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Journal articles on the topic 'N-chlorobenzamide'

Author: Grafiati

Published: 5 June 2025

Last updated: 1 August 2025

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1

Saeed, Aamer, Rasheed Ahmad Khera, Naeem Abbas, Jim Simpson, and Roderick G. Stanley. "N-Butyl-4-chlorobenzamide." Acta Crystallographica Section E Structure Reports Online 64, no. 12 (2008): o2322—o2323. http://dx.doi.org/10.1107/s1600536808036313.

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2

Zheng, Xi, Bo Li, Qiang Wang, and Li Guo. "N-Benzylcarbamothioyl-2-chlorobenzamide." Acta Crystallographica Section E Structure Reports Online 66, no. 7 (2010): o1774. http://dx.doi.org/10.1107/s1600536810023822.

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3

Wisnu, Elok Dea Orens Ubung, Indah Purnama Sary, and Dwi Koko Pratoko. "Sintesis dan Uji Aktivitas Antibakteri Senyawa N-fenil-4-klorobenzamida." Pustaka Kesehatan 6, no. 2 (2018): 212. http://dx.doi.org/10.19184/pk.v6i2.7569.

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N-phenylbenzamide is benzamide derivatives, which is potential as an antibacterial agent. N-phenyl-4-chlorobenzamide is N-phenylbenzamide derivative that substitued by chloro to the para position and it was expected to enhance the antibacterial activity. N-phenyl-4-chlorobenzamide was synthesized by reacting 1,3-diphenyilthiourea and 4-chlorobenzoil chloride. This compound has been purified and provided 53% of product with crystal shape, white color, and melting point of 195-197 oC. The purification of this compound was confirmed by TLC and the structure was identified by 1H-NMR, 13C-NMR, and

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4

Khawar Rauf, M., Michael Bolte, and Amin Badshah. "N-(Benzothiazol-2-yl)-3-chlorobenzamide." Acta Crystallographica Section E Structure Reports Online 65, no. 6 (2009): o1245. http://dx.doi.org/10.1107/s1600536809016481.

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The title molecule, C14H9ClN2OS, exists in the solid state in its amide form with a typical C=O bond length, as well as shortened C—N bonds. The plane containing the HNCO atoms subtends dihedral angles of 12.3 (4) and 8.1 (3)° with the planes of the phenyl ring and benzothiazole group, respectively, whereas the dihedral angle between the planes of the phenyl ring and the benzothiazole group is 5.96 (6)°. In the crystal, molecules form intermolecular N—H...N hydrogen bonds, generating independent scissor-likeR22(8) dimers.

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5

Ghare, Sakshi. "Synthesis of 2-chloro-benzamides for evaluation antimicrobial and disinfectant activity: Part-I." Current Trends in Pharmacy and Pharmaceutical Chemistry 6, no. 1 (2024): 26–27. http://dx.doi.org/10.18231/j.ctppc.2024.009.

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2-Chlorobenzamide derivatives have been synthesized and claimed in this research study. The compound SG1 and SG2 were synthesized by known methods Ethylene diamine and isopropyl amine was dissolved in ethanolic 1 N NaOH separately and to it 2-Chlorobenzoyl chloride was added. The products SG1 and SG2 were collected respectively.

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6

B., Thimme Gowda, C. Mary M., and Jyothi K. "Kinetics and mechanism of oxidation of thiosemicarbazide by substituted-N-chlorobenzamides in aqueous methanol medium." Journal of Indian Chemical Society Vol. 78, Aug 2001 (2001): 407–11. https://doi.org/10.5281/zenodo.5878491.

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Department of Post-Graduate Studies and Research in Chemistry, Mangalore University, Mangalagangothri-574 199, India <em>E-mail</em> : gowdabt@yahoo.com  <em> Fax </em>: 91-824-7423671742424 Manuscript received 18 October 2000, accepted 22 March 2001 The kinetics of oxidation of thiosemicarbazide by <em>N</em>-chlorobenzamide, <em>N</em>-chloro-<em>p</em>-methyl-, <em>N</em>-chloro-<em>p</em>-chloro- and <em>N</em>-chloro-<em>p</em>-nitrobenzamides have been studied in aqueous methanol in the presence of perchloric acid. The reactions show first order kinetics in [oxidant], fractiona

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7

Sow, Salif, Felix Odame, Ngoné Diouf, et al. "Syntheses and X-ray Structure of N-(Benzothiazol-2-yl)-3-chlorobenzamide." International Research Journal of Pure and Applied Chemistry 25, no. 4 (2024): 1–9. http://dx.doi.org/10.9734/irjpac/2024/v25i4861.

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The reaction of 3-chloro-benzoyl chloride and 2-aminobenzothiazole in the presence of potassium thiocyanate yielded a yellowish solid C15H10ClN3OS2 (1). Reaction of 1 with cobalt chloride yield a yellowish solid C14H11ClN2O2S (2) which gives crystal suitable for X-ray analyses. The compounds were characterized by elemental analyses FTIR spectroscopy and melting point measurement. Compound 2 crystallizes in the triclinic space group Pī with the following parameters: a = 7.0299(2) Å b = 7.0466(2) Å c = 14.5490(2) Å a = 103.844(3)° β = 92.929(2)° g = 107.291(3) V = 662.33(4) Å3 Z= 2 R1 = 0.030 wR

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8

COŞMAN, Sertaç. "Experimental Research of the Effects of Benzoylthiourea Derivative Fuel and Gasoline Mixtures on Engine Performance and Emissions." International Journal of Automotive Science and Technology 7, no. 4 (2023): 403–9. http://dx.doi.org/10.30939/ijastech..1397506.

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In this study, the influences of Benzoylthiourea Derivative Fuel N-(2-amino-5-bromo-1,dihydropyridine-1-yl)carbonothioyl)-2-chlorobenzamide as an additive into gas-oline were researched on engine performance and exhaust emissions. For this reason, a single-cylinder four stroke gasoline engine was run at wide open throttle, and 2400, 2800, 3200, 3600 and 4000 rpm engine speeds. The changes of engine torque, power output, specific fuel consumption, thermal efficiency, CO, CO2 and HC emissions were experi-mentally investigated.

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9

Skibiński, Robert, and Łukasz Komsta. "Application of Curve Resolution Algorithms in the Study Drug Photodegradation Kinetics—The Example of Moclobemide." Journal of AOAC INTERNATIONAL 95, no. 3 (2012): 708–12. http://dx.doi.org/10.5740/jaoacint.sge_skibinski.

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Abstract The photodegradation of moclobemide was studied in methanolic media. Ultra-HPLC (UHPLC)/MS/MS analysis proved decomposition to 4-chlorobenzamide as a major degradation product and small amounts of Ro 16-3177 (4-chloro-N-[2-[(2-hydroxyethyl)amino] ethyl]benzamide) and 2-[(4-chlorobenzylidene)amino]-N-[2-ethoxyethenyl]ethenamine. The methanolic solution was investigated spectrophotometrically in the UV region, registering the spectra during 30 min of degradation. Using reference spectra and a multivariate chemometric method (multi- variate curve resolution-alternating least squares), th

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10

M. Salih, Kezhal, and Hashim J. Azeez. "Synthesis and Spectral Characterization of a New Series of N-4-Chlorobenzamide-5- phenylthiazolidin-3-one." Rafidain Journal of Science 27, no. 1 (2018): 15–28. http://dx.doi.org/10.33899/rjs.2018.141182.

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11

Gowda, B. Thimme, and P. Jagan Mohana Rao. "Kinetics and Mechanism of Oxidation of Thiocarbohydrazide by N-Bromoacetamide and N-Chlorobenzamide in Buffered Aqueous and Water-Methanol Media." Zeitschrift für Physikalische Chemie 168, Part_2 (1990): 183–92. http://dx.doi.org/10.1524/zpch.1990.168.part_2.183.

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12

Cabezas, N., M. Martinez, E. Galvez, M. S. Arias, F. Florencio та S. Garcia-Blanco. "Synthesis and structural study of N-(8-isopropyl-nortropan-3-α-yl)-2-methoxy-4-amino-5-chlorobenzamide". Journal of Molecular Structure 172 (лютий 1988): 381–94. http://dx.doi.org/10.1016/0022-2860(88)87030-3.

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13

Kubo, Atsushi, Ryuichi Ikeda, and Daiyu Nakamura. "Structural Phase Transition and Molecular Motion of p-Chlorobenzamide as Studied by the Temperature Variations of 35Cl NQR Frequencies, Chlorine Nuclear Quadrupolar Relaxation Times, and 1H Magnetic Dipolar Relaxation Times." Zeitschrift für Naturforschung A 41, no. 1-2 (1986): 270–74. http://dx.doi.org/10.1515/zna-1986-1-248.

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The temperature dependences of 35Cl NQR frequencies, 35Cl (37Cl) nuclear quadrupolar relaxation times (T1ClQ), 1H NMR absorption, and of 1H NMR relaxation times were observed for p-chlorobenzamide, p-ClC6H4CONH2 and its N-deuterated analog. The existence of three 35Cl NQR lines already reported was confirmed for the known low temperature phase below 316 K. A single sharp 35Cl NQR line was detected in the high temperature phase up to 447 K just below the melting point 451 K. At lower temperatures, three different 35Cl T1ClQ values attributable to the fluctuation of the electric field gradient d

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14

Kesuma, Dini, Tegar Achsendo Yuniarta, Alfiani Damayanti Suherto, Galih Satrio Putra, Sutrisno Sutrisno, and Farida Anwari. "Synthesis, molecular docking, molecular dynamics, pharmacokinetics prediction and bioassay of N-(phenylcarbamothioyl)-4-chlorobenzamide as anti-breast cancer candidate." Journal of Pharmacy & Pharmacognosy Research 13, no. 2 (2025): 551–64. http://dx.doi.org/10.56499/jppres24.2092_13.2.551.

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Context: Breast cancer ranks as the leading cause of mortality among women in Indonesia. Thiourea is a compound containing sulfur atom and nitrogen in which its chemical structure resembles urea compound, which has been applied as an anticancer, such as hydroxyurea, nitrosourea, 5-fluorouracil, and sorafenib. Aims: To develop anticancer candidates as a new compound of thiourea derivative, N-(phenylcarbamothioyl)-4-chloro-benzamide (4-Cl-PCTB). Methods: The compound was synthesized from phenylthiourea and 4-chloro-benzoyl chloride by applying nucleophilic acyl substitution reactivity. The compo

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15

SURESH, P. NAYAK, and THIMME GOWDA B. "Oxidation of Thiosemicarbazide, its Metal Complex and Hydrazones by N-Chlorobenzamide in Aquo-acetic Acid Medium-A Kinetic and Mechanistic Study." Journal of Indian Chemical Society Vol. 69, Oct 1992 (1992): 637–41. https://doi.org/10.5281/zenodo.6018509.

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Department of Post-Graduate Studies and Research in Chemistry, Mangalore University, Mangalagangothri-574 199 <em>Manuscript received 14 August 1991, revised 17 June 1992, accepted 22 July 1992</em> The kinetics of oxidation of thiosemicarbazide (TSC), its zinc metal complex and hydrazones by <em>N</em>-chlorobenzamide (NCB) have been investigated in aquo-acetic acid (1 : 1, v/v) medium in the presence of perchloric acid. The hydrazones studied are benzaldehyde, propionaldehyde, acetone and acetophenone thiosemicarbazones. The oxidations follow first order kinetics in [NCB], fractional order d

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16

Y., Dominic Ravichandran, Kishor Rachna, Hariharasubramanian A., Mohana Priya K., and S. Khora Samanta. "Synthesis and characterization of N-substituted benzimidazole derivatives and study of their antibacterial and antifungal activity." Journal of Indian Chemical Society Vol. 92, Jun 2015 (2015): 915–17. https://doi.org/10.5281/zenodo.5637656.

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Organic Chemistry Division, School of Advanced Sciences, VIT University, Vellore-632 014, Tamilnadu, India <em>E-mail </em>: dominic.y@vit.ac.in Medical Biotechnology Division, School of Bioscience and Technology, VIT University, Vellore-632 014, Tamilnadu, India N-(4-(1<em>H</em>-Benzo[d]imidazol-1-yl)phenyl)-3-nitrobenzamide, N-(4-(1<em>H</em>-benzo[d]imidazol-1-yl)phenyl)-4- chlorobenzamide, 4-(1<em>H</em>-benzo[d]imidazol-1-yl)benzenamine and N-(4-(1<em>H</em>-benzo[<em>d</em>]imidazol-1-yl)phenyl)-4-bromobenzamide were synthesized and characterized by IR and NMR techniques. These N-substi

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17

Annan, Nikoi, and Richard B. Silverman. "New analogs of N-(2-aminoethyl)-4-chlorobenzamide (Ro 16-6491). Some of the most potent monoamine oxidase-B inactivators." Journal of Medicinal Chemistry 36, no. 24 (1993): 3968–70. http://dx.doi.org/10.1021/jm00076a026.

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18

Ahmed, Atteeque, Aamer Saeed, Omar M. Ali, et al. "Exploring Amantadine Derivatives as Urease Inhibitors: Molecular Docking and Structure–Activity Relationship (SAR) Studies." Molecules 26, no. 23 (2021): 7150. http://dx.doi.org/10.3390/molecules26237150.

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This article describes the design and synthesis of a series of novel amantadine-thiourea conjugates (3a–j) as Jack bean urease inhibitors. The synthesized hybrids were assayed for their in vitro urease inhibition. Accordingly, N-(adamantan-1-ylcarbamothioyl)octanamide (3j) possessing a 7-carbon alkyl chain showed excellent activity with IC50 value 0.0085 ± 0.0011 µM indicating that the long alkyl chain plays a vital role in enzyme inhibition. Whilst N-(adamantan-1-ylcarbamothioyl)-2-chlorobenzamide (3g) possessing a 2-chlorophenyl substitution was the next most efficient compound belonging to

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19

Sethi, Ritchu, Sandeep Jain, Sandeep Arora, Deepika Saini, and Neelam Jain. "Synthesis, Characterization and Molecular Docking Studies of Novel N-(benzimidazol-1-ylmethyl)-4-chlorobenzamide Analogues for Potential Anti-inflammatory and Antimicrobial Activity." Anti-Inflammatory & Anti-Allergy Agents in Medicinal Chemistry 17, no. 1 (2018): 16–31. http://dx.doi.org/10.2174/1871523017666180426125141.

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20

Lu, Nan, Chengxia Miao, and Xiaozheng Lan. "Theoretical Investigation of Cp*CO(III)-Mediated Regioselective [4 + 2]-Annulation of N-Chlorobenzamide with Vinyl Acetate for the Synthesis of Isoquinolone." HETEROCYCLES 106, no. 8 (2023): 1385. http://dx.doi.org/10.3987/com-23-14872.

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21

Sagar, Belakavadi K., Hemmige S. Yathirajan, Ravindranath S. Rathore, and Christopher Glidewell. "Four closely related N-(3-benzoyl-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)benzamides: order versus disorder, and similar molecular conformations but different modes of supramolecular aggregation, with a new disordered refinement of 2-amino-3-benzoyl-4,5,6,7-tetrahydrobenzo[b]thiophene." Acta Crystallographica Section C Structural Chemistry 74, no. 1 (2018): 45–53. http://dx.doi.org/10.1107/s2053229617017326.

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Four closely related N-(3-benzoyl-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)benzamides, bearing different substituents on the benzamide ring, have been synthesized and structurally characterized. In each of N-(3-benzoyl-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-3-fluorobenzamide, C22H18FNO2S, (I), N-(3-benzoyl-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-4-chlorobenzamide, C22H18ClNO2S, (II), N-(3-benzoyl-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-2,6-difluorobenzamide, C22H17F2NO2S, (III), and N-(3-benzoyl-4,5,6,7-tetrahydrobenzo[b]thiophen-2-yl)-2-methoxybenzamide, C23H21NO3S, (IV), the last of which

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22

Bondiolotti, Gian Pietro, Maria Donata Galva, Federica Villa, Luigi Sciaba, and Giovanni B. Picotti. "In vitro effects on monoamine uptake and release by the reversible monoamine oxidase-B inhibitors Lazabemide and N-(2-aminoethyl)-p-chlorobenzamide: A comparison with l-deprenyl." Biochemical Pharmacology 50, no. 1 (1995): 97–102. http://dx.doi.org/10.1016/0006-2952(95)00022-r.

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23

Su, Qing, Baolin Xu, Zhoubin Tian, and Ziling Gong. "Design and development of novel 1,2,3-triazole chalcone derivatives as potential anti-osteosarcoma agents via inhibition of PI3K/Akt/mTOR signalling pathway." Acta Pharmaceutica 72, no. 3 (2022): 389–402. http://dx.doi.org/10.2478/acph-2022-0026.

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Abstract Osteosarcoma (OS) is an uncommon tumour that mainly affects bone in children and adolescents. The current treatment options of OS are of limited significance due to their immense side effects. In the present manuscript, we have developed a novel series of 1,2,3-triazole chalcone derivatives as potential agents against OS. The compounds were synthesized and evaluated for their PI3K and mTOR inhibitory activity using luminescent kinase assay, and Lance ultra assay, resp. The entire set of compounds showed significant to moderate inhibition of both kinases in the nanomolar range. The thr

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24

Hasana, Ani Riani, Siswandono Siswandono, and Marcellino Rudyanto. "Synthesis and characterization of 2-Benzamido-NBenzylbenzamide Derivative." JURNAL ILMU KEFARMASIAN INDONESIA 20, no. 2 (2022): 281. http://dx.doi.org/10.35814/jifi.v20i2.1135.

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Anthranilamide derivatives exhibit anti-inflammatory, antipyretic, antibacterial, antiangiogenic, and anticoagulant properties. With an early in silico examination of its analgesic capabilities, this study aimed to generate a novel anthranilamide molecule by altering 2-Benzamido-N-Benzylbenzamide. Modification of anthranilamide with 1/2/3-chloro benzoyl chloride by acylation resulted in the design, synthesis, characterization, and research of the analgesic effects of 2-benzamido-N-benzoylbenzamide derivatives. 2-(2-chlorobenzamido)-N-(2-chlorobenzoyl)benzamide, 2-(3-chlorobenzamido)-N-(3-chlor

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25

Bréthous, Lise, Noemi Garcia-Delgado, Julian Schwartz, Sonia Bertrand, Daniel Bertrand, and Jean-Louis Reymond. "Synthesis and Nicotinic Receptor Activity of Chemical Space Analogues of N-(3R)-1-Azabicyclo[2.2.2]oct-3-yl-4-chlorobenzamide (PNU-282,987) and 1,4-Diazabicyclo[3.2.2]nonane-4-carboxylic Acid 4-Bromophenyl Ester (SSR180711)." Journal of Medicinal Chemistry 55, no. 10 (2012): 4605–18. http://dx.doi.org/10.1021/jm300030r.

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26

Hajós, M., R. S. Hurst, W. E. Hoffmann та ін. "The Selective α7 Nicotinic Acetylcholine Receptor Agonist PNU-282987 [N-[(3R)-1-Azabicyclo[2.2.2]oct-3-yl]-4-chlorobenzamide Hydrochloride] Enhances GABAergic Synaptic Activity in Brain Slices and Restores Auditory Gating Deficits in Anesthetized Rats". Journal of Pharmacology and Experimental Therapeutics 312, № 3 (2004): 1213–22. http://dx.doi.org/10.1124/jpet.104.076968.

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27

Ramesh, Balu, and Masilamani Jeganmohan. "Cobalt(iii)-catalyzed redox-neutral [4+2]-annulation of N-chlorobenzamides/acrylamides with alkylidenecyclopropanes at room temperature." Chemical Communications 57, no. 30 (2021): 3692–95. http://dx.doi.org/10.1039/d1cc00654a.

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An efficient synthesis of substituted 3,4-dihydroisoquinolinones through [4+2]-annulation of N-chlorobenzamides/acrylamides with alkylidenecyclopropanes using a less expensive and air stable Co(iii) catalyst is demonstrated.

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28

Muniraj, Nachimuthu, and Kandikere Ramaiah Prabhu. "Cobalt(III)-Catalyzed [4 + 2] Annulation of N-Chlorobenzamides with Maleimides." Organic Letters 21, no. 4 (2019): 1068–72. http://dx.doi.org/10.1021/acs.orglett.8b04117.

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29

Li, Ru Lin, Lin Wang, and Gang Xue. "Study on Preparation, Biological Activity and Thermal Decomposition of N-Benzoyl-N＇-(4-Chlorobenzamido) Thiourea." Advanced Materials Research 236-238 (May 2011): 1914–18. http://dx.doi.org/10.4028/www.scientific.net/amr.236-238.1914.

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A novel compound N-benzoyl-N＇-(4-chlorobenzamido) thiourea was prepared from benzoyl isothiocyanate which was obtained from benzoyl chloride and potassium thiocyanate, and 4-chlorobenzoyl hydrazine which was obtained from ethyl 4-chlorobenzoate and hydrazine hydrate. IR,1H NMR,13C NMR and elemental analysis were utilized to determine the structure of the thiourea. The biological tests indicated that the target compound had antibacterial activity against bacillus subtilis and taphylo-coccus aurers. Meanwhile, the thermal stability was investigated by thermogrativity（TG） and differential thermog

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30

Chandrakar, Lalta Prasad, Raghunandan Singh, and Rajendrakumar Mishra. "Extraction-spectrophotometric determination of molybdenum with N-m-tolyl-N′-p-chlorophenyl-o-chlorobenzamidine hydrochloride and thiocyanate." Analyst 112, no. 11 (1987): 1511–13. http://dx.doi.org/10.1039/an9871201511.

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31

L., P. CHANDRAKAR, and K. MISHRA R. "Extractive Spectrophotometric Determination of Molybdenum(v) with N-Hydroxy-N-p-chlorophenyl-N'-p-chlorophenyl-o-chlorobenzamidine Hydrochloride in Presence of Thiocyanate." Journal of Indian Chemical Society Vol. 63, Oct 1986 (1986): 920–22. https://doi.org/10.5281/zenodo.6302337.

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D. B. Science College, Gondia (M. B.) Department of Chemistry, Ravishankar University, Raipur-492 010 <em>Manuscript </em>received 12 March <em>2986, </em>revised <em>29 July </em>1986, <em>accepted 23 August 1986</em> A new spectrophotometric method for the determination of molybdenum(v) at ppm level has been developed. The newly synthesised reagent <em>N</em>-hydroxy-<em>N</em>-<em>p</em>-cldorophenyl-<em>N</em>'-<em>p</em>-chlorophenyl-<em>o</em>-chlorobenzamidine hydrochloride has been used as a chelating agent, and ascorbic acid as a reducing agent for reducing M<sup>VI</sup>&nbs

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32

Rosa, Michael De, Keith Brown, Mary McCoy, Kevin Ong та Kimberley Sanford. "13C nuclear magnetic resonance study of π-polarization in 3- and 4-substituted benzamides and N-chlorobenzamides". J. Chem. Soc., Perkin Trans. 2, № 10 (1993): 1787–90. http://dx.doi.org/10.1039/p29930001787.

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33

DE ROSA, M., K. BROWN, M. MCCOY, K. ONG та K. SANFORD. "ChemInform Abstract: 13C NMR Study of π-Polarization in 3- and 4-Substituted Benzamides and N-Chlorobenzamides". ChemInform 25, № 3 (2010): no. http://dx.doi.org/10.1002/chin.199403042.

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34

Chen, Chun-Yi, Hua-Yu Hsieh, Jyh-Horung Chen, Shin-Shin Wang, Jo-Yu Tung, and Lian-Pin Hwang. "Two-stage formation of chloro (N-o-chlorobenzamido-meso-tetraphenylporphyrinato) zinc(II) methylene chloride solvate: Zn(N-NHCO(o-Cl)C6H4-tpp)Cl·CH2Cl2." Polyhedron 26, no. 15 (2007): 4602–8. http://dx.doi.org/10.1016/j.poly.2007.06.021.

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35

Liu, Hailong, Weibiao Han, Chun Li, et al. "Practical Synthesis of Phenanthridinones by Palladium-Catalyzed One-Pot C-C and C-N Coupling Reaction: Extending the Substrate Scope too-Chlorobenzamides." European Journal of Organic Chemistry 2016, no. 2 (2015): 389–93. http://dx.doi.org/10.1002/ejoc.201501170.

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36

Chen, Kwan-Tin, Ming Yang Tsai, Jyh-Horung Chen, Shin-Shin Wang, and Jo-Yu Tung. "Metal complexes of N-o-chlorobenzamido-meso-tetraphenylporphyrin: cis-Tl(N-NCO(o-Cl)C6H4-tpp)(OAc) and trans-Cd(N-NHCO(o-Cl)C6H4-tpp)(OAc) (tpp=5, 10, 15, 20-tetraphenylporphyrinate)." Inorganic Chemistry Communications 13, no. 4 (2010): 506–10. http://dx.doi.org/10.1016/j.inoche.2010.01.022.

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37

Fernández, M. J., M. S. Toledano, E. Gálvez, et al. "Structural, conformational, theoretical and pharmacological study of some amides derived from 3,7-dimethyl-9-[(N-substituted)-4-chlorobenzamido]3,7-diazabicyclo[3.3.1]nonane-9-carboxamide." Journal of Molecular Structure 351 (June 1995): 137–46. http://dx.doi.org/10.1016/0022-2860(94)08489-5.

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Hewlett, William A., Dennis E. Schmidt, N. Scott Mason, Bakula L. Trivedi, Michael H. Ebert, and Tomas de Paulis. "Synthesis and 5-HT-3 Receptor Binding of 2- and 3-(Halo)alkoxyl Substituted (S)-N-(1-Azabicyclo [2.2.2]oct-3-yl)-5-chlorobenzamides as Potential Radioligands." Nuclear Medicine and Biology 25, no. 2 (1998): 141–53. http://dx.doi.org/10.1016/s0969-8051(97)00161-3.

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39

KATO, Shiro, Toshiya MORIE, Naoyuki YOSHIDA, and Jun-ichi MATSUMOTO. "Novel Benzamides as Selective and Potent Gastrokinetic Agents. IV. Synthesis and Structure-Activity Relationships of 2-Substituted 4-Amino-N-((4-benzyl-2-morpholinyl)methyl)-5-chlorobenzamides." CHEMICAL & PHARMACEUTICAL BULLETIN 40, no. 6 (1992): 1470–75. http://dx.doi.org/10.1248/cpb.40.1470.

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40

De Rosa, Michael, David W. Boykin та Alfons L. Baumstark. "17O NMR study of substituent effects in 4-substituted N-chlorobenzamides and comparison with 4-substituted benzamides: sensitivity to ring substituents (ρ) reflects electronic and steric effects". Journal of the Chemical Society, Perkin Transactions 2, № 8 (1997): 1547–50. http://dx.doi.org/10.1039/a700206h.

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41

Medici, Antonio, Giovanni Luongo, Lucio Previtera, Daniele Naviglio, Giovanni Di Fabio, and Armando Zarrelli. "Degradation of Indomethacin in Wastewater: Removal with Sodium Hypochlorite and Analysis of Degradation Byproducts." Molecules 30, no. 10 (2025): 2180. https://doi.org/10.3390/molecules30102180.

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Over the years, the frequent and continuous use of drugs has led to a high presence of emerging micropollutants in wastewater, increasing environmental and health concerns. Among these chemicals, Indomethacin (IND), a widely used anti-inflammatory drug, has been detected up to 150 ng/L in water bodies. Its presence in aquatic environments causes increasing concerns due to its high persistence, limited biodegradability, and resistance to conventional treatment processes. This study examined the degradation of IND via oxidation with sodium hypochlorite (NaClO) and the characterization of the deg

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42

KATO, S., T. MORIE, N. YOSHIDA, and J. MATSUMOTO. "ChemInform Abstract: Novel Benzamides as Selective and Potent Gastrokinetic Agents. Part 4. Synthesis and Structure-Activity Relationships of 2-Substituted 4- Amino-N-((4-benzyl-2-morpholinyl)methyl)-5-chlorobenzamides (IV)." ChemInform 24, no. 9 (2010): no. http://dx.doi.org/10.1002/chin.199309188.

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43

Wu, Zhouping, Qinwen Zheng, Guanghui Lv, et al. "Cobalt(III)-catalyzed C-H activation/annulation cascade reaction of N-chlorobenzamides with 2-acetylenic ketones at room temperature." Synthesis, March 10, 2022. http://dx.doi.org/10.1055/a-1794-1314.

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A mild cascade annulation of Co(III)-catalyzed N-chlorobenzamide with 2-acetylenic ketones at room temperature has been reported. This reaction sets N-Cl bond of N-chlorobenzamide as an internal oxidant, displaying broad functional group tolerance and excellent reverse selectivity of alkyne insertion under mild and safe conditions. The cascade reaction offers a straightforward and mild protocol to construct isoquinolones with high yields at room temperature.

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44

Mohamooda Sumaya, U., D. Reuben Jonathan, E. R. A. Dravida Thendral, B. K. Revathi, and G. Usha. "N,N′-(Ethane-1,2-diyl)bis(2-chlorobenzamide)." IUCrData 1, no. 7 (2016). http://dx.doi.org/10.1107/s2414314616011901.

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The title compound, C16H14Cl2N2O2, crystallized with one half-molecule in the asymmetric unit; the whole molecule is generated by inversion symmetry, the center of inversion being situated at the middle of the bridging –CH2—CH2– bond. The dihedral angle between the amide group and the benzene ring is 52.4 (2)°. In the crystal, molecules are linked by two pairs of N—H...O hydrogen bonds forming a ladder-like structure propagating along thea-axis direction and enclosingR22(14) ring motifs. The compound was refined as a two-component twin [BASF = 0.18 (1)].

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45

Chandra, Devesh, Sachin -, and Upendra Sharma. "Co(III)‐catalyzed regioselective [4+2] annulation of N‐chlorobenzamide with allenes and vinyl acetate." Asian Journal of Organic Chemistry, November 28, 2023. http://dx.doi.org/10.1002/ajoc.202300536.

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A regioselective annulation protocol of N‐chlorobenzamide with allenes and vinyl acetate is reported under a less expensive catalytic system i.e., Co(III) catalysis and Na2CO3 as base. (CO)NH‐Cl acts as both an internal oxidant and a directing group. Allenes are successfully annulated with N‐chlorobenzamide, providing different exocyclic isoquinolone derivatives in good to moderate yield. Notably, vinyl acetate acts as an ethylene surrogate and undergoes annulation under developed protocol to provide isoquinolone in excellent yield. Interestingly, in‐situ deprotection of the acetyl group allow

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46

Gao, Han, Wujie Wang, Xiangying Lv, Gang Lu, and Yuliang Li. "Mechanism of Co(III)-catalyzed annulation of N-chlorobenzamide with styrene and origin of cyclopentadienyl ligand-controlled enantioselectivity." Organic Chemistry Frontiers, 2023. http://dx.doi.org/10.1039/d3qo00038a.

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The mechanism of Co(III)-catalyzed annulation of N-chlorobenzamide with styrene was computationally studied and the effects of chiral cyclopentadienyl (Cp) ligands on enantioselectivity were investigated by using energy decomposition analysis (EDA)....

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47

Gao, Han, Wujie Wang, Xiaofang Zhai, et al. "Origin of Regioselectivity Inversion Tuned by Substrate Electronic Properties in Co(III)‐Catalyzed Annulation of N‐Chlorobenzamide with Alkenes." ChemPlusChem, November 21, 2024. http://dx.doi.org/10.1002/cplu.202400625.

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The mechanisms of Co(III)‐catalyzed annulations of N‐chlorobenzamide with olefins bearing different electronic properties were computationally studied and the origins of regioselectivity reversal were investigated by using energy decomposition analysis (EDA). The alkene migratory insertion step determines the regiochemistry of these reactions. EDA results indicate that the 2,1‐insertion with styrene is favored because there is a weaker Pauli repulsion between the cobaltacycle Co–C σ orbital and the olefin π orbital. Conversely, the 1,2‐insertion with vinyltrimethylsilane is more favorable than

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Wang, Huidong, Xiankun Cao, Jiadong Guo, et al. "BNTA alleviates inflammatory osteolysis by the SOD mediated anti-oxidation and anti-inflammation effect on inhibiting osteoclastogenesis." Frontiers in Pharmacology 13 (September 29, 2022). http://dx.doi.org/10.3389/fphar.2022.939929.

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Abnormal activation and overproliferation of osteoclast in inflammatory bone diseases lead to osteolysis and bone mass loss. Although current pharmacological treatments have made extensive advances, limitations still exist. N-[2-bromo-4-(phenylsulfonyl)-3-thienyl]-2-chlorobenzamide (BNTA) is an artificially synthesized molecule compound that has antioxidant and anti-inflammatory properties. In this study, we presented that BNTA can suppress intracellular ROS levels through increasing ROS scavenging enzymes SOD1 and SOD2, subsequently attenuating the MARK signaling pathway and the transcription

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CABEZAS, N., M. MARTINEZ, E. GALVEZ, M. S. ARIAS, F. FLORENCIO та J. SANZ-APARICIO. "ChemInform Abstract: Synthesis and Structural Study of Tropane Benzamines. Part 3. N-(8-Isopropyl-nortropan-3-β-yl)-2-methoxy-4-amino-5-chlorobenzamide". ChemInform 20, № 40 (1989). http://dx.doi.org/10.1002/chin.198940224.

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Yadav, Suresh Kumar, and Masilamani Jeganmohan. "Cobalt(III)-Catalyzed Regioselective [4 + 2]-Annulation of N-Chlorobenzamides with Substituted Alkenes." Journal of Organic Chemistry, September 26, 2022. http://dx.doi.org/10.1021/acs.joc.2c01588.

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