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Journal articles on the topic 'Mercaptomethyl'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

Charron, Carlie L., Jade M. Cottam Jones, and Craig A. Hutton. "Are Aminomethyl Thioesters Viable Intermediates in Native Chemical Ligation Type Amide Bond Forming Reactions?" Australian Journal of Chemistry 71, no. 9 (2018): 697. http://dx.doi.org/10.1071/ch18198.

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The condensation of N-mercaptomethyl amines and thioesters is a potential route to amides, via aminomethyl thioester intermediates, in a native chemical ligation type process followed by self-cleavage of the ‘mercaptomethyl’ auxiliary. This paper describes investigations towards the preparation of aminomethyl thioesters, and subsequent conversion into amides, from a three-component coupling of formaldehyde, a thioacid, and an amine. Our studies suggest that while such intermediates may be formed en route to amides, no advantages are offered over the direct reaction of the amine and thioacid pr

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2

Tong, Y., M. Alsalama, G. R. Berdiyorov, Sara Iyad Ahmad, and H. Hamoudi. "Nanoarchitectonics of molecular self assembled monolayers by transition metal ion intercalation for enhancement of molecular junction conductivity." RSC Advances 14, no. 30 (2024): 21597–607. http://dx.doi.org/10.1039/d4ra02950j.

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3

Makomo, Hubert, Serge Masson та Monique Saquet. "Convenient syntheses of α-mercaptomethyl phosphonates". Tetrahedron Letters 34, № 45 (1993): 7257–58. http://dx.doi.org/10.1016/s0040-4039(00)79302-6.

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4

Tsuge, Akihiko, Takahiro Okamoto, and Tetsuji Moriguch. "Structure and Conformational Properties of three-layered Cyclophanes prepared by a one-pot Synthesis." Journal of Chemical Research 2007, no. 7 (2007): 429–31. http://dx.doi.org/10.3184/030823407x228786.

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The coupling reactions of substituted bis(bromomethyl)benzene components and tetra(mercaptomethyl)benzene derivatives have been carried out under heterogeneous dilute reaction conditions to afford the three-layered cyclophanes 3a–e as three kinds of conformational isomers in moderate yields.

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5

Farrington, G. K., Alok Kumar, and F. C. Wedler. "A CONVENIENT SYNTHESIS OF DIETHYL (MERCAPTOMETHYL)PHOSPHONATE." Organic Preparations and Procedures International 21, no. 3 (1989): 390–92. http://dx.doi.org/10.1080/00304948909356410.

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6

Li, Chuang, Xiong Xiong Bai, Chuan Jie Cheng, and Zhong Yu Hu. "Preparation of P-and S-Containing UV-Cured Cardanol Polymers via Thiol-Ene Click Chemistry." Advanced Materials Research 771 (September 2013): 63–66. http://dx.doi.org/10.4028/www.scientific.net/amr.771.63.

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Tricardanolic phosphite was synthesized in 65% yield. This cardanol-derived small molecular compound was successfully transformed into UV-cured resin via thiol-ene click reaction, by using 4,4-di (mercaptomethyl) benzophenone as both a photoinitiator and a crosslinker. The fully bio-based P-and S-containing resin is expected to be flame-retardant materials.

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7

Pensato, Soccorsa, Luca Domenico D'Andrea, Carlo Pedone та Alessandra Romanelli. "New Synthetic Route to γ-Mercaptomethyl PNA Monomers". Synthetic Communications 38, № 15 (2008): 2499–506. http://dx.doi.org/10.1080/00397910802219122.

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8

Katritzky, Alan R., Ion Ghiviriga, Daniela C. Oniciu, and Ferenc Soti. "1-(Mercaptomethyl)benzotriazole: Preparation, reactivity and synthetic utility." Journal of Heterocyclic Chemistry 33, no. 6 (1996): 1927–34. http://dx.doi.org/10.1002/jhet.5570330661.

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9

Tank, R., U. Pathak, A. Singh, A. Gupta, and D. C. Gupta. "A convenient one step preparation of crosslinked polystyrene mercaptomethyl resin." Reactive and Functional Polymers 69, no. 4 (2009): 224–28. http://dx.doi.org/10.1016/j.reactfunctpolym.2008.12.022.

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10

Hamad, M. M., S. A. Said, and Y. M. El-Ekyabi. "Synthesis and reactions of 2-mercaptomethyl-1,3,4-oxadiazolin-5-one." Monatshefte für Chemie - Chemical Monthly 127, no. 5 (1996): 549–55. http://dx.doi.org/10.1007/bf00807080.

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11

BORNEMANN, B., and A. MARX. "Synthesis of DNA oligonucleotides containing 5-(mercaptomethyl)-2′-deoxyuridine moieties." Bioorganic & Medicinal Chemistry 14, no. 18 (2006): 6235–38. http://dx.doi.org/10.1016/j.bmc.2006.05.054.

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12

Tacke, Reinhold, Beate Becker, and Hartwig Lange. "(Thioacetoxy-S-methyl)diorganylsilane und (Mercaptomethyl)diorganylsilane: Synthese und Eigenschaften." Journal of Organometallic Chemistry 388, no. 1-2 (1990): 57–62. http://dx.doi.org/10.1016/0022-328x(90)85346-z.

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13

KATRITZKY, A. R., I. GHIVIRIGA, D. C. ONICIU, and F. SOTI. "ChemInform Abstract: 1-(Mercaptomethyl)benzotriazole: Preparation, Reactivity and Synthetic Utility." ChemInform 28, no. 32 (2010): no. http://dx.doi.org/10.1002/chin.199732107.

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14

ABD EL-GHAFFAR, NAHED, NADIA DAWOOD, and BAHYIA EL.SADEK. "SYNTHESIS OF SOME NEW SUBSTITUTED MERCAPTOMETHYL PYRIMIDINES OF POSSIBLE BIOLOGICAL ACTIVITY." Al-Azhar Bulletin of Science 17, Issue 1-A (2006): 161–70. http://dx.doi.org/10.21608/absb.2006.11648.

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15

Bhupathiraju, N. V. S. Dinesh K., and M. Graça H. Vicente. "Synthesis and cellular studies of polyamine conjugates of a mercaptomethyl–carboranylporphyrin." Bioorganic & Medicinal Chemistry 21, no. 2 (2013): 485–95. http://dx.doi.org/10.1016/j.bmc.2012.11.007.

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16

Kondo, Masaru, Hettiarachchige Dona Piyumi Wathsala, Kazunori Ishikawa, et al. "Bayesian Optimization-Assisted Screening to Identify Improved Reaction Conditions for Spiro-Dithiolane Synthesis." Molecules 28, no. 13 (2023): 5180. http://dx.doi.org/10.3390/molecules28135180.

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Bayesian optimization (BO)-assisted screening was applied to identify improved reaction conditions toward a hundred-gram scale-up synthesis of 2,3,7,8-tetrathiaspiro[4.4]nonane (1), a key synthetic intermediate of 2,2-bis(mercaptomethyl)propane-1,3-dithiol [tetramercaptan pentaerythritol]. Starting from the initial training set (ITS) consisting of six trials sampled by random screening for BO, suitable parameters were predicted (78% conversion yield of spiro-dithiolane 1) within seven experiments. Moreover, BO-assisted screening with the ITS selected by Latin hypercube sampling (LHS) further i

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17

Pevzner, L. M. "Intramolecular Cyclization of Mercaptomethyl Derivatives of Alkyl 3-(Furyl)-3-(diethoxyphosphoryl)acrylates." Russian Journal of General Chemistry 91, no. 8 (2021): 1499–511. http://dx.doi.org/10.1134/s1070363221080119.

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18

Shibakami, Motonari, and Minoru Izumi. "Preparation of MonosaccharideHaving (Mercaptomethyl)diacetylene Compounds Using Solid-supportas a Thiol Source." Synlett, no. 10 (2003): 1395–98. http://dx.doi.org/10.1055/s-2003-40853.

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19

Mallinson, P. R., D. D. MacNicol, K. L. McCormack, D. S. Yufit, J. H. Gall, and R. K. Henderson. "Hexakis(mercaptomethyl)benzene: a Structure Possessing Well Ordered Homodromic [SH...S]6Interactions." Acta Crystallographica Section C Crystal Structure Communications 53, no. 1 (1997): 90–92. http://dx.doi.org/10.1107/s0108270196010499.

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20

Arbuzov, B. A., N. R. Fedotova, and V. S. Vinogradova. "Reaction of Sb(III) halides with 1,2-dimethyl-4,5-di(mercaptomethyl)benzene." Bulletin of the Academy of Sciences of the USSR Division of Chemical Science 36, no. 10 (1987): 2171–73. http://dx.doi.org/10.1007/bf00962017.

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21

HAMAD, M. M., S. A. SAID, and Y. M. EL-EKYABI. "ChemInform Abstract: Synthesis and Reactions of 2-Mercaptomethyl-1,3,4-oxadiazolin-5-one." ChemInform 27, no. 36 (2010): no. http://dx.doi.org/10.1002/chin.199636137.

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22

Nichol, A. W., L. A. Angel, T. Moon, and P. S. Clezy. "Lactoperoxidase haem, an iron-porphyrin thiol." Biochemical Journal 247, no. 1 (1987): 147–50. http://dx.doi.org/10.1042/bj2470147.

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The haem prosthetic group of lactoperoxidase can be prepared from the enzyme in high yield by reductive cleavage with mercaptoethanol in 8 M-urea under mild conditions. The product yields porphyrins, after removal of iron, which show visible spectroscopic properties similar to protoporphyrin but are considerably more polar. In the presence of iodoacetamide, a different product is obtained by reductive cleavage. The proton n.m.r. and mass spectra of this compound indicate that the prosthetic group of the enzyme is the iron complex of 18-mercaptomethyl-2,7,12-trimethyl-3,8-divinylporphyrin-13,17

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23

Márquez, V. E., and J. R. Anacona. "Complexes of nickel(II), palladium(II) and platinum(II) with 2,6-bis(mercaptomethyl)pyridine." Polyhedron 16, no. 11 (1997): 1931–35. http://dx.doi.org/10.1016/s0277-5387(96)00445-7.

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24

Janout, V., and P. Čefelín. "Debromination of di- and tetrabrominated compounds by crosslinked poly{1-[p-(mercaptomethyl)phenyl]ethylene}." Polymer 26, no. 5 (1985): 781–85. http://dx.doi.org/10.1016/0032-3861(85)90117-x.

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25

MASTRYUKOVA, T. A., A. E. SHIPOV, G. V. ZHDANOVA, et al. "ChemInform Abstract: Metabolism and Interaction with Esterases of O-Ethyl S-( Methoxycarbonalmethyl)mercaptomethyl Methylphosphonodithioate." ChemInform 22, no. 2 (2010): no. http://dx.doi.org/10.1002/chin.199102363.

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26

Isogai, Hideo, Kenji Tadano та Shinichi Yano. "Liquid crystallinity in polythioethers of 1,4‐bis(mercaptomethyl)benzene (MB) and 4,4′‐bis(mercaptomethyl)biphenyl (MBP) with α,ω‐dibromo‐n‐alkanes and polythioesters of MB and MBP with n‐alkanedioyl dichlorides". Liquid Crystals 35, № 6 (2008): 689–94. http://dx.doi.org/10.1080/02678290802080386.

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27

Bouwman, E., C. E. Westheide, W. L. Driessen, and J. Reedijk. "Synthesis and spectroscopic studies on transition-metal nitrates and thiocyanates of a chelating imidazole-thioether ligand. The crystal structures of diaquabis[5-methyl-4-(ethyl-mercaptomethyl)imidazole]nickel(II) dinitrate, diaquabis[5-methyl-4-(ethyl-mercaptomethyl)imidazole] copper(II) dinitrate and bis[5-methyl-4-(ethyl-mercaptomethyl)imidazole] bis(thiocyanato-N)cobalt(II)." Inorganica Chimica Acta 166, no. 2 (1989): 291–99. http://dx.doi.org/10.1016/s0020-1693(00)80822-1.

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28

Nakamura, Tohru, Hiroshi Kondoh, Mutsuyoshi Matsumoto, and Hisakazu Nozoye. "Recognition properties of the nano-ordered structures of bis(mercaptomethyl)terthiophene monolayers on Au (111)." Synthetic Metals 103, no. 1-3 (1999): 2143–44. http://dx.doi.org/10.1016/s0379-6779(98)00602-x.

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29

von Zabern, I., and R. Nolte. "Activation of the Alternative Pathway of Complement by DL-2-Mercaptomethyl-3-guanidinoethylthiopropanoic Acid (Mergetpa)." Complement 3, no. 2 (1986): 97–104. http://dx.doi.org/10.1159/000467885.

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30

Duckert, Jean-Frédéric, Laurence Balas, and Jean-Claude Rossi. "Synthesis of 5-(mercaptomethyl)-3(E)-undecene-1,11-dioic acid, a non-peptide glutathione analog." Tetrahedron Letters 42, no. 22 (2001): 3709–11. http://dx.doi.org/10.1016/s0040-4039(01)00554-8.

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31

Ghilardi, Carlo A., Stefano Midollini, Annabella Orlandini, and Alberto Vacca. "Reactivity of the tripodal trithiol 1,1,1-tris(mercaptomethyl)ethane toward methyl- and ethyl-mercury halides." Journal of the Chemical Society, Dalton Transactions, no. 20 (1993): 3117. http://dx.doi.org/10.1039/dt9930003117.

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32

Volkers, Phillip I., Thomas B. Rauchfuss, and Scott R. Wilson. "Coordination Chemistry of 3-Mercapto-2-(mercaptomethyl)propanoic Acid (Dihydroasparagusic Acid) with Iron and Nickel." European Journal of Inorganic Chemistry 2006, no. 23 (2006): 4793–99. http://dx.doi.org/10.1002/ejic.200600636.

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33

Du, Weiping, Guiming Zhang, Song Wang, Lianjiang Tan, and Huifang Chen. "Cure Kinetics of an Optical Polythiourethane with Amine Catalyst by IR Analysis." International Journal of Polymer Science 2019 (September 16, 2019): 1–10. http://dx.doi.org/10.1155/2019/8194379.

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An optical polythiourethane based on m-xylylene diisocyanate (XDI) and 4-mercaptomethyl-3,6-dithia-1,8-octanedithiol (BES) has been studied. Triethylamine was adopted as a catalyst, and the solid-state isothermal cure reaction was carried out using FTIR spectroscopy, in the temperature range of 75°C-105°C. The -NCO absorption band of XDI was used to monitor the conversion of diisocyanate into polythiourethane. The reaction rate enhanced with an increase in the content of the catalyst, and the gel time determined by swelling test was shorter for the system with higher catalyst content. Kinetic

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34

Hinchliffe, Philip, Diego M. Moreno, Maria-Agustina Rossi та ін. "2-Mercaptomethyl Thiazolidines (MMTZs) Inhibit All Metallo-β-Lactamase Classes by Maintaining a Conserved Binding Mode". ACS Infectious Diseases 7, № 9 (2021): 2697–706. http://dx.doi.org/10.1021/acsinfecdis.1c00194.

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35

Salgado, H. C., O. A. Carretero, A. G. Scicli, and R. D. Murray. "Effect of DL-2-mercaptomethyl-3-guanidinoethylthiopropanoic acid on the blood pressure response to vasoactive substances." Journal of Pharmacology and Experimental Therapeutics 237, no. 1 (1986): 204–8. https://doi.org/10.1016/s0022-3565(25)24887-x.

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36

Anastasi, Christopher, Mark Broomfield, Ole John Nielsen, and Palle Pagsberg. "Kinetics and mechanisms of the reactions of mercaptomethyl radicals with dioxygen, nitric oxide, and nitrogen dioxide." Journal of Physical Chemistry 96, no. 2 (1992): 696–701. http://dx.doi.org/10.1021/j100181a034.

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37

Adams, Jerry L., Thomas D. Meek, Shau Ming Mong, Randall K. Johnson, and Brian W. Metcalf. "cis-4-Carboxy-6-(mercaptomethyl)-3,4,5,6-tetrahydropyrimidin-2(1H)-one, a potent inhibitor of mammalian dihydroorotase." Journal of Medicinal Chemistry 31, no. 7 (1988): 1355–59. http://dx.doi.org/10.1021/jm00402a018.

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38

Podkoscielny, Wawrzyniec, and Stanisława Szubinska. "Linear polythioesters. XII. Products of polycondensation some isomeric di(mercaptomethyl)trimethylbenzenes with isophthaloyl and terephthaloyl chlorides." Journal of Applied Polymer Science 34, no. 1 (1987): 143–52. http://dx.doi.org/10.1002/app.1987.070340112.

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39

Podkościelny, Wawrzyniec, and Stanisława Szubińska. "Linear polythioesters. XIII.. Products of polycondensation of isomeric di(mercaptomethyl)–dimethylbenzenes with adipoyl and sebacoyl chlorides." Journal of Applied Polymer Science 35, no. 1 (1988): 85–101. http://dx.doi.org/10.1002/app.1988.070350108.

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40

Podkościelny, Wawrzyniec, and Stanisława Szubińska. "Linear polythioesters. XIV. Products of interfacial polycondensation isomeric di(mercaptomethyl) trimethylbenzenes with some aliphatic acid dichlorides." Journal of Applied Polymer Science 35, no. 7 (1988): 1853–61. http://dx.doi.org/10.1002/app.1988.070350711.

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41

Khalifa, Mohamed E. "Synthesis and Evaluation of New 2‐Mercaptomethyl Benzimidazole Scaffolds as Potential Antibacterial, Antioxidant and Cytotoxic Agents." ChemistrySelect 5, no. 34 (2020): 10562–66. http://dx.doi.org/10.1002/slct.202002822.

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42

Tsatsakis, A. M., and Photis Dais. "1H NMR structural analysis of a series of naphthalene-hydroxymethyl-and -mercaptomethyl-carboxylic acids and derivatives." Magnetic Resonance in Chemistry 28, no. 4 (1990): 375–77. http://dx.doi.org/10.1002/mrc.1260280418.

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43

Tian, Tian, Burapol Singhana, Lauren E. Englade-Franklin, Xianglin Zhai, T. Randall Lee, and Jayne C. Garno. "Surface assembly and nanofabrication of 1,1,1-tris(mercaptomethyl)heptadecane on Au(111) studied with time-lapse atomic force microscopy." Beilstein Journal of Nanotechnology 5 (January 9, 2014): 26–35. http://dx.doi.org/10.3762/bjnano.5.3.

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The solution self-assembly of multidentate organothiols onto Au(111) was studied in situ using scanning probe nanolithography and time-lapse atomic force microscopy (AFM). Self-assembled monolayers (SAMs) prepared from dilute solutions of multidentate thiols were found to assemble slowly, requiring more than six hours to generate films. A clean gold substrate was first imaged in ethanolic media using liquid AFM. Next, a 0.01 mM solution of multidentate thiol was injected into the liquid cell. As time progressed, molecular-level details of the surface changes at different time intervals were ca

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44

Suzuki, H., X. P. Gao, C. O. Olopade, and I. Rubinstein. "Neutral endopeptidase modulates VIP-induced vasodilation in hamster cheek pouch vessels in situ." American Journal of Physiology-Regulatory, Integrative and Comparative Physiology 271, no. 2 (1996): R393—R397. http://dx.doi.org/10.1152/ajpregu.1996.271.2.r393.

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The purpose of this study was to determine whether vasoactive intestinal peptide (VIP) dilates resistance arterioles in the in situ systemic circulation and whether inhibitors of neutral endopeptidase (NEP) and angiotensin I-converting enzyme (ACE), two membrane-bound metalloenzymes that are widely distributed in the microcirculation and cleave and inactive VIP, potentiate this response. Using intravital microscopy, we found that VIP (0.05 and 0.1 nmol) induced significant vasodilation in the hamster cheek pouch (13 +/- 1 and 20 +/- 2% increase from baseline, respectively; mean +/- SE; P <

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45

Kuno, N., S. Mizutani, Y. Ohno, et al. "Possible involvement of placental proteases in bradykinin (BK) degradation." Reproduction, Fertility and Development 9, no. 6 (1997): 633. http://dx.doi.org/10.1071/r96045.

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The hydrolysis of bradykinin (BK) by human placental subcellular fractions and pregnancy sera was studied in the presence of inhibitors by measuring amino acids liberated from BK by high-performance liquid chromatography. The effects of the inhibitors DL-2- mercaptomethyl-3-guanidinoethylthiopropionic acid (MGTA, for kininase I), phosphoramidon (for endopeptidase 24.11) and captopril and rentiapril (for angiotensin-converting enzyme [ACE, kininase II]) suggested the essential roles of the above three proteases in BK degradation: among the three proteases, kininase I and endopeptidase 24.11 app

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46

Kálai, Tamás, Péter Sáska, Zoltán Szabó, József Jek[otilde], Olga H. Hankovszky та Kálmán Hideg. "Synthesis of 2-(2-Thienyl)benzimidazoles by the Reaction of 2-(Mercaptomethyl)benzimidazole With β-Electrophilic Esters". Synthetic Communications 27, № 12 (1997): 2041–50. http://dx.doi.org/10.1080/00397919708006808.

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47

Gu, Xuefang, Xian Li, Sijie Wu, et al. "A sensitive hydrazine hydrate sensor based on a mercaptomethyl-terminated trinuclear Ni(ii) complex modified gold electrode." RSC Advances 6, no. 10 (2016): 8070–78. http://dx.doi.org/10.1039/c5ra23809a.

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48

Sola, Joan, and Ramón Yáñez. "Metal complexes of sulphur–nitrogen ligands. Synthesis and characterization of palladium(II) complexes of 3-(mercaptomethyl)piperidine." J. Chem. Soc., Dalton Trans., no. 10 (1986): 2021–24. http://dx.doi.org/10.1039/dt9860002021.

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49

Podkościelny, Wawrzyniec, and Stanisława Szubińska. "Linear polythioesters. XI. Products of polycondensation of some isomeric di(mercaptomethyl)dimethylbenzenes with isophthaloyl and terephthaloyl chlorides." Journal of Applied Polymer Science 32, no. 1 (1986): 3277–97. http://dx.doi.org/10.1002/app.1986.070320130.

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50

Nobes, Ross H., and Leo Radom. "The thermochemistry of the mercaptomethyl (CH2SH+) and thiomethoxy (CH3S+) cations: a comparison of G2 theory and experiment." Chemical Physics Letters 189, no. 6 (1992): 554–59. http://dx.doi.org/10.1016/0009-2614(92)85249-a.

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