Academic literature on the topic 'Methylpyrimidine'

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Journal articles on the topic "Methylpyrimidine"

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Yengoyan, Aleksandr P., Zhermen A. Azaryan, Vergush A. Pivazyan, Emma A. Ghazaryan, Rafael A. Tamazyan, and Armen G. Ayvazyan. "Synthesis and Preliminary Biological Properties Assessment of Novel 2-S-, 4-, 5-Substituted and Bicyclic Derivatives of 6-Methylpyrimidine-4-ol." Letters in Organic Chemistry 17, no. 2 (2020): 149–56. http://dx.doi.org/10.2174/1570178616666190411110415.

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: A series of novel 2-S-, 4-, 5-substituted and bicyclic 6-methylpyrimidine-4-ol derivatives including pyrazole, 1,2,4-triazole and pyridazine moieties in the molecule were synthesized by accessible and efficient methods. Thiopyrazolyl derivatives were obtained from 2-mercapto-6-methylpyrimidin-4-ol. 4-Triazolyl and 4-aminotriazolylpyrimidines were synthesized from the quaternary ammonium salt of pyrimidine and 4-chloro-substituted 2-thiomethyl-6-methylpyrimidine, respectively. The reaction of potassium salt of 1-methyl-6-oxo-1,6-dihydropyridazin-3-ole with ethyl 2-chloro-3-oxobutanoate and su
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Vishnu, Basetti, Poturaju Venkatanarayana, Hosahalli Subramanya, and Potluri Vijay. "A novel and one pot synthesis of ethyl 7,12-dihydro-1,3,6,7,12-pentaazapleiadene5-carboxylates." Journal of Indian Chemical Society Vol. 92, Jun 2015 (2015): 839–42. https://doi.org/10.5281/zenodo.5627332.

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Department of Discovery Chemistry, Aurigene Discovery Technologies Ltd., Hyderabad-500 049, Telangana, India <em>E-mail</em> : vijay_p@aurigene.com, potluri.vijay@gmail.com JNT University, Kukatpally, Hyderabad-500 072, Telangana, India new tandem three-step synthesis of ethyl 7,12-dihydro-1,3,6,7,12-pentaazapleiadene-5-carboxylate derivatives (9a-j) has been accomplished stepwise. Reaction of 4-chloro-6-methylpyrimidine-5-carbonitrile with various 4- substituted 2-nitrobenzeneamines yielded the corresponding 4-(2-nitrophenylamino)-6-methylpyrimidine-5-carbonitriles (7aj). These phenylamino me
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Yasui, Masanori, Yoshimitsu Ishikawa, Takayuki Ishida, Takashi Nogami, and Fujiko Iwasaki. "Bis(hfac)-copper(II) complexes bridged by pyrimidines showing magnetic interactions." Acta Crystallographica Section B Structural Science 57, no. 6 (2001): 772–79. http://dx.doi.org/10.1107/s0108768101013568.

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Crystals of bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)bispyrimidinecopper(II) (1), bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)bis(4-methylpyrimidine)copper(II) (2), bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)bis(quinazoline)copper(II) (3) showed ferromagnetic interactions at extremely low temperature. Crystal structure analyses revealed that these complexes were catena-bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)[μ-pyrimidine-N 1:N 3]copper(II), [Cu(hfac)2(pm)2] n , catena-bis(1,1,1,5,5,5-hexafluoropentane-2,4-dionato)[μ-4-methylpyrimidine-N 1:N 3]copper(II), [Cu(hfac)2(4-Me-pm)] n
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Hřebabecký, Hubert, and Antonín Holý. "Synthesis of Carbocyclic 4'-C-Hydroxymethyl Analogues of Azidodeoxythymidine, Deoxythymidine, Deoxydidehydrothymidine and Thymidine Carba Analogue with Fused Oxetane Ring." Collection of Czechoslovak Chemical Communications 65, no. 3 (2000): 395–406. http://dx.doi.org/10.1135/cccc20000395.

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Tosylation of (±)-1-[trans-4-hydroxy-3,3-bis(hydroxymethyl)cyclopentyl]-5-methylpyrimidine-2(1H),4(3H)-dione (1) and (±)-1-[cis-4-hydroxy-3,3-bis(hydroxymethyl)cyclopentyl]-5-methylpyrimidine-2(1H),4(3H)-dione (2) and treatment of the obtained 1-{(1R*,3R*,4S*)- 4-hydroxy-3-(hydroxymethyl)-3-[(tosyloxy)methyl]cyclopentyl}-5-methylpyrimidine- 2(1H),4(3H)-dione (6) and 1-{(1R*,3S*,4R*)-4-hydroxy-3-(hydroxymethyl)-3-[(tosyloxy)- methyl]cyclopentyl}-5-methylpyrimidine-2(1H),4(3H)-dione (9) with methanolic sodium methoxide gave 1-[(1R*,4S*,6S*)-4-hydroxymethyl-2-oxabicyclo[3.2.0]hept-6-yl]-5-methylp
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Park, Joo-Heon, Kristin Burns, Cynthia Kinsland, and Tadhg P. Begley. "Characterization of Two Kinases Involved in Thiamine Pyrophosphate and Pyridoxal Phosphate Biosynthesis in Bacillus subtilis: 4-Amino-5-Hydroxymethyl-2-Methylpyrimidine Kinase and Pyridoxal Kinase." Journal of Bacteriology 186, no. 5 (2004): 1571–73. http://dx.doi.org/10.1128/jb.186.5.1571-1573.2004.

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ABSTRACT Two Bacillus subtilis genes encoding two proteins (currently annotated ThiD and YjbV) were overexpressed and characterized. YjbV has 4-amino-5-hydroxymethyl-2-methylpyrimidine and 4-amino-5-hydroxymethyl-2-methylpyrimidine pyrophosphate kinase activity and should be reannotated ThiD, and B. subtilis ThiD has pyridoxine, pyridoxal, and pyridoxamine kinase activity and should be reannotated PdxK.
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Volovenko, Olesya, Tetiana Keda, Natalia Skreminska, Demyd Milokhov, Olga Khilya, and Olga Zaporozhets. "2,6-Diamino-1-N-methylpyrimidine as new fluorescent probe for palladium(II) determination using hyphenated technique." Adsorption Science & Technology 35, no. 7-8 (2017): 728–34. http://dx.doi.org/10.1177/0263617417708086.

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The selective and sensitive hyphenated technique for Pd(II) fluorescence and spectrophotometric determination was proposed. The procedure was based on preliminary solid-phase extraction of [PdCl4]2− onto silica modified with quaternary ammonium salts, with the subsequent elution from the surface by 2,6-diamino-1- N-methylpyrimidine solution and measurement of the fluorescence intensity. The luminescence enhancement effect of 2,6-diamino-1- N-methylpyrimidine in the presence of Pd(II) due to the complex formation was applied to the development of sorption-spectroscopic techniques for detecting
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Bai, Jie, Jia Xie, Li-Ting Wang, et al. "Discovery of methylpyrimidine ring-fused diterpenoid analogs as a novel testosterone synthesis promoter." RSC Advances 9, no. 17 (2019): 9709–17. http://dx.doi.org/10.1039/c9ra00702d.

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Tsunobuchi, Yoshihide, Souhei Kaneko, Koji Nakabayashi та Shin-ichi Ohkoshi. "Poly[[diaquadeca-μ2-cyanido-κ20C:N-hexacyanido-κ6C-bis(μ2-5-methylpyrimidine-κ2N:N′)bis(5-methylpyrimidine-κN)tricopper(II)ditungstate(V)] dihydrate]". Acta Crystallographica Section E Structure Reports Online 70, № 2 (2014): m47—m48. http://dx.doi.org/10.1107/s1600536814000166.

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In the title complex, {[Cu3[W(CN)8]2(C5H6N2)4(H2O)2]·2H2O}n, the coordination polyhedron of the eight-coordinated WVatom is a bicapped trigonal prism, in which five CN groups are bridged to CuIIions, and the other three CN groups are terminally bound. Two of the CuIIions lie on a centre of inversion and each of the three independent CuIIcations is pseudo-octahedrally coordinated. In the crystal structure, cyanido-bridged-Cu—W—Cu layers are linked by pillars involving the third independent CuIIion, generating a three-dimensional network with non-coordinating water molecules and 5-methylpyrimidi
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Li, Bowen, Zhiyi Li, Taiping Hu, et al. "Highly efficient blue organic light-emitting diodes from pyrimidine-based thermally activated delayed fluorescence emitters." Journal of Materials Chemistry C 6, no. 9 (2018): 2351–59. http://dx.doi.org/10.1039/c7tc05746f.

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Three highly efficient blue thermally activated delayed fluorescence (TADF) emitters have been synthesized based on pyrimidine, 2-methylpyrimidine and 2-phenylpyrimidine as the acceptor and 10H-spiro[acridan-9,9′-fluorene] as the donor moiety.
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Maimaiti, Yuemaierjiang, and Xieraili Maimaitiyiming. "Fluorescence quenching of methanol-soluble polypyrimidine by aluminum ion." Materials Express 10, no. 7 (2020): 1177–88. http://dx.doi.org/10.1166/mex.2020.1741.

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The different proportion methylpyrimidine ring copolymers has been synthesized and characterized by 1HNMR, 13CNMR and FT-IR spectrum. The detection limit of P80 for Al3+ ions of 7.94 × 10–8 M at the dichloromethane solution. The binding constant (Kb) between copolymers and with Al3+ was 1.10 × 104 M–1. The EDS analysis and XPS spectroscopy can expose that the copolymer and Al3+ had been coordination with each other. The neutral polymers with good recovery properties can be used as sensor detect Al3+ in the organic solvent. The methanol-soluble polymer has been synthesized from methylpyrimidine
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Dissertations / Theses on the topic "Methylpyrimidine"

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Nguyen, Thi Thuy. "Structures and internal dynamics of methylated nitrogen containing aromatic rings probed by means of microwave spectroscopy, quantum chemical calculation and spectral modelling." Electronic Thesis or Diss., Université Paris Cité, 2021. http://www.theses.fr/2021UNIP7368.

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Ce travail est dédié à l'étude des signatures de rotation de six cycles aromatiques contenant de l'azote et un ou deux groupes méthyles (2-méthylthiazole (2MTA), 2-méthypyrrole (2MP), 3-méthylpyrrole (3MP), 2,5-diméthylpyrrole (25DMP) 4,5-diméthylthiazole (45DMTA), 4-méthylpyrimidine (4MPY)) - des précurseurs d'hydrocarbures aromatiques polycycliques qui jouent un rôle crucial en astrochimie et ont le potentiel d'être détectés dans l'espace. Notre étude vise à affiner la compréhension des effets de mouvement(s) de grande amplitude du (des) groupe(s) méthyle(s), en produisant des constantes mol
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Jeng, Cang-Sian, and 鐘蒼賢. "Synthesis and structures of Zn(II) compounds containing 2-aminopyrimidine or 2-amino-4-methylpyrimidine." Thesis, 2009. http://ndltd.ncl.edu.tw/handle/96520855716850152942.

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碩士<br>中原大學<br>化學研究所<br>97<br>The syntheses and structures of a series of zinc compounds [ZnCl2(L1)2] (L1 = 2-Aminopyrimidine), 1; [ZnBr2(L1)2], 2; [ZnI2(L1)2], 3; [ZnBr(OH)(L1)]n, 4; [Zn(NO3)(OH)(L1)]n, 5; [ZnCl2(L2)2] (L2 = 2-Amino-4-methylpyrimidine), 6; [ZnBr2(L2)2], 7; [ZnI2(L2)2], 8, are reported. All compounds have been structurally characterized by X-ray crystallography. Compounds 1 - 3 are same configuration as well as compounds 6 - 8, which consist of a central zinc(II) metal centers coordinated by two organic ligands and two anions, forming a tetrahedral geometry. The C–H---X, N–H---
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Tai, Mei-Chu, and 戴美珠. "Synthesis and Structures of Silver (I)and Copper (II) Complexes Containing2-amino-4-methylpyrimidine Ligand." Thesis, 2004. http://ndltd.ncl.edu.tw/handle/3gu4df.

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碩士<br>中原大學<br>化學研究所<br>92<br>A series of silver (I) complexes of the types [Ag(amp)2](NO3), 1 ; [Ag(amp)2](ClO4), 2 ; [Ag(amp)2](BF4), 3 ; [Ag(amp)2](PF6), 4 and [Cu2(O2CCH3)4(amp)2], 5 have been prepared by the reactions of AgX (X = NO3�{, ClO4�{, BF4�{, PF6�{) and Cu(O2CCH3)2 with amp (amp = 2-amino-4-methylpyrimidine) in methanol solution. All the complexes have been structurally characterized by X-ray crystallography , FT-IR and 1H-NMR spectra. The molecules of complex 1–5 are interlinked through a series of self-complementary double hydrogen bondings to form one –dimensional molecular cha
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Janatková, Tereza. "Syntéza a studium krystalických materiálů pro NLO." Master's thesis, 2018. http://www.nusl.cz/ntk/nusl-382790.

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This thesis is focused on preparation and study of new compounds of chosen organic bases with potential use in nonlinear optics. 2-amino-5-nitropyrimidine, 2-amino-4-methylpyrimidine and their salts with inorganic and organic acids are compounds of the main interest. Diffraction and vibrational-spectroscopic methods of characterization were used in combination with quantum chemical calculation methods. Another aim of this thesis was preparation of new salts of chosen pyrimidine derivates with the use of methylsulphonic acid. Part of this section is devoted to completion of pyridinium methylsul
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Book chapters on the topic "Methylpyrimidine"

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Pardasani, R. T., and P. Pardasani. "Magnetic properties of chromium(III) chloride complex with 1, 3-disuccinimide(4-phenyl-5-ethoxycarbonyl-6- methylpyrimidine-2-one)." In Magnetic Properties of Paramagnetic Compounds. Springer Berlin Heidelberg, 2017. http://dx.doi.org/10.1007/978-3-662-49202-4_465.

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Pardasani, R. T., and P. Pardasani. "Magnetic properties of manganese(II) chloride complex with 1, 3-disuccinimide(4-phenyl-5-ethoxycarbonyl-6-methylpyrimidine-2-one)." In Magnetic Properties of Paramagnetic Compounds. Springer Berlin Heidelberg, 2017. http://dx.doi.org/10.1007/978-3-662-49202-4_643.

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Pardasani, R. T., and P. Pardasani. "Magnetic properties of iron(III) chloride complex with 1, 3-disuccinimide(4-phenyl-5-ethoxycarbonyl-6-methylpyrimidine-2-one)." In Magnetic Properties of Paramagnetic Compounds. Springer Berlin Heidelberg, 2017. http://dx.doi.org/10.1007/978-3-662-53971-2_114.

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Pardasani, R. T., and P. Pardasani. "Magnetic properties of cobalt(II) chloride complex with 1, 3-disuccinimide-(4-phenyl-5-ethoxycarbonyl-6-methylpyrimidine-2-one)." In Magnetic Properties of Paramagnetic Compounds. Springer Berlin Heidelberg, 2017. http://dx.doi.org/10.1007/978-3-662-53971-2_364.

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Pardasani, R. T., and P. Pardasani. "Magnetic properties of nickel(II) chloride complex with 1, 3-disuccinimide(4-phenyl-5-ethoxycarbonyl-6-methylpyrimidine-2-one)." In Magnetic Properties of Paramagnetic Compounds. Springer Berlin Heidelberg, 2017. http://dx.doi.org/10.1007/978-3-662-53971-2_634.

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Pardasani, R. T., and P. Pardasani. "Magnetic properties of copper(II) chloride complex with 1, 3-disuccinimide(4-phenyl-5-ethoxycarbonyl-6-methylpyrimidine-2-one)." In Magnetic Properties of Paramagnetic Compounds. Springer Berlin Heidelberg, 2017. http://dx.doi.org/10.1007/978-3-662-53974-3_184.

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Pardasani, R. T., and P. Pardasani. "Magnetic properties of di-μ-hydroxo-bis(μ-perchlorato-O, O′)-bis[bis(2-amino-4-methylpyrimidine)copper(II)]." In Magnetic Properties of Paramagnetic Compounds. Springer Berlin Heidelberg, 2017. http://dx.doi.org/10.1007/978-3-662-53974-3_79.

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Sako, M. "Cyclization of 4-Methylpyrimidine-5-carboxamides or 4-Methylpyrimidine-5-carbonitriles with a One-Carbon Donor." In Six-Membered Hetarenes with Two Identical Heteroatoms. Georg Thieme Verlag KG, 2004. http://dx.doi.org/10.1055/sos-sd-016-01576.

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Sako, M. "Intramolecular Cyclization of 4-Methylpyrimidine-5-carboxamides." In Six-Membered Hetarenes with Two Identical Heteroatoms. Georg Thieme Verlag KG, 2004. http://dx.doi.org/10.1055/sos-sd-016-01584.

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Kikelj, D. "From 6-Methylpyrimidine-5-carboxylates and Alkynes or Alkenes." In Six-Membered Hetarenes with Two Identical Heteroatoms. Georg Thieme Verlag KG, 2004. http://dx.doi.org/10.1055/sos-sd-016-00850.

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Conference papers on the topic "Methylpyrimidine"

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Dambaev, Aleksandr V., Denis A. Kolesnik, Igor P. Yakovlev, and Tamara L. Semakova. "Formylation of 2-Methylpyrimidine-4,6-diol Under the Conditions of the Vilsmeier–Haack Reaction." In ECSOC 2024. MDPI, 2024. https://doi.org/10.3390/ecsoc-28-20128.

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Faizan, Mohd, Ziya Afroz, Mohammad Jane Alam, Sheeraz Ahmad Bhat, Shabbir Ahmad, and Afaq Ahmad. "Nature and potency interactions of the hydrogen bond through the NBO analysis for charge transfer complex between 2-amino-4-hydroxy-6-methylpyrimidine and 2,3-pyrazinedicarboxylic acid." In 2ND INTERNATIONAL CONFERENCE ON CONDENSED MATTER AND APPLIED PHYSICS (ICC 2017). Author(s), 2018. http://dx.doi.org/10.1063/1.5033245.

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