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Journal articles on the topic 'Microwave-heating assisted solvothermal synthesis'

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Published: 4 June 2021
Last updated: 4 February 2022

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1

Blanita, Gabriela, Gheorghe Borodi, Mihaela D. Lazar, Alexandru-Radu Biris, Lucian Barbu-Tudoran, Ioan Coldea, and Dan Lupu. "Microwave assisted non-solvothermal synthesis of metal–organic frameworks." RSC Advances 6, no. 31 (2016): 25967–74. http://dx.doi.org/10.1039/c5ra26097c.

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2

Liu, Xiaoying, Bozhi Tian, Chengzhong Yu, Bo Tu, and Dongyuan Zhao. "Microwave-Assisted Solvothermal Synthesis of Radial ZnS Nanoribbons." Chemistry Letters 33, no. 5 (May 2004): 522–23. http://dx.doi.org/10.1246/cl.2004.522.

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3

Kesuma, Ruth Febriana, Aep Patah, and Yessi Permana. "Microwave-Assisted Synthesis of DUT-52 and Investigation of Its Photoluminescent Properties." Bulletin of Chemical Reaction Engineering & Catalysis 14, no. 1 (April 15, 2019): 124. http://dx.doi.org/10.9767/bcrec.14.1.2369.124-129.

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A zirconium metal-organic framework (MOF) of DUT-52 (DUT: Dresden University of Technology) was synthesized herein by reacting zirconium tetrachloride (ZrCl4) and 2,6-naphthalenedicarboxylic acid (H2NDC) in DMF under microwave heating at 115 oC for 25 min. This synthetic procedure was more efficient than a solvothermal method, by which a long thermal exposure (24 h) of 100-150 oC was required to produce the same MOF. The MOF has a thermal stability of 560 °C, prior to partial loss of interconnected 2,6-naphthalenedicarboxylate (NDC) linkers at some structure building units (SBU). Crystallinity of this DUT-52 was ca. 77 %, which was the same as one synthesized solvothermally. Diffuse Reflectance UV-Vis spectra revealed an absorption at λex of 287 nm, which was equivalent to a bandgap energy of 4.32 eV. Electron excitations of this DUT-52 at 275 and 300 nm gave emission wavelength of 433 nm (a purple region), indicating a prospective use of DUT-52 as a photoluminescent material. Copyright © 2018 BCREC Group. All rights reservedReceived: 20th January 2018; Revised: 28th September 2018; Accepted: 30th September 2018; Available online: 25th January 2019; Published regularly: April 2019How to Cite: Kesuma, R.F., Patah, A., Permana, Y. (2019). Microwave-Assisted Synthesis of DUT-52 and Investigation of Its Photoluminescent Properties. Bulletin of Chemical Reaction Engineering & Catalysis, 14 (1): 124-129 (doi:10.9767/bcrec.14.1.2369.124-129)Permalink/DOI: https://doi.org/10.9767/bcrec.14.1.2369.124-129
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4

Lai, Li Sze, Yin Fong Yeong, Kok Keong Lau, and Mohd Shariff Azmi. "Fast Synthesis of Highly Crystalline ZIF-8 Using Microwave-Assisted Solvothermal Method." Applied Mechanics and Materials 773-774 (July 2015): 1133–37. http://dx.doi.org/10.4028/www.scientific.net/amm.773-774.1133.

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This paper presents the formation of highly crystalline ZIF-8 using microwave-assisted solvothermal method. The crystallinity of the ZIF-8 particles was characterized using X-ray diffraction. The lattice vibrations of the structure in the ZIF-8 framework were determined through Fourier transforms infrared spectroscopy. The morphology of the ZIF-8 particles was observed through scanning electron microscopy. The results showed that, 0.5 hour was sufficient for the formation of highly crystalline ZIF-8 particles using microwave-assisted solvothermal method under temperature 120 oC.
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5

Lu, Qingyi, Feng Gao, and Sridhar Komarneni. "Microwave-assisted synthesis of one-dimensional nanostructures." Journal of Materials Research 19, no. 6 (June 2004): 1649–55. http://dx.doi.org/10.1557/jmr.2004.0237.

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A microwave-assisted solvothermal method was used for the synthesis of selenium nanorods. The obtained selenium nanorods have axis ratios higher than 100 with their diameters in the range of 30–150 nm. This method is quite simple, rapid, adjustable, and general. Besides the effects of the experimental parameters on the synthesis of the selenium nanorods, the generality of this method has also been investigated, by which other one-dimensional nanostructures, metal lead and semiconductor cadmium sulfide nanorods, were also successfully synthesized.
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6

Christé, Esteves da Silva, and Pinto da Silva. "Evaluation of the Environmental Impact and Efficiency of N-Doping Strategies in the Synthesis of Carbon Dots." Materials 13, no. 3 (January 21, 2020): 504. http://dx.doi.org/10.3390/ma13030504.

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The efficiency and associated environmental impacts of different N-doping strategies of carbon dots (CDs) were evaluated. More specifically, N-doped CDs were prepared from citric acid via two main synthesis routes: Microwave-assisted hydrothermal treatment with addition of N-containing small organic molecules (urea and ethylenediamine (EDA)); and microwave-assisted solvothermal treatment in N-containing organic solvents (n,n-dimethylformamide (DMF), acetonitrile and pyridine). These syntheses produced CDs with similar blue emission. However, XPS analysis revealed that CDs synthesized via both hydrothermal routes presented a better N-doping efficiency (~15 at.%) than all three solvothermal-based strategies (0.6–7 at.%). However, from the former two hydrothermal strategies, only the one involving EDA as a nitrogen-source provided a non-negligible synthesis yield, which indicates that this should be the preferred strategy. This conclusion was supported by a subsequent life cycle assessment (LCA) study, which revealed that this strategy is clearly the most sustainable one from all five studied synthesis routes.
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7

Shen, Yue-Qin, Ying-Jie Zhu, Fei-Fei Chen, Ying-Ying Jiang, Zhi-Chao Xiong, and Feng Chen. "Antibacterial gluey silver–calcium phosphate composites for dentine remineralization." Journal of Materials Chemistry B 6, no. 30 (2018): 4985–94. http://dx.doi.org/10.1039/c8tb00881g.

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8

Jangu, Surendra, Biraj Kanta Satpathy, Mula Raju, Chacko Jacob, and Debabrata Pradhan. "Synthesis of V-shaped MnO2 nanostructure and its composites with reduced graphene oxide for supercapacitor application." Dalton Transactions 50, no. 20 (2021): 6878–88. http://dx.doi.org/10.1039/d1dt00422k.

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9

ZHANG, J., W. QIN, J. ZHANG, Y. WAN, C. CAO, Y. JIN, G. WEI, G. WANG, and L. WANG. "Microwave-assisted Solvothermal Synthesis of YF3:Yb3+, Tm3+ Nanobundles." Chemical Research in Chinese Universities 23, no. 6 (November 2007): 733–35. http://dx.doi.org/10.1016/s1005-9040(07)60159-7.

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10

Guo, Zhanjun, and Zhiliang Chen. "Microwave-assisted solvothermal synthesis and performances of LiMn0.7Fe0.3PO4 nanoplates." Materials and Manufacturing Processes 33, no. 8 (August 30, 2017): 813–16. http://dx.doi.org/10.1080/10426914.2017.1364754.

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11

Lee, Jong-Min, DineshP Amalnerkar, Young Kyu Hwang, Sung Hwa Jhung, Jin-Soo Hwang, and Jong-San Chang. "Microwave Assisted Semi-Solvothermal Synthesis of Nanocrystalline Barium Titanate." Journal of Nanoscience and Nanotechnology 7, no. 3 (March 1, 2007): 952–59. http://dx.doi.org/10.1166/jnn.2007.403.

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12

Choi, Ah-Young, Soo-Wohn Lee, and V. Rodríguez-González. "Microwave-assisted solvothermal synthesis of chrysanthemum-like-VO2 architecture." Journal of Sol-Gel Science and Technology 84, no. 1 (August 17, 2017): 35–41. http://dx.doi.org/10.1007/s10971-017-4481-1.

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13

Ludwig, Jennifer, Cyril Marino, Dominik Haering, Christoph Stinner, Dennis Nordlund, Marca M. Doeff, Hubert A. Gasteiger, and Tom Nilges. "Facile, ethylene glycol-promoted microwave-assisted solvothermal synthesis of high-performance LiCoPO4 as a high-voltage cathode material for lithium-ion batteries." RSC Advances 6, no. 86 (2016): 82984–94. http://dx.doi.org/10.1039/c6ra19767a.

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14

Forsyth, Cory, Tyler Taras, Adam Johnson, Jessica Zagari, Crystal Collado, Markus M. Hoffmann, and Carly R. Reed. "Microwave Assisted Surfactant-Thermal Synthesis of Metal-Organic Framework Materials." Applied Sciences 10, no. 13 (June 30, 2020): 4563. http://dx.doi.org/10.3390/app10134563.

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This research explores the application of surfactants as green solvents for the rapid microwave synthesis of metal-organic framework (MOF) materials. Lead, copper, and iron metal-organic framework materials were synthesized using surfactant-thermal microwave synthesis. The MOF materials were characterized by powder X-ray diffraction, infrared spectroscopy, scanning electron microscopy, and thermogravimetric analysis. With the exception of the iron MOF, which was expected to be amorphous, the MOF materials are crystalline, though generally exhibiting smaller crystals than those achieved with traditional solvothermal synthesis. This green synthetic method reduced synthesis time and reduced the use of traditional organic solvents as the reaction media.
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15

Pham, Hau Quoc, Tai Thien Huynh, At Van Nguyen, Anh Tram Ngoc Mai, Vi Thuy Thi Phan, Long Giang Bach, Nguyen Duy Trinh, and Van Thi Thanh Ho. "Comparison the Rapid Microwave-Assisted Polyol Route and Modified Chemical Reduction Methods to Synthesize the Pt Nanoparticles on the Ti0.7W0.3O2 Support." Solid State Phenomena 279 (August 2018): 181–86. http://dx.doi.org/10.4028/www.scientific.net/ssp.279.181.

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The tungsten-modified titanium dioxide, which prepared through the one-pot solvothermal process, exhibited the large specific surface area (~ 202 m2/g) and greater electrical conductivity (~ 0.022 S/cm). Furthermore, for the comparison purpose to find appropriate approach for the synthesis 20 wt. % Pt NPs/Ti0.7W0.3O2 catalyst, the modified chemical reduction utilizing NaBH4 and the rapid microwave-assisted polyol using ethylene glycol were employed without any surfactants or stabilizers. The characterization of Pt-based electrocatalyst was investigated through XRD, SEM-EDX, TEM measurements. As result, the platinum nanocatalyst formation with the face-centered cubic structure (fcc) and the amount loading on Ti0.7W0.3O2 support approximately 20 wt. % of two synthesized methods. However, the diameter size and distribution of Pt nanoforms have clearly classified in two reduction route. For example, the Pt nanocatalyst, which was created by the rapid microwave-assisted polyol at 160 °C for 2 min, exhibited the good distribution on support with ~3 nm diameter. This could be ascribed to the fast and uniform heating of microwave-assisted and moderate reducing possibility of ethylene glycol. These results indicate that the rapid microwave-assisted polyol was an appropriate approach not only for synthesizing 20 wt. % Pt NPs/Ti0.7W0.3O2 catalyst but also for preparing Pt-based electrocatalysts.
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16

Lee, Young Bum, Seong K. Kim, Seulgi Ji, Wooseok Song, Hee-Suk Chung, Moon Kang Choi, Minbaek Lee, et al. "Facile microwave assisted synthesis of vastly edge exposed 1T/2H-MoS2 with enhanced activity for hydrogen evolution catalysis." Journal of Materials Chemistry A 7, no. 8 (2019): 3563–69. http://dx.doi.org/10.1039/c8ta12080c.

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One-step microwave-assisted solvothermal synthesis of a 1T–2H MoS2 heterostructure with excellent stability and electrocatalytic performance of 1T-MoS2 as a hydrogen evolution catalyst.
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17

You, Bo, Nan Jiang, Meili Sheng, and Yujie Sun. "Microwave vs. solvothermal synthesis of hollow cobalt sulfide nanoprisms for electrocatalytic hydrogen evolution and supercapacitors." Chemical Communications 51, no. 20 (2015): 4252–55. http://dx.doi.org/10.1039/c4cc09849h.

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Hollow cobalt sulfide nanoprisms obtained by a two-step, microwave-assisted synthesis within 15 min exhibit higher hydrogen evolution catalytic activity and better specific capacitance than its counterpart prepared by a traditional solvothermal method.
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18

Khai, Tran Van. "SIMPLE SYNTHESIS OF GRAPHENE NANOSHEETS USING A MICROWAVE–ASSISTED METHOD." Vietnam Journal of Science and Technology 55, no. 1B (March 23, 2018): 30. http://dx.doi.org/10.15625/2525-2518/55/1b/12088.

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In this research, few–layer–graphene (FLG) sheets had been successfully fabricated by using a microwave–assisted method. First, graphite intercalation compounds were prepared from potassium–tetrahydrofuran (K–THF) –expanded graphite by solvothermal process, and then the exfoliation was assisted by microwave radiation and sonication process. The resulted nano–graphene has average thickness about ~ 2 nm with a lateral size of 3–7 μm. Raman analysis showed that the as–synthesized graphene nanosheets contain only a few numbers of structural defects or impurities. X–ray photoelectron spectroscopy and Fourier transform infrared spectroscopy spectra revealed that the nano–graphene consisted of several peaks similar to those of graphite, indicating the effectiveness of the solvothermal reduction method in lowering the oxygen level. The electrical conductivity of the as–synthesized nano–graphene was measured to be 170 S/m. In contrast to the Hummer method, the method is simple, inexpensive, and does not generate toxic gas. This simple method could provide the synthesis of high quality nano–graphene on a large scale.
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19

Koyyada, Ganesh, Nadavala Siva Kumar, Ibrahim H. Al. Ghurabi, Mourad Boumaza, Jae Hong Kim, and Koduru Mallikarjuna. "In situ microwave-assisted solvothermal synthesis via morphological transformation of ZnCo2O4 3D nanoflowers and nanopetals to 1D nanowires for hybrid supercapacitors." RSC Advances 11, no. 11 (2021): 5928–37. http://dx.doi.org/10.1039/d0ra09507a.

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20

Tsai, Teh-Hua, and Chia-Ting Lin. "Rapid Preparation of WO3 Nanorods Via Microwave-Assisted Solvothermal Synthesis." Synthesis and Reactivity in Inorganic, Metal-Organic, and Nano-Metal Chemistry 45, no. 11 (June 9, 2015): 1655–59. http://dx.doi.org/10.1080/15533174.2015.1030291.

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21

Duarte, T. M., L. M. C. Honorio, A. S. Brito, J. K. D. Souza, E. Longo, R. L. Tranquilin, A. G. Souza, I. M. G. Santos, and A. S. Maia. "Synthesis of potassium niobates by the microwave-assisted solvothermal method." IOP Conference Series: Materials Science and Engineering 97 (November 11, 2015): 012001. http://dx.doi.org/10.1088/1757-899x/97/1/012001.

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22

Lim, Chang Sung. "Microwave-Assisted Solvothermal Synthesis and Characterization of Barium Orthovanadate Nanoparticles." Asian Journal of Chemistry 25, no. 5 (2013): 2395–98. http://dx.doi.org/10.14233/ajchem.2013.cslima.

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23

Lee, Ji Sun, I. Suryanarayana, Hye-Young Lee, Young Kyu Hwang, and Jong-San Chang. "Microwave-Assisted Solvothermal Synthesis of CuInSe2 Chalcopyrites." Journal of Nanoscience and Nanotechnology 10, no. 1 (January 1, 2010): 303–8. http://dx.doi.org/10.1166/jnn.2010.1497.

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24

Ramanujam, Prabhu, Bala Vaidhyanathan, Jon Binner, Shaghayegh Ghanizadeh, Zhaoxia Zhou, and Chris Spacie. "Rapid synthesis of nanocrystalline YAG via microwave-assisted solvothermal process." Journal of the American Ceramic Society 101, no. 11 (June 21, 2018): 4864–69. http://dx.doi.org/10.1111/jace.15815.

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25

Lee, Chen-Tao, Fu-Shan Chen, and Chung-Hsin Lu. "Microwave-assisted solvothermal synthesis and characterization of SnO2:Eu3+ phosphors." Journal of Alloys and Compounds 490, no. 1-2 (February 2010): 407–11. http://dx.doi.org/10.1016/j.jallcom.2009.10.019.

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26

Rizzuti, Antonino, Cristina Leonelli, Maria Michela Dell'Anna, Giuseppe Romanazzi, Matilda Mali, Michelina Catauro, and Piero Mastrorilli. "Microwave‐Assisted Solvothermal Controlled Synthesis of Fe‐Co Composite Material." Macromolecular Symposia 395, no. 1 (February 2021): 2000196. http://dx.doi.org/10.1002/masy.202000196.

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27

Wei, Hao, Shuangzhi Chai, Nantao Hu, Zhi Yang, Liangming Wei, and Lin Wang. "The microwave-assisted solvothermal synthesis of a crystalline two-dimensional covalent organic framework with high CO2 capacity." Chemical Communications 51, no. 61 (2015): 12178–81. http://dx.doi.org/10.1039/c5cc04680g.

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28

Huang, Chengjuan, Shuaishuai Ma, Yuqing Zong, Jiandong Gu, Jinjuan Xue, and Mingxin Wang. "Microwave-assisted synthesis of 3D Bi2MoO6 microspheres with oxygen vacancies for enhanced visible-light photocatalytic activity." Photochemical & Photobiological Sciences 19, no. 12 (2020): 1697–706. http://dx.doi.org/10.1039/d0pp00247j.

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29

Xiao, Feng, Liping Fang, Wentao Li, and Dongsheng Wang. "One-step synthesis of aluminum magnesium oxide nanocomposites for simultaneous removal of arsenic and lead ions in water." RSC Advances 5, no. 11 (2015): 8190–93. http://dx.doi.org/10.1039/c4ra13146k.

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Aluminum magnesium oxide nanocomposites were prepared using a one-step microwave assisted solvothermal method, and showed high adsorption capacities for the removal of both As(v) and Pb(ii) ions in water.
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30

Jing, Xunan, Tianhui Liu, Daquan Wang, Jing Liu, and Lingjie Meng. "Controlled synthesis of water-dispersible and superparamagnetic Fe3O4 nanomaterials by a microwave-assisted solvothermal method: from nanocrystals to nanoclusters." CrystEngComm 19, no. 34 (2017): 5089–99. http://dx.doi.org/10.1039/c7ce01191a.

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Highly tunable Fe3O4 nanocrystals and nanoclusters with water-dispersible and superparamagnetic properties were successfully synthesized by a facile and effective microwave-assisted solvothermal method.
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31

Liu, Xiao Lin, Ying Jie Zhu, Bin Yang, Qian Zhang, and Zhi Feng Li. "CuS Nanotubes:Microwave-Solvothermal Synthesis and Photocatalytic Property." Advanced Materials Research 554-556 (July 2012): 605–9. http://dx.doi.org/10.4028/www.scientific.net/amr.554-556.605.

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Copper sulfide (CuS) nanotubes assembled by nanoparticles were successfully synthesized by reaction thiourea with Cu(OH)2nanowire precursor which was obtained using CuCl2and NaOH as raw materials in the solvent ethylene glycol at 80 °C by a facile microwave-assisted solvothermal method. The forming influencing factors of CuS nanotubes were investigated. One of the advantages of this method is that the preparation of CuS nanotubes can well duplicate the shape of the nanowire precursor, thus the simplicity and low cost can be achieved. The products are characterized by X-ray powder diffraction (XRD) and transmission electron microscopy (TEM). The photocatalytic property of the CuS samples was also investigated.
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32

Li, Dongsheng, and Sridhar Komarneni. "Synthesis of Pt Nanoparticles and Nanorods by Microwave-assisted Solvothermal Technique." Zeitschrift für Naturforschung B 61, no. 12 (December 1, 2006): 1566–72. http://dx.doi.org/10.1515/znb-2006-1214.

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Platinum nanoparticles and nanorods were synthesized by microwave-assisted solvothermal techniques. Changing the reaction conditions controlled particle size and morphology. The effects of the reaction conditions, such as the molar ratio of the polyvinylpyrrolidone (PVP) repeating unit to the metal sources, the concentration of metal sources, the reaction temperature, and the presence of distilled water were investigated. Nanoparticles of Pt were approximately 3 nm in size. Produced nanoparticles and nanorods were characterized by transmission electron microscopy. Image JTM software was used to calculate the particle size and size distribution.
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33

Harrison, Katharine L., and Arumugam Manthiram. "Microwave-Assisted Solvothermal Synthesis and Characterization of Various Polymorphs of LiVOPO4." Chemistry of Materials 25, no. 9 (April 2, 2013): 1751–60. http://dx.doi.org/10.1021/cm400227j.

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34

Wang, Xiao-Feng, Yue-Biao Zhang, Hong Huang, Jie-Peng Zhang, and Xiao-Ming Chen. "Microwave-Assisted Solvothermal Synthesis of a Dynamic Porous Metal-Carboxylate Framework." Crystal Growth & Design 8, no. 12 (December 3, 2008): 4559–63. http://dx.doi.org/10.1021/cg800623v.

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35

Patro, Bharati, S. Vijaylakshmi, Raj Kumar Reddy, and Pratibha Sharma. "Microwave-assisted solvothermal synthesis of Cu2ZnSnS4 (CZTS) nanocrystals for photovoltaic applications." Materials Today: Proceedings 3, no. 8 (2016): 2786–94. http://dx.doi.org/10.1016/j.matpr.2016.06.028.

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36

Al-Hazmi, F. S., Ghada H. Al-Harbi, Gary W. Beall, A. A. Al-Ghamdi, A. Y. Obaid, and Waleed E. Mahmoud. "One pot synthesis of graphene based on microwave assisted solvothermal technique." Synthetic Metals 200 (February 2015): 54–57. http://dx.doi.org/10.1016/j.synthmet.2014.12.028.

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37

Ni, Zheng, and Richard I. Masel. "Rapid Production of Metal−Organic Frameworks via Microwave-Assisted Solvothermal Synthesis." Journal of the American Chemical Society 128, no. 38 (September 2006): 12394–95. http://dx.doi.org/10.1021/ja0635231.

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38

Atuchin, Victor, Lei Zhu, Soo Hyun Lee, Dae Hyun Kim, and Chang Sung Lim. "Microwave-Assisted Solvothermal Synthesis of Sr3V2O8 Nanoparticles and Their Spectroscopic Properties." Asian Journal of Chemistry 26, no. 5 (2014): 1290–92. http://dx.doi.org/10.14233/ajchem.2014.17211.

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39

Long, Fei, Shuyi Mo, Yan Zeng, Shangsen Chi, and Zhengguang Zou. "Synthesis of Flower-Like Cu2ZnSnS4Nanoflakes via a Microwave-Assisted Solvothermal Route." International Journal of Photoenergy 2014 (2014): 1–4. http://dx.doi.org/10.1155/2014/618789.

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Flower-like Cu2ZnSnS4(CZTS) nanoflakes were synthesized by a facile and fast one-pot solution reaction using copper(II) acetate monohydrate, zinc acetate dihydrate, tin(IV) chloride pentahydrate, and thiourea as starting materials. The as-synthesized samples were characterized by X-ray diffraction (XRD), Raman scattering analysis, field emission scanning electron microscopy (FESEM) equipped with an energy dispersion X-ray spectrometer (EDS), transmission electron microscopy (TEM), and UV-Vis absorption spectra. The XRD patterns shown that the as-synthesized particles were kesterite CZTS and Raman scattering analysis and EDS confirmed that kesterite CZTS was the only phase of product. The results of FESEM and TEM show that the as-synthesized particles were flower-like morphology with the average size of 1~2 μm which are composed of 50 nm thick nanoflakes. UV-Vis absorption spectrum revealed CZTS nanoflakes with a direct band gap of 1.52 eV.
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40

Prete, Francesca, Antonino Rizzuti, Leonardo Esposito, Antonella Tucci, and Cristina Leonelli. "Highly Homogeneous Al2O3-ZrO2Nanopowder via Microwave-Assisted Hydro- and SolvoThermal Synthesis." Journal of the American Ceramic Society 94, no. 10 (May 25, 2011): 3587–90. http://dx.doi.org/10.1111/j.1551-2916.2011.04594.x.

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41

Liang, Weibin, and Deanna M. D'Alessandro. "Microwave-assisted solvothermal synthesis of zirconium oxide based metal–organic frameworks." Chemical Communications 49, no. 35 (2013): 3706. http://dx.doi.org/10.1039/c3cc40368h.

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42

Ghanbari, Bahareh, Farid Jamali-Sheini, and Ramin Yousefi. "Microwave-assisted solvothermal synthesis and optoelectronic properties of γ-MnS nanoparticles." Journal of Materials Science: Materials in Electronics 29, no. 13 (May 9, 2018): 10976–85. http://dx.doi.org/10.1007/s10854-018-9179-9.

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43

La Porta, Felipe A., Mateus M. Ferrer, Yuri V. B. de Santana, Cristiane W. Raubach, Valéria M. Longo, Júlio R. Sambrano, Elson Longo, Juan Andrés, Máximo S. Li, and José A. Varela. "Synthesis of wurtzite ZnS nanoparticles using the microwave assisted solvothermal method." Journal of Alloys and Compounds 556 (April 2013): 153–59. http://dx.doi.org/10.1016/j.jallcom.2012.12.081.

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44

Liu, Yanxia, Yanli Ma, Yue Jin, Guiqiang Chen, and Xiao Zhang. "Microwave-assisted solvothermal synthesis of sulfur-doped graphene for electrochemical sensing." Journal of Electroanalytical Chemistry 739 (February 2015): 172–77. http://dx.doi.org/10.1016/j.jelechem.2014.12.025.

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45

Cappelluti, M. Davide, Emina Hadzifejzovic, John S. Foord, and Duncan H. Gregory. "Flash microwave-assisted solvothermal (FMS) synthesis of photoactive anatase sub-microspheres with hierarchical porosity." RSC Advances 10, no. 61 (2020): 37233–45. http://dx.doi.org/10.1039/d0ra05796g.

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46

Su, Chang, Jun Lei Liu, Li Huan Xu, Ling Min Wang, Qi Fei Huang, and Cheng Zhang. "Simple and Rapid Synthesis of LiFePO4/C Composite for Lithium Rechargeable Batteries by Microwave-Solvothermal Method Assisted with Short Time Post-Treatment Process." Applied Mechanics and Materials 236-237 (November 2012): 736–40. http://dx.doi.org/10.4028/www.scientific.net/amm.236-237.736.

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A simple and rapid technique to synthesize LiFePO4 by microwave-solvothermal method assisted a short time post-treatment was described. The crystal structure and the charge-discharge performance of the prepared samples were characterized by X-ray diffraction (XRD), scanning electron microscopy (SEM) and galvanostatic charge-discharge testing. The results indicated that this rapid synthesis technique by microwave-solvothermal method combined short time post-treatment was an effective way to obtain LiFePO4 with a single olivine-type crystal structure and small particle size. The electrochemical research indicated that the resulting LiFePO4/C composite could deliver 141.7mAh•g-1 at 0.1C at 25 °C and showed good stability retaining 97% after 45 cycles.
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47

Ashton, Thomas E., David Hevia Borrás, Antonella Iadecola, Kamila M. Wiaderek, Peter J. Chupas, Karena W. Chapman, and Serena A. Corr. "Microwave-assisted synthesis and electrochemical evaluation of VO2 (B) nanostructures." Acta Crystallographica Section B Structural Science, Crystal Engineering and Materials 71, no. 6 (December 1, 2015): 722–26. http://dx.doi.org/10.1107/s2052520615021289.

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Understanding how intercalation materials change during electrochemical operation is paramount to optimizing their behaviour and function and in situ characterization methods allow us to observe these changes without sample destruction. Here we first report the improved intercalation properties of bronze phase vanadium dioxide VO2 (B) prepared by a microwave-assisted route which exhibits a larger electrochemical capacity (232 mAh g−1) compared with VO2 (B) prepared by a solvothermal route (197 mAh g−1). These electrochemical differences have also been followed using in situ X-ray absorption spectroscopy allowing us to follow oxidation state changes as they occur during battery operation.
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48

Kozakova, Z., I. Kuritka, N. E. Kazantseva, V. Babayan, M. Pastorek, M. Machovsky, P. Bazant, and P. Saha. "The formation mechanism of iron oxide nanoparticles within the microwave-assisted solvothermal synthesis and its correlation with the structural and magnetic properties." Dalton Trans. 44, no. 48 (2015): 21099–108. http://dx.doi.org/10.1039/c5dt03518j.

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49

Heilmann, Maria, Hannes Kulla, Carsten Prinz, Ralf Bienert, Uwe Reinholz, Ana Guilherme Buzanich, and Franziska Emmerling. "Advances in Nickel Nanoparticle Synthesis via Oleylamine Route." Nanomaterials 10, no. 4 (April 9, 2020): 713. http://dx.doi.org/10.3390/nano10040713.

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Nickel nanoparticles are an active research area due to their multiple applications as catalysts in different processes. A variety of preparation techniques have been reported for the synthesis of these nanoparticles, including solvothermal, microwave-assisted, and emulsion techniques. The well-studied solvothermal oleylamine synthesis route comes with the drawback of needing standard air-free techniques and often space-consuming glassware. Here, we present a facile and straightforward synthesis method for size-controlled highly monodisperse nickel nanoparticles avoiding the use of, e.g., Schlenk techniques and space-consuming labware. The nanoparticles produced by this novel synthetic route were investigated using small-angle X-ray scattering, transmission electron microscopy, X-ray diffraction, and X-ray spectroscopy. The nanoparticles were in a size range of 4–16 nm, show high sphericity, no oxidation, and no agglomeration after synthesis.
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50

Li, Dongsheng, and Sridhar Komarneni. "Nanoparticles of Pd: Synthesis by Microwave-Solvothermal Method and Optical Properties." Journal of Nanoscience and Nanotechnology 8, no. 8 (August 1, 2008): 3930–35. http://dx.doi.org/10.1166/jnn.2008.184.

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Well-dispersed Pd nanoparticles were synthesized by microwave-assisted solvothermal technique using methanol and ethanol. Particle size and morphology were controlled mainly by the reaction temperature. Particle size of Pd nanoparticles was controlled in the range of 2 to 11 nm by manipulating the reaction conditions. The Pd nanoparticles were characterized by transmission electron microscopy for particle size and shape and UV-Vis spectroscopy for optical properties. UV-Vis spectra showed that synthesized Pd nanoparticles stabilized with PVP had absorption bands at around 280 to 290 nm.
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