures, they either displayed positive or negative dielectric anisotropy. The study gives some guidance into effective structure–property relationships for the design of LCs contain

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3

Caldera Villalobos, Martín, Jesús García Serrano, and Ana María Herrera González. "Synthesis, Characterization and Mesomorphic Properties of N,N'-(1,4-Phenylene(methanylylidene))bis(4-(hexyloxy)aniline)." Advanced Materials Research 976 (June 2014): 75–79. http://dx.doi.org/10.4028/www.scientific.net/amr.976.75.

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Liquid crystals (LCs) are compounds that have properties between isotropic liquids and solid crystal materials. Although there is not a parameter to predict this behavior, the liquid crystals reported until now have common characteristics, for example rigid groups such as columns or rods within its structures, and long hydrocarbon chains that give flexibility. In this work we report the synthesis and characterization of LCN,N'-(1,4-phenylene bis (methanylylidene)) bis (4-(hexyloxy) aniline). The compound was characterized by infrared (IR), raman and1H-nuclear magnetic resonance (1H-NMR) spectr

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4

Koide, Naoyuki. "Synthesis of polymer liquid crystals." Kobunshi 36, no. 2 (1987): 98–101. http://dx.doi.org/10.1295/kobunshi.36.98.

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5

Cheng, Zheng Dong, Min Shuai, Andres Mejia, et al. "Disk-Shaped Colloids: The Synthesis and Applications of ZrP Crystals." Advanced Materials Research 787 (September 2013): 177–83. http://dx.doi.org/10.4028/www.scientific.net/amr.787.177.

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We performed systematic experiments on the synthesis of layered crystal α-ZrP and revealed the control of size, aspect ratio and size polydispersity of disk-shaped crystals. The growth of the disks is mediated by oriented attachment, taking place continuously throughout the hydrothermal treatment between various sized disks. The master of the synthesis of layered crystals will contribute to various applications such as the nanocomposites and liquid crystals.

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6

Vill, V., B. Sauerbrei, H. Fischer, and J. Thiem. "Chemoenzymatic synthesis of discotic liquid crystals." Liquid Crystals 11, no. 6 (1992): 949–52. http://dx.doi.org/10.1080/02678299208030698.

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7

Han, Jie, Xiaoyong Chang, Xiaoguang Wang, Lirong Zhu, Meili Pang, and Jiben Meng. "Microwave-assisted synthesis and liquid crystal properties of 1,3,4-thiadiazole-based liquid crystals." Liquid Crystals 36, no. 2 (2009): 157–63. http://dx.doi.org/10.1080/02678290902752124.

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8

Huang, Yuan Ming, Ye Tang Guo, Qing Lan Ma, and Wei Wei Liu. "Synthesis and Characterization of a Cholesteric Liquid Crystal Cholesteryl Nonanoate." Key Engineering Materials 428-429 (January 2010): 94–97. http://dx.doi.org/10.4028/www.scientific.net/kem.428-429.94.

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A cholesteric liquid crystal cholesteryl nonanoate was synthesized and then characterized by means of differential scanning calorimetry and polarized optical microscopy. As temperature decreased from its clearing point, cholesteric phase was formed for cholesteryl nonanoate and accompanied by continuous evolution of colors in the focal conic textures. Furthermore, beautiful spherulite crystals were observed to grow out of the cholesteric phase as the crystallization continued. The evolution of the colors in recorded textures was contributed to temperature-dependent selective reflection of the

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9

YUAN Guo-liang, 员国良, 崔红梅 CUI Hong-mei, 刘文菊 LIU Wen-ju, 梁立志 LIANG Li-zhi, 张晶梅 ZHANG Jing-mei, and 张芳苗 ZHANG Fang-miao. "Synthesis of Chlorinated Liquid Crystals Using Hexachloroethane." Chinese Journal of Liquid Crystals and Displays 26, no. 4 (2011): 432–36. http://dx.doi.org/10.3788/yjyxs20112604.0432.

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10

Wallace, Jason U., Alexander Shestopalov, Tanya Kosc, and Shaw H. Chen. "Scalable Synthesis of Cholesteric Glassy Liquid Crystals." Industrial & Engineering Chemistry Research 57, no. 12 (2018): 4470–73. http://dx.doi.org/10.1021/acs.iecr.8b00667.

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11

Liang, J. C., and R. Hubbard. "Synthesis of Three Ring Ester Liquid Crystals." Molecular Crystals and Liquid Crystals 128, no. 1-2 (1985): 89–97. http://dx.doi.org/10.1080/00268948508082190.

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12

Jun, Qin, Xie Ming-Gui, Hu Zi-Lun, Zhao Hua-Ming, and Liu Shi-Kui. "Synthesis of Alicyclic Crown Ether Liquid Crystals." Synthetic Communications 22, no. 15 (1992): 2253–58. http://dx.doi.org/10.1080/00397919208019079.

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13

Arakawa, Sei'Ichi, Kei'Ichi Nito, and Jun'Etsu Seto. "Synthesis of Fluorine-Containing Ferroelectric Liquid Crystals." Molecular Crystals and Liquid Crystals 204, no. 1 (1991): 15–25. http://dx.doi.org/10.1080/00268949108046590.

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14

Kumar, Sandeep. "ChemInform Abstract: Synthesis of Columnar Liquid Crystals." ChemInform 45, no. 22 (2014): no. http://dx.doi.org/10.1002/chin.201422243.

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15

MAJNUSZ, JERZY. "Synthesis and properties of oligomeric liquid crystals." Polimery 41, no. 07/08 (1996): 418–22. http://dx.doi.org/10.14314/polimery.1996.418.

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16

Sasnouski, G., V. Lapanik, V. Bezborodov, R. Dabrowski, and J. Dziaduszek. "Synthesis of fluoro substituted quaterphenyl liquid crystals." Phase Transitions 87, no. 8 (2014): 783–89. http://dx.doi.org/10.1080/01411594.2014.893341.

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17

Hsu, C. S., K. F. Shyu, Y. Y. Chuang, and Shin-Tson Wu. "Synthesis of laterally substituted bistolane liquid crystals." Liquid Crystals 27, no. 2 (2000): 283–87. http://dx.doi.org/10.1080/026782900203100.

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18

Hegde, Gurumurthy. "Liquid Crystals: Synthesis, Characterization and its Applications." Current Organic Synthesis 18, no. 4 (2021): 317. http://dx.doi.org/10.2174/157017941804210607153832.

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19

Zhao, Ke-Qing, Pin Hu, Hong-Bo Xu, Wen Wan, Zhong-Yuan Zhou, and Liang-Fu Zhang. "Synthesis and Crystal Structure of Mono-Substituted Ferrocene-Containing Liquid Crystals." Molecular Crystals and Liquid Crystals Science and Technology. Section A. Molecular Crystals and Liquid Crystals 364, no. 1 (2001): 759–68. http://dx.doi.org/10.1080/10587250108025046.

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20

Al-Salman, Rihab, Xiangdong Meng, Jiupeng Zhao, et al. "Semiconductor nanostructures via electrodeposition from ionic liquids." Pure and Applied Chemistry 82, no. 8 (2010): 1673–89. http://dx.doi.org/10.1351/pac-con-09-09-25.

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The fascinating properties of ionic liquids make it possible to synthesize semiconductor nanostructures via a simple and low-cost electrochemical pathway. The present paper summarizes our recent work on the synthesis of Si, Ge, and SixGe1–x nanostructures from ionic liquids: thin films, nanowires and photonic crystals. We also introduce our first results on the template-assisted electrodeposition of SixGe1–x photonic crystals from 1-ethyl-3-methylimidazolium bis(trifluoromethylsulfonyl)amide ([EMIm]Tf2N) ionic liquid, and some optical measurements on the previously prepared Ge photonic crystal

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21

Wu, Xi, Hongcheng Wang, Dongxiong Ling, et al. "Synthesis of GaN Crystals by Nitrogen Pressure-Controlled Recrystallization Technique in Na Alloy Melt." Crystals 11, no. 9 (2021): 1058. http://dx.doi.org/10.3390/cryst11091058.

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GaN crystals are synthesized by recrystallization technique in Na-Li-Ca alloy melt under different N2 pressure. X-ray powder diffraction results confirm that the structure of crystals is GaN with wurtzite type and there still have raw powders remaining. The total mass of GaN decreases with the nitrogen pressure reduces. No GaN crystals are found in the solution under N2 pressure of 0.4 MPa. The morphologies of the crystal are mainly prism and pyramid. The size of the crystal increases when closer to the liquid surface. Raman spectra indicates that these crystals are stress-free and crystal gro

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22

Yao, Dan Shu, Feng Li, Hao Jie Wang, et al. "Synthesis and Characterization of Bowl-Shaped Liquid Crystals with a Core of Calix[6]arene." Advanced Materials Research 396-398 (November 2011): 2202–5. http://dx.doi.org/10.4028/www.scientific.net/amr.396-398.2202.

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A new kind of bowl-shaped liquid crystals were designed and synthesized by esterification. They used a calix[6]arene as central unit and ω- cholesteric alkyl diacid monoester as mesogenic arms. Their chemical structures were confirmed by FTIR and 1HNMR spectra, their mesomorphic properties and phase behavior were investigated by differential scanning calorimetry (DSC), polarizing optical microscopy (POM) and X-Ray Diffraction (XRD) measurements. The results showed that the kind of calix[6]arene bowl-shaped liquid crystals N1-N3 exhibited broad range liquid crystalline phases at moderate temper

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23

Srividhya, D., S. Manjunathan, and S. Thirumaran. "Synthesis and Characterization of New Heterocyclic Liquid Crystals." E-Journal of Chemistry 6, no. 3 (2009): 928–37. http://dx.doi.org/10.1155/2009/697928.

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This investigation enumerates the synthesis and mesomorphic properties of 1,2,3-triazole containing azobenzene liquid crystals. In these liquid crystals the methylene chain length at non polar end was varied from six to ten carbons to investigate the association properties of non polar chain on the melt. The compound was designed to have a polar ether chain at the other side of the molecule adjacent to the triazole ring and synthesized to enhance the dipolar interactions. These alterations in chemical structure produce two series of new liquid crystalline compounds with each series containing

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24

Kong, Xiangfei, Zhiqun He, Hemant Gopee, and Andrew N. Cammidge. "Synthesis and liquid crystal properties of triphenylene liquid crystals bearing polymerisable acrylate and methacrylate groups." Liquid Crystals 38, no. 8 (2011): 943–55. http://dx.doi.org/10.1080/02678292.2011.587132.

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25

Akabane, Toshiyuki, Kazuchika Ohta, Tokihiro Takizawa, Takehiro Matsuse, and Mutsumi Kimura. "Discotic liquid crystals of transition metal complexes, 54: Rapid microwave-assisted synthesis and homeotropic alignment of phthalocyanine-based liquid crystals." Journal of Porphyrins and Phthalocyanines 21, no. 07n08 (2017): 476–92. http://dx.doi.org/10.1142/s108842461750047x.

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The most difficult problem on syntheses of the phthalocyanine-based liquid crystals is the long reaction time. In order to shorten the reaction time, we have developed novel Methods A, B and D, for the syntheses of phthalocyanine-based liquid crystals by using microwave heating and/or adding a phase transfer catalysis of Aliquat 336. A series of phthalocyanine derivatives C[Formula: see text]PcZn(1) ([Formula: see text] 10, 12, 14, 16 and 18: a, b, c and e) could be successfully synthesized in a dramatically short reaction time of 30–60 min using Methods A and B by microwave heating. On the ot

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26

Cheng, Kenneth C. K., Marco A. Bedolla-Pantoja, Young-Ki Kim, et al. "Templated nanofiber synthesis via chemical vapor polymerization into liquid crystalline films." Science 362, no. 6416 (2018): 804–8. http://dx.doi.org/10.1126/science.aar8449.

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Extrusion, electrospinning, and microdrawing are widely used to create fibrous polymer mats, but these approaches offer limited access to oriented arrays of nanometer-scale fibers with controlled size, shape, and lateral organization. We show that chemical vapor polymerization can be performed on surfaces coated with thin films of liquid crystals to synthesize organized assemblies of end-attached polymer nanofibers. The process uses low concentrations of radical monomers formed initially in the vapor phase and then diffused into the liquid-crystal template. This minimizes monomer-induced chang

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27

Pesek, Joseph J., Mark A. Vidensek, and Mary Miller. "Synthesis of chemically bonded liquid crystals for high-performance liquid chromatography." Journal of Chromatography A 556, no. 1-2 (1991): 373–81. http://dx.doi.org/10.1016/s0021-9673(01)96234-x.

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28

Hussain, Mariam, Ethan I. L. Jull, Richard J. Mandle, Thomas Raistrick, Peter J. Hine, and Helen F. Gleeson. "Liquid Crystal Elastomers for Biological Applications." Nanomaterials 11, no. 3 (2021): 813. http://dx.doi.org/10.3390/nano11030813.

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The term liquid crystal elastomer (LCE) describes a class of materials that combine the elastic entropy behaviour associated with conventional elastomers with the stimuli responsive properties of anisotropic liquid crystals. LCEs consequently exhibit attributes of both elastomers and liquid crystals, but additionally have unique properties not found in either. Recent developments in LCE synthesis, as well as the understanding of the behaviour of liquid crystal elastomers—namely their mechanical, optical and responsive properties—is of significant relevance to biology and biomedicine. LCEs are

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29

Del Rosso, Pablo, Sandra Hernandez, and Raúl Garay. "Synthesis and Characterization of Bent-rod Liquid Crystals." Molecules 5, no. 12 (2000): 383–85. http://dx.doi.org/10.3390/50300383.

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30

Campos, Daniella Dias Palombino de, and Celso Aparecido Bertran. "Synthesis of carbonated hydroxyapatite nanorods in liquid crystals." Materials Research 12, no. 3 (2009): 265–68. http://dx.doi.org/10.1590/s1516-14392009000300003.

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31

HYODO, Y., S. YAGI, H. KITAYAMA, and H. NAKAZUMI. "Synthesis of Polymer Liquid Crystals Containing Squarylium Dyes." Journal of the Japan Society of Colour Material 76, no. 1 (2003): 3–8. http://dx.doi.org/10.4011/shikizai1937.76.3.

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32

SUI Yan, 隋. 岩., 郭. 剑. GUO Jian, 李正强 LI Zheng-qiang, and 华瑞茂 HUA Rui-mao. "Synthesis and application of triphenylene discotic liquid crystals." Chinese Journal of Liquid Crystals and Displays 31, no. 1 (2016): 40–46. http://dx.doi.org/10.3788/yjyxs20163101.0040.

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33

GUO Jian, 郭剑, 隋岩 SUI Yan, 李正强 LI Zheng-qiang, and 华瑞茂 HUA Rui-mao. "Synthesis and application of organosiloxane smectic liquid crystals." Chinese Journal of Liquid Crystals and Displays 31, no. 9 (2016): 862–69. http://dx.doi.org/10.3788/yjyxs20163109.0862.

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34

Dellinger, Timothy M., and Paul V. Braun. "Lyotropic Liquid Crystals as Nanoreactors for Nanoparticle Synthesis." Chemistry of Materials 16, no. 11 (2004): 2201–7. http://dx.doi.org/10.1021/cm0349194.

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35

Eastwood, A. J., A. E. A. Contoret, S. R. Farrar, et al. "Synthesis and luminous properties of electroluminescent liquid crystals." Synthetic Metals 121, no. 1-3 (2001): 1659–60. http://dx.doi.org/10.1016/s0379-6779(00)00894-8.

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36

Yu, Miao, Yu J. Zhang, Jian H. Shi, Guo F. Liu, and Hong J. Zhang. "Holmium porphyrin compound liquid crystals: Synthesis and properties." Solid State Sciences 11, no. 11 (2009): 2016–22. http://dx.doi.org/10.1016/j.solidstatesciences.2009.06.022.

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37

Hsu, C. S., K. T. Tsay, A. C. Chang, S. R. Wang, and S. T. Wu. "Synthesis of fluorinated naphthylphenylacetylenic and naphthylphenyldiacetylenic liquid crystals." Liquid Crystals 19, no. 4 (1995): 409–14. http://dx.doi.org/10.1080/02678299508032000.

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38

Xie, Ming-Gui, Shi-Kui Liu, Gang-Liu, Long-Zhang Li, and Qing Jiang. "Synthesis of diaza-crown-ether cholesteric liquid crystals." Liquid Crystals 21, no. 3 (1996): 313–16. http://dx.doi.org/10.1080/02678299608032839.

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39

Pavluchenko, A. I., N. I. Smirnova, V. F. Petrov, et al. "Synthesis and Properties of new Halogenated Liquid Crystals." Molecular Crystals and Liquid Crystals Science and Technology. Section A. Molecular Crystals and Liquid Crystals 265, no. 1 (1995): 41–45. http://dx.doi.org/10.1080/10587259508041676.

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40

Lin, Yuhui, and L. C. Chien. "Photo-Asymmetric Synthesis of Helicenes in Liquid Crystals." Molecular Crystals and Liquid Crystals Science and Technology. Section A. Molecular Crystals and Liquid Crystals 301, no. 1 (1997): 267–82. http://dx.doi.org/10.1080/10587259708041777.

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41

Ster, D., U. Baumeister, J. Lorenzo Chao, C. Tschierske, and G. Israel. "Synthesis and mesophase behaviour of ionic liquid crystals." Journal of Materials Chemistry 17, no. 32 (2007): 3393. http://dx.doi.org/10.1039/b705519f.

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42

Timmons, Daren J., Abraham J. Jordan, Angelo A. Kirchon, et al. "Asymmetric flavone-based liquid crystals: synthesis and properties." Liquid Crystals 44, no. 9 (2017): 1436–49. http://dx.doi.org/10.1080/02678292.2017.1281450.

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43

Węgłowska, Dorota, Przemysław Kula, and Jakub Herman. "High birefringence bistolane liquid crystals: synthesis and properties." RSC Advances 6, no. 1 (2016): 403–8. http://dx.doi.org/10.1039/c5ra15291g.

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Twenty both symmetrical and non-symmetrical bistolanes with terminal alkyl, alkoxy and alkylsulfanyl chain and lateral methyl or ethyl group have been synthesized via Sonogashira cross-coupling and their mesomorphic properties have been studied.

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44

Kusumoto, Tetsuo, Ken-ichi Sato, Gullapalli Kumaraswamy, Tamejiro Hiyama, Tadaaki Isozaki, and Yoshiichi Suzuki. "Synthesis and Properties of Deuterated Antiferroelectric Liquid Crystals." Chemistry Letters 24, no. 12 (1995): 1147. http://dx.doi.org/10.1246/cl.1995.1147.

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45

Suzuki, Yoshiichi, Tadaaki Isozaki, Tetsuo Kusumoto, and Tamejiro Hiyama. "Synthesis and Properties of Dimeric Antiferroelectric Liquid Crystals." Chemistry Letters 24, no. 8 (1995): 719–20. http://dx.doi.org/10.1246/cl.1995.719.

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46

Kumar, Sandeep, and Sanjay K. Varshney. "Design and Synthesis of Discotic Nematic Liquid Crystals." Organic Letters 4, no. 2 (2002): 157–59. http://dx.doi.org/10.1021/ol010200v.

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47

Zhao, Ke-Qing, Pin Hu, and Hong-Bo Xu. "Synthesis and Structure of 1,4-Diazabutadiene Liquid Crystals." Molecular Crystals and Liquid Crystals Science and Technology. Section A. Molecular Crystals and Liquid Crystals 364, no. 1 (2001): 801–8. http://dx.doi.org/10.1080/10587250108025051.

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48

Wu, Long-Hai, Yen-Chih Wang, and Chain-Shu Hsu. "Synthesis and characterization of thiophene-containing liquid crystals." Liquid Crystals 27, no. 11 (2000): 1503–13. http://dx.doi.org/10.1080/026782900750018672.

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49

Spells, Darrell J., Christopher Lindsey, Larry R. Dalton, and Shin-Tson Wu. "Synthesis of terminally substituted stilbene-tolane liquid crystals." Liquid Crystals 29, no. 12 (2002): 1529–32. http://dx.doi.org/10.1080/02678290110113496.

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50

Poryvai, Anna, Terezia Vojtylová-Jurkovičová, Michal Šmahel, et al. "Determination of Optical Purity of Lactic Acid-Based Chiral Liquid Crystals and Corresponding Building Blocks by Chiral High-Performance Liquid Chromatography and Supercritical Fluid Chromatography." Molecules 24, no. 6 (2019): 1099. http://dx.doi.org/10.3390/molecules24061099.

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Liquid crystals (LCs) are among the most prominent materials of the current information age, mainly due to their well-known application in liquid crystal displays (LCDs). Their unique electro-optical properties stem from their ability to form organised structures (mesophases) on the transition from solid state to isotropic liquid. Molecules of LCs in a mesophase still maintain the anisotropy of solid crystals, while simultaneously exhibiting the fluidity of liquids, which gives the system the ability to react immediately to external stimuli such as electric or magnetic fields, light, mechanica

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