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Journal articles on the topic 'Mechanical ball milling'

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1

Zewude, Dagmawi Abebe, Hironori Izawa, and Shinsuke Ifuku. "Optimization of Chitin Nanofiber Preparation by Ball Milling as Filler for Composite Resin." Journal of Composites Science 6, no. 7 (2022): 197. http://dx.doi.org/10.3390/jcs6070197.

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Chitin nanofiber is a nanomaterial produced by pulverizing chitin, the main component of crab shells. Since it has excellent mechanical properties, it is expected to be used as a reinforcing material to strengthen materials. Chitin was mechanically ground in water using a ball mill to prepare nanofibers. The ball size, total ball weight, and milling time were varied, and the resulting water dispersion and the cast film were analyzed to optimize the conditions for efficient preparation. The length and width of the nanofibers were also measured by SEM and AFM observations. The size of the balls
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2

Kim, Minju, Gyu Min Kim, Won-Seok Chang, and Young-Kee Kim. "Enhancing Microalgae Content in Biocomposites through a Mechanical Grinding Method." Polymers 15, no. 23 (2023): 4557. http://dx.doi.org/10.3390/polym15234557.

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Microalgae-based biocomposites are gaining traction as ecofriendly and cost-effective alternatives to conventional petroleum-based plastics. However, achieving a homogeneous dispersion of microalgae within a biocomposite matrix remains a challenge. In this study, we investigated the effect of the size of dried microalgae (Chlorella sp.) on the quality of biocomposites. Ball milling, a mechanical grinding process, was used to control the size of the pretreated dried microalgae. Our results demonstrate that the microalgae size strongly depends on the total weight of the stainless-steel balls, ra
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3

Zhang, Lei, Zhifu Huang, Yangzhen Liu, et al. "Effects of Mechanical Ball Milling Time on the Microstructure and Mechanical Properties of Mo2NiB2-Ni Cermets." Materials 12, no. 12 (2019): 1926. http://dx.doi.org/10.3390/ma12121926.

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Mo2NiB2-Ni cermets have been extensively investigated due to their outstanding properties. However, studies have not systematically examined the effect of the powder milling process on the cermets. In this study, Mo, Ni, and B raw powders were subjected to mechanical ball milling from 1 h to 15 h. XRD patterns of the milled powders confirmed that a new phase was not observed at milling times of 1 h to 15 h. With the increase in the mechanical ball milling time from 1 h to 11 h, raw powders were crushed to small fragments, in addition to a more uniform distribution, and with the increase in the
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4

Zuo, Min, De Gang Zhao, Zhen Qing Wang, Hao Ran Geng, Hui Jun Zhang, and Long Pu. "Investigation on an Al/WC Composite Coating of A356 Alloy Fabricated by Mechanical Alloying." Materials Science Forum 788 (April 2014): 231–35. http://dx.doi.org/10.4028/www.scientific.net/msf.788.231.

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In this paper, Al/WC composite coatings on A356 alloy were prepared by mechanical alloying, and their mechanical properties were characterized. The processing parameters for mechanical milling treatment, such as the premixing process of Al and WC powders, the ball-to-powder weight ratio and the milling duration, have been optimized, and the optimum ball-to-powder weight ratio and milling time were determined to be 14:1 and 12 h, respectively. It was found that premixed Al and WC powders have no significant influence on Brinell hardness due to the powders adhering to the balls and milling tank
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5

Zheng, Minli, Chunsheng He, and Shucai Yang. "Thermo-mechanical coupling behaviour when milling titanium alloy with micro-textured ball-end cutters." Proceedings of the Institution of Mechanical Engineers, Part E: Journal of Process Mechanical Engineering 234, no. 6 (2020): 562–75. http://dx.doi.org/10.1177/0954408920931958.

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The high-speed milling of titanium alloy is a very complex nonlinear dynamic cutting process, and there are mutual coupling effects between multiple physical fields of the tool. Therefore, the thermo-mechanical coupling behavior of micro-textured ball-end milling cutters during the cutting of titanium alloy was studied in depth, combined with theoretical calculations, milling experiments and simulation analysis. First, based on the experimental data of milling titanium alloy, the stress field of the micro-textured ball-end milling cutter was solved. Then, the dimensional method was used to sol
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6

Xu, Jian Lin, Liang Zhang, Qiang Guo, Sheng Gang Zhou, and Chong Feng. "Research on the Preparation of Antimony Nanoparticles by Mechanical Ball Milling." Key Engineering Materials 609-610 (April 2014): 244–49. http://dx.doi.org/10.4028/www.scientific.net/kem.609-610.244.

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Taking antimony powder with 75μm of average particle size as raw material, the antimony nanoparticles were synthesized by mechanical ball milling. Crystalline structure, morphology and particle size of the antimony nanoparticles were characterized by XRD, TEM and FT-IR. The effect of milling mediums and ball milling speed on results antimony nanoparticles were studied using dry grinding and wet grinding methods. The results show that the antimony nanoparticles can be prepared successfully by wet process of ball milling. When the ball milling speed is 150 r/min and the milling mediums is a comp
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7

Gao, Ziqi, Quanjiabao Han, Jianbang Liu, et al. "Dispersion of Carbon Nanotubes Improved by Ball Milling to Prepare Functional Epoxy Nanocomposites." Coatings 13, no. 3 (2023): 649. http://dx.doi.org/10.3390/coatings13030649.

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There has been an increase in interest in developing functional polymer composites based on green chemistry principles. The purpose of this study was to investigate the preparation of functional epoxy/carbon nanotube nanocomposites using ball milling methods. In contrast to mechanical mixing, ball milling promoted good dispersion of CNTs within the epoxy matrix, thereby improving their mechanical properties and electrical conductivity. In epoxy nanocomposites with ball milling, Young’s modulus and tensile strength were increased by 653% and 150%, respectively, when CNT loading was 1.0 vol%. Ad
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8

Liu, Hongjin, Mingkun Fu, Shaozhi Pang, et al. "Effect of Ball-Milled Feedstock Powder on Microstructure and Mechanical Properties of Cu-Ni-Al-Al2O3 Composite Coatings by Cold Spraying." Coatings 13, no. 5 (2023): 948. http://dx.doi.org/10.3390/coatings13050948.

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Cu, Ni and Al powders mixed in a certain stoichiometric proportion were ground via ball milling and deposited as coatings using low pressure cold spraying (LPCS) technology. The effect of particle morphology on the powder structure as well as the microstructure, composition and mechanical properties of the coatings was studied. The results revealed a core–shell structure of ball-milled powders. Compared with a mechanically mixed (MM) coating, coatings after ball milling at a rotation speed of 200 rpm exhibited the most uniform composition distribution and a lower degree of porosity (by 0.29%).
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9

Li, C. J., Q. X. Zhang, Q. Yuan, et al. "Nanocrystalline Cu90Nb10 Alloy Produced by Mechanical Alloying." Advanced Materials Research 750-752 (August 2013): 752–55. http://dx.doi.org/10.4028/www.scientific.net/amr.750-752.752.

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Nanocrystalline Cu90Nb10 alloy was produced by high energy ball milling mechanical alloying (MA). The effects of ball milling time on the microstructure and mechanical property of this alloy in the process of MA were investigated. The results show: up to 10 at.% Nb could be dissolved into Cu matrix by MA; the powder particles became compacted and homogeneous with increasing the ball milling time, and the deformation degree also increased synchronously; the grain size of this alloy was refined gradually, and it reached the minimum value of 11.5 nm after 30h milling; the microhardness of this al
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10

Zhang, Yi Rong, and Hou Jun Qi. "Based on the Titanium Alloy Milling Forces Modeling and Simulation Study." Advanced Materials Research 1004-1005 (August 2014): 1231–35. http://dx.doi.org/10.4028/www.scientific.net/amr.1004-1005.1231.

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A common mechanical model of ball-end milling cutter is analyzed in this paper, and take advantage of the orthogonal experiment method to make experiment of milling to identify the milling force coefficients with the titanium alloy material as the test object.Then put the coefficients in the mechanical model of ball to use MATLAB software to predict the milling force. The results of experiment and results of simulation are basically identical, it shows that the mechanics model of ball milling is proved to be correct.
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11

Simić, Marko, Jovana Ružić, Dušan Božić, and Jelena Stašić. "The Effect of Ball-Powder Ratio on The Mechanical and Structural Properties of CuZrB Composite Materials Fabricated by Powder Metallurgy." Metallurgical and Materials Data 1, no. 1 (2023): 19–24. http://dx.doi.org/10.30544/mmd4.

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Copper matrix composites exhibit excellent mechanical and thermal properties. The composite consists of copper (Cu), zirconium (Zr), and boron (B) and is produced using the powder metallurgy technique. The high-energy ball milling was applied for mechanical alloying of the Cu-Zr-B powder mixture to achieve the desired ratio for obtaining a copper matrix reinforced with ZrB2 ceramic particles. The milling times of 10 and 40 hours for two different ball-to-powder ratios are investigated for a powder mixture with a composition of Cu-2.71Zr-2.27B (wt.%). XRD and SEM analyses were employed to deter
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12

de Castro, Mauricio, Osvaldo Mitsuyuki Cintho, and José Deodoro Trani Capocchi. "Comparative Study of Mechanical Activation Improved by High Energy Ball Mills in Chromium Oxide Reduction." Materials Science Forum 802 (December 2014): 41–45. http://dx.doi.org/10.4028/www.scientific.net/msf.802.41.

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The processes of high-energy milling and gained importance among the unconventional methods. In this work, we seek to compare the power supply two types of high energy mills (vibratory mill (SPEX) and planetary mill) with the variation of the milling power. The millings were carried out with a mixture of chromium oxide and aluminum metalic. The reduction of chromium oxide does not occur instantaneously, but gradually as the progress of milling with mechanical activation of powders, this mechanical activation occurs leading to the solid state reaction occurs. The results were obtained for therm
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13

Yusoff, Mahani, and Zuhailawati H. "Effect of Ball Size on Nanostructured Copper-tungsten Carbide Composite Prepared by Mechanical Alloying." Journal of Tropical Resources and Sustainable Science (JTRSS) 1, no. 2 (2013): 31–34. http://dx.doi.org/10.47253/jtrss.v1i2.638.

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In this study, nanostructured copper tungsten carbide composite was produced by mechanical alloying. Mechanical alloying was carried out by milling of copper (Cu), tungsten (W) and graphite mixture at 40 h with milling speed of 400 rpm in planetary ball mill using two different ball sizes. The crystallite size of the powder milled with 10 mm ball is smaller than 20 mm ball due to higher collision frequency. Lower expansion of Cu lattice was found for the powder milled with 20 mm ball than that of 10 mm ball. The composite obtain by milling with 20 mm ball had produced greater impact energy tha
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14

Wang, Ge, Qiang Li, Ying Gao, Jing Na Gao, Yu Ying Zhu, and Zhi Gang Chao. "Influence of Ball Milling Parameters on Preparation of Ti50Cu23Ni20Sn7 Amorphous Alloys Powder." Applied Mechanics and Materials 55-57 (May 2011): 819–24. http://dx.doi.org/10.4028/www.scientific.net/amm.55-57.819.

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Ti50Cu23Ni20Sn7 amorphous alloys powder was prepared by mechanical alloying (MA) in a high-energy planetary ball mill. Milling parameters such as rotational velocity of ball mill, ball to powder weight ratio as well as milling time were throughly investigated. Mechanism of mechanical alloying was throughly discussed.
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15

Falcão, Railson Bolsoni, Edgar Djalma Campos Carneiro Dammann, Cláudio José da Rocha, and Ricardo Mendes Leal Neto. "An Investigation on the Mechanical Alloying of TiFe Compound by High-Energy Ball Milling." Materials Science Forum 660-661 (October 2010): 329–34. http://dx.doi.org/10.4028/www.scientific.net/msf.660-661.329.

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This work reports the efforts to obtain TiFe intermetallic compound by high-energy ball milling of Ti and Fe powder mixtures. This process route has been used to provide a better hydrogen intake in this compound. Milling was carried out in a SPEX mill at different times. Strong adherence of material at the vial walls was seen to be the main problem at milling times higher than 1 hour. Attempts to solve this problem were accomplished by adding different process control agents, like ethanol, stearic acid, low density polyethylene, benzene and cyclohexane at variable quantities and keeping consta
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16

Liu, Yue, Jie Guang Song, W. L. Zhu, D. L. Zhang, H. B. Wen, and R. Huang. "Effect of Ball Milling Technology on Properties of Refractory Waste." Key Engineering Materials 927 (July 29, 2022): 143–48. http://dx.doi.org/10.4028/p-49gm95.

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With the popularization of "sponge city" in the whole country, the use of permeable bricks is increasing every year. Although the raw materials required for the preparation of permeable bricks are widely sourced, there are few reports on the process of using refractory waste to prepare permeable bricks. It is the ball milling process of refractory waste. The effects of ball milling time, ball mill rotation speed, and ball-to-material ratio on the properties of refractory waste were mainly studied. Through the experimental results and analysis, the following conclusions can be drawn: with the i
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17

Suñol, Joan-Josep, and Lluisa Escoda. "Novel Materials Synthesis by Mechanical Alloying/Milling." Materials 15, no. 19 (2022): 6973. http://dx.doi.org/10.3390/ma15196973.

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18

Xue, Yujie, Mingqi Zhang, Jizhi Zhou, and Yufeng Zhang. "Efficient Al Recovery from Aluminum Dross with Simultaneous AlN Separation by a Mechanical Method." Waste 1, no. 1 (2022): 40–51. http://dx.doi.org/10.3390/waste1010004.

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Aluminum dross (AD) is a hazardous waste that contains valuable metallic Al and reactive aluminum nitride (AlN). The intergrowth of Al and AlN presents a challenge to Al recovery and AlN removal. In the current work, a mechanical milling method was developed to separate Al and AlN. Steel bars and balls were used as grinding media. The AD particle size decreased after milling and was distributed in the ranges 0.425–2 mm, 0.15–0.425 mm, 0.08–0.15 mm, and <0.08 mm. The particle size distribution was affected by the ball milling media and grinding time. Steel ball media had a better grinding ef
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19

Coelho, Rodrigo Estevam. "Design of a Machine by Low Cost and the High Performance for Produced Powder Materials." Materials Science Forum 530-531 (November 2006): 192–96. http://dx.doi.org/10.4028/www.scientific.net/msf.530-531.192.

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Mechanical alloying and mechanical fine grinding processes are mostly based on the high energy milling technique. Equipment of a horizontal high-energy ball mill that has been developed in the Cefet-BA is a low cost machine with high performance. These milling machines are equipped with a cylindrical stainless steel horizontal container. Inside the container, a chamber of water circulation is used to maintain, powdered materials, the room temperature. The grinding container inside to chamber horizontal container is a container, cylindrical stainless steel, opened of the two sides. The containe
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20

Lou, Shu Mei, Chuan Dong Qu, Guang Xin Guo, et al. "Effect of Fabrication Parameters on the Performance of 0.5 wt.% Graphene Nanoplates-Reinforced Aluminum Composites." Materials 13, no. 16 (2020): 3483. http://dx.doi.org/10.3390/ma13163483.

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Aluminum composites reinforced by graphene nanoplates(GNP) with a mass fraction of 0.5% (0.5 wt.% GNP/Al) were fabricated using cold pressing and hot pressing. An orthogonal test was used to optimize the fabrication parameters. Ball milling time, ball milling speed, and ultrasonic time have the largest influence on the uniformity of the graphene in the composites. Afterwards, the microstructure, interfacial properties, and fracture morphology of the composites obtained with different parameters were further analyzed. The results show that ball milling time and ball milling speed have obvious i
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21

Bor, Amgalan, Battsetseg Jargalsaikhan, Jehyun Lee, and Heekyu Choi. "Effect of Different Milling Media for Surface Coating on the Copper Powder Using Two Kinds of Ball Mills with Discrete Element Method Simulation." Coatings 10, no. 9 (2020): 898. http://dx.doi.org/10.3390/coatings10090898.

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This study investigated the effect of three different ball materials on the metal-based carbon nanotube (CNT) composites used as surface coatings on metal-powder to fabricate high-quality nanocomposites. The effect of ball material, different rotation speeds, and milling times on the coating characteristics of the metal-based nanocomposite were studied. The mechanical dry coating was used to fabricate CNT coatings on the surface of copper powder particles via two different ball milling machines such as a traditional ball mill and a stirred ball mill. We explored the effect of the milling media
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22

de Alencar e Silva, Gustavo Souza, Ricardo Mendes Leal Neto, Vinícius André Rodrigues Henriques, Carlos Alberto Alves Cairo, and Alfeu Saraiva Ramos. "Structural Evaluation of Mechanically Alloyed W-50at%C Powders." Materials Science Forum 899 (July 2017): 9–12. http://dx.doi.org/10.4028/www.scientific.net/msf.899.9.

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Tungsten carbide is potentially attractive for development of catalysts and widely used for fabrication of cutting tools due to its high hardness and wear resistance while the ball milling can improve the mechanical properties from the metastable structures and nanomaterials. The aim of this work was to evaluate the phase transformations during milling of the W-50at%C elemental powder mixture under argon atmosphere in a planetary P-5 ball mill using WC-Co balls (10 mm diameter) and vials (225 mL), 200 rpm, and a ball-to-powder weight ratio of 10:1. Samples were collected into the vial after di
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23

Wang, Yu, Fengming Xiang, Xiaobo Yuan, Biaobiao Yang, Fenglin Wang, and Yunping Li. "Effects of Processing Parameters on the Microstructure and Mechanical Properties of Nanoscaled WC-10Co Cemented Carbide." Materials 15, no. 13 (2022): 4472. http://dx.doi.org/10.3390/ma15134472.

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This work was mainly focused on the processing-parameter-related microstructure and properties of ultrafine WC-10Co-0.4VC-0.5Cr3C2 cemented carbide. The samples were prepared via a spark plasma sintering (SPS) technique using nano WC and Co powders and the corresponding inhibitor VC and Cr3C2 powders. The influence of the processing process on the microstructure and mechanical properties of ultrafine-grained cemented carbide was investigated under different ball-milling times and sintering temperatures. The results showed that the grain size of WC decreased with increasing ball-milling time an
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24

Zhang, Bo. "Research of Milling Technique on V/Si by Mechanical Alloying." Advanced Materials Research 881-883 (January 2014): 1479–82. http://dx.doi.org/10.4028/www.scientific.net/amr.881-883.1479.

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V/Si binary powders were mechanical alloyed in ball milling machine. The change of microstructure of V/Si powders during mechanical alloying was investigated. The results showed that during ball milling, the size of mixture powders was reduced gradually and the particle shape transited to a ball. Silicon atoms dissolved in vanadium lattice to be a solid solution. The crystal powders were eventually to amorphous state.
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25

Urban, Petr, Fátima Ternero Fernández, Rosa María Aranda Louvier, Raquel Astacio Lopez, and Francisco G. Cuevas. "Mechanical Crystallization of Amorphous Ti<sub>50</sub>Al<sub>30</sub>Ni<sub>20</sub> Alloy Prepared by Mechanical Alloying." Materials Science Forum 1059 (April 25, 2022): 3–8. http://dx.doi.org/10.4028/p-c543h4.

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Laser diffraction, Scanning Electron Microscopy (SEM), X-ray Diffraction (XRD), Transmission Electron Microscopy (TEM) and Differential Scanning Calorimetry (DSC) were employed to characterize the particle size, morphology and structure of mechanically alloyed Ti50Al30Ni20 alloy. Cyclic amorphous-crystalline-amorphous phase transformations were investigated during mechanical alloying, using high-energy ball milling technique. After 20 h of milling, an amorphous/nanocrystalline phase was obtained. This amorphous/nanocrystalline phase tended to transform into crystalline grains after 50 h of mil
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26

Kim, H. S., B. Madavali, T. J. Eom, et al. "Effect Of Different Mechanical Milling Processes On Morphology And Microstructural Changes Of Nano And Micron Al-Powders." Archives of Metallurgy and Materials 60, no. 2 (2015): 1235–39. http://dx.doi.org/10.1515/amm-2015-0105.

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Abstract In this research, effect of the various mechanical milling process on morphology and microstructural changes of nano and micron Al-powders was studied. The milling of Al-powders was performed by both high energy and low energy ball milling process. The influence of milling (pulverizing) energy on the structural changes of Al-powders was studied. Al-nanoparticles were agglomerated during the MA and its size was increased with increasing milling while micron Al-powder gets flattened shape during high energy ball milling due to severe plastic deformation. Meanwhile, structural evolution
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27

Cheng, Cai, Zhao, Yang, Chen, and Li. "Microstructure and Mechanical Properties of Nanocrystalline Al-Zn-Mg-Cu Alloy Prepared by Mechanical Alloying and Spark Plasma Sintering." Materials 12, no. 8 (2019): 1255. http://dx.doi.org/10.3390/ma12081255.

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In this study, Al, Zn, Mg and Cu elemental metal powders were chosen as the raw powders. The nanocrystalline Al-7Zn-2.5Mg-2.5Cu bulk alloy was prepared by mechanical alloying and spark plasma sintering. The effect of milling time on the morphology and crystal structure was investigated, as well as the microstructure and mechanical properties of the sintered samples. The results show that Zn, Mg and Cu alloy elements gradually dissolved in α-Al with the extension of ball milling time. The morphology of the ball-milled Al powder exhibited flaking, crushing and welding. When the ball milling time
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Allafe Razzaghi, Zahra, Abbas Kianvash, and Abolfazl Tutunchi. "Magnetic and Thermal Studies of Iron-Based Amorphous Alloys Produced by a Combination of Melt-Spinning and Ball Milling." Advanced Materials Research 1163 (April 2021): 99–105. http://dx.doi.org/10.4028/www.scientific.net/amr.1163.99.

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In this study, we demonstrate the synthesis of an Fe78Si9B10P3 amorphous alloy by three pathways: mechanical alloying, melt-spinning and a combination of melt-spinning and ball milling. Microstructure, thermal stability and soft magnetic properties of the melt-spun and mechanically alloyed powders are comparatively studied. Ball milling of previously melt-spun samples led to an amorphous powder with an average particle size of ~2.4 μm after 20 hrs of milling. Mechanical alloying of elemental Fe-Si-B-P powders in a planetary ball mill for up to 100 hrs led only to a partial amorphisation of pow
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29

Liu, Xiaochu, Sen He, Zhuan Zhao, Xincheng Xie, Jinrui Xiao, and Zhongwei Liang. "The Effect of the Displacement Amplitude on the Fretting Wear of GCr15 Steel with a TiC Coating." Materials 15, no. 19 (2022): 6628. http://dx.doi.org/10.3390/ma15196628.

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In the present paper, the effect of mechanical ball milling time on the fretting wear of GCr15 steel balls at different displacement amplitudes is investigated. TiC powder coating was fabricated on the surface of GCr15 steel balls using various process times, and the fretting wear tests were conducted on an AISI 52100 steel disk with the applied force of 80 N. Additionally, various displacement amplitudes (10 μm, 20 μm, and 60 μm) were selected. Specimen attributes and wear scars were characterized using an inverted metallographic microscope, a microhardness tester, an X-ray diffractometry ana
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Li, Wei, and Kang Sun. "A New Technology of Producing Fe-TiC Powder by Mechanical Activation-Reductive Diffusion." Advanced Materials Research 199-200 (February 2011): 1813–18. http://dx.doi.org/10.4028/www.scientific.net/amr.199-200.1813.

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A lower-temperature and cost-efficient way is developed to produce Fe-TiC powders. Fe-TiC is produced by means of mechanical activation -reductive diffusion with ilmenite and graphite. The feasibility of this method and the kinetics of the carbothermic reduction are studied with both natural ilmenite and synthetic ilmenite, respectively. The result approved that Fe-TiC powder could be produced by this new technique; moreover, the particles were prominently diminished in size and activated after ball milling. No obvious reactions were detected when ball milling time was less than 8h by EPMA and
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31

Hajalilou, A., M. Hashim, R. Ebrahimi-Kahrizsangi, H. Mohamed Kamari, and S. Kanagesan. "Parametric optimization of NiFe2O4 nanoparticles synthesized by mechanical alloying." Materials Science-Poland 32, no. 2 (2014): 281–91. http://dx.doi.org/10.2478/s13536-013-0173-x.

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AbstractIn this study, the Taguchi robust design method is used for optimizing ball milling parameters including milling time, rotation speed and ball to powder weight ratio in the planetary ball milling of nanostructured nickel ferrite powder. In fact, the current work deals with NiFe2O4 nanoparticles mechanochemically synthesized from NiO and Fe2O3 powders. The Taguchi robust design technique of system optimization with the L9 orthogonal array is performed to verify the best experimental levels and contribution percentages (% ρ) of each parameter. Particle size measurement using SEM gives th
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32

Jeong, Wonki, Se-Eun Shin, and Hyunjoo Choi. "Microstructure and Mechanical Properties of Titanium–Equine Bone Biocomposites." Metals 10, no. 5 (2020): 581. http://dx.doi.org/10.3390/met10050581.

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Microstructure and mechanical properties of Ti-6Al-4V/equine bone (EB) composites fabricated by ball milling and spark plasma sintering (SPS) have been investigated. Ti-6Al-4V/EB composites were successfully fabricated by a planetary ball-milling of spherical Ti6Al4V powder and natural EB powder and SPS at 1000 °C within 15 min under 50 MPa. EB was uniformly dispersed in the Ti6Al4V matrix owing to ball-milling, and beta phase transformation temperature of 1000 °C provided phase stability. The composites containing 0.5 wt.% EB exhibit Vickers hardness and elastic modulus of 540.6 HV and 130.5
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33

Wang, Xiaojie, Qian Fang, Tiejun Zheng, et al. "Enhancing Sodium-Ion Energy Storage of Commercial Activated Carbon by Constructing Closed Pores via Ball Milling." Nanomaterials 14, no. 1 (2023): 65. http://dx.doi.org/10.3390/nano14010065.

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Mechanical ball milling is a prevalent technology for material preparation and also serves as a post-treatment method to modify electrode materials, thus enhancing electrochemical performances. This study explores the microstructure modification of commercial activated carbon through mechanical ball milling, proving its efficacy in increasing sodium-ion energy storage. The evolution of activated carbon’s physical and chemical properties during ball milling was systematically examined. It was observed that the quantity of closed pores and the graphitization degree in activated carbon increased
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34

Feng, Xiujuan, Rilong Xiao, Sékou Mohamed Condé, et al. "Preparation of Humic Acid from Weathered Coal by Mechanical Energy Activation and Its Properties." Minerals 14, no. 7 (2024): 648. http://dx.doi.org/10.3390/min14070648.

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Humic acid (HA) is rich in functional groups with high activity, which can effectively improve the soil environment. The large reserves of weathered coal in China provide sufficient raw material guarantee for HA extraction and utilization. At present, the activation side of weathered coal is still the main technical difficulty that restricts HA extraction. In this study, the weathered coal from Inner Mongolia was used as the raw material, and the mechanical energy was used to activate the weathered coal through a planetary ball mill, which improved the extraction rate of HA and optimized the m
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Ramos, Alfeu Saraiva, Erika Coaglia Trindade Ramos, and Carlos de Moura Neto. "Preparation of Ta-12.5Si-25B Powders by Mechanical Alloying." Materials Science Forum 530-531 (November 2006): 197–202. http://dx.doi.org/10.4028/www.scientific.net/msf.530-531.197.

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The present work reports on the preparation of the Ta5SiB2 compound by highenergy ball milling and subsequent heat treatment from elemental Ta-12.5at%Si-25at%B powder mixture. The milling process was carried out at room temperature in a planetary ball mill under argon atmosphere. Following the milling process, the powders were heat-treated at 1200oC for 4h under Ar atmosphere in order to obtain the equilibrium microstructure. The milled and heat-treated powders were characterized by X-ray diffraction (XRD) and scanning electron microscopy (SEM). Results indicated that the Si peaks disappeared
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Ferraretto, Ana Clara, Erika Coaglia Trindade Ramos, and Alfeu Saraiva Ramos. "On the Phase Transformation in Mechanically Alloyed Ni-Nb and Ni-Ta and Ni-Nb-Ta Powders." Materials Science Forum 727-728 (August 2012): 222–26. http://dx.doi.org/10.4028/www.scientific.net/msf.727-728.222.

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This paper reports on the phase transformation during the preparation of Ni-25Nb, Ni-25Ta, Ni-20Nb-5Ta and Ni-15Nb-10Ta (at-%) powders by high-energy ball milling from elemental powders. The milling process was performed in a planetary ball milling using stainless steel balls and vials, rotary speed of 300rpm, and a ball-to-powder of 10:1. To minimize contamination and spontaneous ignition the powders were handled under argon atmosphere in a glove box. The milled powders were characterized by means of X-ray diffraction techniques. Results indicated that the Ni atoms were preferentially dissolv
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Yoon, K., and J. H. Ahn. "Properties Of MgB2/Ga Composites Prepared By Mechanical Alloying." Archives of Metallurgy and Materials 60, no. 2 (2015): 1271–74. http://dx.doi.org/10.1515/amm-2015-0112.

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Abstract In this study, we examined the effect of Ga-doping and mechanical alloying in MgB2 on microstructural and phase evolution. A comparison was made between in-situ and ex-situ processed Mg-B-Ga samples. Densification was markedly improved by ex-situ sintering of ball-milled MgB2+Ga. The Ga-doping and ball-milling prior to sintering resulted in the formation of impurity phases such as MgO, Ga5Mg2 and Ga2O3. Lattice parameter of MgB2 increased with increasing ball-milling duration as well as by Ga-doping.
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38

Zeng, Jinsong, Lu Liu, Jinpeng Li, Jiran Dong, and Zheng Cheng. "Properties of cellulose nanofibril produced from wet ball milling after enzymatic treatment vs. mechanical grinding of bleached softwood kraft fibers." BioResources 15, no. 2 (2020): 3809–20. http://dx.doi.org/10.15376/biores.15.2.3809-3820.

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Cellulose nanofibril (CNF) is a class of promising and renewable nanocellulosic material due to its unique dimensional characteristics and appealing properties. CNF preparations based on TEMPO pretreatment followed by high-pressure homogenization have been studied intensively, while the high energy consumption and the environmental issues remain challenges to their application. Mechanical refining processes have been commonly applied at the academic and industrial relevant scales for CNF production. In this study, bleached softwood kraft pulp was subjected to high-efficiency wet ball milling (
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39

Gaurav, Anand, and Gayatri Paul. "Synthesis and Characterization of Graphene Oxide Nanosheets by Mechanical Exfoliation Using Ball Milling." Journal of Physics: Conference Series 2818, no. 1 (2024): 012034. http://dx.doi.org/10.1088/1742-6596/2818/1/012034.

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Abstract Graphene Oxide Nanosheets (GONs) are synthesized by reduction of graphite powder using mechanical exfoliation through ball milling under wet condition. Pure graphite is subjected to peeling, exfoliation, and fragmentation in the presence of a reducing agent for a duration of 30 hours to achieve few layered GONs. Intermediate samples throughout the duration of ball milling are extracted from the wet slurry to investigate the characteristics of the milling process. The extracted samples are investigated under XRD, FESEM, Raman spectroscopy, BET and FTIR to understand the synthesis proce
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Shailendra, V. Dhanal, Devadi Husainkhan, G. Akkimardi V, and A. Kori S. "Ni-Mn-Al Heusler Alloy Samples Preparation by Mechanical Alloying Method and Study of their Investigated Properties." Indian Journal of Science and Technology 15, no. 39 (2022): 1997–2003. https://doi.org/10.17485/IJST/v15i39.935.

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Abstract <strong>Objective:</strong>&nbsp;In this work, ternary Ni-Mn-Al Heusler alloy powder samples were fabricated using mechanical alloying technique to study its alloy formation mechanism and the effects of mechanical alloying on the investigated properties.&nbsp;<strong>Methods:</strong>&nbsp;The samples were prepared using high energy planetary ball mill under argon conditions. The milling time of 0 h (hour/hours), 5 h, 10 h and 15 h were selected to see the progress of alloy formation. The microstructural, compositional, thermal and magnetic studies of ball milled powder samples were c
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Yusop, M., De Liang Zhang, and M. Wilson. "Microstructure and Morphology of Alumina-Iron Nanocomposite Powders Produced by High Energy Mechanical Milling." Advanced Materials Research 29-30 (November 2007): 131–34. http://dx.doi.org/10.4028/www.scientific.net/amr.29-30.131.

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Alumina-iron nanocomposite powders containing 5vol.% of iron were fabricated by high-energy ball milling with different ball-to-powder weight ratios (BPRs) as part of the study of ceramic-metal nanocomposite magnetic materials. The microstructure and morphology of the composite powders were characterized using the X-ray diffraction, optical microscopy and scanning electron microscopy. XRD analysis and SEM examination in combination with energy dispersive X-ray spectrometry confirmed that the nanocomposite structure of the powder particles formed only after 8 hours milling for both BPRs used. W
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Jin, Yong Ping, and Ming Hu. "Effect of Ball Milling on Mechanical Properties of Graphite/Copper Matrix Composites." Advanced Materials Research 217-218 (March 2011): 936–40. http://dx.doi.org/10.4028/www.scientific.net/amr.217-218.936.

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3wt% graphite/copper matrix composites had been prepared after mechanical ball milling, pressing, vacuum hot pressed sintering and hot extrusion. With tensile test, hardness test and impact test, utilizing material testing machine, Vickers hardness tester, impact machine, optical microscope and scanning electron microscopy, effect of milling time on mechanical property of graphite/copper matrix composites had been investigated. The results show that after mechanical milling and hot extrusion, microstructure had been refined, distribution of graphite phase and cohesion between copper and graphi
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Falls, M., D. Meysing, S. Lonkar, et al. "Development of highly digestible animal feed from lignocellulosic biomass Part 1: Oxidative lime pretreatment (OLP) and ball milling of forage sorghum1." Translational Animal Science 1, no. 2 (2017): 208–14. http://dx.doi.org/10.2527/tas2017.0024.

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Abstract To feed a growing population, alternative sources of animal feed (e.g., lignocellulose) are needed to replace grains (e.g., corn). Oxidative lime pretreatment (OLP) increases lignocellulose digestibility by removing lignin and hemicellulose acetyl content. Adding a mechanical pretreatment (e.g., ball milling) further improves digestibility. This study determines the effectiveness of OLP and ball milling to enhance the ruminant digestibility of lignocellulose. For forage sorghum, the 48-h in vitro TDN were 40, 64, and 84 g nutrients digested/100 g organic matter (OM) for raw, short-ter
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Kanunnikova, Olga M., V. V. Aksenova, and G. A. Dorofeev. "Ball-Milling Stimulated Mechanochemical Processes in the System “Titanium-Toluene”." Materials Science Forum 946 (February 2019): 351–56. http://dx.doi.org/10.4028/www.scientific.net/msf.946.351.

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The present work deals with the investigation of the transformations of the solid and liquid phases at high energy planetary ball milling of toluene together with titanium powder. The sequence of structural toluene transformations using FT-IR spectroscopy was investigated. Phase constitutions and morphology of ball milled titanium powders were studied by X-ray diffraction and scanning electron microscopy. It is shown that mechanically induced destruction of toluene occurs by the mechanism of catalytic cracking. During ball milling, concentration of aromatic hydrocarbons in the liquid phase dec
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Qin, Yue Ning, Yu Zhen Wang, Hong Bin Wen, et al. "Manufacture and Performance of the Al<sub>2</sub>O<sub>3</sub>/Al Compound Powder and Cermet with the Powder Metallurgy." Materials Science Forum 1080 (January 30, 2023): 41–47. http://dx.doi.org/10.4028/p-f2og5p.

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On the one hand, cermet has the advantages of metal materials, and on the other hand, it maintains the excellent properties of ceramic materials, and is a very important new engineering material. In this paper, the alumina/aluminum cermet material composite powder was prepared by ball milling, and its densification properties were characterized and studied to provide reference for the preparation of high-performance cermet materials. When the ball milling time is more than 6h, the distribution of alumina particles around the aluminum powder is relatively uniform. The research shows that: with
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Eom, JiYong, and HyukSang Kwon. "Improved lithium insertion/extraction properties of single-walled carbon nanotubes by high-energy ball milling." Journal of Materials Research 23, no. 9 (2008): 2458–66. http://dx.doi.org/10.1557/jmr.2008.0291.

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The effects of ball milling on lithium (Li) insertion/extraction properties into/from single-walled carbon nanotubes (SWNTs) were investigated. The SWNTs were synthesized on supported catalysts by thermal chemical-vapor deposition method, purified, and mechanically ball-milled by high-energy ball milling. The purified SWNTs and the ball-milled SWNTs were electrochemically inserted/extracted with Li. The structural and chemical modifications in the ball-milled SWNTs change the insertion/extraction properties of Li ions into/from the ball-milled SWNTs. The reversible capacity (Crev) increases wi
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Wang, Xiao Peng, Shu Long Xiao, Yu Yong Chen, Zhi Guang Liu, and Kee Do Woo. "Microstructure and Characteristics of Ti-Nb-Sn-HA Composite Powder Fabricated by Mechanical Alloying." Applied Mechanics and Materials 55-57 (May 2011): 886–91. http://dx.doi.org/10.4028/www.scientific.net/amm.55-57.886.

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A novel biocomposite Ti-35wt%Nb-2.5wt%Sn-15wt%HA powders was synthesized by high energy ball mill(HEBM) for various periods of time. The microstructure and characteristics of the milled powder particles were investigated. Results showed that in the composite powders milled for 4h, Ti was still exhibited primary α phase, with the increase of ball milling time up to 8h, Ti transformed into primary β phase and a little α phase, after ball milling for 12h, Ti transformed into β phase fully. the transform temperature was 380.06°C. And TEM and PSD results indicated that nanostructure was obtained af
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48

Fonseca, A., S. Kanagaraj, Monica S. A. Oliveira, and José A. O. Simões. "Enhanced UHMWPE Reinforced with MWCNT through Mechanical Ball-Milling." Defect and Diffusion Forum 312-315 (April 2011): 1238–43. http://dx.doi.org/10.4028/www.scientific.net/ddf.312-315.1238.

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In this work, nanocomposites of ultrahigh molecular weight polyethylene (UHMWPE) reinforced with multiwalled carbon nanotubes (MWCNTs) were evaluated for their ability to produce nanocomposites with superior mechanical properties. As homogeneity of the nanocomposite plays an important role into final mechanical properties, mechanical ball-milling is used to prepare homogeneous UHMWPE/MWCNTs powders, where special emphasis is given to milling-time optimization. Mechanical ball-milling seems to be a suitable and rather simple technique for preparing nanocomposites even outside laboratory conditi
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Li, C. J., G. Chen, Q. Yuan, et al. "Effects of Ball Milling Time on the Microstructure and Mechanical Property of Cu90Al10 Alloy." Advanced Materials Research 750-752 (August 2013): 663–66. http://dx.doi.org/10.4028/www.scientific.net/amr.750-752.663.

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Nanostructured Cu90Al10 alloy powders were prepared by high energy ball milling mechanical alloying (MA). Up to 10 at.% Al could be dissolved into copper by mechanical alloying at room temperature. Effects of milling time on phase transformation, structural characteristics, and mechanical property of powders were investigated by using X-ray diffraction (XRD), Optical Microscopy (OM) and microhardness tester. The results show: with increasing the milling time, the powder particle size increased gradually, and then it tended to be homogeneous. The grain size of the alloy decreased gradually, but
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Lalaoua, Samira, Bouguerra Bouzabata, Safia Alleg, Abedelmalik Djekoun, and David Shmool. "Structure Evolution of La(OH)3 /Fe Composite during Ball Milling." Journal of Nano Research 65 (December 2020): 123–34. http://dx.doi.org/10.4028/www.scientific.net/jnanor.65.123.

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Fe-10wt% La (OH)3 composite powders have been fabricated by ball milling, under argon atmosphere for milling periods of 0, 5 and 10 h, respectively. Changes in structural, morphological, thermal and magnetic properties of the powders during mechanical alloying and during subsequent annealing have been examined by X-ray diffraction, scanning electron microscopy (SEM), differential scanning calorimetry (DSC) and vibrating sample magnetometer (VSM). XRD results: showed the formation of new phases (Fe and LaFeO3 perovskite) created through the ball milling. The results showed that the crystalline
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