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Journal articles on the topic 'Microwave Assisted Organic Synthesis (MWAOS)'

Author: Grafiati

Published: 3 June 2025

Last updated: 31 July 2025

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1

Mullasseril, Abhilash. "Substituent Effects on Solvent-Free Synthesis (MWAOS) of Dihydroquinazolinones by the Addition of Isatoic Anhydride to a Series of Phenyl-Substituted N-(Phenylmethylidene) Anilines." Journal of Chemistry 2013 (2013): 1–4. http://dx.doi.org/10.1155/2013/790878.

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The present study concentrates on the synthesis of a series of dihydroquinazolinones by applying the green concept Microwave Assisted Organic Synthesis (MWAOS) with high atom economy. A series of phenyl-substituted N-(phenylmethylidene) anilines are coupled with isatoic anhydride using a microwave oven.

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2

Barbosa, André D. S., Salete S. Balula, Filipe A. Almeida Paz, Baltazar de Castro, and Luís Cunha-Silva. "Porous Metal-Organic Framework Materials: Microwave Assisted Synthesis and Oxidative Catalytic Tests." Materials Science Forum 730-732 (November 2012): 1024–29. http://dx.doi.org/10.4028/www.scientific.net/msf.730-732.1024.

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Metal-Organic Framework Materials MIL‑101(Cr) ([Cr3X(H2O)2O(bdc)3]∙n(H2O), where X− = F− or OH−, n ≈ 25 and H2bdc stands for 1,4-benzene-dicarboxylic acid] and MOF‑5(Zn) [Zn4O(bdc)3] were prepared by hydrothermal or solvothermal methods as well as Microwave‑Assisted Synthesis (MWAS), for which the detailed synthetic parameters were optimized. The crystal structures were confirmed by powder X-ray diffraction and the materials were further characterized by FT‑IR absorption spectroscopy. MIL‑101(Cr) and MOF‑5(Zn) showed weak catalytic activity in the oxidation of terpene, thiophene and cis-cycloo

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3

Menéndez, J. Carlos. "Microwave Assisted Organic Synthesis." Synthesis 2006, no. 01 (2006): 186. http://dx.doi.org/10.1055/s-2006-925464.

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4

Keglevich, Gyorgy, Alajos Grun, Erika Balint, Nora Zsuzsa Kiss, and Erzsebet Jablonkai. "Microwave-Assisted Organophosphorus Synthesis." Current Organic Chemistry 17, no. 5 (2013): 545–54. http://dx.doi.org/10.2174/1385272811317050009.

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5

Katritzky, Alan R., and Sandeep K. Singh. "Microwave-assisted heterocyclic synthesis." Arkivoc 2003, no. 13 (2003): 68–86. http://dx.doi.org/10.3998/ark.5550190.0004.d09.

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6

Evangelista, E. A., M. R. C. Couri, R. B. Alves, D. S. Raslan, and R. P. F. Gil. "Microwave‐Assisted Xanthone Synthesis." Synthetic Communications 36, no. 16 (2006): 2275–80. http://dx.doi.org/10.1080/00397910600639653.

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7

Lidström, Pelle, Jason Tierney, Bernard Wathey, and Jacob Westman. "Microwave assisted organic synthesis—a review." Tetrahedron 57, no. 45 (2001): 9225–83. http://dx.doi.org/10.1016/s0040-4020(01)00906-1.

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8

Lidstroem, Pelle, Jason Tierney, Bernard Wathey, and Jacob Westman. "ChemInform Abstract: Microwave Assisted Organic Synthesis." ChemInform 33, no. 8 (2010): no. http://dx.doi.org/10.1002/chin.200208292.

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9

GIGUERE, R. J. "ChemInform Abstract: Microwave-Assisted Organic Synthesis." ChemInform 24, no. 48 (2010): no. http://dx.doi.org/10.1002/chin.199348306.

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10

Agrawal, Y. K., N. C. Desai, and N. D. Mehta. "Microwave‐Assisted Synthesis of Azocalixarenes." Synthetic Communications 37, no. 13 (2007): 2243–52. http://dx.doi.org/10.1080/00397910701397086.

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11

He, Ling, Ju-Lian Li, Jian-Jun Zhang, Pu Su, and Shi-Long Zheng. "Microwave Assisted Synthesis of Melatonin." Synthetic Communications 33, no. 5 (2003): 741–47. http://dx.doi.org/10.1081/scc-120016317.

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12

Ghafarzadeh, Mohammad, Ebrahim Saeedian Moghadam, and Fereshteh Faraji. "Microwave Assisted Synthesis of Dibenzoxazepines." Journal of Heterocyclic Chemistry 50, no. 4 (2013): 754–57. http://dx.doi.org/10.1002/jhet.1548.

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13

Klinowski, Jacek, Filipe A. Almeida Paz, Patrícia Silva, and João Rocha. "Microwave-Assisted Synthesis of Metal–Organic Frameworks." Dalton Trans. 40, no. 2 (2011): 321–30. http://dx.doi.org/10.1039/c0dt00708k.

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14

Rebrov, E. V. "Microwave-assisted organic synthesis in microstructured reactors." Russian Journal of General Chemistry 82, no. 12 (2012): 2060–69. http://dx.doi.org/10.1134/s1070363212120262.

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15

韩, 谢. "Organic Drug Synthesis Assisted with Microwave Irradiation." Journal of Microwave Chemistry 01, no. 01 (2017): 15–21. http://dx.doi.org/10.12677/mc.2017.11004.

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16

Pathak, Arpit Kumar, Chetna Ameta, Rakshit Ameta, and Pinki B. Punjabi. "Microwave-Assisted Organic Synthesis in Ionic Liquids." Journal of Heterocyclic Chemistry 53, no. 6 (2015): 1697–705. http://dx.doi.org/10.1002/jhet.2515.

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17

Mateev, Emilio, Ali Irfan, Alexandrina Mateeva, Maya Georgieva, and Alexander Zlatkov. "Microwave-assisted organic synthesis of pyrroles (Review)." Pharmacia 71 (March 25, 2024): 1–10. http://dx.doi.org/10.3897/pharmacia.71.e119866.

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The detection of pyrrole rings in numerous organic compounds with various pharmacological activities, emphasizes its huge importance in medicinal chemistry. Thus, the synthesis of pyrroles continues to arouse interest and Paal-Knorr condensation is considered to be the main synthetic route. A significant advance has been made since the MW activation was introduced in the organic synthesis which can be confirmed with the rapid growth of the published papers on that topic. Microwave irradiation is gaining popularity since faster reaction time, higher yields, easier work-up and reduced energy inp

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18

Mateev, Emilio, Ali Irfan, Alexandrina Mateeva, Maya Georgieva, and Alexander Zlatkov. "Microwave-assisted organic synthesis of pyrroles (Review)." Pharmacia 71, no. () (2024): 1–10. https://doi.org/10.3897/pharmacia.71.e119866.

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The detection of pyrrole rings in numerous organic compounds with various pharmacological activities, emphasizes its huge importance in medicinal chemistry. Thus, the synthesis of pyrroles continues to arouse interest and Paal-Knorr condensation is considered to be the main synthetic route. A significant advance has been made since the MW activation was introduced in the organic synthesis which can be confirmed with the rapid growth of the published papers on that topic. Microwave irradiation is gaining popularity since faster reaction time, higher yields, easier work-up and reduced energy inp

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19

Strauss, CR, and RW Trainor. "Developments in Microwave-Assisted Organic Chemistry." Australian Journal of Chemistry 48, no. 10 (1995): 1665. http://dx.doi.org/10.1071/ch9951665.

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Microwave-assisted organic chemistry is reviewed in the context of the methods employed. A range of technical difficulties indicated that specifically designed reactors were required. Hence, the CSIRO continuous microwave reactor (CMR) and microwave batch reactor (MBR) were developed for organic synthesis. On the laboratory scale, they operated at temperatures (pressures) up to 200°C (1400 kPa) and 260°C (10 MPa), respectively. Advantages and applications of the units are discussed, along with safety issues. Features include the capability for rapid, controlled heating and cooling of reaction

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20

Kruithof, Art, Eelco Ruijter, and Romano V.A. Orru. "Microwave-Assisted Multicomponent Synthesis of Heterocycles." Current Organic Chemistry 15, no. 2 (2011): 204–36. http://dx.doi.org/10.2174/138527211793979817.

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21

Cieslik, Wioleta, Maciej Serda, Agata Kurczyk, and Robert Musiol. "Microwave Assisted Synthesis of Monoazanaphthalene Scaffolds." Current Organic Chemistry 17, no. 5 (2013): 491–503. http://dx.doi.org/10.2174/1385272811317050006.

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22

Abe, Taichi, Akira Miyazawa, Yuji Kawanishi, and Hideo Konno. "Microwave-Assisted Synthesis of Metal Complexes." Mini-Reviews in Organic Chemistry 8, no. 3 (2011): 315–33. http://dx.doi.org/10.2174/157019311796197346.

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23

Nakamura, Takashi, Ritsuko Nagahata, and Kazuhiko Takeuchi. "Microwave-Assisted Polyester and Polyamide Synthesis." Mini-Reviews in Organic Chemistry 8, no. 3 (2011): 306–14. http://dx.doi.org/10.2174/157019311796197454.

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24

Yi, Xiangyan, Zhipeng Zhang, He Huang, Jonathan B. Baell, Yang Yu та Fei Huang. "Microwave-Assisted Synthesis of α-Diazoesters". Chinese Journal of Organic Chemistry 39, № 2 (2019): 544. http://dx.doi.org/10.6023/cjoc201807031.

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25

Sagar, A. D., N. A. Shinde, and B. P. Bandgar. "MICROWAVE-ASSISTED SYNTHESIS OF TRIARYL PHOSPHATES." Organic Preparations and Procedures International 32, no. 3 (2000): 269–71. http://dx.doi.org/10.1080/00304940009355923.

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26

Guzmán-Lucero, Diego, Natalya V. Likhanova, Herbert Höpfl, Javier Guzmán, Dmitri Likhatchev, and Rafael Martínez-Palou. "Efficient microwave-assisted synthesis of bisimides." Arkivoc 2006, no. 10 (2006): 7–20. http://dx.doi.org/10.3998/ark.5550190.0007.a02.

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27

Nichols, Christie E., Dani Youssef, Robert G. Harris, and Amitabh Jha. "Microwave-assisted synthesis of curcumin analogs." Arkivoc 2006, no. 13 (2006): 64–72. http://dx.doi.org/10.3998/ark.5550190.0007.d07.

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28

Bound, D. James, B. K. Bettadaiah, and P. Srinivas. "Microwave-Assisted Synthesis of Alkyl Thiocyanates." Synthetic Communications 43, no. 8 (2013): 1138–44. http://dx.doi.org/10.1080/00397911.2011.622848.

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29

Taddei, Maurizio, Giacomo Minetto, and L. Raffaella Lampariello. "Microwave-Assisted Synthesis of Polysubstituted Pyridazines." Synlett, no. 18 (2005): 2743–46. http://dx.doi.org/10.1055/s-2005-918926.

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30

Jebasingh, B., and V. Alexander. "Microwave‐Assisted Synthesis of 1,4,7,10‐Tetraazacyclododecane." Synthetic Communications 36, no. 5 (2006): 653–57. http://dx.doi.org/10.1080/15459620500408850.

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31

Sagar, A. D., D. S. Patil, and B. P. Bandgar. "Microwave Assisted Synthesis of Triaryl Cyanurates." Synthetic Communications 30, no. 10 (2000): 1719–23. http://dx.doi.org/10.1080/00397910008087214.

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32

Shah, Sakshi, and Baldev Singh. "Microwave-Assisted Synthesis of Spiro-Isoxazolidines." Journal of Heterocyclic Chemistry 50, no. 4 (2013): 959–62. http://dx.doi.org/10.1002/jhet.1803.

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33

Kutuk, Halil, and Nalan Turkoz. "Microwave-Assisted Synthesis of Disulfides." Phosphorus, Sulfur, and Silicon and the Related Elements 186, no. 7 (2011): 1515–22. http://dx.doi.org/10.1080/10426507.2010.520174.

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34

Chandrasekharam, M., Ch Srinivasa Rao, Surya P. Singh, et al. "Microwave-assisted synthesis of metalloporphyrazines." Tetrahedron Letters 48, no. 14 (2007): 2627–30. http://dx.doi.org/10.1016/j.tetlet.2007.02.007.

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35

Piras, Leonarda, Chiara Ghiron, Giacomo Minetto, and Maurizio Taddei. "Microwave-assisted synthesis of tetrahydroindoles." Tetrahedron Letters 49, no. 3 (2008): 459–62. http://dx.doi.org/10.1016/j.tetlet.2007.11.114.

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36

Luo, Guanglin, Ling Chen, and Graham S. Poindexter. "Microwave-assisted synthesis of aminopyrimidines." Tetrahedron Letters 43, no. 33 (2002): 5739–42. http://dx.doi.org/10.1016/s0040-4039(02)01190-5.

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37

Collman, James P., and Richard A. Decréau. "Microwave-assisted synthesis of corroles." Tetrahedron Letters 44, no. 6 (2003): 1207–10. http://dx.doi.org/10.1016/s0040-4039(02)02792-2.

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38

Jankowski, Christopher K., Gaëtan LeClair, Jacqueline MR Bélanger, Jocelyn RJ Paré, and Marie-Rose VanCalsteren. "Microwave-assisted Diels-Alder synthesis." Canadian Journal of Chemistry 79, no. 12 (2001): 1906–9. http://dx.doi.org/10.1139/v01-183.

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The synthesis of isoquinolinone carboxylates was performed using arecoline or its isomer N-methyl tetrahydro pyridine carboxylate with Danishefsky's diene via thermal or microwave assisted Diels-Alder reaction. The comparison of both condensation modes showed that the microwave method not only afforded higher yields of the adducts, but also lead to the formation of a new α,β-unsaturated pyridyl ketone. All structures were identified with the help of high resolution 2D NMR.Key words: Diels-Alder microwave assisted reaction, microwave synthesis, Michael, diene, isoquinoline carboxylate synthesis

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39

Keller, Walter E. "ChemInform Abstract: Microwave-Assisted Organic Synthesis: Application of Microwave Energy in Organic Synthesis. Part 1." ChemInform 33, no. 25 (2010): no. http://dx.doi.org/10.1002/chin.200225255.

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40

Agarwal, Alka, Sanjeev Kumar, and Anand Maurya. "Microwave-Assisted Synthesis of Heterocyclic Scaffolds." SynOpen 08, no. 03 (2024): 138–52. http://dx.doi.org/10.1055/s-0043-1775379.

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AbstractIn recent years, there has been a notable surge in the utilization of microwave energy, leading to the emergence of innovative and groundbreaking methods across various branches of chemistry, including organic synthesis, materials science, heterocyclic chemistry, and medicinal chemistry. This comprehensive literature review delves into the microwave-assisted organic synthesis of specific heterocycles, illuminating its effectiveness in producing diverse molecules with heightened efficiency and selectivity. The review highlights the significant role of microwave irradiation as a potent m

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41

Bordoni, Cinzia, Cecilia Maria Cima, Elisa Azzali, Gabriele Costantino, and Andrea Brancale. "Microwave-assisted organic synthesis of nucleoside ProTide analogues." RSC Advances 9, no. 35 (2019): 20113–17. http://dx.doi.org/10.1039/c9ra01754b.

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42

Adachi, Kaoru, Takeru Iwamura, and Yoshiki Chujo. "Microwave Assisted Synthesis of Organic-Inorganic Polymer Hybrids." Polymer Bulletin 55, no. 5 (2005): 309–15. http://dx.doi.org/10.1007/s00289-005-0436-8.

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43

Patel, Devang, and Bhumika Patel. "ChemInform Abstract: Microwave Assisted Organic Synthesis: An Overview." ChemInform 43, no. 13 (2012): no. http://dx.doi.org/10.1002/chin.201213238.

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44

Loupy, Andre, Laurence Perreux, and Alain Petit. "ChemInform Abstract: Solvent-Free Microwave-Assisted Organic Synthesis." ChemInform 33, no. 19 (2010): no. http://dx.doi.org/10.1002/chin.200219288.

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45

Chetna, Ameta, Ameta Aarti, Ameta Rakshit, B. Punjabi P., and C. Ameta Suresh. "Microwave assisted organic synthesis : A green chemical approach." Journal of Indian Chemical Society Vol. 88, Aug 2011 (2011): 1165–85. https://doi.org/10.5281/zenodo.5786068.

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Microwave Chemistry Laboratory, Department of Chemistry, Mohanlal Sukhadia University, Udaipur-313 001, Rajasthan, India Department of Chemistry, G. N. G. P.G. College, Udaipur-313 002, Rajasthan, India Department of Pure & Applied Chemistry, University of Kota, Kota-324 005, Rajasthan, India Pacific College of Basic and Applied Sciences, Pacific University, Debari, Udaipur-313 024, Rajasthan, India <em>E-mail</em> : ameta_sc@yahoo.com <em>Manuscript received 11 April 2011, accepted 18 April 2011</em>  

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46

Elgemeie, Galal H., and Doaa M. Masoud. "Recent trends in microwave assisted synthesis of fluorescent dyes." Pigment & Resin Technology 45, no. 6 (2016): 381–407. http://dx.doi.org/10.1108/prt-04-2015-0036.

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Purpose This paper aims to focus on the most popular technique nowadays, the use of microwave irradiation in organic synthesis; in a few years, most chemists will use microwave energy to heat chemical reactions on a laboratory scale. Also, many scientists use microwave technology in the industry. They have turned to microwave synthesis as a frontline methodology for their projects. Microwave and microwave-assisted organic synthesis (MAOS) has emerged as a new “lead” in organic synthesis. Design/methodology/approach Using microwave radiation for synthesis and design of fluorescent dyes is of gr

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47

Wang, Ya'nan, Chong Wang, Yuming Qi, Guokai Li, Xiaoliu Li, and Kerang Wang. "Microwave-Assisted Synthesis of Perylene Monoimide Derivatives." Chinese Journal of Organic Chemistry 41, no. 2 (2021): 702. http://dx.doi.org/10.6023/cjoc202008010.

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48

Sugamoto, Kazuhiro, Yoh‐ichi Matsushita, Yu‐hei Kameda, Masahiko Suzuki, and Takanao Matsui. "Microwave‐assisted Synthesis of N‐Hydroxyphthalimide Derivatives." Synthetic Communications 35, no. 1 (2005): 67–70. http://dx.doi.org/10.1081/scc-200046498.

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49

Katritzky, Alan R., Adam S. Vincek, and Kazuyuki Suzuki. "Microwave-assisted synthesis of peptidyl phosphorus ylides." Arkivoc 2005, no. 5 (2005): 116–26. http://dx.doi.org/10.3998/ark.5550190.0006.511.

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50

Zuo, Hua, Geo Jose, Zhu-bo Li, Bu-Hyun Moon, Dong-Soo Shin, and Manjunath Ghate. "Microwave-assisted synthesis of fluorinated coumarino sulfonamides." Arkivoc 2008, no. 2 (2008): 183–89. http://dx.doi.org/10.3998/ark.5550190.0009.220.

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