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Journal articles on the topic 'Molecular self-Assembly of insulating'

Author: Grafiati

Published: 4 June 2021

Last updated: 25 May 2024

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1

Onoda, Mitsuyoshi, Kazuya Tada, and Hiroshi Nakayama. "Conducting Polymer/Insulating Polymer Composite Films Prepared by the Molecular Self-Assembly Process." Japanese Journal of Applied Physics 38, Part 1, No. 6A (June 15, 1999): 3736–41. http://dx.doi.org/10.1143/jjap.38.3736.

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2

Onoda, Mitsuyoshi, Kazuya Tada, and Hiroshi Nakayama. "Preparation of conducting polymer/insulating polymer composite films using molecular self-assembly process." Synthetic Metals 102, no. 1-3 (June 1999): 1253. http://dx.doi.org/10.1016/s0379-6779(98)01454-4.

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3

Kittelmann, Markus, Philipp Rahe, and Angelika Kühnle. "Molecular self-assembly on an insulating surface: interplay between substrate templating and intermolecular interactions." Journal of Physics: Condensed Matter 24, no. 35 (August 16, 2012): 354007. http://dx.doi.org/10.1088/0953-8984/24/35/354007.

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4

Onoda, Mitsuyoshi, Daisuke Fujita, Kenichiro Isaki, and Hiroshi Nakayama. "Preparation and functions of conductive polymer/insulating polymer composite films using molecular self-assembly." Electrical Engineering in Japan 128, no. 1 (July 15, 1999): 1–8. http://dx.doi.org/10.1002/(sici)1520-6416(19990715)128:1<1::aid-eej1>3.0.co;2-j.

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5

Rahe, Philipp, Markus Nimmrich, and Angelika Kühnle. "Substrate Templating upon Self-Assembly of Hydrogen-Bonded Molecular Networks on an Insulating Surface." Small 8, no. 19 (July 6, 2012): 2969–77. http://dx.doi.org/10.1002/smll.201200681.

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6

Onoda, Mitsuyoshi, Daisuke Fujita, Kenichiro Isaki, and Hiroshi Nakayama. "Preparation of Conducting Polymer/Insulating Polymer Composite Films Using Molecular Self-Assembly Process and Its Function." IEEJ Transactions on Fundamentals and Materials 117, no. 12 (1997): 1227–32. http://dx.doi.org/10.1541/ieejfms1990.117.12_1227.

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7

Rahe, Philipp, Markus Nimmrich, and Angelika Kühnle. "Templating: Substrate Templating upon Self-Assembly of Hydrogen-Bonded Molecular Networks on an Insulating Surface (Small 19/2012)." Small 8, no. 19 (October 2, 2012): 2968. http://dx.doi.org/10.1002/smll.201290103.

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8

Hauke, Christopher M., Ralf Bechstein, Markus Kittelmann, Christof Storz, Andreas F. M. Kilbinger, Philipp Rahe, and Angelika Kühnle. "Controlling Molecular Self-Assembly on an Insulating Surface by Rationally Designing an Efficient Anchor Functionality That Maintains Structural Flexibility." ACS Nano 7, no. 6 (May 15, 2013): 5491–98. http://dx.doi.org/10.1021/nn401589u.

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9

Wang, Youyuan, Yudong Li, Zhanxi Zhang, Haisen Zhao, and Yanfang Zhang. "Repair Performance of Self-Healing Microcapsule/Epoxy Resin Insulating Composite to Physical Damage." Applied Sciences 9, no. 19 (October 1, 2019): 4098. http://dx.doi.org/10.3390/app9194098.

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Minor physical damage can reduce the insulation performance of epoxy resin, which seriously threatens the reliability of electrical equipment. In this paper, the epoxy resin insulating composite was prepared by a microcapsule system to achieve its self-healing goal. The repair performance to physical damage was analyzed by the tests of scratch, cross-section damage, electric tree, and breakdown strength. The results show that compared with pure epoxy resin, the composite has the obvious self-healing performance. For mechanical damage, the maximum repair rate of physical structure is 100%, and the breakdown strength can be restored to 83% of the original state. For electrical damage, microcapsule can not only attract the electrical tree and inhibit its propagation process, but also repair the tubules of electrical tree effectively. Moreover, the repair rate is fast, which meets the application requirements of epoxy resin insulating material. In addition, the repair behavior is dominated by capillarity and molecular diffusion on the defect surface. Furthermore, the electrical properties of repaired part are greatly affected by the characteristics of damage interface and repair product. In a word, the composite shows better repair performance to physical damage, which is conducive to improving the reliability of electrical insulating materials.

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10

Baker, MV, and J. Landau. "Self Assembled Alkanethiolate Monolayers as Thin Insulating Films." Australian Journal of Chemistry 48, no. 6 (1995): 1201. http://dx.doi.org/10.1071/ch9951201.

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Simple devices that contain alkanethiolate monolayers sandwiched between conducting films were prepared by fixing a gold film to the surface of an alkanethiolate monolayer (on a gold substrate) with silver paint. These devices, and similar devices that did not contain alkanethiolate monolayers, were tested as resistors in d.c . circuits. The devices that contained octadecanethiolate monolayers had resistances of approximately 1012 Ω, 10 orders of magnitude higher than the resistance of devices that contained no monolayers. Sulfur- terminated alkanethiolate monolayers were prepared by treatment of carboxylic acid-terminated monolayers with vapours of thionyl chloride followed by vapours of hexane-1,6-dithiol. Attempts to use the sulfur-containing groups at the surface of this monolayer as 'molecular glue' to attach a flexible gold film to the surface of the monolayer were unsuccessful.

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11

Bayrak, Türkan, Nagesh Jagtap, and Artur Erbe. "Review of the Electrical Characterization of Metallic Nanowires on DNA Templates." International Journal of Molecular Sciences 19, no. 10 (October 3, 2018): 3019. http://dx.doi.org/10.3390/ijms19103019.

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The use of self-assembly techniques may open new possibilities in scaling down electronic circuits to their ultimate limits. Deoxyribonucleic acid (DNA) nanotechnology has already demonstrated that it can provide valuable tools for the creation of nanostructures of arbitrary shape, therefore presenting an ideal platform for the development of nanoelectronic circuits. So far, however, the electronic properties of DNA nanostructures are mostly insulating, thus limiting the use of the nanostructures in electronic circuits. Therefore, methods have been investigated that use the DNA nanostructures as templates for the deposition of electrically conducting materials along the DNA strands. The most simple such structure is given by metallic nanowires formed by deposition of metals along the DNA nanostructures. Here, we review the fabrication and the characterization of the electronic properties of nanowires, which were created using these methods.

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12

Dionne, Eric R., Fadwa Ben Amara, and Antonella Badia. "An electrochemical immittance analysis of the dielectric properties of self-assembled monolayers." Canadian Journal of Chemistry 98, no. 9 (September 2020): 471–79. http://dx.doi.org/10.1139/cjc-2020-0005.

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The ability of organic self-assembled monolayers (SAMs) to act as insulating barriers to electron transfer, ion transport, or molecular diffusion is critical to their application in a variety of technologies. The use of appropriate analytical tools to characterize the dielectric properties of these molecular thin films is important for the control of structural defects and establishing structure–property relations. In this context, we analyze the ionic permeability and dielectric response of SAMs formed from a homologous series of n-alkanethiolates (CH3(CH2)nS, where n = 9, 11, 13, 15, 17, and 19) on gold using the immittance quantities of the complex impedance, capacitance, and permittivity available from the same electrochemical impedance spectroscopy (EIS) measurement. The most sensitive parameters and frequency range for characterizing the capacitive behavior and assessing the ion-blocking quality of the SAMs under non-Faradaic conditions are identified. We also investigate the effect of chain length on the interfacial capacitance and dielectric constant of ionic insulating SAMs. The advantages of the capacitance quantity and related permittivity data over traditional impedance representations and equivalent electric circuit modeling are discussed.

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13

Makarova, Marina V., Yuji Okawa, Elisseos Verveniotis, Kenji Watanabe, Takashi Taniguchi, Christian Joachim, and Masakazu Aono. "Self-assembled diacetylene molecular wire polymerization on an insulating hexagonal boron nitride (0001) surface." Nanotechnology 27, no. 39 (August 30, 2016): 395303. http://dx.doi.org/10.1088/0957-4484/27/39/395303.

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14

Rahe, Philipp, Markus Nimmrich, Andreas Greuling, Jens Schütte, Irena G. Stará, Jiří Rybáček, Gloria Huerta-Angeles, Ivo Starý, Michael Rohlfing, and Angelika Kühnle. "Toward Molecular Nanowires Self-Assembled on an Insulating Substrate: Heptahelicene-2-carboxylic acid on Calcite (101̅4)." Journal of Physical Chemistry C 114, no. 3 (December 28, 2009): 1547–52. http://dx.doi.org/10.1021/jp911287p.

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15

Marischal, Louis, Aurélie Cayla, Guillaume Lemort, Valentin Laurent, Christine Campagne, and Éric Devaux. "Heating filament with Self-Regulation Temperature by Coating a Metallic Yarn with a Conductive Polymer Composite." Solid State Phenomena 333 (June 10, 2022): 69–79. http://dx.doi.org/10.4028/p-6e06b7.

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Nowadays, the heating textiles are used in many fields of applications as medicine or comfort. The heating property for the most part of these textiles was ensured by electrical conductive fiber as metallic yarn thanks to Joule Effect. A challenge for heating textile is to have an electrical conductive fiber which has a temperature self-regulation at the comfort temperature. Thanks to this temperature self-regulation, the heating textile reaches more autonomy. To develop this kind of textile, conductive polymer composite (CPC), which is the combination between an insulating polymer and electrical conductivity nanofillers [1], is made by melt spinning. The temperature self-regulation is provided by the positive temperature coefficient (PTC) effect, which allows switching between an electrical conductivity state and an insulating state when the CPC is close to a transition phase temperature (glass transition temperature or melt temperature). However, when the PTC effect can take place at the melting point, the mechanical properties are not involved. So to maintain the final product an immiscible polymer blend was used: one polymer was the CPC and the second polymer was an insulating polymer with a higher melting point than the target temperature. In fact, the CPC involve the electrical conductivity and the PTC effect, whereas the insulating polymer involves the mechanical properties. However, a high electrical conductivity is necessary to reach the comfort temperature (defined around 42°) by Joule Effect. So to reach this temperature, the coating on a metallic yarn by the conductive immiscible polymer blend was used. The electrical conductivity of this product was improved by the metallic yarn and the self-regulating temperature by the PTC effect of the immiscible polymer blend (figure 1). In this paper the immiscible polymer blend used is a polycaprolactone (PCL) filled with multiwall carbon nanotubes (MWCNT) and a polypropylene (PP). In fact, in a previous paper the co-continuity and the selective localisation of the fillers in the PCL for this blend was studied [2]. The influence of the thickness CPC coating and the influence of the structure of metallic yarn were studied on the electrical conductivity, the Joule Effect and PTC effect.

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16

Citron, A., W. Kühn, A. Rogner, W. Schimassek, and O. Stoltz. "Investigation of a self-magnetically insulated Bθ-diode." Laser and Particle Beams 5, no. 4 (November 1987): 565–72. http://dx.doi.org/10.1017/s0263034600003116.

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An ion diode, where the insulating magnetic Bθ-field is produced by the diode current itself, has been investigated. Using a novel Thomson-parabola spectrometer that is capable of detecting up to 41 beam traces at a single shot and a carbon activation diagnostic the ion beam has been analyzed. The diode, operating at “KALIF”, delivers ion beams of 750 kA at energies of about 0·7 MeV. The focusing version of the diode shows a focus size of 1 cm2, the beam is neutralized to 98–99%, the proton content is about 60%.

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17

Gaberle, Julian, David Z. Gao, Alexander L. Shluger, Ania Amrous, Franck Bocquet, Laurent Nony, Franck Para, Christian Loppacher, Simon Lamare, and Fréderic Cherioux. "Morphology and Growth Mechanisms of Self-Assembled Films on Insulating Substrates: Role of Molecular Flexibility and Entropy." Journal of Physical Chemistry C 121, no. 8 (February 20, 2017): 4393–403. http://dx.doi.org/10.1021/acs.jpcc.6b12738.

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18

Bhushan, Bharat. "Biomimetics: lessons from nature–an overview." Philosophical Transactions of the Royal Society A: Mathematical, Physical and Engineering Sciences 367, no. 1893 (April 28, 2009): 1445–86. http://dx.doi.org/10.1098/rsta.2009.0011.

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Nature has developed materials, objects and processes that function from the macroscale to the nanoscale. These have gone through evolution over 3.8 Gyr. The emerging field of biomimetics allows one to mimic biology or nature to develop nanomaterials, nanodevices and processes. Properties of biological materials and surfaces result from a complex interplay between surface morphology and physical and chemical properties. Hierarchical structures with dimensions of features ranging from the macroscale to the nanoscale are extremely common in nature to provide properties of interest. Molecular-scale devices, superhydrophobicity, self-cleaning, drag reduction in fluid flow, energy conversion and conservation, high adhesion, reversible adhesion, aerodynamic lift, materials and fibres with high mechanical strength, biological self-assembly, antireflection, structural coloration, thermal insulation, self-healing and sensory-aid mechanisms are some of the examples found in nature that are of commercial interest. This paper provides a broad overview of the various objects and processes of interest found in nature and applications under development or available in the marketplace.

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19

Shi, Haiyang, Weigen Chen, Fu Wan, Lingling Du, Shuhua Zhang, Weiran Zhou, Jiayi Zhang, Yingzhou Huang, and Chengzhi Zhu. "Application of Self-Assembled Raman Spectrum-Enhanced Substrate in Detection of Dissolved Furfural in Insulating Oil." Nanomaterials 9, no. 1 (December 23, 2018): 17. http://dx.doi.org/10.3390/nano9010017.

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Accurate detection of dissolved aging features in transformer oil is the key to judging the aging degree of oil-paper insulation. In this work, in order to realize in situ detection of furfural dissolved in transformer oil, silver nanoparticles were self-assembled on the surface of gold film with P-aminophenylthiophenol (PATP) as a coupling agent. Rhodamine-6G (R6G) was used as the probe molecule to test the enhancement effect. By optimizing the molecular concentration, molecular deposition time, and silver sol deposition time of PATP, the nanoparticles were made more uniform and compact, and an enhanced substrate with rich hot spots was obtained. The optimum substrate was developed, and surface-enhanced Raman spectroscopy (SERS) detection of trace furfural dissolved in transformer oil was realized. The results showed that the substrate prepared under the conditions of 0.1 mol/L PATP, 5 h deposition in PATP and 12 h immersion in silver sol, had the best reinforcement effect (that is, uniform and compact particle arrangement and no particle clusters). By use of this substrate, the minimum detectable concentration of furfural in transformer oil was about 1.06 mg/L, which provides a new method for fast and nondestructive detection of transformer aging diagnosis.

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20

Guo, Hao Min, Xin Hua Li, Zhi Fei Zhao, and Yu Qi Wang. "Tunable Ferromagnetism above Room-Temperature in Self-Assembled (In,Mn)As Diluted Magnetic Semiconductor Quantum Dots on Be-Doped Al_xGa_1-XAs Template by Molecular Beam Epitaxy." Advanced Materials Research 476-478 (February 2012): 793–98. http://dx.doi.org/10.4028/www.scientific.net/amr.476-478.793.

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With the introduction of Be-doped AlxGa1-xAs template, self-assembled In0.79Mn0.21As quantum dots samples were prepared on semi-insulating (001) GaAs substrates by molecular beam epitaxy. High quantum dots density was confirmed by the atomic force microscopy. The ferromagnetism of the samples was revealed by superconducting quantum interference device magnetometer analysis at 10K, and the Curie temperatures ranging from 292 to 314K were able to be regulated by adjusting Al content and Be dopant in Be-doped AlxGa1-xAs templates, implying the feasible application of spintronic devices.

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21

Aleknavičienė, Indrė, Martynas Talaikis, Rima Budvytyte, and Gintaras Valincius. "The Impact of an Anchoring Layer on the Formation of Tethered Bilayer Lipid Membranes on Silver Substrates." Molecules 26, no. 22 (November 15, 2021): 6878. http://dx.doi.org/10.3390/molecules26226878.

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Tethered bilayer lipid membranes (tBLMs) have been known as stable and versatile experimental platforms for protein–membrane interaction studies. In this work, the assembly of functional tBLMs on silver substrates and the effect of the molecular chain-length of backfiller molecules on their properties were investigated. The following backfillers 3-mercapto-1-propanol (3M1P), 4-mercapto-1-butanol (4M1B), 6-mercapto-1-hexanol (6M1H), and 9-mercapto-1-nonanol (9M1N) mixed with the molecular anchor WC14 (20-tetradecyloxy-3,6,9,12,15,18,22 heptaoxahexatricontane-1-thiol) were used to form self-assembled monolayers (SAMs) on silver, which influenced a fusion of multilamellar vesicles and the formation of tBLMs. Spectroscopic analysis by SERS and RAIRS has shown that by using different-length backfiller molecules, it is possible to control WC14 anchor molecules orientation on the surface. An introduction of increasingly longer surface backfillers in the mixed SAM may be related to the increasing SAMs molecular order and more vertical orientation of WC14 at both the hydrophilic ethylenoxide segment and the hydrophobic lipid bilayer anchoring alkane chains. Since no clustering of WC14 alkane chains, which is deleterious for tBLM integrity, was observed on dry samples, the suitability of mixed-component SAMs for subsequent tBLM formation was further interrogated by electrochemical impedance spectroscopy (EIS). EIS showed the arrangement of well-insulating tBLMs if 3M1P was used as a backfiller. An increase in the length of the backfiller led to increased defectiveness of tBLMs. Despite variable defectiveness, all tBLMs responded to the pore-forming cholesterol-dependent cytolysin, vaginolysin in a manner consistent with the functional reconstitution of the toxin into phospholipid bilayer. This experiment demonstrates the biological relevance of tBLMs assembled on silver surfaces and indicates their utility as biosensing elements for the detection of pore-forming toxins in liquid samples.

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22

Zhou, W. L., J. Wiemann, K. L. Stokes, and C. J. O’Connor. "Monodisperse Pbse Nanoparticle Self-Assembling Nanoarrays Before and After Annealing." Microscopy and Microanalysis 7, S2 (August 2001): 314–15. http://dx.doi.org/10.1017/s1431927600027641.

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A variety of semiconductor and metal nanoparticles can be synthesized and tunable in size from about 10 to 200 Å using size-selective separation technique. Preparation of monodisperse samples enables systematic characterization of the structural, electron, and optical properties of materials as they evolve from molecular to bulk in the nanometer size range. Sample uniformity makes it possible to manipulate nanocrystals into close-packed, glassy and ordered nanocrystal. At inter-particle separations 5-100 Å, dipole-dipole interactions lead to energy transfer between neighboring nanocrystals, and electronic tunneling between proximal nanocrystals gives rise to dark and photoconductivity. The fabrication of monodisperse ordered nanoarrays with the inter-particle separations less than 5Å will be very important to study its physical properties since interaction between neighboring nanocrystals cause otherwise insulating assemblies to become semiconducting, metallic, or superconducting depending on nanocrystals composition. Here we present the fabrication of monodisperse PbSe nanoarrays with inter-particle distance less than 5 Å and its nanostructure study.

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23

Mirjani, Fatemeh, Joseph M. Thijssen, George M. Whitesides, and Mark A. Ratner. "Charge Transport Across Insulating Self-Assembled Monolayers: Non-equilibrium Approaches and Modeling To Relate Current and Molecular Structure." ACS Nano 8, no. 12 (November 25, 2014): 12428–36. http://dx.doi.org/10.1021/nn505115a.

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24

Vettraino, M., B. Ye, X. He, and D. M. Antonelli. "ChemInform Abstract: Self-assembled Molecular Nanowires in Mesoporous Transition Metal Oxide Hosts: Conducting Peas in an Insulating Pod." ChemInform 32, no. 42 (May 24, 2010): no. http://dx.doi.org/10.1002/chin.200142258.

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25

Liang, Songmiao, Jian Xu, Lihui Weng, Lina Zhang, Xinglin Guo, and Xiaoli Zhang. "Long-Range Self-Governing Motion of Polymer Gel on a Gradiently Charged Insulating Substrate." ChemPhysChem 8, no. 6 (April 23, 2007): 899–905. http://dx.doi.org/10.1002/cphc.200600745.

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26

Lee, Kyunam, Dong Joo Min, Jong-Jin Park, Soo Young Park, and Ji Eon Kwon. "Molecular Designs to Achieve High-Rate and Ultra-Stable Organic Electrode Materials for Future Sustainable Batteries." ECS Meeting Abstracts MA2022-02, no. 1 (October 9, 2022): 2. http://dx.doi.org/10.1149/ma2022-0212mtgabs.

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Organic electrode materials (OEMs) are recently drawing much attention as a promising alternative to conventional transition metal oxide electrodes due to their many advantages, including abundance, sustainability, bio-compatibility, low cost, and easy tunability.[1] Most importantly, the flexible nature of organic materials due to loosely packed intermolecular structures allows fast diffusion for charge-carrying ions, which is essential for the high-rate performance of electrode materials. However, in practice, most OEMs still suffer from slow rate capability and low capacity utilization due to their electrically insulating nature. In a typical battery, the rate capability of an electrode is determined by the kinetic factors for the following three steps during the charge/discharge processes: i) redox reaction of active materials, ii) electron conduction through the active materials and the conductive carbon additives to the current collector, iii) and ion diffusion inside the active materials.[2] Previously, most studies have focused on improving the electrical conductivity of OEMs to achieve high-rate capability; however, such attempts typically sacrificed their specific capacity and/or cycle stability. Here, we present novel molecular design strategies to achieve high-rate capability of OEMs without deterioration of their specific capacity and cycle stability. First, we recently proposed that a small structural reorganization of the redox center during the redox reaction would be a key to achieving fast rate capability in OEMs for the first time.[3] We revealed that a novel p-type redox center phenoxazine (PXZ) had faster redox kinetics than its widely used analogue phenothiazine (PTZ) due to negligibly smaller structural changes, which was evidenced by theoretical calculations using the density functional theory (DFT) method and experimental measurements. In practical coin-cells, such low reorganization of the PXZ center led to high-rate performance (73% capacity retention at 20C) of a PXZ trimer electrode material (3PXZ) with a narrow voltage plateau at 3.7 V vs. Li/Li+. Then, in this presentation, we introduce our new OEMs bearing n-type redox centers with low reorganization energy, including tetrazine (Tz)[4-6] and thieno-isoindigo (TIIG).[7] The new OEMs showed superior rate capability (> 50% capacity retention at 50C) and high cycle stability (> 80% capacity retention after 500 cycles). Finally, we present novel OEMs spontaneously forming various nanostructures via self-assembly after fabricating electrodes.[8] The high surface area of the nanostructured OEMs provided fast electron transfer from the insulating active materials to the conductive carbons and easy access of the charge-carrying ions to the active materials, leading to ultrafast rate performance (> 50% capacity retention at 100C) even with high active content more than 70 wt% in the electrode. References [1] P. Poizot et al., Chem. Rev. 2020, 120, 6490. [2] Y. Tang et al., Chem. Soc. Rev. 2015, 44, 5926. [3] K. Lee et al., Energy Environ. Sci. 2020, 13, 4142. [4] D. J. Min et al. ChemSusChem 2019, 12, 503. [5] D. J. Min et al. Molecules 2021, 26, 894. [6] D. J. Min et al. manuscript in preparation. [7] J.-J. Park et al. manuscript in preparation. [8] K. Lee et al. manuscript in preparation.

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27

Kwon, Min Hee, Dong Kyu Han, Si Joong Kwon, and Jin Yeol Kim. "Fabrication and Micropatterning of Conducting Polymer Nano-Films for Electronic Displays." Solid State Phenomena 124-126 (June 2007): 591–94. http://dx.doi.org/10.4028/www.scientific.net/ssp.124-126.591.

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We investigate the electrical conductive poly(3,4-ethylenedioxythiophene) (PEDOT) nanofilms and micropatterning prepared by vapor-phase polymerization method using self-assembling teacnique. The thin conductive films were uniformly fabricated between 20 and 100 nm, there surface resistance wasenhanced until to 102 /square, and the light-transmittance were also increased as up to 95 %. We report a fabrication of electrically conducting PEDOT pattern on a electrically insulating substrate using a microcontact printing method. Then, patterns are successfully obtained with line widths down to 3 .

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28

Ahmed, I., S. De Gendt, and C. Merckling. "Self-regulating plasma-assisted growth of epitaxial BaBiO₃ thin-film on SrTiO₃-buffered Si(001) substrate." Journal of Applied Physics 132, no. 22 (December 14, 2022): 225304. http://dx.doi.org/10.1063/5.0101227.

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The BaBiO3 perovskite oxide is an interesting material system because of its superconductivity when p-doped and the predicted topological insulating nature when n-doped. Single crystalline BaBiO3 films are grown by molecular beam epitaxy with high quality utilizing the adsorption-controlled regime, where volatile Bi is supplied in excess in the presence of oxygen radicals. BaBiO3 films are integrated on Si(001) substrates through growth on a SrTiO3(001) buffer layer. Despite the 11.77% lattice mismatch, by systematically varying growth parameters, such as plasma conditions, substrate temperature, and metallic fluxes, a growth window for the BaBiO3 is well-established. Within the optimum growth window, films are stoichiometric and of high crystalline quality based on the different physical characterization techniques. The development of robust layers is facilitated by accessing the self-regulating regime, where only the stoichiometric quantity of Bi sticks during the epitaxy.

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29

Paixao, Pablo A., Flávio S. Michels, Samuel L. Oliveira, Alem-Mar B. Goncalves, Cauê A. Martins, Anderson R. L. Caires, and Diego C. B. Alves. "Miniaturized 3D-Printed Cell Enables Water/Ethanol Quantification Using Electrochemical Impedance Spectroscopy." Sensors 24, no. 1 (December 26, 2023): 131. http://dx.doi.org/10.3390/s24010131.

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A miniaturized and low-cost electrochemical 3D-printed system for rapid and accurate quantification of ethanol content in ethanol fuel using electrochemical impedance spectroscopy (EIS) was developed. The monolithic design of the system incorporates insulating thermoplastic electrode separators, with only the cover being mobile, allowing for easy assembly and handling. The portable device, measuring approximately 26 × 24 mm, has a maximum capacity of 1 mL, making it suitable for lab-on-a-chip and portable analysis. By utilizing the dielectric constant of ethanol and ethanol fuel mixtures with water, the miniaturized EIS cell quantifies ethanol content effectively. To validate its performance, we compared measurements from four gas stations with a digital densimeter, and the values obtained from the proposed system matched perfectly. Our miniaturized and low-cost electrochemical 3D-printed device can be printed and assembled in two hours, offering a cost-effective solution for fast and precise ethanol quantification. Its versatility, affordability, and compatibility with lab-on-a-chip platforms make it easily applicable, including for fuel quality control and on-site analysis in remote locations.

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30

Zhou, Jiahui, Haikun Zheng, Wei Sheng, Xiaoru Hao, and Xinmin Zhang. "Preparation and Anti-Icing Properties of Zirconia Superhydrophobic Coating." Molecules 29, no. 8 (April 18, 2024): 1837. http://dx.doi.org/10.3390/molecules29081837.

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Zirconia (ZrO2) is a ceramic material with high-temperature resistance and good insulating properties. Herein, for the first time, the surface of ZrO2 was modified with docosanoic acid (DCA) to improve its self-cleaning and hydrophobic properties. This surface modification transformed the surface of ZrO2 from hydrophilic to superhydrophobic. A two-step spraying method was used to prepare the superhydrophobic surface of ZrO2 by sequentially applying a primer and a topcoat. The primer was a solution configured using an epoxy resin as the adhesive and polyamide as the curing agent, while the topcoat was a modified ZrO2 solution. The superhydrophobic surface of ZrO2 exhibited a contact angle of 154° and a sliding angle of 4°. Scanning electron microscopy, X-ray diffraction, energy-dispersive X-ray spectroscopy, thermogravimetric analysis, and other analytical techniques were used to characterize the prepared zirconia particles and their surfaces. Moreover, results from surface self-cleaning and droplet freezing tests showed that DCA-modified ZrO2 can be well combined, and its coatings show good self-cleaning and anti-icing properties on TA2 bases.

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31

Shashkin, V. I., and N. V. Vostokov. "Solution of the problem of charge-carrier injection into an insulating layer under self-consistent boundary conditions at contacts." Semiconductors 42, no. 11 (November 2008): 1309–14. http://dx.doi.org/10.1134/s1063782608110122.

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32

Heita Shafudah, Natangue, Hiroki Nagai, Yutaka Suwazono, Ryuhei Ozawa, Yukihiro Kudoh, Taiju Takahashi, Takeyoshi Onuma, and Mitsunobu Sato. "Hydrophilic Titania Thin Films from a Molecular Precursor Film Formed via Electrospray Deposition on a Quartz Glass Substrate Precoated with Carbon Nanotubes." Coatings 10, no. 11 (October 29, 2020): 1050. http://dx.doi.org/10.3390/coatings10111050.

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Titania precursor films were electrosprayed on a quartz glass substrate, which was pre-modified with an ultra-thin film obtained by spin-coating a single-walled carbon nanotube (SWCNT) dispersed solution. The X-ray diffraction patterns of the thin films obtained by heat-treating the precursor films at 500 °C in air for 1 h indicated that the formed crystals were anatase. A new route to fabricate transparent thin films on the insulating substrate via electrospray deposition (ESD) was thus attained. The photoluminescence spectrum of the thin film showed a peak at 2.23 eV, assignable to the self-trapped exciton of anatase. The Raman spectrum of the thin film demonstrated that heat treatment is useful for removing SWCNTs. The thin film showed a water contact angle of 14 ± 2° even after being kept under dark conditions for 1 h, indicating a high level of hydrophilicity. Additionally, the thin film had a super-hydrophilic surface with a water contact angle of 1 ± 1° after ultraviolet light irradiation with an intensity of 4.5 mW cm−2 at 365 nm for 1 h. The importance of Ti3+ ions in the co-present amorphous phase, which was dominantly formed via the ESD process, for hydrophilicity was also clarified by means of X-ray photoelectron spectroscopy.

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Gabriunaite, Inga, Gintaras Valincius, Albinas Žilinskas, and Aušra Valiūnienė. "Tethered Bilayer Membrane Formation on Silanized Fluorine Doped Tin Oxide Surface." Journal of The Electrochemical Society 169, no. 3 (March 1, 2022): 037515. http://dx.doi.org/10.1149/1945-7111/ac5c96.

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Silane compound was synthesized via click chemistry and a mixture of synthesis products without purification was used to form the self-assembled monolayers on metal oxide conducting films of fluorine doped tin oxide (FTO). Silanized FTO surfaces triggered rupture of multilamellar vesicles and formed electrically insulating tethered bilayer membranes (tBLMs). In contrast to well-known hybrid bilayer membranes on silane monolayers such as ones formed from octadecyltrichlorosilane, tBLMs on FTO contained water-ion reservoir between solid surface and phospholipid bilayer sheet. They demonstrated biological relevance and ability to reconstitute the pore-forming protein channels such as α-hemolysin from Staphylococcus aureus and melittin. The addition of cholesterol to tBLMs decreased the membrane-damaging effect of melittin, while the opposite was observed in the case of α-hemolysin. The tBLMs can be regenerated multiple times without losing their functionality. The described methodology (both synthesis and formation of anchor monolayer) can be extended to any oxide film surface by properly adjusting chemical composition of molecular anchor and silanization conditions. This makes the proposed biomimetic membrane system attractive for various applications including biomedical sensors for the detection of pore-forming toxins.

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34

Mahadhy, Ally, Bo Mattiasson, Eva StåhlWernersson, and Martin Hedström. "Evaluation of Polytyramine Film and 6-Mercaptohexanol Self-Assembled Monolayers as the Immobilization Layers for a Capacitive DNA Sensor Chip: A Comparison." Sensors 21, no. 23 (December 6, 2021): 8149. http://dx.doi.org/10.3390/s21238149.

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The performance of a biosensor is associated with the properties of an immobilization layer on a sensor chip. In this study, gold sensor chips were modified with two different immobilization layers, polytyramine film and 6-mercaptohexanol self-assembled monolayer. The physical, electrochemical and analytical properties of polytyramine film and mercaptohexanol self-assembled monolayer modified gold sensor chips were studied and compared. The study was conducted using atomic force microscopy, cyclic voltammetry and a capacitive DNA-sensor system (CapSenze™ Biosystem). The results obtained by atomic force microscopy and cyclic voltammetry indicate that polytyramine film on the sensor chip surface possesses better insulating properties and provides more spaces for the immobilization of the capture probe than a mercaptohexanol self-assembled monolayer. A capacitive DNA sensor hosting a polytyramine single-stranded DNA-modified sensor chip displayed higher sensitivity and larger signal amplitude than that of a mercaptohexanol single-stranded DNA-modified sensor chip. The linearity responses for polytyramine single-stranded DNA- and mercaptohexanol single-stranded DNA-modified sensor chips were obtained at log concentration ranges, equivalent to 10−12 to 10−8 M and 10−10 to 10−8 M, with detection limits of 4.0 × 10−13 M and 7.0 × 10−11 M of target complementary single-stranded DNA, respectively. Mercaptohexanol single-stranded DNA- and polytyramine single-stranded DNA-modified sensor chips exhibited a notable selectivity at an elevated hybridization temperature of 50 °C, albeit the signal amplitudes due to the hybridization of the target complementary single-stranded DNA were reduced by almost 20% and less than 5%, respectively.

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Lee, Juho, Hyeonwoo Yeo, and Yong-Hoon Kim. "Quasi-Fermi level splitting in nanoscale junctions from ab initio." Proceedings of the National Academy of Sciences 117, no. 19 (April 23, 2020): 10142–48. http://dx.doi.org/10.1073/pnas.1921273117.

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The splitting of quasi-Fermi levels (QFLs) represents a key concept utilized to describe finite-bias operations of semiconductor devices, but its atomic-scale characterization remains a significant challenge. Herein, the nonequilibrium QFL or electrochemical potential profiles within single-molecule junctions obtained from the first-principles multispace constrained-search density-functional formalism are presented. Benchmarking the standard nonequilibrium Green’s function calculation results, it is first established that algorithmically the notion of separate electrode-originated nonlocal QFLs should be maintained within the channel region during self-consistent finite-bias electronic structure calculations. For the insulating hexandithiolate junction, the QFL profiles exhibit discontinuities at the left and right electrode interfaces and across the molecule the accompanying electrostatic potential drops linearly and Landauer residual-resistivity dipoles are uniformly distributed. For the conducting hexatrienedithiolate junction, on the other hand, the electrode QFLs penetrate into the channel region and produce split QFLs. With the highest occupied molecular orbital entering the bias window and becoming a good transport channel, the split QFLs are accompanied by the nonlinear electrostatic potential drop and asymmetric Landauer residual-resistivity dipole formation. Our findings underscore the importance of the first-principles extraction of QFLs in nanoscale junctions and point to a future direction for the computational design of next-generation semiconductor devices.

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Zakaria, Nor Farhani, Shahrir Rizal Kasjoo, Muammar Mohamad Isa, Zarimawaty Zailan, Mohd Khairuddin Md Arshad, and Aimin Song. "Improved Rectification Performance and Terahertz Detection in Hybrid Structure of Self-Switching Device (SSD) and Planar Barrier Diode (PBD) Using Two-Dimensional Device Simulation." Solid State Phenomena 301 (March 2020): 111–17. http://dx.doi.org/10.4028/www.scientific.net/ssp.301.111.

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Recently, simulations of In0.48Ga0.52As-based Planar Barrier Diode (PBD) and Self-Switching Device (SSD) as millimeter-wave rectifiers were reported. Both PBD and SSD have a planar structure, but with different insulating shapes and working principles. In this work, a hybrid structure of the reported PBD and SSD in a parallel configuration is proposed, to exploit the advantages of each device. The advantages of high rectifying properties in the SSD and fast switching rate of the PBD are combined in this hybrid structure in order to obtain an improved rectification performance at zero-bias in the near terahertz frequency region. Analysis of the curvature co-efficient, γ, which is defined as the ratio of the second order to the first order derivative of the device’s I-V function was performed to evaluate the rectification performance. AC transient analyses were then executed in various frequencies to imitate the high-frequency signal inputs. By using this hybrid structure, the highest value of γ achieved has been improved to ~19 V-1 at 70 mV, and ~6 V-1 at zero-bias (compared to the previous results on PBDs). The estimated cut-off frequency obtained was ~360 GHz (0.36 THz), operating at zero-bias.

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Wang, Wenlu, Anton B. Resing, Zhaoyi Zheng, Keith A. Brown, and Joerg G. Werner. "Tunable Conformal Electrodeposition of Ultra-Thin Polymeric Films for Electrolyte Interphases." ECS Meeting Abstracts MA2023-01, no. 22 (August 28, 2023): 1560. http://dx.doi.org/10.1149/ma2023-01221560mtgabs.

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Functional coatings and interphases influence the stability and performance parameters of electrodes in various applications. Polymer thin films offer a wide range of molecular structures and compositions for tunable functionalities that can be custom designed to the needs of an application. In solid-state energy storage devices in particular, electrolyte-type polymeric interfaces between battery components and materials with disparate functions, such as the active electrode material and solid electrolyte could overcome some of these incompatibility detriments and the increase in contact resistance over long-term operation. In high-performance micro scale power sources, 3D thin-film all-solid-state batteries show great potential as they take advantage of both short ion diffusion distances for high-rate capability with low heat generation, as well as the third dimension for high material loading and energy density. Therefore, conformal deposition methods for ultra-thin polymeric electrolyte interphases on the interior surface of electrodes with mesoscale 3D architectures and complex porosity are in demand. Here, we report a molecular design concept of dual-functional molecules that contain electrochemically active end groups for self-limiting electropolymerization, and a core molecular motif that determines the thin film functionality. The electrodeposition of this monomer represents a non-line-of-sight coating method for polymer thin films with independently tailorable functionalities and tunable properties on conductive substrates with arbitrary shape. We exemplify this method using monomers with poly(ethylene glycol) (PEG) as the core motif for lithium-ion transport and phenol as electrochemically active end groups. We studied the electrodeposition of the monomers, poly(ethylene glycol) diphenol (PEGDP), and demonstrate their self-limiting film formation mechanism (Figure 1a) which originates from the insulating nature of resulting poly(PEGDP) film that confines the charge transfer reaction. We present an exhaustive exploration of their material-processing-structure-property relationships that reveals the multi-scale control over the ultrathin-film properties. For example, the uniform film thickness is tunable from 10 to 100s of nanometer through electrodeposition conditions and molecular design, while their molecular permeability and electronic resistance can be tailored from pervious to fully blocking. We show that the electrodeposited functional interphases fully coat complex 3D electrode architectures (Figure 1b top: uncoated carbon electrode, bottom: film coated carbon electrode) with retention of their functionality in a battery. This work demonstrates that rational molecular design enables the conformal electrodeposition of ultrathin functional coatings with solid polymer electrolyte properties on 3D structured electrodes that will enable designer interphases in various solid-state battery architectures and chemistries. Figure 1

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38

Hara, Michihiro, Takao Umeda, and Hiroyuki Kurata. "Fabrication and Characterisation of Organic EL Devices in the Presence of Cyclodextrin as an Interlayer." Sensors 21, no. 11 (May 25, 2021): 3666. http://dx.doi.org/10.3390/s21113666.

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This study examined glass-based organic electroluminescence in the presence of a cyclodextrin polymer as an interlayer. Glass-based organic electroluminescence was achieved by the deposition of five layers of N,N’-Bis(3-methylphenyl)N,N’-bis(phenyl)-benzidine, cyclodextrin polymer (CDP), tris-(8-hydroxyquinolinato) aluminium LiF and Al on an indium tin oxide-coated glass substrate. The glass-based OEL exhibited green emission owing to the fluorescence of tris-(8-hydroxyquinolinato) aluminium. The highest luminance was 19,620 cd m−2. Moreover, the glass-based organic electroluminescence device showed green emission at 6 V in the curved state because of the inhibited aggregation of the cyclodextrin polymer. All organic molecules are insulating, but except CDP, they are standard molecules in conventional organic electroluminescence devices. In this device, the CDP layer contained pores that could allow conventional organic molecules to enter the pores and affect the organic electroluminescence interface. In particular, self-association was suppressed, efficiency was improved, and light emission was observed without the need for a high voltage. Overall, the glass-based organic electroluminescence device using CDP is an environmentally friendly device with a range of potential energy saving applications.

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39

Won, T., and H. Morkoc. "Self-aligned In/sub 0.52/Al/sub 0.48/As/In/sub 0.53/Ga/sub 0.47/As heterojunction bipolar transistors with graded interface on semi-insulating InP grown by molecular beam epitaxy." IEEE Electron Device Letters 10, no. 3 (March 1989): 138–40. http://dx.doi.org/10.1109/55.31694.

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40

Pochan, Darrin, and Oren Scherman. "Introduction: Molecular Self-Assembly." Chemical Reviews 121, no. 22 (November 24, 2021): 13699–700. http://dx.doi.org/10.1021/acs.chemrev.1c00884.

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41

KRATOCHVÍLOVÁ, IRENA, ADRIANA ZAMBOVA, JEREMIAH MBINDYO, BAHARAK RAZAVI, and JOSEF HOLAKOVSKÝ. "CURRENT-VOLTAGE CHARACTERIZATION OF ALKANETHIOL SELF-ASSEMBLED MONOLAYERS IN METAL NANOWIRES." Modern Physics Letters B 16, no. 05n06 (March 10, 2002): 161–69. http://dx.doi.org/10.1142/s0217984902003609.

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An electric-field assisted assembly has been used to place rod-shaped, metal-organic, molecule-metal nanowires onto lithographically defined metal pads allowing the electrical characterization of metal-molecule self-assembled monolayer-metal containing nanowires. Our results show that the parameters of metal-molecule metal junctions are close to previously published data, so we have constructed systems containing insulating monolayers with reasonable properties.

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NARANTHATTA, MILI C., V. RAMKUMAR, and DILLIP KUMAR CHAND. "Self-assembly of self-assembled molecular triangles." Journal of Chemical Sciences 126, no. 5 (September 2014): 1493–99. http://dx.doi.org/10.1007/s12039-014-0702-0.

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43

Coropceanu, Igor, Eric M. Janke, Joshua Portner, Danny Haubold, Trung Dac Nguyen, Avishek Das, Christian P. N. Tanner, et al. "Self-assembly of nanocrystals into strongly electronically coupled all-inorganic supercrystals." Science 375, no. 6587 (March 25, 2022): 1422–26. http://dx.doi.org/10.1126/science.abm6753.

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Colloidal nanocrystals of metals, semiconductors, and other functional materials can self-assemble into long-range ordered crystalline and quasicrystalline phases, but insulating organic surface ligands prevent the development of collective electronic states in ordered nanocrystal assemblies. We reversibly self-assembled colloidal nanocrystals of gold, platinum, nickel, lead sulfide, and lead selenide with conductive inorganic ligands into supercrystals exhibiting optical and electronic properties consistent with strong electronic coupling between the constituent nanocrystals. The phase behavior of charge-stabilized nanocrystals can be rationalized and navigated with phase diagrams computed for particles interacting through short-range attractive potentials. By finely tuning interparticle interactions, the assembly was directed either through one-step nucleation or nonclassical two-step nucleation pathways. In the latter case, the nucleation was preceded by the formation of two metastable colloidal fluids.

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WILD, M., S. BERNER, H. SUZUKI, L. RAMOINO, A. BARATOFF, and T. A. JUNGA. "Molecular Assembly and Self-Assembly: Molecular Nanoscience for Future Technologies." Annals of the New York Academy of Sciences 1006, no. 1 (December 2003): 291–305. http://dx.doi.org/10.1196/annals.1292.020.

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45

de Wild, Michael, Simon Berner, Hitoshi Suzuki, Luca Ramoino, Alexis Baratoff, and Thomas A. Jung. "Molecular Assembly and Self-Assembly: Molecular Nanoscience for Future Technologies." CHIMIA International Journal for Chemistry 56, no. 10 (October 1, 2002): 500–505. http://dx.doi.org/10.2533/000942902777680162.

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46

Jonoska, Nataša, and Nadrian C. Seeman. "Computing by molecular self-assembly." Interface Focus 2, no. 4 (February 8, 2012): 504–11. http://dx.doi.org/10.1098/rsfs.2011.0117.

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The paper reviews two computing models by DNA self-assembly whose proof of principal have recently been experimentally confirmed. The first model incorporates DNA nano-devices and triple crossover DNA molecules to algorithmically arrange non-DNA species. This is achieved by simulating a finite-state automaton with output where golden nanoparticles are assembled to read-out the result. In the second model, a complex DNA molecule representing a graph emerges as a solution of a computational problem. This supports the idea that in molecular self-assembly computing, it may be necessary to develop the notion of shape processing besides the classical approach through symbol processing.

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CHEN, JingXiao, RenXi ZHUO, XiaoDing XU, XianZheng ZHANG, and ChangSheng CHEN. "Molecular self-assembly of peptide." SCIENTIA SINICA Chimica 41, no. 2 (March 1, 2011): 221–38. http://dx.doi.org/10.1360/032010-782.

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48

Grover, Martha A. "Control of molecular self-assembly." Journal of Process Control 27 (March 2015): 36–37. http://dx.doi.org/10.1016/j.jprocont.2015.01.008.

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Ravoo, Bart Jan. "Frontiers of Molecular Self‐Assembly." Israel Journal of Chemistry 59, no. 10 (October 2019): 868. http://dx.doi.org/10.1002/ijch.201900122.

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MacLeod, J. M., and F. Rosei. "Molecular Self-Assembly on Graphene." Small 10, no. 6 (October 24, 2013): 1038–49. http://dx.doi.org/10.1002/smll.201301982.

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