Academic literature on the topic 'Localised surface plasmon resonance (LSPR)'
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Journal articles on the topic "Localised surface plasmon resonance (LSPR)"
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Kuzminova, Anna, Pavel Solař, Peter Kúš, and Ondřej Kylián. "Double Plasmon Resonance Nanostructured Silver Coatings with Tunable Properties." Journal of Nanomaterials 2019 (April 1, 2019): 1–8. http://dx.doi.org/10.1155/2019/1592621.
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Plasmonic materials that exhibit dual or multiple localised surface plasmon resonances (LSPRs) due to their high application potential in biosensing and biodetection are gaining increasing attention. Here, we report on the novel strategy suitable for the production of silver nanostructured dual-LSPR coatings. This fully vacuum-based technique uses a magnetron sputtering of Ag and a gas aggregation source of silver nanoparticles. It is shown that when combined, produced Ag nano-islands and nanoparticles exhibit due to their different sizes and shapes two independent LSPRs in the visible part of spectra. Furthermore, the intensities and positions of individual LSPR may be precisely controlled by the amount of sputter-deposited nano-islands and a number of Ag nanoparticles, which opens new possibilities for the tailor-made production of novel platforms for surface-enhanced spectroscopic biodetection.
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Bousiakou, Leda G., Hrvoje Gebavi, Lara Mikac, Stefanos Karapetis, and Mile Ivanda. "Surface Enhanced Raman Spectroscopy for Molecular Identification- a Review on Surface Plasmon Resonance (SPR) and Localised Surface Plasmon Resonance (LSPR) in Optical Nanobiosensing." Croatica chemica acta 92, no. 4 (2019): 479–94. http://dx.doi.org/10.5562/cca3558.
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Surface plasmon resonance (SPR) allows for real-time, label-free optical detection of many chemical and biological substances. Having emerged in the last two decades, it is a widely used technique due to its non-invasive nature, allowing for the ultra-sensitive detection of a number of analytes. This review article discusses the principles, providing examples and illustrating the utility of SPR within the frame of plasmonic nanobiosensing, while making comparisons with its successor, namely localized surface plasmon resonance (LSPR). In particular LSPR utilizes both metal nanoparticle arrays and single nanoparticles, as compared to a continuous film of gold as used in traditional SPR. LSPR, utilizes metal nanoparticle arrays or single nanoparticles that have smaller sizes than the wavelength of the incident light, measuring small changes in the wavelength of the absorbance position, rather than the angle as in SPR. We introduce LSPR nanobiosensing by describing the initial experiments performed, shift-enhancement methods, exploitation of the short electromagnetic field decay length, and single nanoparticle sensors are as pathways to further exploit the strengths of LSPR nanobiosensing. Coupling molecular identification to LSPR spectroscopy is also explored and thus examples from surface-enhanced Raman spectroscopy are provided. The unique characteristics of LSPR nanobiosensing are emphasized and the challenges using LSPR nanobiosensors for detection of biomolecules as a biomarker are discussed.
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Mu, Haiwei, Jianxin Wang, Qiang Liu, Wei Liu, Xianli Li, Jingwei Lv, Chao Liu, Famei Wang, Tao Sun, and Paul K. Chu. "Localized Surface Plasmon Resonance Properties of Concentric Dual-Ring Nanodisk." Nano 14, no. 06 (June 2019): 1950071. http://dx.doi.org/10.1142/s1793292019500711.
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The extinction spectral properties based on localized surface plasmon resonance (LSPR) of the concentric dual-ring nanodisk (CDRN) structure are investigated by discrete dipole approximation (DDA) and plasmon hybridization theory. The CDRN nanostructure shows flexible tunable multipole resonances in the near-infrared regime and the coupled resonance wavelengths depend on the structural parameters of the nanostructure, which has great potential in multichannel LSPR-based bio-sensing applications.
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Dey, Priyanka, Shaoli Zhu, Kristofer J. Thurecht, Peter M. Fredericks, and Idriss Blakey. "Self assembly of plasmonic core–satellite nano-assemblies mediated by hyperbranched polymer linkers." J. Mater. Chem. B 2, no. 19 (2014): 2827–37. http://dx.doi.org/10.1039/c4tb00263f.
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Zhang, Xingguang, Aijun Du, Huaiyong Zhu, Jianfeng Jia, Jun Wang, and Xuebin Ke. "Surface plasmon-enhanced zeolite catalysis under light irradiation and its correlation with molecular polarity of reactants." Chem. Commun. 50, no. 90 (2014): 13893–95. http://dx.doi.org/10.1039/c4cc03225j.
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The catalytic performance of zeolites can be boosted by the electric near-field enhancement (ENFE) of plasmonic Au-NPs induced by the localised surface plasmon resonance (LSPR) under visible light irradiation.
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Wang, Chun Zi, Kai Huang, Na Gao, Zhi Ming Wu, and Jun Yong Kang. "Tunable DUV Locolized Plasmonic Absorption by Al Metallic Nanoparticles Arrays." Applied Mechanics and Materials 621 (August 2014): 65–70. http://dx.doi.org/10.4028/www.scientific.net/amm.621.65.
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We dominated localized surface plasmon resonance (LSPR) of aluminum (Al) by controlling their size and density. We report the implementation of Al nanoparticles (NPs) fabricated on the surface of the Ta2O5layer on glass for localized surface plasmon resonances (LSPRs) coupling. The size, density controllable small Al NPs were fabricated using oblique angle deposition method. The optical properties of the NPs array were studied by UV spectrophotometer and finite-difference time-domain (FDTD) simulations. We found that the LSP resonance wavelength of different sizes of Al NPs array exists a blue shift in the extinction spectrum as the particle size decreases.
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Hong, Yoochan, Yong-Min Huh, Dae Sung Yoon, and Jaemoon Yang. "Nanobiosensors Based on Localized Surface Plasmon Resonance for Biomarker Detection." Journal of Nanomaterials 2012 (2012): 1–13. http://dx.doi.org/10.1155/2012/759830.
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Localized surface plasmon resonance (LSPR) is induced by incident light when it interacts with noble metal nanoparticles that have smaller sizes than the wavelength of the incident light. Recently, LSPR-based nanobiosensors were developed as tools for highly sensitive, label-free, and flexible sensing techniques for the detection of biomolecular interactions. In this paper, we describe the basic principles of LSPR-based nanobiosensing techniques and LSPR sensor system for biomolecule sensing. We also discuss the challenges using LSPR nanobiosensors for detection of biomolecules as a biomarker.
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Reyes Gómez, Faustino, Rafael Rubira, Sabrina Camacho, Cibely Martin, Robson da Silva, Carlos Constantino, Priscila Alessio, Osvaldo Oliveira, and J. Mejía-Salazar. "Surface Plasmon Resonances in Silver Nanostars." Sensors 18, no. 11 (November 8, 2018): 3821. http://dx.doi.org/10.3390/s18113821.
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The recent development of silver nanostars (Ag-NSs) is promising for improved surface-enhanced sensing and spectroscopy, which may be further exploited if the mechanisms behind the excitation of localized surface plasmon resonances (LSPRs) are identified. Here, we show that LSPRs in Ag-NSs can be obtained with finite-difference time-domain (FDTD) calculations by considering the nanostars as combination of crossed nanorods (Ag-NRs). In particular, we demonstrate that an apparent tail at large wavelengths ( λ ≳ 700 nm) observed in the extinction spectra of Ag-NSs is due to a strong dipolar plasmon resonance, with no need to invoke heterogeneity (different number of arms) effects as is normally done in the literature. Our description also indicates a way to tune the strongest LSPR at desired wavelengths, which is useful for sensing applications.
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Chen, L., M. Sakamoto, R. Sato, and T. Teranishi. "Determination of a localized surface plasmon resonance mode of Cu7S4 nanodisks by plasmon coupling." Faraday Discussions 181 (2015): 355–64. http://dx.doi.org/10.1039/c4fd00239c.
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Plasmon properties such as peak position, extinction cross-section and local electric field intensity are strongly dependent on excited, localized surface plasmon resonance (LSPR) modes. In non-spherical copper chalcogenide nanoparticles, assignment of the LSPR peaks to the corresponding oscillation modes has been controversial and requires experimental verification. We determined the in-plane LSPR mode of roxbyite Cu7S4 nanodisks from the plasmon coupling effect of nanodisks in solution. Compared with individual Cu7S4 nanodisks, self-assembled Cu7S4 nanodisk arrays in chloroform exhibited a blue-shifted LSPR peak with weaker optical density. This strongly suggests that the singular LSPR peak in the near-infrared region mainly originates from the in-plane oscillation mode. In addition, we demonstrate that the same LSPR peak can be readily tuned by controlling the number of disks in the array.
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Wu, Fan, Lin Cheng, and Wenhui Wang. "Surface Plasmon Resonance of Large-Size Ag Nanobars." Micromachines 13, no. 4 (April 18, 2022): 638. http://dx.doi.org/10.3390/mi13040638.
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Silver nanobars have attracted much attention due to their distinctive localized surface plasmon resonance (LSPR) in the visible and near-infrared regions. In this work, large-size Ag nanobars (length: 400~1360 nm) working at a longer-wavelength near-infrared range (>1000 nm) have been synthesized. By using the finite-difference time-domain (FDTD) simulation, the LSPR properties of a single large-size Ag nanobar are systematically investigated. The LSPR in Ag nanobar can be flexibly tuned in a wide wavelength range (400~2000 nm) by changing the bar length or etching the bar in the length direction. Our work provides a flexible way to fabricate nanoparticle arrays using large-size nanobars and throws light on the applications of large-size nanomaterials on wide spectral absorbers, LSPR-based sensors and nanofilters.
Dissertations / Theses on the topic "Localised surface plasmon resonance (LSPR)"
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Watkins, William L. "Study and development of localised surface plasmon resonance based sensors using anisotropic spectroscopy." Electronic Thesis or Diss., Sorbonne université, 2018. https://accesdistant.sorbonne-universite.fr/login?url=https://theses-intra.sorbonne-universite.fr/2018SORUS505.pdf.
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La résonance de plasmon de surface localisée (LSPR) est définie comme l’oscillation collective du nuage d’électrons de conduction induite par un champ électrique externe. Dans le cas de nanoparticules composé de métaux nobles tels que l’or, l’argent, ou le cuivre,la résonance est localisée dans le visible ou le proche UV. La polarisabilité d’une nanoparticule est directement proportionnelle à quatre paramètres clefs : son volume, sa composition, sa forme et son milieu environnant. Ce sont ces propriétés qui font que la LSPR peut être utilisée à des fin de capteur. Dans le cas d’une particule isotrope, tel que la sphère, le spectre LSPR montre un seul pic d’absorption. Dans le cas d’une particule anisotrope, tel qu’une ellipsoïde, le spectre d’absorption a deux maxima distincts. Si on calcule la section efficace d’absorption en considérant une lumière non polarisée, on obtient deux maxima. Le point clef de ce type de système est la possibilité de découpler les deux résonances en utilisant une lumière polarisée. Dans cette description le système anisotrope est considéré comme microscopique, c’est à dire qu’il ne s’agit que d’une ou deux particules. Dans le cas d’un échantillon macroscopique, tel qu’une solution colloïdale d’ellipsoïdes ou nanotiges, le spectre d’absorption aura toujours deux maxima d’absorption, mais ceux-ci ne pourront pas être découplés car l’échantillon n’est pas globalement anisotrope. En revanche, si l’échantillon présente une anisotropie globale telle que des nanotiges alignés, ou des nanosphères organisées en ligne, il est possible d’avoir un spectre de plasmon dépendant de la polarisation de la lumière. Être capable de découpler les résonances d’un échantillon anisotrope permet de mesurer un spectre différentiel en prenant la différence des deux spectres d’absorption. Cela est expérimentalement possible en utilisant la spectroscopie de transmis- sion anisotrope qui permet la mesure de l’anisotropie optique. L’avantage est d’obtenir un spectre relative et différentiel donc plus stable et reproductible. De plus il est maintenant possible de suivre l’évolution de la réponse optique des particules plasmoniques, non plus en mesurant un déplacement spectral, mais en mesurant le changement d’intensité du signal à une longueur d’onde fixe. Cette méthode est utilisée pour deux cas d’études qui sont la mesure de l’interaction du dihydrogène avec des nanoparticules d’or, ainsi que la détection de faible pression partielle de dihydrogène dans un gaz porteur (argon, et air) à l’aide de palladium, pour des applications de capteur d’hydrogèneLocalised surface plasmon resonance (LSPR) is defined as the collective oscillation of the conduction electron cloud induced by an external electric field. In the case of nanoparticles composed of noble metals such as gold, silver, or copper, the resonance is located in the visible or near UV range. The polarisability of a nanoparticle is directly proportional to four key parameters: its volume, its composition, its shape and its surrounding environment. It is these properties that make LSPR useful for sensor applications. In the case of isotropic particles, such as spheres, the LSPR spectrum shows only one absorption peak. In the case of an anisotropic particle, such as an ellipsoid, the absorption spectrum has two or more distinct peaks. If the absorption cross-section is measured with unpolarised light, multiple maxima are obtained. The key point for these type of systems is the possibility to decouple the resonances using polarised light. In this description the anisotropic system is considered microscopic, i.e. it is only made of one or two particles. In the case of a macroscopic sample, such as a colloidal solution of ellipsoids or nanorods, the absorption spectrum will always have multiple absorption maxima, and they cannot be decoupled because the sample is not globally anisotropic.On the other hand, if the sample has a global anisotropy such as aligned nanorods, or nanosphere organised in lines, it is possible to have a plasmon spectrum dependent on the light polarisation. Being able to decouple the resonances of an anisotropic sample makes it possible to measure a differential spectrum by taking the difference of the two absorption spectra. This is experimentally possible by using anisotropic transmission spectroscopy which measures the optical anisotropy. The advantage is to obtain a relative and differential spectrum more stable and reproducible. Moreover, it is now possible to follow the evolution of the optical response of the plasmonic particles no longer by measuring a spectral shift but by measuring the change in intensity of the signal at a fixed wavelength. This method is used on two case studies which are the measurement of the interaction of dihydrogen with gold nanoparticles, as well as the detection of low partial pressure of dihydrogen in a carrier gas (argon, and air) using palladium nanoparticles, for hydrogen sensing applications
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Rapisarda, Antonino. "Localized Surface Plasmon Resonance: Nanoscale Sensing for Processes at Interfaces." Doctoral thesis, Università di Catania, 2017. http://hdl.handle.net/10761/4022.
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This PhD thesis reports the use the emerging surface-sensitive optical technique of localized surface plasmon resonance (LSPR) to characterize the interaction of relevant classes of biomolecules, e.g. peptides, proteins, lipids and DNA strands, at solid-liquid interfaces, with an emphasis on deciphering kinetics and pathways of dynamic adsorption processes.
LSPR-based biosensor exploits the high sensitivity of the plasmon frequency to refractive index changes confined to 5-30 nanometers around the metal nanoparticles deposited on the sensor surface to monitor in situ and in real time the interaction of unlabeled biological molecules skipping the misleading contribution from the bulk of solution affecting conventional optical technique, e.g. SPR and OWLS.
In the present dissertation the advantages of applying this powerful technique are thoroughly demonstrated by investigating four case studies concerning relevant aspects for the biointerfaces science. The case of study 1 will involve the adsorption kinetics of single and binary solution of proteins onto model hydrophilic and hydrophobic surfaces. The analysis of the adsorption kinetics reveals that competitive adsorption occurs, at physiological pH 7.4 and relatively high ionic strength (NaCl 0.1 M), favoring the heavier protein (fibronectin, in our case), which is shown to adsorb faster and in larger amount than the lighter one (human serum albumin, in our case). The case of study 2 will discuss the DNA hybridization process for binary solutions of respectively perfectly matching (PM) and single base mismatching (MM) 93-mer ssDNA from KRAS codon 12, with a surface tethered probe complementary to the PM sequence. Sensitivity down to obtaining down to 10 nM and 13 nM, respectively for PM and MM were obtained, showing that the hybridization process occurs at a lower rate for MM with respect to PM target. The competitive hybridization was accounted for by an inhibition model, where the non-complementary sequences kinetically hinder the hybridization of the perfect matching sequences, owing to their above mentioned affinity constant differences for the same probe. The case of study 3 will cover the kinetics of phospholipid vesicle adsorption on silicon oxide surfaces as function of pH. Two different regimes have been observed for acidic and basic conditions. At low pH, vesicles adsorption showed one-step exponential kinetics. Moreover, no significantly variation of the adsorption rate was observed over the investigated pH range 3-6, suggesting the process is controlled by Van der Waals interactions and steric forces. At high pH, vesicles adsorb showing two-step kinetic. Furthermore, it was observed that the rate of the first step slows down linearly with the increasing of pH, suggesting that the process is primarily driven by vesicle-surface electrostatic repulsion. The case of study 4 will report preliminary results from the study of pH stimuli-responsive smart surfaces, formed by gold nanodisks array of an LSPR sensor chip decorated with Trichogin GA IV and two of its positively-charged analogs, i.e. Lipo-Lys and L20, in which four and eight Lysines positive charged residues have been introduced respectively. The surface-bound peptides exhibit reversible and rapid switching between conformations and can withstand several cycles of swelling and collapsing with no significant loss from the surfaces.
Overall, the results here reported demonstrated the great potential of LSPR technique as a unique tool to monitor specific and non-specific biomolecular interactions at interfaces in application fields ranging from biosensing to materials science.
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Schenström, Karl. "Biofunctionalization of a Fiber Optics-Based LSPR Sensor." Thesis, Linköpings universitet, Molekylär fysik, 2016. http://urn.kb.se/resolve?urn=urn:nbn:se:liu:diva-125726.
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When exposed to light, metal nanoparticles exhibit a phenomenon known as LSPR, Localized Surface Plasmon Resonance. The wavelengths at which LSPR occurs is very dependent on the refractive index of the surrounding medium. Binding of biomolecules to the surface of gold nanoparticles result in a change in the refractive index that can be detected spectrophotometrically by monitoring the LSPR peak shift. When functionalized with the corresponding ligand(s), gold nanoparticles can be utilized in biosensors to detect the presence and concentration of a predetermined analyte. However, the system must exhibit high specificity and give rise to a detectable shift for analytes in the desired concentration range to be of commercial interest. The aim of the diploma project was to investigate and optimize the biofunctionalization and performance of a fiber optics based LSPR biosensor. Three ligand systems were investigated for detection of antibodies (IgG), insulin and avidin. Binding of the analyte to the ligand caused a shift of a few nanometers when using spherical gold nanoparticles. The shifts were significantly larger when using gold nanorods. When using the IgG and insulin ligands, only minor unspecific binding was observed. The setup thus shows great potential for use in a wide range of sensing applications.
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Marchesini, Matteo. "Plasmon decay dynamics in hybrid metal/doped-semiconductor nanostructures." Master's thesis, Alma Mater Studiorum - Università di Bologna, 2021. http://amslaurea.unibo.it/23223/.
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The study of interactions between plasmonic nanomaterials and dielectrics is a thriving field of research, which in recent years proved that such nanostructures can be applied in a wide range of applications, from sensing to catalysts. These are all based on the nanoscale surface interactions happening between the nanomaterials and their surrounding environment. In this thesis, the possible interaction between plasmonic nanoparticles and the V doping states in the Anatase (TiO_2) bandgap, rather than in their undoped counterpart, is studied. The aim is to better understand the dynamics of these phenomena, and obtaining insights on the V states position in the TiO_2 bandgap. The work done encompasses all the steps needed to achieve the experimental results: from the preparation and characterisation of the samples, to the simulations of the phenomena involved, until the actual measurements of their optical properties and the discussion of the results. The findings achieved are not decisive in explaining the dynamics involved, but preliminary interpretations could be formulated. Moreover, the specific investigations displayed in this thesis have never been done before in literature, and the work performed might be used in the future as a starting point for more thorough and deep studies of these phenomena.
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Geng, Xi. "Bioenabled Synthesis of Anisotropic Gold and Silver Nanoparticles." Diss., Virginia Tech, 2017. http://hdl.handle.net/10919/86274.
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Anisotropic plasmonic noble metallic nanoparticles (APMNs) have received enormous attention due to their distinct geometric features and fascinating physicochemical properties. Owing in large part to their tailored localized surface plasmon resonance (LSPR) and the intensive electromagnetic field at the sharp corners and edges, APMNs are exceptionally well suited for biomedical applications such as biosensing, bioimaging, diagnostics and therapeutics. Although a rich variety of surfactant-assisted colloidal routes have been developed to prepare well-defined APMNs, biomedical applications necessitate tedious and rigorous purification processes for the complete removal of toxic surfactants. In this dissertation, we aim to develop generic bioenabled green synthetic methodologies towards APMNs. By applying a series of thermodynamic, kinetic and seed quality control, a series of APMNs with varied morphologies such as branched nanostars and triangular nanoprisms have been successfully prepared.
We first presented the preparation of gold nanostars (Au NSTs) through a two-step approach utilizing a common Good's buffer, HEPES, as a weak reducing agent. Single crystalline Au NSTs with tunable branches up to 30 nm in length were produced and the halide ions rather than the ionic strength played a significant roles on the length of the branches of Au NSTs. Then consensus sequence tetratricopetide repeat (CTPR) proteins with increasing number of repeats were used as model proteins to probe the effects of concentration as well as the protein shape on the morphology and resulting physicochemical properties of plasmonic gold nanoparticles.
Since the underlying growth mechanism for the biomimetic synthesis of APMNs remains elusive and controversial, the other objective is to elucidate the molecular interactions between inorganic species and biopolymers during the course of NP evolution. Fluorescent quenching and 2D NMR experiments have confirmed the moderate binding affinity of CTPR to the Au(0) and Au(III). We observed that the initial complexation step between gold ions and CTPR3 is ionic strength dependent. Furthermore, we also found that NPs preferentially interact with the negatively charged face of CTPR3 as observed in 2D NMR. Knowledge of binding behavior between biospecies and metal ions/NPs will facilitate rational deign of proteins for biomimetic synthesis of metallic NPs.
A modified seed-mediated synthetic strategy was also developed for the growth of silver nanoprisms with low shape polydispersity, narrow size distribution and tailored plasmonic absorbance. During the seed nucleation step, CTPR proteins are utilized as potent stabilizers to facilitate the formation of planar-twinned Ag seeds. Ag nanoprisms were produced in high yield in a growth solution containing ascorbic acid and CTPR-stabilized Ag seeds. From the time-course UV-Vis and transmission electron microscopy (TEM) studies, we postulate that the growth mechanism is the combination of facet selective lateral growth and thermodynamically driven Ostwald ripening.
By incorporation of seeded growth and biomimetic synthesis, gold nanotriangles (Au NTs) with tunable edge length were synthesized via a green chemical route in the presence of the designed CTPR protein, halide anions (Br⁻) and CTPR-stabilized Ag seeds. The well-defined morphologies, tailored plasmonic absorbance from visible-light to the near infrared (NIR) region, colloidal stability and biocompatibility are attributed to the synergistic action of CTPR, halide ions, and CTPR-stabilized Ag seeds.
We also ascertained that a vast array of biosustainable materials including negatively charged lignin and cellulose derivatives can serve as both a potent stabilizers and an efficient nanocrystal modifiers to regulate the growth of well-defined Ag nanoprisms using a one-pot or seeded growth strategy. The influential effects of reactants and additives including the concentration of sodium lignosulfonate, H2O2 and NaBH4 were studied in great detail. It implies that appropriate physicochemical properties rather than the specific binding sequence of biomaterials are critical for the shaped-controlled growth of Ag NTs and new synthetic paradigms could be proposed based on these findings.
Last but not the least, we have demonstrated the resulting APMNs, particularly, Au NSTs and Ag NTs exhibit remarkable colloidal stability, enhanced SERS performance, making them promising materials for biosensing and photothermal therapy. Since the Ag nanoprisms are susceptible to morphological deformation in the presence of strong oxidant, they also hold great potential for the colorimetric sensing of oxidative metal cation species such as Fe3+, Cr3+, etc.Ph. D.
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Danilov, Artem. "Design, characterisation and biosensing applications of nanoperiodic plasmonic metamaterials." Thesis, Aix-Marseille, 2018. http://www.theses.fr/2018AIXM0110/document.
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Cette thèse considère de nouvelles architectures prometteuses des métamatériaux plasmoniques pour biosensing, comprenant: (I) des réseaux périodiques 2D de nanoparticules d'Au, qui peuvent supporter des résonances des réseaux de surface couplées de manière diffractive; (II) Reseaux 3D à base de cristaux plasmoniques du type d'assemblage de bois. Une étude systématique des conditions d'excitation plasmonique, des propriétés et de la sensibilité à l'environnement local dans ces géométries métamatérielles est présentée. On montre que de tels réseaux peuvent combiner une très haute sensibilité spectrale (400 nm / RIU et 2600 nm / RIU, ensemble respectivement) et une sensibilité de phase exceptionnellement élevée (> 105 deg./RIU) et peuvent être utilisés pour améliorer l'état actuel de la technologie de biosensing the-art. Enfin, on propose une méthode de sondage du champ électrique excité par des nanostructures plasmoniques (nanoparticules uniques, dimères). On suppose que cette méthode aidera à concevoir des structures pour SERS (La spectroscopie du type Raman à surface renforcée), qui peut être utilisée comme une chaîne d'information supplémentaire à un biocapteur de transduction optiqueThis thesis consideres novel promissing architechtures of plasmonic metamaterial for biosensing, including: (I) 2D periodic arrays of Au nanoparticles, which can support diffractively coupled surface lattice resonances; (II) 3D periodic arrays based on woodpile-assembly plasmonic crystals, which can support novel delocalized plasmonic modes over 3D structure. A systematic study of conditions of plasmon excitation, properties and sensitivity to local environment is presented. It is shown that such arrays can combine very high spectral sensitivity (400nm/RIU and 2600 nm/RIU, respectively) and exceptionally high phase sensitivity (> 105 deg./RIU) and can be used for the improvement of current state-of-the-art biosensing technology. Finally, a method for probing electric field excited by plasmonic nanostructures (single nanoparticles, dimers) is proposed. It is implied that this method will help to design structures for SERS, which will later be used as an additional informational channel for biosensing
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Chamorro, Coral William. "Microstructure, chemistry and optical properties in ZnO and ZnO-Au nanocomposite thin films grown by DC-reactive magnetron co-sputtering." Thesis, Université de Lorraine, 2014. http://www.theses.fr/2014LORR0253/document.
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Les matériaux composites peuvent présenter des propriétés qu'aucun des composants individuels ne présente. En outre, à l'échelle du nanomètre les nanocomposites peuvent présenter de nouvelles propriétés par rapport à l'état massif ou à des macrocomposites des mêmes composants en raison d’effets de confinement et d’effets quantiques liés à la taille. Les nanocomposites semi-conducteur/métal sont très intéressants en raison de leurs uniques propriétés catalytiques et opto-électroniques et la possibilité de les ajuster facilement. Ce travail de thèse étudie les interactions spécifiques et les propriétés physiques qui se manifestent dans les films minces de ZnO et nanocomposites ZnO-Au synthétisés par pulvérisation magnétron réactive continue. Premièrement, il est observé qu’il est possible d'ajuster les propriétés microstructurales et optiques des couches de ZnO en réglant les paramètres expérimentaux. La croissance épitaxiale de ZnO sur saphir a été réalisée pour la première fois dans des conditions riches en oxygène sans assistance thermique. En outre, une étude des propriétés optiques met en évidence la relation étroite entre les propriétés optiques et de la chimie des défauts dans les couches minces de ZnO. Un modèle a été proposé pour expliquer la grande dispersion des valeurs de gap rencontrées dans la littérature. Deuxièmement, il a été possible de révéler l'influence profonde de l'incorporation de l'or dans la matrice de ZnO sur des propriétés importantes dans des films nanocomposites. En outre, la présence de défauts donneurs (accepteurs) au sein de la matrice ZnO se permet de réduire (oxyder) les nanoparticules d’or. Ce travail de recherche contribue à une meilleure compréhension des nanocomposites semi-conducteurs/métal et révèle le rôle important de l'état de la matrice semi-conductrice et de la surface des particules pour les propriétés finales du matériauComposite materials can exhibit properties that none of the individual components show. Moreover, composites at the nanoscale can present new properties compared to the bulk state or to macro-composites due to confinement and quantum size effects. The semiconductor/metal nanocomposites are highly interesting due to their unique catalytic and optoelectronic properties and the possibility to tune them easily. This PhD work gives insight into the specific interactions and resulting physical properties occurring in ZnO and ZnO-Au nanocomposite films grown by reactive DC magnetron sputtering. The results can be summarized in two points: First, it was possible to tune the microstructural and optical properties of ZnO. Epitaxial growth of ZnO onto sapphire was achieved for the first time in O2-rich conditions without thermal assistance. Also, a study of the optical properties highlights the close relationship between the bandgap energy (E_g ) and the defect chemistry in ZnO films. A model was proposed to explain the large scatter of the E_g values reported in the literature. Second, the deep influence of the incorporation of gold into the ZnO matrix on important material properties was revealed. Moreover, the presence of donor (acceptor) defects in the matrix is found to give rise to the reduction (oxidation) of the Au nanoparticles. This research work contributes to a better understanding of semiconductor/metal nanocomposites revealing the key role of the state of the semiconductor matrix
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Aksoy, Fuat Yigit. "Interaction of Metal Nanoparticles with Fluorophores and Their Effect on Fluorescence." Doctoral thesis, Saechsische Landesbibliothek- Staats- und Universitaetsbibliothek Dresden, 2009. http://nbn-resolving.de/urn:nbn:de:bsz:14-ds-1240302257150-32578.
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Metal nanoparticles have recently gained popularity in many research areas due to their nanosize-related properties. Depending on the size of the metal nanoparticle, their mode of interaction with electromagnetic radiation and the outcome of this interaction vary; in turn the effect exerted on a protein which is conjugated to a nanoparticle varies, because different sized nanoparticles demonstrate different modes of energy transfer with electromagnetic radiation and molecules conjugated to them. Very small cluster with sizes around 1 – 1.2 nm tend to get excited by incident light and emit fluorescence, whereas larger nanoparticles absorb the incoming light very strongly due to their LSPR. In this study we observed the outcomes of the interaction between two types of nanoparticles, namely gold and gold/silver alloyed nanoparticles with the fluorescence emission of two fluorophores, namely eGFP and rPhiYFP; and demonstrated a bioassay where the fluorescence modulation by gold nanoparticles can be used as the sensing strategy. Lastly, we demonstrated the potential of autofluorescent gold nanoparticles as intracellular reporters.
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Rye, Jan-Michael. "Spatial Modulation Spectroscopy Of Single Nano-Objects In A Liquid Environment For Biosensing Applications." Thesis, Lyon, 2017. http://www.theses.fr/2017LYSE1053/document.
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Le développement de méthodes rapides, précises et ultra-sensibles pour la détection d'analytes cibles en solution est crucial pour la recherche et les applications potentielles en médecine ou biologie moléculaire. Une approche très prometteuse consiste à développer des nano-capteurs à partir de nano-objets métalliques (NOM) qui présentent une résonance d'extinction dans leur réponse optique. Cette résonance nommée résonance de plasmon de surface localisée (RPSL) peut être ajustée spectralement en jouant sur la nature, la morphologie et l'environnement du NOM. Mesurer des modifications sur la RPSL de nano-objets individuels en présence d'analytes cibles doit permettre de s'affranchir des effets de moyennes dans les mesures d'ensemble. De plus, cela ouvre la voie vers le développement d'échantillons micrométriques pour des tests multicibles sans étiquette (« label-free »).Dans ce travail on a développé un nouveau dispositif expérimental basé sur la technique de spectroscopie à modulation spatiale (SMS) permettant de sonder la réponse optique de NOM individuels en milieu liquide. En parallèle des méthodes de synthèse ont été mises au point pour obtenir des échantillons sondes stables permettant des mesures sur NOM unique, en particulier sur des bipyramides d'or qui présentent de nombreuses qualités intrinsèques faisant d'elles de bonnes candidates pour le « bio-sensing ».Des mesures ont été réalisées dans des environnements d'indice variable et les changements détectés sont en bon accord avec les simulations théoriques. De plus, de nombreuses études ont été réalisées pour comprendre l'influence des nombreux paramètres agissant sur la réponse optique des systèmes étudiésAdvances in the development of rapid, accurate and highly sensitive methods for detecting target analytes in solution will provide crucial tools for research and applications in medicine and molecular biology. One of the currently most promising approaches is the development of nanosensors based on the localized surface plasmon resonance (LSPR) of noble metal nano-objects (MNOs), which is an optical response that depends on their size, shape, composition and local environment. The ability to measure the modification of the reponse of a single MNO in the presence of a target analyte would allow each object to act as an independent probe with increased sensitivity as the signal would be isolated from the averaging effects of ensemble measurements. Furthermore it would allow the development of micrometric, functionalized multiprobe samples for multitarget label-free assays.In this work, a novel experimental setup based on the spatial modulation spectroscopy (SMS) technique has been developed to measure the optical response of individual nano-objects in a liquid environment. In parallel, a new technique has also been developed to elaborate stable probes for measurements with the new setup, with a focus on gold bipyramids due to numerous qualities that make them excellent candidates for biosensing probes. The setup has been used to measure the response of individual objects in environments of different real refractive indices and the detected changes have been shown to be in good agreement with theoretical calculations. Numerical studies have also been performed to investigate the influence on the optical response of numerous factors encountered in the studied systems
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Kaya, Zeynep. "Controlled and localized synthesis of molecularly imprinted polymers for chemical sensors." Thesis, Compiègne, 2015. http://www.theses.fr/2015COMP2220.
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Les polymères à empreintes moléculaires (MIP), également appelés "anticorps en plastique", sont des récepteurs biomimétiques synthétiques qui sont capables de reconnaître et lier une molécule cible avec une affinité et une spécificité comparables à celles des récepteurs naturels tels que des enzymes ou des anticorps. En effet, les MIP sont utilisés comme éléments de reconnaissance synthétiques dans les biocapteurs et biopuces pour la détection de petits analytes et les protéines. La technique d'impression moléculaire est basée sur la formation de cavités de reconnaissance spécifiques dans des matrices polymères par un procédé de moulage à l'échelle moléculaire. Pour la conception de capteurs et biopuces, une cinétique d'adsorption et une réponse du capteur rapide, l'intégration des polymères avec des transducteurs, et une haute sensibilité de détection sont parmi les principaux défis. Dans cette thèse, ces problèmes ont été abordés par le développement de nanocomposites MIP / d'or via le greffage du MIP sur les surfaces en utilisant des techniques de polymérisation dédiées comme l'ATRP qui est une technique de polymérisation radicalaire contrôlée (CRP). Ces techniques CRP sophistiquées sont en mesure d'améliorer considérablement les matériaux polymères. L'utilisation de l'ATRP dans le domaine de MIP a été limitée jusqu'à présent en raison de son incompatibilité inhérente avec des monomères acides comme l'acide méthacrylique (MAA), qui est de loin le monomère fonctionnel le plus largement utilisé dans les MIP. Ici, un nouveau procédé est décrit pour la synthèse de MIP par ATRP photo-initiée utilisant fac-[Ir(Ppy)3] comme catalyseur. La synthèse est possible à température ambiante et est compatible avec des monomères acides. Cette étude élargit considérablement la gamme de monomères fonctionnels et de molécules empreintes qui peuvent être utilisés lors de la synthèse de MIP par ATRP. La méthode proposée a été utilisée pour la fabrication de nanocomposites hiérarchiquement organisés sur des surfaces métalliques nanostructurés avec des nano-trous et nano-ilots, présentant des effets plasmoniques pour l'amplification du signal. La synthèse de films de MIP à l'échelle du nanomètre localisés sur la surface d'or a été démontrée. Des méthodes de transduction optiques, à savoir la résonance de plasmons de surface localisée (LSPR) et la spectroscopie Raman exaltée par effet de surface (SERS) ont été exploitées. Ces techniques se sont montrées prometteuses pour l'amélioration de la limite de détection dans la détection d'analytes biologiquement pertinents, y compris les protéines et le médicament propranololMolecularly imprinted polymers (MIPs), also referred to as plastic antibodies, are synthetic biomimetic receptors that are able to bind target molecules with similar affinity and specificity as natural receptors such as enzymes or antibodies. Indeed, MIPs are used as synthetic recognition elements in biosensors and biochips for the detection of small analytes and proteins. The molecular imprinting technique is based on the formation of specific recognition cavities in polymer matrices by a templating process at the molecular level. For sensor and biochip development, fast binding kinetics of the MIP for a rapid sensor response, the integration of the polymers with transducers, and a high sensitivity of detection are among the main challenges. In this thesis, the above issues are addressed by developing MIP/gold nanocomposites by grafting MIPs on surfaces, using dedicated techniques like atom transfer radical polymerization (ATRP) which is a versatile controlled radical polymerization (CRP) technique. Theses ophisticated CRP techniques, are able to greatly improve the polymeric materials. The use of ATRP in the MIP field has been limited so far due to its inherent incompatibility with acidic monomers like methacrylic acid (MAA), which is by far the most widely used functional monomer. Herein, a new method is described for the MIP synthesis through photo-initiated ATRP using fac-[Ir(ppy)3] as ATRP catalyst. The synthesis is possible at room temperature and is compatible with acidic monomers. This study considerably widens the range of functional monomers and thus molecular templates that can be used when MIPs are synthesized by ATRP. The proposed method was used for fabrication of hierarchically organised nanocomposites based on MIPs and nanostructured metal surfaces containing nanoholes or nanoislands, exhibiting plasmonic effects for signal amplification. The fabrication of nanometer scale MIP coatings localized on gold surface was demonstrated. Optical transduction methods, namely Localized Surface Plasmon Resonance (LSPR) and Surface Enhanced Raman Spectroscopy (SERS) were exploited and shown that they hold great promise for enhancing the limit of detection in sensing of biologically relevant analytes including proteins and the drug propranolol
Book chapters on the topic "Localised surface plasmon resonance (LSPR)"
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Raj, Aparna, and Riju K. Thomas. "Localized Surface Plasmon Resonance (LSPR) Applications of Gold (Au) and Silver (Ag) Nanoparticles." In Optical and Molecular Physics, 43–69. Boca Raton: Apple Academic Press, 2021. http://dx.doi.org/10.1201/9781003150053-4.
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Wei, Jianjun, Zheng Zeng, and Yongbin Lin. "Localized Surface Plasmon Resonance (LSPR)-Coupled Fiber-Optic Nanoprobe for the Detection of Protein Biomarkers." In Biosensors and Biodetection, 1–14. New York, NY: Springer New York, 2017. http://dx.doi.org/10.1007/978-1-4939-6848-0_1.
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Vaskevich, Alexander, and Israel Rubinstein. "Localized Surface Plasmon Resonance (LSPR) Transducers Based on Random Evaporated Gold Island Films: Properties and Sensing Applications." In Nanoplasmonic Sensors, 333–68. New York, NY: Springer New York, 2012. http://dx.doi.org/10.1007/978-1-4614-3933-2_14.
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Vergara-Irigaray, Nuria, Michèle Riesen, Gianluca Piazza, Lawrence F. Bronk, Wouter H. P. Driessen, Julianna K. Edwards, Wadih Arap, et al. "Local Surface Plasmon Resonance (LSPR)." In Encyclopedia of Nanotechnology, 1224. Dordrecht: Springer Netherlands, 2012. http://dx.doi.org/10.1007/978-90-481-9751-4_100361.
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H. Mahdi, Rasha, and Hussein A. Jawad. "Plasmonic Optical Nano-Antenna for Biomedical Applications." In Plasmonic Nanostructures - Basic Concepts, Optimization and Applications. IntechOpen, 2023. http://dx.doi.org/10.5772/intechopen.105458.
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Plasmonics attract significant attention of the researchers due to Plasmon’s surpassing ability to match free space electromagnetic (EM) excitation into the nano-scale size and conduct the light-tissue interaction in this scale. Plasmonic nano-antennas (PNAs) is a coupling of EM waves into Localized Surface Plasmon Resonance (LSPR) which is considered as an interesting subject for theoretical and experimental study. This presents a new concept of the confinement of light in subwavelength scales with huge local fields which can generate very high near field intensities because of their LSPR. The generated field is invested in various applications that are depending on near field enhancement produced by plasmonic optical nano-antennas (PONAs) such as Surface-Enhanced Raman Spectroscopy (SERS), biosensing, spectral imaging and cancer treatment. Bowtie shape PNAs (PBNAs) can transfer the light field efficiently by converting the light from external space into a subwavelength spectral region with the improvement at an optical wavelength in a tiny area between its antenna arms. The local EM field production in a gap area is the main reason to suggest PBNAs shape if the frequency of the incident EM waves coincide the structural resonance peak so it is acting as a tunable hot spot.
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Gambhir, Kaweri, and Agnikumar G. Vedeshwar. "Types of Nonlinear Interactions between Plasmonic-Excitonic Hybrids." In Plasmonics [Working Title]. IntechOpen, 2022. http://dx.doi.org/10.5772/intechopen.105833.
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The unique ability of plasmonic structures to concentrate and manipulate photonic signals in deep sub-wavelength domain provides new efficient pathways to generate, guide, modulate and detect light. Due to collective oscillations exhibited by the conducting electrons of metallic nanoparticles, their local fields can be greatly enhanced at the localized surface plasmon resonance (LSPR). Hence, they offer a versatile platform, where localized surface plasmons can be tuned over a broad range of wavelengths by controlling their shape, size and material properties. It has been realized that plasmonic excitations can strengthen nonlinear optical effects in three ways. First, the coupling between the incident beam of light and surface plasmons results in a strong local confinement of the electromagnetic fields, which in turn enhances the optical response. Second, the sensitivity of plasmonic excitations toward the dielectric properties of the metal and the surrounding medium forms the basis for label-free plasmonic sensors. Finally, the excitation and relaxation dynamics of plasmonic nanostructures responds to a timescale of femtoseconds regime, thus allowing ultrafast processing of the incident optical signals. This chapter aims to discuss all the aforementioned interactions of plasmons and their excitonic hybrids in detail and also represent a glimpse of their experimental realizations.
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"Local Surface Plasmon Resonance (LSPR)." In Encyclopedia of Nanotechnology, 1808. Dordrecht: Springer Netherlands, 2016. http://dx.doi.org/10.1007/978-94-017-9780-1_100485.
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Bhargav, Anjali, and Neeraj Kumar Rai. "SPR-Based Biosensors in the Diagnostics and Therapeutics." In Recent Advances in Biosensor Technology, 78–96. BENTHAM SCIENCE PUBLISHERS, 2023. http://dx.doi.org/10.2174/9789815123739123010007.
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To analyze the physio-chemical measures of the cellular environment and display them in digital units, transducing methods are applied in biosensors. The label.free biosensors employ biophysical characteristics such as spectroscopic methods, crystallization, and Surface plasmonic resonance (SPR) to determine the availability or concentration of substances. SPR is a method to elucidate interaction among biomolecules exhibiting affinity binding, structural changes, or alteration in pathological conditions. SPR methods are now employed in conjunction with a variety of transducer topologies, including optical fibers, nanoparticle-based SPR, immobilized or localized SPR (LSPR), long-range SPR, image SPR, immune-assay-based SPR, and phase sensing SPR biosensors' versatile configuration allows for the early detection of several illnesses, such as COVID-19, dengue, non-invasive cancer, biomarker-based fetuses identification, therapeutic antibody characterization, drug monitoring, etc. SPR system is leading in diagnostics and therapeutics with various advantages, such as their portable size, cost-effectiveness, quick result, and easy-to-handle method, but at extension, this technique needs development to ensure high sensitivity, averting background effect and evolution of label-free direct detector to quantify real sample. This chapter reviews the model’s instrumentation and bioassay of clinical samples from SPR and its associated biosensor.
Conference papers on the topic "Localised surface plasmon resonance (LSPR)"
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Vasilevskiy, M. "MODELLING OF ENVIRONMENT SENSORS BASED ON THE SURFACE PLASMON RESONANCE EFFECT." In Mathematical modeling in materials science of electronic component. LLC MAKS Press, 2020. http://dx.doi.org/10.29003/m1516.mmmsec-2020/50-51.
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Surface plasmons (SPs) are collective excitations of free electrons in a conducting medium bounded by a surface or interface with a dielectric. They can originate surface plasmon-polaritons (SPPs), which are evanescent waves involving electron density oscillations and the associated electromagnetic (EM) field whose amplitude decays exponentially with distance from the surface. SPPs are characterised by a dispersion curve (frequency vs wavevector along the interface) that lies outside of the light cone, so they cannot be excited directly by propagating light; however, it is possible to excite them using the Attenuated Total internal Reflection (ATR) method or a periodic grating. SPs in a confined geometry such as a metallic sphere are localised in space and characterised by discrete frequencies (a single one in the case of sphere, two or three in the case of an ellipsoid). They can be excited directly by propagating light if its frequency coincides with the localised SP frequency, giving rise to the Localized Surface Plasmon Resonance (LSPR). Both SPPs and LSPR are highly sensitive to the dielectric constant of the surrounding media and can be used for environment sensing (e.g. gas molecules that adsorb onto the structure’s surface).
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Chamanzar, Maysamreza, and Ali Adibi. "On-chip localized surface Plasmon resonance (LSPR) sensing." In 2011 IEEE Photonics Conference (IPC). IEEE, 2011. http://dx.doi.org/10.1109/pho.2011.6110471.
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Chamanzar, Maysamreza, Zhixuan Xia, Ehsan Shah Hosseini, Siva Yegnanarayanan, and Ali Adibi. "On-chip Localized Surface Plasmon Resonance (LSPR) Sensing using Hybrid Plasmonic-photonic-fluidic Structures." In CLEO: Science and Innovations. Washington, D.C.: OSA, 2012. http://dx.doi.org/10.1364/cleo_si.2012.cth4l.3.
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Rivero, Pedro J., Miguel Hernaez, Javier Goicoechea, Ignacio R. Matias, and Francisco J. Arregui. "Optical fiber refractometers based on localized surface plasmon resonance (LSPR) and lossy mode resonance (LMR)." In OFS2014 23rd International Conference on Optical Fiber Sensors, edited by José M. López-Higuera, Julian D. C. Jones, Manuel López-Amo, and José L. Santos. SPIE, 2014. http://dx.doi.org/10.1117/12.2059259.
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Gezgin, Serap Yiğit, Abdullah Kepceoğlu, and Hamdi Şükür Kılıç. "An investigation of localised surface plasmon resonance (LSPR) of Ag nanoparticles produced by pulsed laser deposition (PLD) technique." In TURKISH PHYSICAL SOCIETY 32ND INTERNATIONAL PHYSICS CONGRESS (TPS32). Author(s), 2017. http://dx.doi.org/10.1063/1.4976367.
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Dewasi, Avijit, and Anirban Mitra. "Ag-nanoislands Mediated TiO2 Multilayer Thin Films towards Perfect Absorber." In JSAP-OSA Joint Symposia. Washington, D.C.: Optica Publishing Group, 2018. http://dx.doi.org/10.1364/jsap.2018.18p_211b_4.
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Shin, Yong-Beom, Na rae Jo, and Ki joong Lee. "Ultra-Sensitive Detection of Biomarker using Localized Surface Plasmon Resonance (LSPR) enhanced by ELISA." In European Conference on Biomedical Optics. Washington, D.C.: OSA, 2015. http://dx.doi.org/10.1364/ecbo.2015.95371f.
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Algorri, J. F., B. García-Cámara, A. García-García, V. Urruchi, and J. M. Sánchez-Pena. "Theoretical modeling of a Localized Surface Plasmon Resonance (LSPR) based fiber optic temperature sensor." In OFS2014 23rd International Conference on Optical Fiber Sensors, edited by José M. López-Higuera, Julian D. C. Jones, Manuel López-Amo, and José L. Santos. SPIE, 2014. http://dx.doi.org/10.1117/12.2059657.
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Santavanond, Kawintida, Charusluk Viphavakit, Wisarn Patchoo, Hala El-Khozondar, and Waleed Mohammed. "Numerical Investigation of Localized Surface Plasmon Resonance (LSPR) based Sensor for Glucose Level Monitoring." In 2021 Second International Symposium on Instrumentation, Control, Artificial Intelligence, and Robotics (ICA-SYMP). IEEE, 2021. http://dx.doi.org/10.1109/ica-symp50206.2021.9358441.
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Shin, Yong-Beom, Na rae Jo, and Ki joong Lee. "Ultra-sensitive detection of biomarker using localized surface plasmon resonance (LSPR) enhanced by ELISA." In European Conferences on Biomedical Optics, edited by J. Quincy Brown and Volker Deckert. SPIE, 2015. http://dx.doi.org/10.1117/12.2183063.
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