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Journal articles on the topic 'Molybdenum electrodeposition'

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Published: 4 June 2021
Last updated: 15 February 2022

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1

Zach, M. P., K. H. Ng, and R. M. Penner. "Molybdenum Nanowires by Electrodeposition." Science 290, no. 5499 (December 15, 2000): 2120–23. http://dx.doi.org/10.1126/science.290.5499.2120.

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2

Bélanger, Daniel, Guylaine Laperriére, and Benoît Marsan. "The electrodeposition of amorphous molybdenum sulfide." Journal of Electroanalytical Chemistry 347, no. 1-2 (April 1993): 165–83. http://dx.doi.org/10.1016/0022-0728(93)80086-w.

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3

McEvoy, Todd M., and Keith J. Stevenson. "Elucidation of the electrodeposition mechanism of molybdenum oxide from iso- and peroxo-polymolybdate solutions." Journal of Materials Research 19, no. 2 (February 2004): 429–38. http://dx.doi.org/10.1557/jmr.2004.19.2.429.

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The cathodic electrodeposition of molybdenum oxide thin films prepared from aqueous solutions containing iso-polymolybdates and peroxo-polymolybdates is described. Chronocoulometry, x-ray photoelectron spectroscopy, spectroelectrochemistry, and electrochemical quartz crystal microgravimetry were used to establish corresponding reaction mechanisms for films grown at different deposition potentials. Electrodeposition from acidified iso-polymolybdate solutions proceeds by the reduction of molybdic acid, whereas deposition from aqueous peroxo-based solutions involves the graded reduction of several solution components, primarily comprising molybdic acid and peroxo-polymolybdates. Careful regulation of the deposition potential allows for controlled growth of distinct molybdenum oxide compositions producing films with varied water content and valency.
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4

Gómez, Elvira, Eva Pellicer, and Elisa Vallés. "Electrodeposition of soft-magnetic cobalt–molybdenum coatings containing low molybdenum percentages." Journal of Electroanalytical Chemistry 568 (July 2004): 29–36. http://dx.doi.org/10.1016/j.jelechem.2003.12.032.

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5

Malyshev, Victor, Angelina Gab, Dmytro Shakhnin, Cristina Donath, Elena Ionela Neacsu, Ana Maria Popescu, and Virgil Constantin. "Influence of Electrolysis Parameters on Mo and W Coatings Electrodeposited from Tungstate, Molybdate and Tungstate-Molybdate Melts." Revista de Chimie 69, no. 9 (October 15, 2018): 2411–15. http://dx.doi.org/10.37358/rc.18.9.6544.

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Molybdenum and tungsten coatings electrodeposition from halide-oxide and oxide melts has been realized. The influence of electrolysis conditions on physico-chemical properties of deposits has been studied. Coating structure control has been realized with the help of change of atmosphere composition above the bath and application of non-stationary current regimes during electrodeposition.
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6

KOYAMA, Koichiro, and Makoto IGUCHI. "Smooth Electrodeposition of Molybdenum from Oxide Melts." Denki Kagaku oyobi Kogyo Butsuri Kagaku 63, no. 2 (February 5, 1995): 161–63. http://dx.doi.org/10.5796/kogyobutsurikagaku.63.161.

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7

Hahn, Benjamin P., and Keith J. Stevenson. "Cathodic Electrodeposition of Mixed Rhenium-Molybdenum Oxides." ECS Transactions 6, no. 25 (December 19, 2019): 17–26. http://dx.doi.org/10.1149/1.2943221.

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8

Morón-Vera, Lydia E., and Julieta Torres. "Study of Electrodeposition of Molybdenum-Tin Alloys." ECS Transactions 3, no. 17 (December 21, 2019): 1–7. http://dx.doi.org/10.1149/1.2721501.

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9

Hahn, Benjamin P., and Keith J. Stevenson. "Cathodic electrodeposition of mixed molybdenum–selenium oxides." Journal of Electroanalytical Chemistry 638, no. 1 (January 2010): 151–60. http://dx.doi.org/10.1016/j.jelechem.2009.10.006.

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10

Dubrovskiy, Anton, Olga Makarova, and Sergey Kuznetsov. "Effect of the Molybdenum Substrate Shape on Mo2C Coating Electrodeposition." Coatings 8, no. 12 (December 3, 2018): 442. http://dx.doi.org/10.3390/coatings8120442.

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By electrochemical synthesis in the NaCl-KCl-Li2CO3 (1.5 wt.%)-Na2MoO4 (8.0 wt.%) melt on molybdenum, substrates with different configuration Mo2C coatings with the hexagonal lattice were obtained. The influence of the substrate form on the structure of Mo2C cathodic deposits was studied. The molybdenum carbide coatings on a molybdenum substrate (Mo2C/Mo) show a catalytic activity in the water–gas shift (WGS) reaction by at least three orders of magnitude higher than that of the bulk Mo2C phase. The catalytic activity remained constant during 500 h for the water–gas shift reaction.
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11

Aladjov, B. "Electrodeposition of Molybdenum and Molybdenum Carbide Coatings from Oxide Based Molten Salts." ECS Proceedings Volumes 1992-16, no. 1 (January 1992): 488–99. http://dx.doi.org/10.1149/199216.0488pv.

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12

Rajaei, V., K. Raeissi, M. Shamanian, and H. Rashtchi. "Electrodeposition and Characterization of Nanocrystalline Nickel- Molybdenum Alloy." Journal of Advanced Materials In Engineering 35, no. 1 (June 1, 2016): 71–81. http://dx.doi.org/10.18869/acadpub.jame.35.1.71.

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13

HARA, Motoi, and Tomoyuki TSUCHIDA. "Formation of Molybdenum Silicide by Molten Salt Electrodeposition." Journal of the Surface Finishing Society of Japan 49, no. 11 (1998): 1233–34. http://dx.doi.org/10.4139/sfj.49.1233.

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14

Guerfi, A., and LÊ H. Dao. "Electrochromic Molybdenum Oxide Thin Films Prepared by Electrodeposition." Journal of The Electrochemical Society 136, no. 8 (August 1, 1989): 2435–36. http://dx.doi.org/10.1149/1.2097408.

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15

Ved’, M. V., N. D. Sakhnenko, A. V. Karakurchi, and S. I. Zyubanova. "Electrodeposition of iron-molybdenum coatings from citrate electrolyte." Russian Journal of Applied Chemistry 87, no. 3 (March 2014): 276–82. http://dx.doi.org/10.1134/s1070427214030057.

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16

Mercier, Dimitri, Elise Delbos, Hanane El Belghiti, Jackie Vigneron, Muriel Bouttemy, and Arnaud Etcheberry. "Study of Copper Electrodeposition Mechanism on Molybdenum Substrate." Journal of The Electrochemical Society 160, no. 12 (2013): D3103—D3109. http://dx.doi.org/10.1149/2.017312jes.

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17

Nagirnyi, V. M., R. D. Apostolova, and E. M. Shembel’. "Electrodeposition of molybdenum oxide and its structural characteristics." Russian Journal of Applied Chemistry 79, no. 9 (September 2006): 1438–42. http://dx.doi.org/10.1134/s1070427206090096.

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18

Dergacheva, M. B., K. A. Urazov, and N. V. Pen’kova. "Electrodeposition of CuInSe2 films onto a molybdenum electrode." Russian Journal of Applied Chemistry 83, no. 4 (April 2010): 653–58. http://dx.doi.org/10.1134/s1070427210040154.

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19

Kushkhov, H. B. "Joint Electrodeposition of Molybdenum, Tungsten and Molybdenum-Tungsten Alloys from Oxy-Halide Melts." ECS Proceedings Volumes 2002-19, no. 1 (January 2002): 831–39. http://dx.doi.org/10.1149/200219.0831pv.

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20

Fomichev, V. T., A. V. Savchenko, and G. P. Gubarevich. "STUDY OF THE COBALT-MOLYBDENE ALLOY ELECTRODEPOSITION PROCESS IN STATIONARY AND PULSE ELECTROLYESIS." IZVESTIA VOLGOGRAD STATE TECHNICAL UNIVERSITY, no. 6(241) (June 29, 2020): 86–91. http://dx.doi.org/10.35211/1990-5297-2020-6-241-86-91.

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The polarization curve method was used to study the process of co-deposition of cobalt and molybdenum using a constant and pulsed current of different duty cycle. The effect of the electrolyte composition, the parameters of the pulsed current on the current efficiency and the composition of the cobalt-molybdenum alloy is shown.
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21

Karabanov, Sergey M., Yulia M. Stryuchkova, Dmitriy V. Suvorov, Gennadiy P. Gololobov, Dmitry Yu Tarabrin, Nikolay B. Rybin, and Evgeniy V. Slivkin. "Electrodeposition of Ni-Mo Defect-Free Alloy from Ammonium-Citrate Electrolyte in Pulse Current Mode." MRS Advances 2, no. 58-59 (2017): 3585–89. http://dx.doi.org/10.1557/adv.2017.474.

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ABSTRACT Electrodeposition in pulse current mode of nickel-molybdenum alloy on a nickel substrate was studied. The range of current density variation from 2 to 9 A/dm2 was investigated. The range of pulse and pause step lengths is from tens to hundreds of milliseconds. SEM-images of applied coatings surfaces are obtained. The method of energy dispersive spectroscopy determined that the molybdenum content in the coating is 21-24 wt%. It was found that under transient pulse mode of electrolysis, with the pulse step corresponding to hundreds of milliseconds, the most rigid and smooth coatings of the electrolytic nickel-molybdenum alloy are obtained from ammonium-citrate electrolyte. It is shown that the percentage of nickel in the alloy does not depend on the electrolysis mode.
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22

Pavlov, M. P., N. V. Morozova, and V. N. Kudryavtsev. "Electrodeposition of nickel-molybdenum alloys from ammonium citrate baths containing intermediate valence molybdenum compounds." Protection of Metals 43, no. 5 (September 2007): 459–64. http://dx.doi.org/10.1134/s0033173207050074.

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23

Delphine, S. Mary, M. Jayachandran, and C. Sanjeeviraja. "Pulsed electrodeposition and characterization of molybdenum diselenide thin film." Materials Research Bulletin 40, no. 1 (January 2005): 135–47. http://dx.doi.org/10.1016/j.materresbull.2004.09.008.

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24

Kuznetsov, V. V., K. E. Golyanin, and T. V. Pshenichkina. "Electrodeposition of iron-molybdenum alloy from ammonia-citrate electrolyte." Russian Journal of Electrochemistry 48, no. 11 (November 2012): 1107–12. http://dx.doi.org/10.1134/s1023193512110109.

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25

Ivanova, N. D., S. V. Ivanov, E. I. Boldyrev, and O. A. Stadnik. "Electrodeposition of metal molybdenum from electrolytes containing hydrofluoric acid." Protection of Metals 42, no. 4 (July 2006): 354–58. http://dx.doi.org/10.1134/s0033173206040084.

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26

Malyshev, V. V. "Electrochemical processes and implementation of molybdenum electrodeposition in melts." Russian Metallurgy (Metally) 2006, no. 2 (March 2006): 126–32. http://dx.doi.org/10.1134/s0036029506020042.

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27

Delbos, E., H. El Belghiti, D. Mercier, J. Vigneron, M. Bouttemy, and A. Etcheberry. "Study of the Copper Electrodeposition Mechanism on Molybdenum Substrate." ECS Transactions 50, no. 52 (April 1, 2013): 95–101. http://dx.doi.org/10.1149/05052.0095ecst.

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28

Stepanova, L. I., and O. G. Purovskaya. "Electrodeposition of Nickel-Based alloys with tungsten and molybdenum." Metal Finishing 96, no. 11 (November 1998): 50–53. http://dx.doi.org/10.1016/s0026-0576(98)80871-4.

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29

Gao, Bingliang, Toshiyuki Nohira, and R. Hagiwara. "Electrodeposition of Molybdenum in LiTFSI-CsTFSI Melt at 150ºC." ECS Transactions 3, no. 35 (December 21, 2019): 323–31. http://dx.doi.org/10.1149/1.2798675.

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30

Hasan, Siti Nur, Min Xu, and Edouard Asselin. "Electrodeposition of metallic molybdenum and its alloys – a review." Canadian Metallurgical Quarterly 58, no. 1 (August 27, 2018): 1–18. http://dx.doi.org/10.1080/00084433.2018.1511252.

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31

Karakurkchi, A. V., M. V. Ved’, N. D. Sakhnenko, and I. Yu Yermolenko. "Electrodeposition of iron–molybdenum–tungsten coatings from citrate electrolytes." Russian Journal of Applied Chemistry 88, no. 11 (November 2015): 1860–69. http://dx.doi.org/10.1134/s1070427215011018x.

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32

Chassaing, E., K. Vu Quang, and R. Wiart. "Mechanism of nickel-molybdenum alloy electrodeposition in citrate electrolytes." Journal of Applied Electrochemistry 19, no. 6 (November 1989): 839–44. http://dx.doi.org/10.1007/bf01007931.

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33

Nestor, Uwitonze, Wei Chen, and Yan-Xia Chen. "Electrochemical performance of Mo2C@PtRu synthesized by electrochemical deposition method on methanol oxidation." JOURNAL OF ADVANCES IN CHEMISTRY 12, no. 2 (December 16, 2016): 3989–95. http://dx.doi.org/10.24297/jac.v12i2.2155.

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The electrodeposition of Platinum and Ruthenium nanoparticles into Molybdenum carbide/ glassy carbon electrodes and their catalytic activity for the oxidatlon of methanol are described. These Mo2C@PtRu electrodes exhibit good activity with respect to the catalytic oxidation of methanol. The electrodes exhibited excellent long term stabilty in the acidic methanol solutions.
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34

Nestor, Uwitonze, Wei Chen, and Yan-Xia Chen. "Electrochemical performance of Mo2C@PtRu synthesized by electrochemical deposition method on methanol oxidation." JOURNAL OF ADVANCES IN CHEMISTRY 12, no. 2 (December 16, 2015): 3989–95. http://dx.doi.org/10.24297/jac.v12i2.6698.

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The electrodeposition of Platinum and Ruthenium nanoparticles into Molybdenum carbide/ glassy carbon electrodes and their catalytic activity for the oxidatlon of methanol are described. These Mo2C@PtRu electrodes exhibit good activity with respect to the catalytic oxidation of methanol. The electrodes exhibited excellent long term stabilty in the acidic methanol solutions.
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35

Yue, Gao, and Xi Ping Guo. "Electrodeposition and the Optimization of Molybdenum Layer on Nb-Ti-Si Based Ultra-High Alloys from Aqueous Solution." Materials Science Forum 913 (February 2018): 396–405. http://dx.doi.org/10.4028/www.scientific.net/msf.913.396.

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Depositing a molybdenum layer through electrodeposition is a possible and economical way to prepare Mo layer. It could be a new preparation of MoSi2coating on Nb-Ti-Si based alloys combined with halide pack cementation. In this paper, the effects of pre-coated Re layer on the substrate, pH of the electrolyte, water to acetate ratio and the applied current density on the deposition were investigated and optimized to obtain low oxygen content, adherent molybdenum coating on Nb-Ti-Si based alloys. The surface morphology and cross section were characterized by SEM. The thickness of the deposit is about 6 μm and nodules and cracks were observed on the surface. EDS and EPMA analysis suggested the presence of Mo and its oxides in the deposit; XPS results confirmed the presence of Mo, Mo2O3and MoO3in the as-deposited layer. The crystal structure of as-prepared coating was amorphous by the XRD investigation, and the metallic molybdenum was the main existence form of the molybdenum element in the deposit.
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36

Popczyk, Magdalena, Julian Kubisztal, and Antoni Budniok. "Electrodeposition and Thermal Treatment of Nickel Coatings Containing Molybdenum and Silicon." Materials Science Forum 514-516 (May 2006): 1182–85. http://dx.doi.org/10.4028/www.scientific.net/msf.514-516.1182.

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Ni+Mo+Si coatings were obtained by electrolytic codeposition of crystalline nickel with molybdenum and silicon powders from an electrolyte containing suspension of these powders. These coatings were obtained in galvanostatic conditions, at the current density of -0.100 A cm-2. Thermal treatment of these coatings in argon atmosphere was done at temperature of 1100oC for 1 hour. A scanning electron microscope was used for surface morphology characterization of the coatings. Chemical composition of obtained coatings was determined by Xray fluorescence spectroscopy method and phase composition investigations were conducted by Xray diffraction method. It was found that introduction of molybdenum and silicon into nickel matrix, causes of obtained coatings about very rough surface. Thermal treatment of these coatings influenced their surface. The surface after thermal treatment is more compact and less rough than the as-deposited one.
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37

Poorahong, Sujittra, Ricardo Izquierdo, and Mohamed Siaj. "An efficient porous molybdenum diselenide catalyst for electrochemical hydrogen generation." J. Mater. Chem. A 5, no. 39 (2017): 20993–1001. http://dx.doi.org/10.1039/c7ta05826h.

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A simple approach to fabricate a vertically aligned porous MoSe2 by a two-step co-electrodeposition/etching method was proposed. The etching process induces MoSe2 porous 3D structure formation. The porous MoSe2 nanosheet exhibits a high electrocatalytic performance for hydrogen evolution.
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38

Dauletbay, Akbar, Washington Braida, Mihail Nauryzbaev, Leila Kudreeva, Andrey Kurbatov, and Akyl Tulegenov. "Electrodeposition of Mo/MoOx on Copper Substrate from Dimethyl Sulfoxide Solutions." Eurasian Chemico-Technological Journal 13, no. 3-4 (May 4, 2011): 253. http://dx.doi.org/10.18321/ectj215.

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<p>Molybdenum (Mo) is a refractory metal used principally as an alloying agent in steels, cast irons, and super alloys to enhance hardness, strength, toughness, wear and corrosion resistance and it is also widely used in catalytic applications, lubricants and pigments. The single electrodeposition of Mo from aqueous solutions cannot be achieved but Mo it can be co-deposited as an alloy with iron group metals (induced co-deposition). In this study, the electrodeposition of Mo/MoO<sub>x</sub> from dimethyl sulfoxide solutions on a copper substrate has been investigated. Different experimental electrodeposition parameters have been assessed (i.e., supporting electrolyte concentration and small amounts of water to the electrolytic bath) to analyze their influence on mechanism of induced Mo/MoO<sub>x</sub> deposition. Linear scan voltammetry has been used to follow up the electrodeposition of Mo/MoO<sub>x</sub> films. Film morphology has been characterized using scanning electron microscopy (SEM), compositional analysis was performed using X-ray photoelectron spectroscopy. Mo bearing films were also chemically characterized by ICP-OES analysis. An electrodeposition mechanism was developed and discussed.</p>
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39

NAKAMURA, Toyohisa. "Electrodeposition of molybdenum sulfide films from nonaqueous solvents by using molybdenum foil as the counterelectrode." Journal of the Surface Finishing Society of Japan 41, no. 11 (1990): 1163–67. http://dx.doi.org/10.4139/sfj.41.1163.

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40

KONNO, Hidetaka, Takashi ITO, Masaru OTANI, and Keiko SASAKI. "Electrodeposition of Mixed Valence Molybdenum Oxyhydroxide Films and Their Characterization." Journal of the Surface Finishing Society of Japan 50, no. 10 (1999): 909–14. http://dx.doi.org/10.4139/sfj.50.909.

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41

Crousier, J., M. Eyraud, J. P. Crousier, and J. M. Roman. "Influence of substrate on the electrodeposition of nickel-molybdenum alloys." Journal of Applied Electrochemistry 22, no. 8 (August 1992): 749–55. http://dx.doi.org/10.1007/bf01027505.

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42

Syed, Rajak, S. K. Ghosh, P. U. Sastry, G. Sharma, R. C. Hubli, and J. K. Chakravartty. "Electrodeposition of thick metallic amorphous molybdenum coating from aqueous electrolyte." Surface and Coatings Technology 261 (January 2015): 15–20. http://dx.doi.org/10.1016/j.surfcoat.2014.11.073.

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43

Ghosh, S. K., C. Srivastava, S. Nath, and J. P. Celis. "Simple Formation of Nanostructured Molybdenum Disulfide Thin Films by Electrodeposition." International Journal of Electrochemistry 2013 (2013): 1–7. http://dx.doi.org/10.1155/2013/138419.

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Nanostructured molybdenum disulfide thin films were deposited on various substrates by direct current (DC) electrolysis form aqueous electrolyte containing molybdate and sulfide ions. Post deposition annealing at higher temperatures in the range 450–700°C transformed the as-deposited amorphous films to nanocrystalline structure. High temperature X-ray diffraction studies clearly recorded the crystal structure transformations associated with grain growth with increase in annealing temperature. Surface morphology investigations revealed featureless structure in case of as-deposited surface; upon annealing it converts into a surface with protruding nanotubes, nanorods, or dumbbell shape nanofeatures. UV-visible and FTIR spectra confirmed about the presence of Mo-S bonding in the deposited films. Transmission electron microscopic examination showed that the annealed MoS2films consist of nanoballs, nanoribbons, and multiple wall nanotubes.
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44

Gómez, Elvira, Eva Pellicer, and Elisa Vallés. "Intermediate molybdenum oxides involved in binary and ternary induced electrodeposition." Journal of Electroanalytical Chemistry 580, no. 2 (July 2005): 238–44. http://dx.doi.org/10.1016/j.jelechem.2005.03.031.

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45

Bigos, A., E. Bełtowska-Lehman, P. Indyka, M. J. Szczerba, M. Kot, and M. Grobelny. "Electrodeposition and Properties of Nanocrystalline Ni-Based Alloys with Refractory Metal from Citrate Baths / Elektroosadzanie I Własciwosci Nanokrystalicznych Stopów Na Osnowie Niklu Z Trudnotopliwym Metalem Z Kapieli Cytrynianowych." Archives of Metallurgy and Materials 58, no. 1 (March 1, 2013): 247–53. http://dx.doi.org/10.2478/v10172-012-0181-6.

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The main aim of the present work was to determine the optimal conditions for electrodeposition of metallic Ni-Mo coatings of enhanced micromechanical properties. These alloys were electrodeposited on the ferritic steel substrate, under galvanostatic regime in a system with a rotating disk electrode (RDE), from an aqueous citrate complex solution containing nickel and molybdenum salts. The effect of the electrolyte solution pH (adjusted by sulphuric acid or ammonia) on the molybdenum content and on deposit quality as well as on the current efficiency of the electrodeposition process, has been studied. It was established that increase of bath pH is correlated with gradual increase of molybdenum content in deposits up to pH 7, where the maximum concentration of Mo(VI) electroactive citrate complex ions [MoO4(Cit)H]4- (Cit= C6H5O7-3 ) in plating bath was observed. In the selected bath of the optimum pH value, the effect of cathodic current density, as a crucial operating parameter which strongly controls the chemical composition and microstructure parameters (e.g. phase compositions, crystallite size), on the mechanical and tribological properties of the resulting coatings has been determined. It has been shown that - under all investigated current density range - crack-free, well adherent Ni-Mo coatings, characterized by microhardness of 6.5-7.8 GPa, were obtained. Alloys deposited at higher tested current densities (above 3.5 A/dm2) were characterized by compact and uniform microstructure, and thus had the highest wear and friction resistance.
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46

Santos, Hugo Sousa, Alessandra Alves Correa, Murilo Fernando Gromboni, and Lucia Helena Mascaro. "Electrodeposition study of the Cu-Zn-Mo system in citrate/sulfate medium." Eclética Química Journal 44, no. 1SI (November 20, 2019): 26. http://dx.doi.org/10.26850/1678-4618eqj.v44.1si.2019.p26-35.

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Alloys and composites that contain molybdenum have been studied due to their excellent properties, such as corrosion resistance and catalytic activity. In this work, the parameters for Cu-Zn-Mo system electrodeposition were studied, such as deposition potentials and concentration of electroactive species. The deposition potentials were examined using cyclic voltammetry and anodic linear stripping voltammetry (ALSV), the deposit morphology was evaluated using scanning electron microscopy (SEM) and crystallographic characterization was carried out for X-ray diffraction (XRD). The voltammetry studies indicated co-deposition of the metals in potentials more negative than -1.2 V, and a potential deposition at -1.5 V was chosen. The coatings presented morphology compact with small agglomerated particles with cauliflower structures, and the content of molybdenum, copper, and zinc ranged from 5 to 8%, 30 to 40% and 20 to 28%, respectively.
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47

Farmakis, Kostas S., and Ioannis G. Poulios. "Characterization of Electrodeposited Molybdenum Black Surface Coatings." Zeitschrift für Naturforschung A 44, no. 6 (June 1, 1989): 533–37. http://dx.doi.org/10.1515/zna-1989-0608.

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Molybdenum black has been produced in thin coating form (3 μm) on prepared aluminium surfaces by the method of electrodeposition. The microstructure of the coating has been identified as one of flat irregular platelets belonging to a material which can be described as quasi-amorphous. Its chemical composition is 90 wt% MoO2 · 2 H2O and 10 wt% Ni(OH)2 · Mo-black appears to be a good absorber of solar radiation. Absorbance values as high as 93% have been measured for the visible region of the solar energy spectrum. It has been identified that the coating is of semiconducting nature and that the dominant conduction mechanism is the Schottky emission mechanism. Photoelectrochemical measurements have finally provided evidence for photon-induced electrochemical processes at the Mo-black electrodes.
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48

Nisar, Talha, Torsten Balster, and Veit Wagner. "Mechanical transfer of electrochemically grown molybdenum sulfide layers to silicon wafer." Journal of Applied Electrochemistry 51, no. 9 (May 13, 2021): 1279–86. http://dx.doi.org/10.1007/s10800-021-01570-0.

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Abstract Large area MoS2 ultra-thin film deposition is one of the big challenges in the recent years. Electrodeposition provides an opportunity to grow such ultra-thin films on large scale. However, the transfer of the electrochemically grown film is challenging. Standard transfer of those thin films is done by wet etching in which the underlying substrate is etched. In this work, the polymer coated electrodeposited MoS2 films on Au are separated mechanically from the underlying substrate by using ultra-sonication. Collapse of micron-sized bubbles produced by ultra-sonication at the interface of Au and silicon substrate provides enough energy for separation due to their weak adhesion. The Au layer is then removed by standard Au-etchant (K/KI) and the polymer coated film is transferred to a desired substrate. Ammonium tetrathiomolybdate (ATTM) has been used as precursor material for the electrodeposition of the films. Initial electrochemically grown films consist of MoS3 which is reduced to MoS2 by a post-annealing step at 450–900 °C. Obtained films are investigated by AFM, Raman, UV–Vis and XPS. Crystal quality improves by increasing the post-annealing temperature. The thickness of the thinnest film was found to be equivalent to 2 monolayers of MoS2, which is desirable for future electronics. Graphic abstract
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49

NISHIYAMA, Naoki, Shigeyoshi MORISAKI, and Nobuyoshi BABA. "Effect of electrolytic conditions on electrodeposition of the blue molybdenum oxide." Journal of the Surface Finishing Society of Japan 40, no. 1 (1989): 146–47. http://dx.doi.org/10.4139/sfj.40.146.

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50

Kuznetsov, V. V., and T. V. Pshenichkina. "Kinetics of cathodic reactions in the electrodeposition of cobalt-molybdenum alloy." Russian Journal of Electrochemistry 46, no. 4 (April 2010): 401–10. http://dx.doi.org/10.1134/s1023193510040051.

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